Atch 4 Bldg 155 Lead-Asbestos Report.pdf

Customer Project:

Reference #: Date: 6/17/2019

Analysis and Method

Discussion

Qualifications

CA Labs

Dedicated to Dedicated to Dedicated to Dedicated to

QualityQualityQualityQuality

Crisp Analytical, L.L.C.

1929 Old Denton Road

Carrollton, TX 75006

Phone 972-242-2754

Fax 972-242-2798

CA Labs, L.L.C.

12232 Industriplex, Suite 32

Baton Rouge, LA 70809

Phone 225-751-5632

Fax 225-751-5634

Materials Characterization - Bulk Asbestos Analysis Laboratory Analysis Report - Polarized Light

Asbestos & Technical Services

P.O. Box 2574

Cheyenne, WY 82003 061319FEW155, FE Warren Bldg. 155

CAL19063874AG

Summary of polarized light microscopy (PLM / Stereomicroscopy bulk asbestos analysis) using the methods described in 40CFR Part 763

Appendix E to Subpart E (Interim and EPA 600 / R-93 / 116 (Improved). The sample is first viewed with the aid of a stereomicroscope. Numerous liquid slide preparations are created for analysis under the polarized microscope where identifications and quantifications are preformed. Calibrated liquid refractive oils are used as liquid mouting medium. These oils are used for identification (dispersion staining). A calibrated visual estimation is reported, should any asbestiform mineral be present. Other techniques such as acid washing are used in conjugation with refractive oils for detection of smaller quantities of asbestos. All asbestos percentages are based on calibrated visual estimation traceable to NIST standards for regulated asbestos. Traceability to measurement and calibration is achieved by using known amounts and types of asbestos from standards where analyst and laboratory accuracy are measured. As little as 0.001% asbestos can be detected in favorable samples, while detection in unfavorable samples may approach the detection limit of 0.50% (well above the laboratory definition of trace).

Vermiculite containing samples may contain trace amounts of actinolite/tremolite. When not detected by PLM, these samples should be analyzed using TEM methods and / or water separation techniques. Suspected actinolite/vermiculite presence will be indicated through the sample comment section of this report.

Fibrous talc containing samples may contain a regulated asbestos fiber known as anthophyllite. Under certain conditions the same fiber may actually contain both talc and anthophyllite (a phenomenon called intergrowth). Again, TEM detection methods are recommended. CA Labs PLM report comments will denote suspected amounts of asbestiform anthophyllite with talc, where further analysis is recommended.

Some samples (floor tiles, surfacings, etc.) may contain fibers too small to be detectable by PLM analysis and should be analyzed by TEM bulk protocols.

AIHA LAP, LLC Laboratory #102929

A "trace asbestos" will be reported if the analyst observes far less than 1% asbestos. CA Labs defines "trace asbestos" as a few fibers detected by the analyst in several preparations and will indicate as such under these circumstances.

Since allowable variation in quantification of samples close to 1% is high, <1% may be reported. Such results are ideal for point counting, and the technique is mandatory for friable samples (NESHAP, Nov. 1990 and clarification letter 8 May 1991) under 1% percent asbestos or "trace asbestos".

In order to make all initial PLM reports issued from CA Labs NESHAP compliant, all <1% asbestos results (except floor tiles) will be point counted at no additional charge.

CA Labs is accredited by the National Voluntary Accreditation Program (NVLAP) for selected test methods for airborne fiber analysis (TEM), and for bulk asbestos fiber analysis (PLM). CA Labs is also accredited by AIHA LAP, LLC. in the PLM asbestos field of testing for Industrial Hygiene. All analysts have completed college courses or hold a degree in a natural science (geology, biology, or environmental science). Recognition by a state professional board in one these disciplines is preferred, but not required. Extensive in-house training programs are used to augment the educational background of the analyst. The Laboratory Director and Quality Manager have received supplemental McCrone Research training for asbestos identification. Analysis performed at Crisp Analytical Labs, LLC 1929 Old Denton Road Carrollton, TX 75006

Dallas NVLAP Lab Code 200349-0 TEM/PLM TCEQ# T104704513-15-3 TDH 30-0235

Labs

A

C

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Overview of Project Sample Material Containing Asbestos

Customer Project: 061319FEW155, FE Warren Bldg. 155 CA Labs Project #: CAL19063874AG gray sealant white surfaced gray sealant tan surfaced tan compound tan compound (beneath tape)

Glossary of abbreviations (non-asbestos fibers and non-fibrous minerals):

2% Chrysotile

061319FE

W155-2 2-1

Window Caulking/ white surfaced gray sealant

CA Labs

Dedicated to Dedicated to Dedicated to Dedicated to

QualityQualityQualityQuality

Crisp Analytical, L.L.C.

