Lead Test.pdf

05/23/2022Printed

Project

OTIE-L

1010659

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

8:55

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

OTIE-Barksdale

TABLE OF CONTENTS

PagesDescriptionReport Name

This report consists of this Table of Contents and the following pages:

1010659_r02_01_ProjectSamples Ana-Lab Project P:1010659 C:OTIE Project Sample Cross Reference t:304

1010659_r03_03_ProjectResults Ana-Lab Project P:1010659 C:OTIE Project Results t:304 4

1010659_r10_05_ProjectQC Ana-Lab Project P:1010659 C:OTIE Project Quality Control Groups 1

1010659_r99_09_CoC__1_of_1 Ana-Lab CoC OTIE 1010659_1_of_1 1

8 Total Pages:

Form rptTOC1N Created 12/19/2019 v.2.0LDSClient v1.18.20.2160

Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Email: projectmanger@ana-lab.com

Report Page 1 of 9

Sample Cross Reference

1010659

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-Barksdale

5/23/2022Printed

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

2089281 HW22007 Bldg 5755 Paint Chips 05/06/2022 07:30:00 05/06/2022

Bottle 01 Plastic bag

Bottle 02 Prepared Bottle: TCLP Extract (Batch 1006729) Volume: 1128.00000 mL <== Derived from 01 ( 56.4 ml )

Bottle 03 Prepared Bottle: TCLP Extract for Metals (Batch 1006729) Volume: 1128.00000 mL <== Derived from 01 ( 56.4 ml )

Bottle 04 Prepared Bottle: TCLP Acid Digestion (Batch 1006932) Volume: 50.00000 mL <== Derived from 03 ( 10 ml )

ReceivedTimeTakenSample IDSample

Method Bottle PrepSet Preparation QcGroup Analytical

EPA 6020A 04 05/12/2022 1007611 05/17/20221006932

2089282 HW22008 Bldg 5766 Paint Chips 05/06/2022 07:45:00 05/06/2022

Bottle 01 Plastic bag

Bottle 02 Prepared Bottle: TCLP Extract (Batch 1006729) Volume: 1156.00000 mL <== Derived from 01 ( 57.8 ml )

Bottle 03 Prepared Bottle: TCLP Extract for Metals (Batch 1006729) Volume: 1156.00000 mL <== Derived from 01 ( 57.8 ml )

Bottle 04 Prepared Bottle: TCLP Acid Digestion (Batch 1006932) Volume: 50.00000 mL <== Derived from 03 ( 10 ml )

ReceivedTimeTakenSample IDSample

Method Bottle PrepSet Preparation QcGroup Analytical

EPA 6020A 04 05/12/2022 1007611 05/17/20221006932

2089283 HW22009 Bldg 5743 Paint Chips 05/06/2022 08:00:00 05/06/2022

Bottle 01 Plastic bag

Bottle 02 Prepared Bottle: TCLP Extract (Batch 1006729) Volume: 1366.00000 mL <== Derived from 01 ( 68.3 ml )

Bottle 03 Prepared Bottle: TCLP Extract for Metals (Batch 1006729) Volume: 1366.00000 mL <== Derived from 01 ( 68.3 ml )

Bottle 04 Prepared Bottle: TCLP Acid Digestion (Batch 1006932) Volume: 50.00000 mL <== Derived from 03 ( 10 ml )

ReceivedTimeTakenSample IDSample

Method Bottle PrepSet Preparation QcGroup Analytical

EPA 6020A 04 05/12/2022 1007611 05/17/20221006932

2089284 HW22010 Bldg 5778 Paint Chips 05/06/2022 08:10:00 05/06/2022

Bottle 01 Plastic bag

Bottle 02 Prepared Bottle: TCLP Extract (Batch 1006729) Volume: 790.00000 mL <== Derived from 01 ( 39.5 ml )

Bottle 03 Prepared Bottle: TCLP Extract for Metals (Batch 1006729) Volume: 790.00000 mL <== Derived from 01 ( 39.5 ml )

Bottle 04 Prepared Bottle: TCLP Acid Digestion (Batch 1006932) Volume: 50.00000 mL <== Derived from 03 ( 10 ml )

ReceivedTimeTakenSample IDSample

Form rptPROJPrepN Created 12'20/2019 v1.1LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 2 of 9

Sample Cross Reference

1010659

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-Barksdale

5/23/2022Printed

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

2089284 HW22010 Bldg 5778 Paint Chips 05/06/2022 08:10:00 05/06/2022

Bottle 01 Plastic bag

Bottle 02 Prepared Bottle: TCLP Extract (Batch 1006729) Volume: 790.00000 mL <== Derived from 01 ( 39.5 ml )

