BB90 Geotechnical Data Report STEP 1 Pg 269-562.pdf

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Attached to
Big Bend Left Abutment Collector Pipe System Federal contract opportunity
Solicitation number
W9128F23B0005
Issued by
Department of the Army Corps of Engineers Engineering District Omaha

About this file

This federal contract opportunity solicitation is for the Big Bend Replacement of Left Abutment Collector Pipe System project located in Fort Thompson, South Dakota. The contractor shall furnish all personnel, services, equipment, materials and other requirements necessary for replacement of slotted and solid pipes, placement of a two stage filter, installation of manholes, backfill, and seeding. A two-step IFB process will be used, with step one proposals due by January 4, 2023 at 2:00 PM Central Time. A site visit is scheduled for December 12, 2022 at 10:00 AM Central Time. The solicitation number is W9128F23B0005 and is being conducted by the Department of the Army Corps of Engineers Omaha District.

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Appendix C: Laboratory Data

1" 3/4" 1/2" 3/8" #4 #10 #20 #40 #80 #200 LL PL PI

PH21-01

D-3

1.7'-2.0' SC 100.0 100.0 100.0 100.0 100.0 97.8 89.4 75.9 51.9 15.3 Visual Class, Sieve Hydro

D-4 3.0'-4.1' 10YR 4/2 Dark Grayish Brown Poorly

Graded Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 98.5 76.8 29.4 14.4 7.9 Visual Class, Sieve Hydro

D-6 5.5'-5.9' 2.5Y 5/2 Grayish Brown Silty, Clayey

Sand SC-SM 100.0 100.0 100.0 100.0 100.0 100.0 99.7 95.3 64.6 15.1 Visual Class, Sieve Hydro

D-8 8.0'-9.5' 2.5Y 5/1 Gray Lean Clay with Sand CL 100.0 100.0 100.0 100.0 100.0 100.0 99.4 97.2 90.8 82.8 30 22 8 Visual Class, Sieve Hydro, AL

D-10 18.0'-19.5' 2.5Y 6/2 Light Brownish Gray Poorly

Graded Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 97.7 88.5 49.9 5.7 Visual Class, Sieve Hydro

D-12 28.0'-29.5' 2.5Y 4/3 Olive Brown Poorly Graded

Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 98.6 86.9 43.7 5.8 Visual Class, Sieve Hydro

D-14 38.0'-39.5' 2.5Y 4/3 Olive Brown Poorly Graded

Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 98.9 85.7 43.3 7.5 Visual Class, Sieve Hydro

PH21-02

D-2

1.0'-2.0' 10YR 4/4 Dark Yellowish Brown

Clayey Sand SC 100.0 100.0 100.0 97.6 95.5 89.3 63.4 27.6 17.6 13.0 Visual Class, Sieve Hydro

D-3 3.0'-4.0' 2.5Y 5/1 Gray Clayey Sand SC 100.0 100.0 100.0 97.0 95.1 93.8 91.5 83.1 55.2 14.5 Visual Class, Sieve Hydro

D-4 4.0'-4.5' 2.5Y 4/1 Dark Gray Sandy Lean Clay CL 100.0 100.0 100.0 100.0 100.0 96.2 90.2 84.2 73.9 60.7 32 19 13 Visual Class, Sieve Hydro, AL

D-7 8.6'-9.5' 2.5Y 6/2 Light Brownish Gray Poorly

Graded Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 99.9 97.6 63.8 9.5 Visual Class, Sieve Hydro

D-9 18.0'-19.5' 2.5Y 5/3 Light Olive Brown Poorly

Graded Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 98.7 90.4 52.9 6.8 Visual Class, Sieve Hydro

D-10 23.0'-24.5' 2.5Y 5/2 Grayish Brown Poorly Graded

Sand SP 100.0 100.0 100.0 100.0 100.0 99.9 94.9 73.6 19.1 4.1 Visual Class, Sieve Hydro

D-12 33.0'-34.5' 2.5Y 5/2 Grayish Brown Poorly Graded

Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 95.1 51.3 10.8 4.0 Visual Class, Sieve Hydro

PH21-03

D-2

28.0'-29.5' 2.5Y 4/3 Olive Brown Poorly Graded

Sand with Silt SP-SM 100.0 100.0 100.0 100.0 100.0 99.8 95.6 77.7 44.3 6.2 Visual Class, Sieve Hydro

D-3 33.0'-34.5' 2.5Y 4/3 Olive Brown Poorly Graded

Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 99.6 93.2 45.7 6.0 Visual Class, Sieve Hydro

Terracon Project No. 05215156

USCSDepth (ft)

2.5Y 4/3 Olive Brown Clayey Sand

AtterbergSieve % Passing

Big Bend Dam RW Collector Pipe Replacement Fort Thompson, SD

Required Tests

Received 6-28-2021

DescriptionBoring and Sample Nos.

Terracon Project No. 05215156

USCSDepth (ft)

AtterbergSieve % Passing

Big Bend Dam RW Collector Pipe Replacement Fort Thompson, SD

Required Tests

Received 6-28-2021

DescriptionBoring and Sample Nos.