1929 Old Denton Road

Carrollton, TX 75006

Phone 972-242-2754

Fax 972-242-2798

CA Labs, L.L.C.

12232 Industriplex, Suite 32

Baton Rouge, LA 70809

Phone 225-751-5632

Fax 225-751-5634

Sample # Layer

Analysts Physical Description of

Subsample

Asbestos type / calibrated visual estimate percent

List of Affected Building

Material Types

061319FE

W155-1 1-1 Window Glaze/ gray sealant 2% Chrysotile

2% Chrysotile

16-2 tan compound (beneath tape) 2% Chrysotile

061319FE

W155-16 16-1

Drywall/ tan surfaced tan compound

Dallas NVLAP Lab Code 200349-0 TEM/PLM TCEQ# T104704513-15-3 TDH 30-0235

AIHA LAP, LLC Laboratory #102929 ca - carbonate gypsum - gypsum bi - binder or - organic ma - matrix mi - mica ve - vermiculite ot - other pe - perlite qu - quartz fg - fiberglass mw - mineral wool wo - wollastinite ta - talc sy - synthetic ce - cellulose br - brucite ka - kaolin (clay) pa - palygorskite (clay)

This report relates to the items tested. This report is not to be used by the customer to claim product certification, approval or endorsement by NVLAP, NIST, AIHA LAP, LLC, or any other agency of the federal government. This report may not be reproduced except in full without written permission from CA Labs. These results are submitted pursuant to CA Labs' current terms and sale, condition of sale, including the company's standard warranty and limitations of liability provisions and no responsibility or liability is assumed for the manner in which the results are used or interpreted. Unless notified in writing to return the samples covered by this report, CA Labs will store the samples for a period of ninety (90) days before discarding. A shipping or handling fee may be assessed for the return of any samples.

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Polarized Light Asbestiform Materials Characterization

Customer Info: Attn: Customer Project:

6/17/2019

6/14/19 10:30AM

Phone # 6/13/2019

Fax #

Senior Analyst

Julio Robles

CA Labs

Dedicated to Dedicated to Dedicated to Dedicated to

QualityQualityQualityQuality

Crisp Analytical, L.L.C.

1929 Old Denton Road

Carrollton, TX 75006

Phone 972-242-2754

Fax 972-242-2798

CA Labs, L.L.C.

12232 Industriplex, Suite 32

Baton Rouge, LA 70809

Phone 225-751-5632

Fax 225-751-5634

CA Labs Project #:

Asbestos & Technical Services

061319FEW155, FE Warren

Bldg. 155

CAL19063874AG

P.O. Box 2574

Cheyenne, WY 82003 Date:

Turnaround Time: Samples Received:

307-214-0904 24 hours Date Of Sampling:

Purchase Order #:

Sample # Com ment

Layer

Analysts Physical Description of

Subsample

Homo-geneo us

(Y/N)

Asbestos type / calibrated visual estimate percent

Non-asbestos fiber type / percent

Non-fibrous type

/ percent

061319FE

W155-1 1-1 Window Glaze/ gray sealant y 2% Chrysotile 98% qu,ca

061319FE

W155-2 2-1

Window Caulking/ white surfaced gray sealant n 2% Chrysotile 98% qu,bi,ca

061319FE

W155-3 3-1 Drywall/ gray surfacing y None Detected 100% qu,bi

061319FE

W155-4 4-1

Compound and Floor

Sealant/ white sealant y None Detected 100% qu,ma,bi

061319FE

W155-5 5-1

Caulking, Foundation/ brown sealant y None Detected

100% qu,ma,bi,ca

061319FE

W155-6 6-1

CMU Surface Compound/ gray surfaced tan finishing compound n None Detected 100% qu,mi,bi,ca

061319FE

W155-7 7-1 Drywall/ gray surfacing y None Detected 100% qu,bi

Dallas NVLAP Lab Code 200349-0 TEM/PLM TCEQ# T104704513-15-3 TDH 30-0235

AIHA LAP, LLC Laboratory #102929 Analysis Method: Interim (40CFR Part 763 Appendix E to Subpart E) / Improved (EPA-600 / R-93/116). All samples received in good condition unless noted.