Bottle 03 Prepared Bottle: TCLP Extract for Metals (Batch 1006729) Volume: 790.00000 mL <== Derived from 01 ( 39.5 ml )

Bottle 04 Prepared Bottle: TCLP Acid Digestion (Batch 1006932) Volume: 50.00000 mL <== Derived from 03 ( 10 ml )

ReceivedTimeTakenSample IDSample

Method Bottle PrepSet Preparation QcGroup Analytical

EPA 6020A 04 05/12/2022 1007611 05/17/20221006932

Form rptPROJPrepN Created 12'20/2019 v1.1LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 3 of 9

05/23/2022Printed:

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-L

1010659

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

OTIE-Barksdale

Results

Sample Results

2089281 HW22007 Bldg 5755 Paint Chips

07:30:00

ClientCollected by:

05/06/2022Received:

Solid & Chemical Materials

Taken:

Oneida Total Integra PO:

05/06/2022

EPA 6020A 05/17/2022 19:11:00 CSF1007611Analyzed

Parameter Results Units RL Flags CAS Bottle

1006932 13:50:0005/12/2022Prepared:

55.6 mg/L E0.050 7439-92-1TCLP Lead 04NELAC

2089282 HW22008 Bldg 5766 Paint Chips

07:45:00

ClientCollected by:

05/06/2022Received:

Solid & Chemical Materials

Taken:

Oneida Total Integra PO:

05/06/2022

EPA 6020A 05/17/2022 19:22:00 CSF1007611Analyzed

Parameter Results Units RL Flags CAS Bottle

1006932 13:50:0005/12/2022Prepared:

60.1 mg/L E0.050 7439-92-1TCLP Lead 04NELAC

2089283 HW22009 Bldg 5743 Paint Chips

08:00:00

ClientCollected by:

05/06/2022Received:

Solid & Chemical Materials

Taken:

Oneida Total Integra PO:

05/06/2022

EPA 6020A 05/17/2022 19:26:00 CSF1007611Analyzed

Parameter Results Units RL Flags CAS Bottle

1006932 13:50:0005/12/2022Prepared:

37.5 mg/L 0.050 7439-92-1TCLP Lead 04NELAC

2089284 HW22010 Bldg 5778 Paint Chips

08:10:00

ClientCollected by:

05/06/2022Received:

Solid & Chemical Materials

Taken:

Oneida Total Integra PO:

05/06/2022

Form rptPROJRESN Created 12/19/2019v1.2LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 4 of 9

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-L

1010659

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

2089284 HW22010 Bldg 5778 Paint Chips

08:10:00

ClientCollected by:

05/06/2022Received:

Solid & Chemical Materials

Taken:

Oneida Total Integra PO:

05/06/2022

EPA 6020A 05/17/2022 19:30:00 CSF1007611Analyzed

Parameter Results Units RL Flags CAS Bottle

1006932 13:50:0005/12/2022Prepared:

169 mg/L E0.050 7439-92-1TCLP Lead 04NELAC

Sample Preparation

2089281 HW22007 Bldg 5755 Paint Chips 05/06/2022Received:

05/06/2022

05/09/2022 13:17:02 CALCalculated13:17:0205/09/2022Prepared:

VerifiedEnvironmental Fee (per Project)z

EPA 1311 05/11/2022 16:00:00 SRH1006729Analyzed1006729 16:00:0005/11/2022Prepared:

SOL EXT 1 mlTCLP Extraction Non-Volatile 01NELAC

EPA 3005A 05/12/2022 13:50:00 CAS1006932Analyzed1006729 16:00:0005/11/2022Prepared:

50/10 mlMetals Digestion TCLP Extract 03z

2089282 HW22008 Bldg 5766 Paint Chips 05/06/2022Received:

05/06/2022

EPA 1311 05/11/2022 16:00:00 SRH1006729Analyzed1006729 16:00:0005/11/2022Prepared:

SOL EXT 1 mlTCLP Extraction Non-Volatile 01NELAC

Form rptPROJRESN Created 12/19/2019v1.2LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 5 of 9

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-L

1010659

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

2089282 HW22008 Bldg 5766 Paint Chips 05/06/2022Received:

05/06/2022

EPA 3005A 05/12/2022 13:50:00 CAS1006932Analyzed1006729 16:00:0005/11/2022Prepared:

