Final Report FTS Tower Sludge TE - 3.pdf

ANALYTICAL REPORT

Eurofins Lancaster Laboratories Env, LLC 2425 New Holland Pike Lancaster, PA 17601 Tel: (717)656-2300

Laboratory Job ID: 410-64534-1 Client Project/Site: GoodFelllow AFB Sludge

For:

Bhate Environmental 1608 13th Avenue South Suite 300 Birmingham, Alabama 35205

Attn: Mr. Brad Jackson

Authorized for release by:

12/7/2021 7:09:57 AM

John Cady, Senior Project Manager (832)763-8082 John.Cady@Eurofinset.com

The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD, and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note exceptions. Noncompliant quality control (QC) is further explained in narrative comments.

· QC results that exceed the upper limits and are associated with non-detect samples are qualified but further narration is not required since the bias is high and does not change a non-detect result. Further narration is also not required with QC blank detection when the associated sample concentration is non-detect or more than ten times the level in the blank.

· Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise specified in the method.

· Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative.

Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency requirements/permits.

Measurement uncertainty values, as applicable, are available upon request.

Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. Times are local to the area of activity.

Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not performed within 15 minutes of collection.

This report shall not be reproduced except in full, without the written approval of the laboratory.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence (either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.

John Cady Senior Project Manager

12/7/2021 7:09:57 AM

Client: Bhate Environmental Project/Site: GoodFelllow AFB Sludge

Laboratory Job ID: 410-64534-1

Page 2 of 27 12/7/2021

Table of Contents

Client: Bhate Environmental Project/Site: GoodFelllow AFB Sludge

Laboratory Job ID: 410-64534-1

Eurofins Lancaster Laboratories Env, LLC

12/7/2021

Cover Page

Table of Contents

Definitions/Glossary

Case Narrative

Detection Summary

Client Sample Results

Surrogate Summary

QC Sample Results

QC Association Summary

Lab Chronicle

Certification Summary

Method Summary

Sample Summary

Chain of Custody

Receipt Checklists

Definitions/Glossary Job ID: 410-64534-1Client: Bhate Environmental

Project/Site: GoodFelllow AFB Sludge

Qualifiers

GC/MS VOA

Qualifier Description

D The reported value is from a dilution.

Qualifier

U Indicates the analyte was analyzed for but not detected.

GC/MS Semi VOA Qualifier Description

M Manual integrated compound.

Qualifier

U Indicates the analyte was analyzed for but not detected.

GC Semi VOA Qualifier Description

4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.

Qualifier

D The reported value is from a dilution.

M Manual integrated compound.

S1- Surrogate recovery exceeds control limits, low biased.

U Indicates the analyte was analyzed for but not detected.

Metals Qualifier Description

B Blank contamination: The analyte was detected above one-half the reporting limit in an associated blank.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

U Indicates the analyte was analyzed for but not detected.

General Chemistry Qualifier Description

U Indicates the analyte was analyzed for but not detected.

Qualifier

Glossary These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

1C Result is from the primary column on a dual-column method.

2C Result is from the confirmation column on a dual-column method.

CFL Contains Free Liquid

CFU Colony Forming Unit

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MCL EPA recommended "Maximum Contaminant Level"

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

MPN Most Probable Number

MQL Method Quantitation Limit

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

NEG Negative / Absent

POS Positive / Present

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Definitions/Glossary

Project/Site: GoodFelllow AFB Sludge

Glossary (Continued)

These commonly used abbreviations may or may not be present in this report.

PQL Practical Quantitation Limit

Abbreviation

PRES Presumptive

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TNTC Too Numerous To Count

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Page 5 of 27 12/7/2021

Case Narrative Client: Bhate Environmental Job ID: 410-64534-1 Project/Site: GoodFelllow AFB Sludge

Job ID: 410-64534-1

Laboratory: Eurofins Lancaster Laboratories Env, LLC

Narrative

Job Narrative 410-64534-1

Receipt The sample was received on 11/23/2021 11:37 AM. Unless otherwise noted below, the sample arrived in good condition, and, where required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 1.5°C and 4.0°C

Receipt Exceptions The Field Sampler was not listed on the Chain of Custody.

The Chain-of-Custody (COC) was incomplete as received and/or improperly completed. There was not a sample ID or collection information listed on the COC or containers received. The sample ID was entered as FTS Tower Sludge and the collection information was entered as 11/22/21 at 07:30 per client.

Sample containers were received unlabeled. FTS Tower Sludge (410-64534-1)

GC/MS VOA

No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.

GC/MS Semi VOA No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.

GC Semi VOA Method TX_1005: The following sample was diluted due to the abundance of non-target analytes: FTS Tower Sludge (410-64534-1). A more concentrated analysis was not possible.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.

Metals Method 6020A_DOD5: The TCLP leachate blank for batch 410-199562 contained Lead above the reporting limit (RL). This target analyte concentration was less than the TCLP Regulatory Hazard Limit. The associated sample(s) were also below the TCLP Regulatory Hazard

Limit for this analyte; therefore, re-extraction was not performed.Associated Sample(s): FTS Tower Sludge (410-64534-1)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.

General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.

