DRAFT PWS Attch 7 List of Analytical Tests.pdf

PWS Attachment 7

DRAFT

Analytical Tests

DESCRIPTION OF TEST

GAS CHROMOTOGRAPHY MASS SPECTROSCOPY (GC/MS)

Volatile Priority Pollutants - 40 CFR 136 Purgeable Halocarbons (EPA 601) Purgeable Aromatics (EPA 602) Acrolein and Acrylonitrile (EPA 603) SVolatile Organics (EPA 624) Low-molecular Weight Priority Contaminates (EPA 558)

Acid Extractable Priority Pollutants Cresols Phenols

Base - Neutral Extractable Priority Pollutants Polynuclear Aromatic Hydrocarbons Halo Ethers Benzidines Chlorinated Hydrocarbons Nitroaromatics and Isophorone Phthalate Esters Nitrosamines 1,2-Diphenylhydrazine (as Azobenzene)

GAS CHROMOTOGRAPHY/ELECTRON CAPTURE DETECTOR

(GC/ECD)

Pesticides, herbicides, polychlorinated biphenyl compounds (PCBs)

In water (routine) In soil (routine) PCB's in soil (within 24 hours) PCB's in water (within 24 hours) PCB's in oil (routine) PCB's in oil (within 24 hours) PCB wipe test (report as mg/100 cm2

GAS CHROMATOGRAPHY/FLAME IONIZATION DECTECTOR (GC/FID)

Total petroleum hydrocarbons, gasoline, diesel In water: routine within 24 hours In soil: routine within 24 hours

Weak Anion Exchange SPE, LC-MS/MS EPA Method 533, 537 or 537.1

GenX In water: routine In soil: routine

Benzene-toluene-ethyl benzene-xylene (BTEX) EPA 8021B / OK Method

In water: routine within 24 hours In soil: routine within 24 hours

ASBESTOS

Air samples - Transmission electron microscopy (TEM) (NIOSH 7402, modified) routine (within 48 hours) blank

Phase contrast microscopy (PCM) (NIOSH 7400) routine within 24 hours blank

Bulk analysis - Polarized Light Microscopy (PLM) routine within 24 hours point counting

Water samples routine

DESCRIPTION OF WASTE

DIOXINS

2,3,7,8-Tetrachlorodibenzo-P-Dioxin routine

HAZARDOUS WASTE ANALYSES

Specific Gravity - Standard Methods 2710 Ignitability - 40 CFR 261.21 Corrosivity - 40 CFR 261.22 Reactivity - 40 CFR 261.23

Toxicity Characteristic Leaching Procedure (TCLP) - 40 CFR 268.40 Extraction procedure Metals analysis Metals, RCRA 8, SW-846, land disposal restricted Pesticides analysis Organic analyses Volatile organics Semi-volatile organics Full TCLP Scan Minus RCRA 8 (305A/7000B)

OTHER ANALYSIS

Total dry solids (sludge) Volatile solids (sludge) pH (sludge) Thermal content (BTUs/unit weight) Infrared spectra Soil permeability Total halogens (TOX, waste oil)

Total Metals (Method 6010A, SW-846) 26 metals Single metal Digestion

WATER/ WASTEWATER QUALITY

WATER/ WASTEWATER Chemistry pH, as part of laboratory testing pH, onsite with portable calibrated meter Acidity, as CaCO3 Alkalinity, as CaCO3 Biochemical Oxygen Demand (BOD) Carbonaceous Biochemical Oxygen Demand Chemical Oxygen Demand (COD) Chlorophyll-A Color Oil and Grease Total Dissolved Solids Total Organic Carbon Total Suspended Solids Turbidity Ammonia nitrogen Bromide Chloride Chlorine, total residual Cyanide, free, amenable to chlorination (CATC), SM 4500-CN-G Cyanide, total, 40 CFR 141.23(k)(1), Fluoride Glycols (EPA 8015B) Methylene chloride Nitrate nitrogen Nitrite nitrogen Nitrate/nitrite Nitrogen, kjeldahl Nitrogen, organic Phenols Phosphates, Total as P Sulfate Sulfide, as S Sulfite, as SO3 Surfactants

WATER/WASTEWATER METALS

Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Chromium, hexavalent Chromium, total Cobalt Copper Iron Lead Magnesium Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Titanium Zinc

Water/Wastewater Biologicals, 40 CFR 136.3 Table IA Fecal coliform Escherichia coli Enterococcus

Disinfectant Biproducts

THM

HAA

Radioactivity - 40 CFR 136.3 Table IE Alpha, total Beta, total Radium, total Radium 226, total

Report Mold - Colony Forming Units (includes media) air bulk swipe

Report Bacteria - Colony Forming Units (includes media) air bulk swipe

Microscopy Allergenco slide analysis (spore trap-visual microscopic analysis)

Tape lift analysis

CFU Specification (up to 8 species) Air Bulk Swipe

INDUSTRIAL HYGIENE SAMPLES - ORGANIC

Formaldehyde analysis of sample Media Air Swipe

Formaldehyde analysis of blank Air Swipe

Gas Chromatography, air samples Charcoal tube – 1st Parameter Charcoal tube– Each Additional Passive Badge – 3 Parameters Passive Badge – Blank

Gas Chromatography/Mass Spectroscopy (GC/MS) Qualitative scan – air Qualitative scan - bulk Qualitative scan - swipe Quantitative scan – air Quantitative scan - bulk

Quantitative scan – swipe

High Pressure Liquid Chromatography (HPLC) MDI , TDI , HDI , NDI media1 MDI, TDI, HDI, NDI in air Analysis of blank air sample

INDUSTRIAL HYGIENE SAMPLES - INORGANIC

High Pressure Liquid Chromatography (HPLC), air samples Inorganic Acids Anion Scan

Scanning Electron Microscopy (SEM) Analysis of sample, air Analysis of sample, bulk Analysis of sample, swipe Photo documentation, per photo

Metals (including preparation), air samples Analysis for first parameter Each additional parameter Analysis for special parameters

Metals – solids, bulk Sample Preparation Analysis for first parameter Each additional parameter Analysis for special parameters

Gravimetric Analysis, air Total Particulates Respirable Fraction

Metals Primary Standard for Eight RCRA, SW-846 Sample Preparation Inorganic Secondary Standard Parameters

Sample Collection and Measurements Sample Collection/Routine, including asbestos bulk and air sampling/On Site, (Hourly Rate) including prep and stabilization

Sample Collection, asbestos abatement project air monitoring, full PPE, (Hourly Rate)

Sample Collection/EMERGENCY RESPONSE (24 hour, 7-days per week basis)

Outfall depth measurement for manning equation, 4 outfalls

Consultation Services Travel/Per Diem IAW Performance Work Statement and Government Travel Regulations

On-site consultation and workplace evaluations by Certified Industrial Hygienist. Quote as hourly rate.

Fish tissue, EPA 200.8, SW-846 Method 3050B

OTHER TEST (as needed basis, price to be negotiated at the time of order.)

Miscellaneous test / emergent contaminate Miscellaneous services