50/10 mlMetals Digestion TCLP Extract 03z

2089283 HW22009 Bldg 5743 Paint Chips 05/06/2022Received:

05/06/2022

EPA 1311 05/11/2022 16:00:00 SRH1006729Analyzed1006729 16:00:0005/11/2022Prepared:

SOL EXT 1 mlTCLP Extraction Non-Volatile 01NELAC

EPA 3005A 05/12/2022 13:50:00 CAS1006932Analyzed1006729 16:00:0005/11/2022Prepared:

50/10 mlMetals Digestion TCLP Extract 03z

2089284 HW22010 Bldg 5778 Paint Chips 05/06/2022Received:

05/06/2022

EPA 1311 05/11/2022 16:00:00 SRH1006729Analyzed1006729 16:00:0005/11/2022Prepared:

SOL EXT 1 mlTCLP Extraction Non-Volatile 01NELAC

EPA 3005A 05/12/2022 13:50:00 CAS1006932Analyzed1006729 16:00:0005/11/2022Prepared:

50/10 mlMetals Digestion TCLP Extract 03z

Form rptPROJRESN Created 12/19/2019v1.2LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 6 of 9

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066

Project

OTIE-L

1010659

2600 Dudley Rd. Kilgore, Texas 75662 R: 3306 State Highway 135 N, Kilgore, TX 75662 Office: 903-984-0551 * Fax: 903-984-5914

Qualifiers:

E - Estimated Value

We report results on an As Received (or Wet) basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at

Ana-lab corporate laboratory which holds International, Federal, and state accreditations. Please see https://www.ana-lab-work.com/index.php/accreditations/

These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of

Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.

RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical

Abstract Service number. RL is our Reporting Limit, or Minimum Quantitation Level. The RL takes into account the Instrument

Detection Limit (IDL), Method Detection Limit (MDL), and Practical Quantitation Limit (PQL), and any dilutions and/or concentrations performed during sample preparation (EQL). Our analytical result must be above this RL before we report a value in the 'Results' column of our report (without a 'J' flag). Otherwise, we report ND (Not Detected above RL), because the result is "<" (less than) the number in the RL column. MAL is Minimum Analytical Level and is typically from regulatory agencies. Unless we report a result in the result column, or interferences prevent it, we work to have our RL at or below the MAL.

Trey Peery, MA, Project Manager

Form rptPROJRESN Created 12/19/2019v1.2LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 7 of 9

Project

OTIE-L

1010659

Quality Control

Oneida Total Integrated Enterprises (OTIE)

Keely Meadows

1220 Kennestone Circle

Suite 106

Marietta, GA 30066 Printed 05/23/2022

EPA 6020A 1007611Analytical Set

Blank

FileUnitsMQLMDLReadingPrepSetParameter

TCLP Lead 1006932 ND 0.010 0.010 mg/L 123640120

CCV

FileLimits%Recover%UnitsKnownReadingParameter

TCLP Lead 0.049 0.05 mg/L 98.0 90.0 - 110 123640119

TCLP Lead 0.0531 0.05 mg/L 106 90.0 - 110 123640126

TCLP Lead 0.0504 0.05 mg/L 101 90.0 - 110 123640135

ICV

FileLimits%Recover%UnitsKnownReadingParameter

TCLP Lead 0.0507 0.05 mg/L 101 90.0 - 110 123640078

LCS Dup

Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter

TCLP Lead 1006932 0.504 0.507 0.500 85.1 - 115 101 101 mg/L 0.593 14.0

MSD

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

TCLP Lead 2089582 2.52 2.54 0.0362 2.50 85.0 - 116 99.4 100 mg/L 0.802 20.0

* Out RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%

Blank - Method Blank (reagent water or other blank matrices that contains all reagents except standard(s) and is processed simultaneously with and under the same conditions as samples; carried through preparation and analytical procedures exactly like a sample; monitors); CCV - Continuing Calibration Verification (same standard used to prepare the curve; typically a mid-range concentration; verifies the continued validity of the calibration curve); MSD - Matrix Spike Duplicate (replicate of the matrix spike; same solution and amount of target analyte added to the MS is added to a third aliquot of sample; quantifies matrix bias and precision.); ICV - Initial

Calibration Verification; LCS Dup - Laboratory Control Sample Duplicate (replicate LCS; analyzed when there is insufficient sample for duplicate or MSD; quantifies accuracy and precision.)

Form rptPROJQCGN Created 12/30//2019 v1.0LDSClient v1.18.20.2160 Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111

Report Page 8 of 9

1010659 CoC Print Group 001 of 001

Report Page 9 of 9