Eurofins Lancaster Laboratories Env, LLC Page 6 of 27 12/7/2021

Detection Summary

Project/Site: GoodFelllow AFB Sludge

Client Sample ID: FTS Tower Sludge Lab Sample ID: 410-64534-1

☼C6-C12

LOQ

6200 mg/Kg

DL

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA100D180000 TX 1005

☼C6-C28 Summary 6200 mg/Kg3100 Total/NA100180000 TX 1005

☼C6-C35 Summary 6200 mg/Kg3100 Total/NA100180000 TX 1005

Arsenic 20 ug/L6.8 TCLP112 J 6020A

Barium 20 ug/L7.5 TCLP11000 B 6020A

Lead 5.0 ug/L0.71 TCLP145 B 6020A

Ignitable to Air 1.0 NONE1.0 Total/NA1No 261.21

Ignitable to Flame 1.0 NONE1.0 Total/NA1No 261.21

Ignitable to Friction 1.0 NONE1.0 Total/NA1No 261.21

Ignitable to Water 1.0 NONE1.0 Total/NA1No 261.21 pH 0.01 S.U.0.01 Soluble17.6 9045C

Temperature 0.01 Degrees C0.01 Soluble119.6 9045C

Corrosivity 0.01 NONE0.01 Soluble1no 9045C

Eurofins Lancaster Laboratories Env, LLC

This Detection Summary does not include radiochemical test results.

Page 7 of 27 12/7/2021

Client Sample Results

Project/Site: GoodFelllow AFB Sludge

Lab Sample ID: 410-64534-1Client Sample ID: FTS Tower Sludge Matrix: SolidDate Collected: 11/22/21 07:30

Date Received: 11/23/21 11:37

Method: 8260C DOD - Volatile Organic Compounds (GC/MS) - TCLP

LOQ DL

1,1-Dichloroethene 12 U 20 6.0 ug/L 12/04/21 03:19 20

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

20 6.0 ug/L 12/04/21 03:19 201,2-Dichloroethane 12 U

200 10 ug/L 12/04/21 03:19 202-Butanone 20 U

20 6.0 ug/L 12/04/21 03:19 20Benzene 12 U

20 6.0 ug/L 12/04/21 03:19 20Carbon tetrachloride 12 U

20 6.0 ug/L 12/04/21 03:19 20Chlorobenzene 12 U

20 6.0 ug/L 12/04/21 03:19 20Chloroform 12 U

20 6.0 ug/L 12/04/21 03:19 20Tetrachloroethene 12 U

20 6.0 ug/L 12/04/21 03:19 20Trichloroethene 12 U

20 4.0 ug/L 12/04/21 03:19 20Vinyl chloride 10 U

1,2-Dichloroethane-d4 (Surr) 106 81 - 118 12/04/21 03:19 20

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 101 12/04/21 03:19 2085 - 114

Dibromofluoromethane (Surr) 108 12/04/21 03:19 2080 - 119

Toluene-d8 (Surr) 101 12/04/21 03:19 2089 - 112

Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP

LOQ DL

1,4-Dichlorobenzene 0.0050 U 0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 12,4,5-Trichlorophenol 0.0050 U

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 12,4,6-Trichlorophenol 0.0050 U

0.025 0.0050 mg/L 12/02/21 18:00 12/06/21 13:16 12,4-Dinitrotoluene 0.010 U

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 12-Methylphenol 0.0050 U

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 14-Methylphenol 0.0050 U

0.0025 0.00055 mg/L 12/02/21 18:00 12/06/21 13:16 1Hexachlorobenzene 0.0011 U

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 1Hexachlorobutadiene 0.0050 U

0.025 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 1Hexachloroethane 0.0050 U

0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 13:16 1Nitrobenzene 0.0050 U M

0.025 0.0050 mg/L 12/02/21 18:00 12/06/21 13:16 1Pentachlorophenol 0.020 U

0.025 0.010 mg/L 12/02/21 18:00 12/06/21 13:16 1Pyridine 0.020 U

2,4,6-Tribromophenol (Surr) 76 43 - 140 12/02/21 18:00 12/06/21 13:16 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

2-Fluorobiphenyl (Surr) 69 12/02/21 18:00 12/06/21 13:16 144 - 119

2-Fluorophenol (Surr) 46 12/02/21 18:00 12/06/21 13:16 119 - 119

Nitrobenzene-d5 (Surr) 78 12/02/21 18:00 12/06/21 13:16 144 - 120

Phenol-d5 (Surr) 35 12/02/21 18:00 12/06/21 13:16 110 - 67 p-Terphenyl-d14 (Surr) 64 12/02/21 18:00 12/06/21 13:16 150 - 134

Method: 6020A - Metals (ICP/MS) - TCLP

LOQ DL

Arsenic 12 J 20 6.8 ug/L 12/04/21 08:56 12/06/21 16:52 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

20 7.5 ug/L 12/04/21 08:56 12/06/21 16:52 1Barium 1000 B

5.0 1.5 ug/L 12/04/21 08:56 12/06/21 16:52 1Cadmium 4.0 U

20 3.3 ug/L 12/04/21 08:56 12/06/21 16:52 1Chromium 8.0 U

5.0 0.71 ug/L 12/04/21 08:56 12/06/21 16:52 1Lead 45 B

10 2.8 ug/L 12/04/21 08:56 12/06/21 16:52 1Selenium 8.0 U

5.0 1.7 ug/L 12/04/21 08:56 12/06/21 16:52 1Silver 4.0 U

Eurofins Lancaster Laboratories Env, LLC

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Client Sample Results

Project/Site: GoodFelllow AFB Sludge

Lab Sample ID: 410-64534-1Client Sample ID: FTS Tower Sludge Matrix: SolidDate Collected: 11/22/21 07:30

Date Received: 11/23/21 11:37

Method: 7470A - Mercury (CVAA) - TCLP

LOQ DL

Mercury 0.16 U 0.20 0.079 ug/L 12/04/21 09:22 12/06/21 16:39 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

General Chemistry

LOQ DL

Ignitable to Air No 1.0 1.0 NONE 11/30/21 16:40 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 1.0 NONE 11/30/21 16:40 1Ignitable to Flame No