Preparation Method: HCL acid washing for carbonate based samples, chemical reduction for organically bound components, oil immersion for identification of asbestos types by dispersion attaining / becke line method.

ca - carbonate gy - gypsum bi - binder or - organic ma - matrix mi - mica ve - vermiculite ot -other pe - perlite qu - quartz fg - fiberglass mw - mineral wool wo - wollastonite ta - talc sy - synthetic ce - cellulose br - brucite ka - kaolin (clay) pa - palygorskite (clay) Approved Signatories:

Stanley Massett Technical Manager

Analyst Tanner Rasmussen

1. Fire Damage significant fiber damage - reported percentages reflect unaltered fibers

2. Fire Damage no significant fiber damages effecting fibrous percentages

3. Actinolite in association with Vermiculite

4. Layer not analyzed - attached to previous positive layer and contamination is suspected

5. Not enough sample to analyze

6. Anthophyllite in association with Fibrous Talc

7. Contamination suspected from other building materials

8. Favorable scenario for water separation on vermiculite for possible analysis by another method

9. < 1% Result point counted positive

10. TEM analysis suggested

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6/17/2019

6/14/19 10:30AM

Phone # 6/13/2019

Fax #

Senior Analyst

Julio Robles

CA Labs

Dedicated to Dedicated to Dedicated to Dedicated to

QualityQualityQualityQuality

Crisp Analytical, L.L.C.

1929 Old Denton Road

Carrollton, TX 75006

Phone 972-242-2754

Fax 972-242-2798

CA Labs, L.L.C.

12232 Industriplex, Suite 32

Baton Rouge, LA 70809

Phone 225-751-5632

Fax 225-751-5634

CA Labs Project #:

Asbestos & Technical Services

061319FEW155, FE Warren

Bldg. 155

CAL19063874AG

P.O. Box 2574

Cheyenne, WY 82003 Date:

Turnaround Time: Samples Received:

307-214-0904 24 hours Date Of Sampling:

Purchase Order #:

Sample # Com ment

Layer

Analysts Physical Description of

Subsample

Homo-geneo us

(Y/N)

Asbestos type / calibrated visual estimate percent

Non-asbestos fiber type / percent

Non-fibrous type

/ percent

7-2 white drywall with paper n None Detected 10% ce 90% qu,gy

061319FE

W155-8 8-1 Wall Patching/ gray sealant y None Detected 100% qu,ca

061319FE

W155-9 9-1 Black Sealant/ tan surfacing y None Detected 100% qu,bi

061319FE

W155-10 10-1

CMU Surface Compound/ gray plaster y None Detected 100% qu,ca

061319FE

W155-11 11-1 Pipe Sealant/ tan covering n None Detected

20% fg

30% ce 50% qu,ma,bi

11-2 yellow fibrous insulation y None Detected 100% fg

061319FE

W155-12 12-1

CMU Surface Compound/ gray surfaced tan finishing compound n None Detected 100% qu,mi,bi,ca

Dallas NVLAP Lab Code 200349-0 TEM/PLM TCEQ# T104704513-15-3 TDH 30-0235

AIHA LAP, LLC Laboratory #102929 Analysis Method: Interim (40CFR Part 763 Appendix E to Subpart E) / Improved (EPA-600 / R-93/116). All samples received in good condition unless noted.