1.0 1.0 NONE 11/30/21 16:40 1Ignitable to Friction No

1.0 1.0 NONE 11/30/21 16:40 1Ignitable to Water No

60 20 mg/Kg 11/29/21 10:49 11/30/21 17:44 1Cyanide, Reactive 50 U

160 53 mg/Kg 11/29/21 10:49 11/29/21 13:58 1Sulfide, Reactive 140 U

1.0 1.0 % 11/23/21 23:04 1Percent Moisture 67.8

General Chemistry - Soluble

LOQ DL

pH 7.6 0.01 0.01 S.U. 12/01/21 11:51 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.01 0.01 Degrees C 12/01/21 11:51 1Temperature 19.6

0.01 0.01 NONE 12/01/21 11:51 1Corrosivity no

Lab Sample ID: 410-64534-1Client Sample ID: FTS Tower Sludge Matrix: SolidDate Collected: 11/22/21 07:30

Percent Solids: 32.2Date Received: 11/23/21 11:37

Method: TX 1005 - Texas - Total Petroleum Hydrocarbon (GC)

LOQ DL

>C12-C28 6200 U 6200 3100 mg/Kg ☼ 11/30/21 12:17 12/01/21 01:05 100

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

6200 3100 mg/Kg 11/30/21 12:17 12/01/21 01:05 100☼>C28-C35 6200 U

6200 3400 mg/Kg 11/30/21 12:17 12/01/21 01:05 100☼C6-C12 180000 D

6200 3100 mg/Kg 11/30/21 12:17 12/01/21 01:05 100☼C6-C28 Summary 180000

6200 3100 mg/Kg 11/30/21 12:17 12/01/21 01:05 100☼C6-C35 Summary 180000 o- terphenyl (Surr) 64 S1- 70 - 130 11/30/21 12:17 12/01/21 01:05 100

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Trifluorotoluene (Surr) 73 11/30/21 12:17 12/01/21 01:05 10070 - 130

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Surrogate Summary

Project/Site: GoodFelllow AFB Sludge

Method: 8260C DOD - Volatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (81-118) (85-114) (80-119) (89-112)

DCA BFB DBFM TOL

104 105 108 101LCS 410-201409/4

Percent Surrogate Recovery (Acceptance Limits)

Lab Control Sample

104 104 110 101MB 410-201409/6 Method Blank

Surrogate Legend

DCA = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8260C DOD - Volatile Organic Compounds (GC/MS) Prep Type: TCLPMatrix: Solid

Lab Sample ID Client Sample ID (81-118) (85-114) (80-119) (89-112)

DCA BFB DBFM TOL

106 101 108 101410-64534-1

Percent Surrogate Recovery (Acceptance Limits)

FTS Tower Sludge

102 103 108 104410-64534-1 MS FTS Tower Sludge

103 105 106 104410-64534-1 MSD FTS Tower Sludge

Surrogate Legend

DCA = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (43-140) (44-119) (19-119) (44-120) (10-67) (50-134)

TBP FBP 2FP NBZ PHL TPHd14

81 70 51 81 40 82LCS 410-200852/3-A

Percent Surrogate Recovery (Acceptance Limits)

Lab Control Sample

83 69 50 3878 83LCSD 410-200852/4-A Lab Control Sample Dup

74 64 44 3474 78MB 410-200852/2-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol (Surr)

FBP = 2-Fluorobiphenyl (Surr)

2FP = 2-Fluorophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPHd14 = p-Terphenyl-d14 (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS) Prep Type: TCLPMatrix: Solid

Lab Sample ID Client Sample ID (43-140) (44-119) (19-119) (44-120) (10-67) (50-134)

TBP FBP 2FP NBZ PHL TPHd14

76 69 46 78 35 64410-64534-1

Percent Surrogate Recovery (Acceptance Limits)

FTS Tower Sludge

Surrogate Legend

TBP = 2,4,6-Tribromophenol (Surr)

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Page 10 of 27 12/7/2021

Surrogate Summary

Project/Site: GoodFelllow AFB Sludge FBP = 2-Fluorobiphenyl (Surr)

2FP = 2-Fluorophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPHd14 = p-Terphenyl-d14 (Surr)

Method: TX 1005 - Texas - Total Petroleum Hydrocarbon (GC) Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (70-130) (70-130)

OTP TFT

64 S1- 73410-64534-1

Percent Surrogate Recovery (Acceptance Limits)

FTS Tower Sludge

72 67 S1-410-64534-1 MS FTS Tower Sludge

94 80410-64534-1 MSD FTS Tower Sludge

81 M 86 MLCS 410-199625/2-A Lab Control Sample

77 82 MLCSD 410-199625/3-A Lab Control Sample Dup

74 74MB 410-199625/1-A Method Blank

Surrogate Legend

OTP = o- terphenyl (Surr)

TFT = Trifluorotoluene (Surr)

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QC Sample Results

Project/Site: GoodFelllow AFB Sludge

Method: 8260C DOD - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 410-201409/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 201409

LOQ DL

1,1-Dichloroethene 0.60 U 1.0 0.30 ug/L 12/03/21 21:13 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.60 U 0.301.0 ug/L 12/03/21 21:13 11,2-Dichloroethane

1.0 U 0.5010 ug/L 12/03/21 21:13 12-Butanone

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Benzene

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Carbon tetrachloride

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Chlorobenzene

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Chloroform

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Tetrachloroethene

0.60 U 0.301.0 ug/L 12/03/21 21:13 1Trichloroethene

0.50 U 0.201.0 ug/L 12/03/21 21:13 1Vinyl chloride

1,2-Dichloroethane-d4 (Surr) 104 81 - 118 12/03/21 21:13 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

104 12/03/21 21:13 14-Bromofluorobenzene (Surr) 85 - 114

110 12/03/21 21:13 1Dibromofluoromethane (Surr) 80 - 119

101 12/03/21 21:13 1Toluene-d8 (Surr) 89 - 112

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-201409/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 201409

1,1-Dichloroethene 20.0 20.8 ug/L 104 71 - 131

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,2-Dichloroethane 20.0 22.0 ug/L 110 73 - 128

2-Butanone 250 285 ug/L 114 56 - 143

Benzene 20.0 20.5 ug/L 103 79 - 120

Carbon tetrachloride 20.0 21.2 ug/L 106 72 - 136

Chlorobenzene 20.0 19.4 ug/L 97 82 - 118

Chloroform 20.0 21.1 ug/L 106 79 - 124

Tetrachloroethene 20.0 19.2 ug/L 96 74 - 129

Trichloroethene 20.0 20.4 ug/L 102 79 - 123

Vinyl chloride 20.0 19.5 ug/L 97 58 - 137

1,2-Dichloroethane-d4 (Surr) 81 - 118

Surrogate

LCS LCS

Qualifier Limits%Recovery

1054-Bromofluorobenzene (Surr) 85 - 114

108Dibromofluoromethane (Surr) 80 - 119

101Toluene-d8 (Surr) 89 - 112

Client Sample ID: FTS Tower SludgeLab Sample ID: 410-64534-1 MS Matrix: Solid Prep Type: TCLP Analysis Batch: 201409

1,1-Dichloroethene 12 U 400 449 D ug/L 112 71 - 131

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,2-Dichloroethane 12 U 400 429 D ug/L 107 73 - 128

2-Butanone 20 U 5000 5300 D ug/L 106 56 - 143

Benzene 12 U 400 416 D ug/L 104 79 - 120

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Project/Site: GoodFelllow AFB Sludge

Method: 8260C DOD - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: FTS Tower SludgeLab Sample ID: 410-64534-1 MS Matrix: Solid Prep Type: TCLP Analysis Batch: 201409

Carbon tetrachloride 12 U 400 449 D ug/L 112 72 - 136

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Chlorobenzene 12 U 400 401 D ug/L 100 82 - 118

Chloroform 12 U 400 429 D ug/L 107 79 - 124

Tetrachloroethene 12 U 400 408 D ug/L 102 74 - 129

Trichloroethene 12 U 400 412 D ug/L 103 79 - 123

Vinyl chloride 10 U 400 415 D ug/L 104 58 - 137

1,2-Dichloroethane-d4 (Surr) 81 - 118

Surrogate

MS MS

Qualifier Limits%Recovery

1034-Bromofluorobenzene (Surr) 85 - 114

108Dibromofluoromethane (Surr) 80 - 119

104Toluene-d8 (Surr) 89 - 112

Client Sample ID: FTS Tower SludgeLab Sample ID: 410-64534-1 MSD Matrix: Solid Prep Type: TCLP Analysis Batch: 201409

1,1-Dichloroethene 12 U 400 444 D ug/L 111 71 - 131 1 20

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,2-Dichloroethane 12 U 400 440 D ug/L 110 73 - 128 3 20

2-Butanone 20 U 5000 5550 D ug/L 111 56 - 143 4 20

Benzene 12 U 400 420 D ug/L 105 79 - 120 1 20

Carbon tetrachloride 12 U 400 454 D ug/L 114 72 - 136 1 20

Chlorobenzene 12 U 400 410 D ug/L 103 82 - 118 2 20

Chloroform 12 U 400 437 D ug/L 109 79 - 124 2 20

Tetrachloroethene 12 U 400 420 D ug/L 105 74 - 129 3 20

Trichloroethene 12 U 400 415 D ug/L 104 79 - 123 1 20

Vinyl chloride 10 U 400 409 D ug/L 102 58 - 137 1 20

1,2-Dichloroethane-d4 (Surr) 81 - 118

Surrogate

MSD MSD

Qualifier Limits%Recovery

1054-Bromofluorobenzene (Surr) 85 - 114

106Dibromofluoromethane (Surr) 80 - 119

104Toluene-d8 (Surr) 89 - 112

Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 410-200852/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 201807 Prep Batch: 200852

LOQ DL

1,4-Dichlorobenzene 0.0050 U 0.010 0.0025 mg/L 12/02/21 18:00 12/06/21 11:49 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.0050 U 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 12,4,5-Trichlorophenol

0.0050 U 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 12,4,6-Trichlorophenol

0.010 U 0.00500.025 mg/L 12/02/21 18:00 12/06/21 11:49 12,4-Dinitrotoluene

0.0050 U 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 12-Methylphenol

0.0050 U 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 14-Methylphenol

Eurofins Lancaster Laboratories Env, LLC

Page 13 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 410-200852/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 201807 Prep Batch: 200852

LOQ DL

Hexachlorobenzene 0.0011 U 0.0025 0.00055 mg/L 12/02/21 18:00 12/06/21 11:49 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.0050 U 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 1Hexachlorobutadiene

0.0050 U 0.00250.025 mg/L 12/02/21 18:00 12/06/21 11:49 1Hexachloroethane

0.0050 U M 0.00250.010 mg/L 12/02/21 18:00 12/06/21 11:49 1Nitrobenzene

0.020 U 0.00500.025 mg/L 12/02/21 18:00 12/06/21 11:49 1Pentachlorophenol

0.020 U 0.0100.025 mg/L 12/02/21 18:00 12/06/21 11:49 1Pyridine

2,4,6-Tribromophenol (Surr) 74 43 - 140 12/06/21 11:49 1

MB MB

Surrogate

12/02/21 18:00

Dil FacPrepared AnalyzedQualifier Limits%Recovery

64 12/02/21 18:00 12/06/21 11:49 12-Fluorobiphenyl (Surr) 44 - 119

44 12/02/21 18:00 12/06/21 11:49 12-Fluorophenol (Surr) 19 - 119

74 12/02/21 18:00 12/06/21 11:49 1Nitrobenzene-d5 (Surr) 44 - 120

34 12/02/21 18:00 12/06/21 11:49 1Phenol-d5 (Surr) 10 - 67

78 12/02/21 18:00 12/06/21 11:49 1p-Terphenyl-d14 (Surr) 50 - 134

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-200852/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 201807 Prep Batch: 200852