Preparation Method: HCL acid washing for carbonate based samples, chemical reduction for organically bound components, oil immersion for identification of asbestos types by dispersion attaining / becke line method.

ca - carbonate gy - gypsum bi - binder or - organic ma - matrix mi - mica ve - vermiculite ot -other pe - perlite qu - quartz fg - fiberglass mw - mineral wool wo - wollastonite ta - talc sy - synthetic ce - cellulose br - brucite ka - kaolin (clay) pa - palygorskite (clay) Approved Signatories:

Stanley Massett Technical Manager

Analyst Tanner Rasmussen

1. Fire Damage significant fiber damage - reported percentages reflect unaltered fibers

2. Fire Damage no significant fiber damages effecting fibrous percentages

3. Actinolite in association with Vermiculite

4. Layer not analyzed - attached to previous positive layer and contamination is suspected

5. Not enough sample to analyze

6. Anthophyllite in association with Fibrous Talc

7. Contamination suspected from other building materials

8. Favorable scenario for water separation on vermiculite for possible analysis by another method

9. < 1% Result point counted positive

/data/wordandspreadsheets/templates/asbestos/PLMReport.xls (Revision 3 3/7/17) Page 4 of 5

6/17/2019

6/14/19 10:30AM

Phone # 6/13/2019

Fax #

Senior Analyst

Julio Robles

CA Labs

Dedicated to Dedicated to Dedicated to Dedicated to

QualityQualityQualityQuality

Crisp Analytical, L.L.C.

1929 Old Denton Road

Carrollton, TX 75006

Phone 972-242-2754

Fax 972-242-2798

CA Labs, L.L.C.

12232 Industriplex, Suite 32

Baton Rouge, LA 70809

Phone 225-751-5632

Fax 225-751-5634

CA Labs Project #:

Asbestos & Technical Services

061319FEW155, FE Warren

Bldg. 155

CAL19063874AG

P.O. Box 2574

Cheyenne, WY 82003 Date:

Turnaround Time: Samples Received:

307-214-0904 24 hours Date Of Sampling:

Purchase Order #:

Sample # Com ment

Layer

Analysts Physical Description of

Subsample

Homo-geneo us

(Y/N)

Asbestos type / calibrated visual estimate percent

Non-asbestos fiber type / percent

Non-fibrous type

/ percent

061319FE

W155-13 13-1

CMU Surface Compound/ tan surfaced tan finishiing compound n None Detected 100% qu,mi,bi,ca

13-2 gray plaster y None Detected 100% qu,ca

061319FE

W155-14 14-1

CMU Surface Compound/ tan surfaced tan finishiing compound n None Detected 100% qu,mi,bi,ca

14-2 gray plaster y None Detected 100% qu,ca

061319FE

W155-15 15-1

T-Lock Shingle and Tar/ black roofing shingle with brown gravel y None Detected 6% ce 94% qu,bi

061319FE

W155-16 16-1

Drywall/ tan surfaced tan compound n 2% Chrysotile 98% qu,mi,bi,ca

16-2 tan compound (beneath tape) y 2% Chrysotile 98% qu,mi,ca

Dallas NVLAP Lab Code 200349-0 TEM/PLM TCEQ# T104704513-15-3 TDH 30-0235

AIHA LAP, LLC Laboratory #102929 Analysis Method: Interim (40CFR Part 763 Appendix E to Subpart E) / Improved (EPA-600 / R-93/116). All samples received in good condition unless noted.

Preparation Method: HCL acid washing for carbonate based samples, chemical reduction for organically bound components, oil immersion for identification of asbestos types by dispersion attaining / becke line method.

ca - carbonate gy - gypsum bi - binder or - organic ma - matrix mi - mica ve - vermiculite ot -other pe - perlite qu - quartz fg - fiberglass mw - mineral wool wo - wollastonite ta - talc sy - synthetic ce - cellulose br - brucite ka - kaolin (clay) pa - palygorskite (clay) Approved Signatories:

Stanley Massett Technical Manager

Analyst Tanner Rasmussen

1. Fire Damage significant fiber damage - reported percentages reflect unaltered fibers

2. Fire Damage no significant fiber damages effecting fibrous percentages

3. Actinolite in association with Vermiculite

4. Layer not analyzed - attached to previous positive layer and contamination is suspected

5. Not enough sample to analyze

6. Anthophyllite in association with Fibrous Talc

7. Contamination suspected from other building materials

8. Favorable scenario for water separation on vermiculite for possible analysis by another method

9. < 1% Result point counted positive

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