1,4-Dichlorobenzene 0.250 0.145 mg/L 58 29 - 112

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

2,4,5-Trichlorophenol 0.250 0.193 mg/L 77 53 - 123

2,4,6-Trichlorophenol 0.250 0.198 mg/L 79 50 - 125

2,4-Dinitrotoluene 0.250 0.195 mg/L 78 57 - 128

2-Methylphenol 0.250 0.185 mg/L 74 30 - 117

4-Methylphenol 0.250 0.171 mg/L 69 25 - 120

Hexachlorobenzene 0.250 0.196 mg/L 79 53 - 125

Hexachlorobutadiene 0.250 0.144 mg/L 58 22 - 124

Hexachloroethane 0.250 0.148 mg/L 59 21 - 115

Nitrobenzene 0.250 0.197 mg/L 79 45 - 121

Pentachlorophenol 0.500 0.393 mg/L 79 35 - 138

Pyridine 0.500 0.264 mg/L 53 23 - 120

2,4,6-Tribromophenol (Surr) 43 - 140

Surrogate

LCS LCS

Qualifier Limits%Recovery

702-Fluorobiphenyl (Surr) 44 - 119

512-Fluorophenol (Surr) 19 - 119

81Nitrobenzene-d5 (Surr) 44 - 120

40Phenol-d5 (Surr) 10 - 67

82p-Terphenyl-d14 (Surr) 50 - 134

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-200852/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 201807 Prep Batch: 200852

1,4-Dichlorobenzene 0.250 0.139 mg/L 56 29 - 112 4 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

2,4,5-Trichlorophenol 0.250 0.210 mg/L 84 53 - 123 8 20

Eurofins Lancaster Laboratories Env, LLC

Page 14 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-200852/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 201807 Prep Batch: 200852

2,4,6-Trichlorophenol 0.250 0.206 mg/L 82 50 - 125 4 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

2,4-Dinitrotoluene 0.250 0.213 mg/L 85 57 - 128 9 20

2-Methylphenol 0.250 0.185 mg/L 74 30 - 117 0 20

4-Methylphenol 0.250 0.169 mg/L 68 25 - 120 1 20

Hexachlorobenzene 0.250 0.195 mg/L 78 53 - 125 1 20

Hexachlorobutadiene 0.250 0.139 mg/L 55 22 - 124 4 20

Hexachloroethane 0.250 0.144 mg/L 57 21 - 115 3 20

Nitrobenzene 0.250 0.206 mg/L 82 45 - 121 5 20

Pentachlorophenol 0.500 0.410 mg/L 82 35 - 138 4 20

Pyridine 0.500 0.252 mg/L 50 23 - 120 5 30

2,4,6-Tribromophenol (Surr) 43 - 140

Surrogate

LCSD LCSD

Qualifier Limits%Recovery

692-Fluorobiphenyl (Surr) 44 - 119

502-Fluorophenol (Surr) 19 - 119

78Nitrobenzene-d5 (Surr) 44 - 120

38Phenol-d5 (Surr) 10 - 67

83p-Terphenyl-d14 (Surr) 50 - 134

Method: TX 1005 - Texas - Total Petroleum Hydrocarbon (GC)

Client Sample ID: Method BlankLab Sample ID: MB 410-199625/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199826 Prep Batch: 199625

LOQ DL

>C12-C28 20 U 20 10 mg/Kg 11/30/21 12:17 11/30/21 21:57 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

20 U 1020 mg/Kg 11/30/21 12:17 11/30/21 21:57 1>C28-C35

20 U 1120 mg/Kg 11/30/21 12:17 11/30/21 21:57 1C6-C12

20 U 1020 mg/Kg 11/30/21 12:17 11/30/21 21:57 1C6-C28 Summary

20 U 1020 mg/Kg 11/30/21 12:17 11/30/21 21:57 1C6-C35 Summary o- terphenyl (Surr) 74 70 - 130 11/30/21 21:57 1

MB MB

Surrogate

11/30/21 12:17

Dil FacPrepared AnalyzedQualifier Limits%Recovery

74 11/30/21 12:17 11/30/21 21:57 1Trifluorotoluene (Surr) 70 - 130

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-199625/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199826 Prep Batch: 199625

>C12-C28 252 219 M mg/Kg 87 75 - 125

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

C6-C12 251 209 M mg/Kg 83 75 - 125

C6-C28 Summary 503 428 mg/Kg 85 75 - 125 o- terphenyl (Surr) M 70 - 130

Surrogate

LCS LCS

Qualifier Limits%Recovery

86 MTrifluorotoluene (Surr) 70 - 130

Eurofins Lancaster Laboratories Env, LLC

Page 15 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

Method: TX 1005 - Texas - Total Petroleum Hydrocarbon (GC)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-199625/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199826 Prep Batch: 199625

>C12-C28 252 217 M mg/Kg 86 75 - 125 1 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

C6-C12 251 209 M mg/Kg 83 75 - 125 0 20

C6-C28 Summary 503 426 mg/Kg 85 75 - 125 0 20 o- terphenyl (Surr) 70 - 130

Surrogate

LCSD LCSD

Qualifier Limits%Recovery

82 MTrifluorotoluene (Surr) 70 - 130

Client Sample ID: FTS Tower SludgeLab Sample ID: 410-64534-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 199826 Prep Batch: 199625

>C12-C28 6200 U 781 6200 U mg/Kg NC 75 - 125☼

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

C6-C12 180000 D 778 153000 D 4 mg/Kg -3301 75 - 125☼

C6-C28 Summary 180000 1560 153000 4 mg/Kg -1732 75 - 125☼

C6-C35 Summary 180000 1560 153000 4 mg/Kg -1732 75 - 125☼ o- terphenyl (Surr) 70 - 130

Surrogate

MS MS

Qualifier Limits%Recovery

67 S1-Trifluorotoluene (Surr) 70 - 130

Client Sample ID: FTS Tower SludgeLab Sample ID: 410-64534-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 199826 Prep Batch: 199625

>C12-C28 6200 U 781 6200 U mg/Kg NC 75 - 125 NC 20☼

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

C6-C12 180000 D 778 164000 D 4 mg/Kg -1906 75 - 125 7 20☼

C6-C28 Summary 180000 1560 164000 4 mg/Kg -1026 75 - 125 7 20☼

C6-C35 Summary 180000 1560 164000 4 mg/Kg -1026 75 - 125 7 20☼ o- terphenyl (Surr) 70 - 130

Surrogate

MSD MSD

Qualifier Limits%Recovery

80Trifluorotoluene (Surr) 70 - 130

Method: 6020A - Metals (ICP/MS)

Client Sample ID: Method BlankLab Sample ID: MB 410-201496/1-A Matrix: Solid Prep Type: Total Recoverable Analysis Batch: 202067 Prep Batch: 201496

LOQ DL

Arsenic 16 U 20 6.8 ug/L 12/04/21 08:56 12/06/21 16:14 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

16 U 7.520 ug/L 12/04/21 08:56 12/06/21 16:14 1Barium

4.0 U 1.55.0 ug/L 12/04/21 08:56 12/06/21 16:14 1Cadmium

8.0 U 3.320 ug/L 12/04/21 08:56 12/06/21 16:14 1Chromium

2.5 U 0.715.0 ug/L 12/04/21 08:56 12/06/21 16:14 1Lead

Eurofins Lancaster Laboratories Env, LLC

Page 16 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

Method: 6020A - Metals (ICP/MS) (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 410-201496/1-A Matrix: Solid Prep Type: Total Recoverable Analysis Batch: 202067 Prep Batch: 201496

LOQ DL

Selenium 8.0 U 10 2.8 ug/L 12/04/21 08:56 12/06/21 16:14 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

4.0 U 1.75.0 ug/L 12/04/21 08:56 12/06/21 16:14 1Silver

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-201496/2-A Matrix: Solid Prep Type: Total Recoverable Analysis Batch: 202067 Prep Batch: 201496

Arsenic 5000 4680 ug/L 94 84 - 116

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Barium 5000 4990 ug/L 100 86 - 114

Cadmium 500 504 ug/L 101 87 - 115

Chromium 5000 4610 ug/L 92 85 - 116

Lead 500 495 ug/L 99 88 - 115

Selenium 1000 1020 ug/L 102 80 - 120

Silver 500 483 ug/L 97 85 - 116

Method: 7470A - Mercury (CVAA)

Client Sample ID: Method BlankLab Sample ID: MB 410-201499/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 202044 Prep Batch: 201499

LOQ DL

Mercury 0.16 U 0.20 0.079 ug/L 12/04/21 09:22 12/06/21 16:31 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-201499/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 202044 Prep Batch: 201499

Mercury 1.00 0.982 ug/L 98 82 - 119

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: 9012 - Cyanide, Reactive

Client Sample ID: Method BlankLab Sample ID: MB 410-199054/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199868 Prep Batch: 199054

LOQ DL

Cyanide, Reactive 50 U 60 20 mg/Kg 11/29/21 08:54 11/30/21 17:19 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-199054/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199868 Prep Batch: 199054

Cyanide, Reactive 963 500 U mg/Kg 3 0 - 5.14

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Eurofins Lancaster Laboratories Env, LLC

Page 17 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

Method: 9034 - Sulfide, Reactive

Client Sample ID: Method BlankLab Sample ID: MB 410-199054/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199224 Prep Batch: 199054

LOQ DL

Sulfide, Reactive 140 U 160 54 mg/Kg 11/29/21 08:54 11/29/21 13:58 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-199054/15-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 199224 Prep Batch: 199054

Sulfide, Reactive 538 447 mg/Kg 83 56 - 104

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: 9045C - pH

Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-200194/1-A Matrix: Solid Prep Type: Soluble Analysis Batch: 200214 pH 7.00 7.1 S.U. 102 95 - 105

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Eurofins Lancaster Laboratories Env, LLC

Page 18 of 27 12/7/2021

QC Association Summary

Project/Site: GoodFelllow AFB Sludge

GC/MS VOA

Leach Batch: 200860

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 1311410-64534-1 FTS Tower Sludge TCLP

Solid 1311410-64534-1 MS FTS Tower Sludge TCLP

Solid 1311410-64534-1 MSD FTS Tower Sludge TCLP

Analysis Batch: 201409

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260C DOD 200860410-64534-1 FTS Tower Sludge TCLP

Solid 8260C DODMB 410-201409/6 Method Blank Total/NA

Solid 8260C DODLCS 410-201409/4 Lab Control Sample Total/NA

Solid 8260C DOD 200860410-64534-1 MS FTS Tower Sludge TCLP

Solid 8260C DOD 200860410-64534-1 MSD FTS Tower Sludge TCLP

GC/MS Semi VOA

Leach Batch: 199562

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 1311410-64534-1 FTS Tower Sludge TCLP

Prep Batch: 200852

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3510C 199562410-64534-1 FTS Tower Sludge TCLP

Solid 3510CMB 410-200852/2-A Method Blank Total/NA

Solid 3510CLCS 410-200852/3-A Lab Control Sample Total/NA

Solid 3510CLCSD 410-200852/4-A Lab Control Sample Dup Total/NA

Analysis Batch: 201807

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8270D 200852410-64534-1 FTS Tower Sludge TCLP

Solid 8270D 200852MB 410-200852/2-A Method Blank Total/NA

Solid 8270D 200852LCS 410-200852/3-A Lab Control Sample Total/NA

Solid 8270D 200852LCSD 410-200852/4-A Lab Control Sample Dup Total/NA

GC Semi VOA

Prep Batch: 199625

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid TX_1005_S_Pre p

410-64534-1 FTS Tower Sludge Total/NA

Solid TX_1005_S_Pre p

MB 410-199625/1-A Method Blank Total/NA

Solid TX_1005_S_Pre p

LCS 410-199625/2-A Lab Control Sample Total/NA

Solid TX_1005_S_Pre p

LCSD 410-199625/3-A Lab Control Sample Dup Total/NA

Solid TX_1005_S_Pre p

410-64534-1 MS FTS Tower Sludge Total/NA

Solid TX_1005_S_Pre p

410-64534-1 MSD FTS Tower Sludge Total/NA

Analysis Batch: 199826

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid TX 1005 199625410-64534-1 FTS Tower Sludge Total/NA

Solid TX 1005 199625MB 410-199625/1-A Method Blank Total/NA

Eurofins Lancaster Laboratories Env, LLC

Page 19 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

GC Semi VOA (Continued)

Analysis Batch: 199826 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid TX 1005 199625LCS 410-199625/2-A Lab Control Sample Total/NA

Solid TX 1005 199625LCSD 410-199625/3-A Lab Control Sample Dup Total/NA

Solid TX 1005 199625410-64534-1 MS FTS Tower Sludge Total/NA

Solid TX 1005 199625410-64534-1 MSD FTS Tower Sludge Total/NA

Metals

Leach Batch: 199562

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 1311410-64534-1 FTS Tower Sludge TCLP

Prep Batch: 201496

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3005A 199562410-64534-1 FTS Tower Sludge TCLP

Solid 3005AMB 410-201496/1-A Method Blank Total Recoverable

Solid 3005ALCS 410-201496/2-A Lab Control Sample Total Recoverable

Prep Batch: 201499

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 7470A 199562410-64534-1 FTS Tower Sludge TCLP

Solid 7470AMB 410-201499/1-A Method Blank Total/NA

Solid 7470ALCS 410-201499/2-A Lab Control Sample Total/NA

Analysis Batch: 202044

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 7470A 201499410-64534-1 FTS Tower Sludge TCLP

Solid 7470A 201499MB 410-201499/1-A Method Blank Total/NA

Solid 7470A 201499LCS 410-201499/2-A Lab Control Sample Total/NA

Analysis Batch: 202067

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 6020A 201496410-64534-1 FTS Tower Sludge TCLP

Solid 6020A 201496MB 410-201496/1-A Method Blank Total Recoverable

Solid 6020A 201496LCS 410-201496/2-A Lab Control Sample Total Recoverable

General Chemistry

Analysis Batch: 198318

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid Moisture410-64534-1 FTS Tower Sludge Total/NA

Prep Batch: 199054

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 7.3.4410-64534-1 FTS Tower Sludge Total/NA

Solid 7.3.4MB 410-199054/1-A Method Blank Total/NA

Solid 7.3.4LCS 410-199054/15-A Lab Control Sample Total/NA

Solid 7.3.4LCS 410-199054/2-A Lab Control Sample Total/NA

Analysis Batch: 199224

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 9034 199054410-64534-1 FTS Tower Sludge Total/NA

Solid 9034 199054MB 410-199054/1-A Method Blank Total/NA

Eurofins Lancaster Laboratories Env, LLC

Page 20 of 27 12/7/2021

Project/Site: GoodFelllow AFB Sludge

General Chemistry (Continued)

Analysis Batch: 199224 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 9034 199054LCS 410-199054/15-A Lab Control Sample Total/NA

Analysis Batch: 199822

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 261.21410-64534-1 FTS Tower Sludge Total/NA

Analysis Batch: 199868

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 9012 199054410-64534-1 FTS Tower Sludge Total/NA

Solid 9012 199054MB 410-199054/1-A Method Blank Total/NA

Solid 9012 199054LCS 410-199054/2-A Lab Control Sample Total/NA

Leach Batch: 200194

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid DI Leach410-64534-1 FTS Tower Sludge Soluble

Solid DI LeachLCS 410-200194/1-A Lab Control Sample Soluble

Analysis Batch: 200214

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 9045C 200194410-64534-1 FTS Tower Sludge Soluble

Solid 9045C 200194LCS 410-200194/1-A Lab Control Sample Soluble

Eurofins Lancaster Laboratories Env, LLC

Page 21 of 27 12/7/2021

Lab Chronicle

Project/Site: GoodFelllow AFB Sludge

Client Sample ID: FTS Tower Sludge Lab Sample ID: 410-64534-1 Matrix: SolidDate Collected: 11/22/21 07:30

Date Received: 11/23/21 11:37

Leach 1311 12/02/21 18:05 CZ7N200860 ELLE

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared or Analyzed

Batch

Number

Dilution

Factor

TCLP

Analysis 8260C DOD 20 201409 12/04/21 03:19 K4WN ELLETCLP

Leach 1311 199562 12/01/21 15:32 UNWS ELLETCLP

Prep 3510C 200852 12/02/21 18:00 QQ3P ELLETCLP

Analysis 8270D 1 201807 12/06/21 13:16 P7EB ELLETCLP

Leach 1311 199562 12/01/21 15:32 UNWS ELLETCLP

Prep 3005A 201496 12/04/21 08:56 UAMX ELLETCLP

Analysis 6020A 1 202067 12/06/21 16:52 UCIG ELLETCLP

Leach 1311 199562 12/01/21 15:32 UNWS ELLETCLP

Prep 7470A 201499 12/04/21 09:22 UAMX ELLETCLP

Analysis 7470A 1 202044 12/06/21 16:39 UEFS ELLETCLP

Analysis 261.21 1 199822 11/30/21 16:40 DI9Q ELLETotal/NA

Prep 7.3.4 199054 11/29/21 10:49 USE1 ELLETotal/NA

Analysis 9012 1 199868 11/30/21 17:44 JCG7 ELLETotal/NA

Prep 7.3.4 199054 11/29/21 10:49 USE1 ELLETotal/NA

Analysis 9034 1 199224 11/29/21 13:58 USE1 ELLETotal/NA

Leach DI Leach 200194 12/01/21 10:55 DZU8 ELLESoluble

Analysis 9045C 1 200214 12/01/21 11:51 DZU8 ELLESoluble

Analysis Moisture 1 198318 11/23/21 23:04 OEL4 ELLETotal/NA

Client Sample ID: FTS Tower Sludge Lab Sample ID: 410-64534-1 Matrix: SolidDate Collected: 11/22/21 07:30

Percent Solids: 32.2Date Received: 11/23/21 11:37

Prep TX_1005_S_Prep 11/30/21 12:17 DFX4199625 ELLE

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis TX 1005 100 199826 12/01/21 01:05 UHEW ELLETotal/NA

Laboratory References:

ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL (717)656-2300

Eurofins Lancaster Laboratories Env, LLC

Page 22 of 27 12/7/2021

Accreditation/Certification Summary

Project/Site: GoodFelllow AFB Sludge

Laboratory: Eurofins Lancaster Laboratories Env, LLC Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.

Authority Program Identification Number Expiration Date

A2LA Dept. of Defense ELAP 1.01 11-30-22

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

9012 7.3.4 Solid Cyanide, Reactive

9034 7.3.4 Solid Sulfide, Reactive

Moisture Solid Percent Moisture

Texas NELAP T104704194-21-40 08-31-22

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

261.21 Solid Ignitable to Air

261.21 Solid Ignitable to Flame

261.21 Solid Ignitable to Friction

261.21 Solid Ignitable to Water

9012 7.3.4 Solid Cyanide, Reactive

9034 7.3.4 Solid Sulfide, Reactive

9045C Solid Corrosivity

9045C Solid Temperature

Moisture Solid Percent Moisture

Eurofins Lancaster Laboratories Env, LLC

Page 23 of 27 12/7/2021

Method Summary

Project/Site: GoodFelllow AFB Sludge

Method Method Description LaboratoryProtocol

SW8468260C DOD Volatile Organic Compounds (GC/MS) ELLE

SW8468270D Semivolatile Organic Compounds (GC/MS) ELLE

TCEQTX 1005 Texas - Total Petroleum Hydrocarbon (GC) ELLE

SW8466020A Metals (ICP/MS) ELLE

SW8467470A Mercury (CVAA) ELLE

40CFR261261.21 Ignitability ELLE

SW8469012 Cyanide, Reactive ELLE

SW8469034 Sulfide, Reactive ELLE

SW8469045C pH ELLE

EPAMoisture Percent Moisture ELLE

SW8461311 TCLP Extraction ELLE

SW8463005A Preparation, Total Recoverable or Dissolved Metals ELLE

SW8463510C Liquid-Liquid Extraction (Separatory Funnel) ELLE

SW8465030C Purge and Trap ELLE

SW8467.3.3 Cyanide, Reactive ELLE

SW8467.3.4 Sulfide, Reactive ELLE

SW8467470A Preparation, Mercury ELLE

ASTMDI Leach Deionized Water Leaching Procedure ELLE

TCEQTX_1005_S_Prep Extraction - Texas Total petroleum Hyrdocarbons ELLE

Protocol References:

40CFR261 = 40 CFR Part 261

ASTM = ASTM International

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TCEQ = Texas Commission of Environmental Quality

Laboratory References:

ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL (717)656-2300

Eurofins Lancaster Laboratories Env, LLC

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Sample Summary

Project/Site: GoodFelllow AFB Sludge

Lab Sample ID Client Sample ID Matrix Collected Received

410-64534-1 FTS Tower Sludge Solid 11/22/21 07:30 11/23/21 11:37

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Login Sample Receipt Checklist

Client: Bhate Environmental Job Number: 410-64534-1

Login Number: 64534

Question Answer Comment

Creator: Lugardo, Tamara

List Source: Eurofins Lancaster Laboratories Env, LLC

List Number: 1

TrueThe cooler's custody seal is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable (</=6C, not frozen).

TrueCooler Temperature is recorded.

N/AWV: Container Temperature is acceptable (</=6C, not frozen).

N/AWV: Container Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

FalseCOC is filled out with all pertinent information. Refer to Job Narrative for details.

TrueThere are no discrepancies between the containers received and the COC.

FalseSample containers have legible labels. Refer to Job Narrative for details.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueThere is sufficient vol. for all requested analyses.

FalseIs the Field Sampler's name present on COC? Refer to Job Narrative for details.

N/ASample custody seals are intact.

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