D-4 38.0'-39.5' 2.5Y 5/2 Grayish Brown Poorly Graded

Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 96.6 51.9 9.6 3.0 Visual Class, Sieve Hydro

PH21-04

D-1

18.0'-19.5' 2.5Y 6/1 Dark Gray Poorly Graded

Sand SP 100.0 100.0 100.0 100.0 100.0 99.9 97.3 80.1 35.2 2.7 Visual Class, Sieve Hydro

D-3 28.0'-29.5' 2.5Y 6/1 Dark Gray Poorly Graded

Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 98.2 84.2 40.8 4.2 Visual Class, Sieve Hydro

PH21-05

D-1

18.0'-19.5' 2.5Y 5/1 Gray Poorly Graded Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 98.0 75.2 33.1 3.8 Visual Class, Sieve Hydro

D-2 23.0'-24.5' 2.5Y 5/1 Gray Poorly Graded Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 98.4 68.2 7.9 2.4 Visual Class, Sieve Hydro

D-11 63.0'-64.5' Gley 1 4/N Dark Gray Sandy Silt ML 100.0 100.0 100.0 100.0 100.0 100.0 100.0 99.9 99.0 53.1 Visual Class, Sieve Hydro

D-13 74.5'-76.0' Gley 1 5/N Gray Poorly Graded Sand with Silt SP-SM 100.0 100.0 100.0 100.0 99.1 97.8 94.2 78.5 26.3 10.2 Visual Class, MA

D-14 78.0'-79.5' 2.5Y 5/1 Gray Silty Sand SM 100.0 100.0 100.0 100.0 100.0 99.4 97.2 76.9 39.8 17.3 Visual Class, Sieve Hydro

D-16 84.1'-84.5' 2.5Y 4/1 Dark Gray Well Graded Sand with Silt and Gravel SW-SM 100.0 100.0 94.3 91.8 83.5 72.4 53.0 32.7 14.0 7.0 Visual Class, MA

PH21-06B

D-3

4.0'-4.5' 2.5Y 5/1 Gray Sandy Lean Clay CL 100.0 100.0 100.0 100.0 99.7 98.5 96.0 90.8 75.4 60.2 26 18 8 Visual Class, Sieve Hydro, AL

D-5 8.0'-9.5' 2.5Y 5/2 Grayish Brown Silty Sand SM 100.0 100.0 100.0 100.0 100.0 100.0 99.0 86.2 44.8 14.5 Visual Class, Sieve Hydro

D-6 13.0'-14.5' 2.5Y 5/2 Grayish Brown Poorly Graded

Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 99.2 87.2 44.6 8.1 Visual Class, Sieve Hydro

PH21-06

D-2

23.0'-24.5' 2.5Y 4/3 Olive Brown Poorly Graded

Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 99.5 90.4 51.5 7.9 Visual Class, Sieve Hydro

D-9 48.0'-49.5' 2.5Y 5/1 Gray Sandy Silt ML 100.0 100.0 100.0 100.0 100.0 100.0 99.9 99.2 95.7 64.4 Visual Class, Sieve Hydro

D-10 53.0'-53.7' 2.5Y 3/1 Very Dark Gray Silty Sand SM 100.0 100.0 100.0 100.0 98.9 98.5 95.8 88.8 44.7 19.6 Visual Class, Sieve Hydro

D-11 53.7'-54.5' 2.5Y 3/1 Very Dark Gray Sandy Silt ML 100.0 100.0 100.0 100.0 100.0 99.9 99.8 99.4 96.6 51.3 Visual Class, Sieve Hydro

Terracon Project No. 05215156

USCSDepth (ft)

AtterbergSieve % Passing

Big Bend Dam RW Collector Pipe Replacement Fort Thompson, SD

Required Tests

Received 6-28-2021

DescriptionBoring and Sample Nos.

D-12 58.0'-60.0' 2.5Y 3/1 Very Dark Gray Poorly

Graded Sand SP 100.0 100.0 100.0 100.0 100.0 100.0 99.6 91.6 19.9 4.8 Visual Class, Sieve Hydro

D-13 63.5'-65.0' 2.5Y 3/2 Very Dark Grayish Brown

Clayey Sand SC 100.0 100.0 100.0 100.0 99.5 99.3 98.8 94.9 59.8 12.6 Visual Class, Sieve Hydro

D-15 69.0'-69.5' 10YR 5/2 Grayish Brown Well Graded

Sand with Silt SW-SM 100.0 100.0 100.0 98.9 91.0 82.5 72.3 36.3 12.1 8.3 Visual Class, MA

D-16 73.0'-73.8' 10YR 5/2 Grayish Brown Well Graded

Sand with Clay SW-SC 100.0 100.0 93.6 93.6 88.6 76.4 39.4 17.0 11.4 9.3 Visual Class, Sieve Hydro

D-17 73.8'-74.5' 2.5Y 4/2 Dark Grayish Brown Silty

Sand SM 100.0 100.0 96.0 96.0 95.1 94.6 93.9 87.5 48.7 15.2 Visual Class, Sieve Hydro

D-18 78.0'-79.5' 2.5Y 5/2 Grayish Brown Poorly Graded

Sand with Silt SP-SM 100.0 100.0 100.0 100.0 99.8 98.9 90.9 61.3 25.4 7.7 Visual Class, MA

BH20-01

D-7

9.0'-10.0' 2.5Y 6/2 Light Brownish Gray Poorly

Graded Sand with Clay SP-SC 100.0 100.0 100.0 100.0 100.0 100.0 91.6 63.9 31.1 5.8 Visual Class, Sieve Hydro

BH20-02

D-5

8.0'-10.0' 2.5Y 6/2 Light Brownish Gray Silty

Sand SM 100.0 100.0 100.0 100.0 100.0 100.0 99.4 90.2 59.0 16.0 Visual Class, Sieve Hydro

BH20-03

D-4

3.0'-40' 10YR 4/4 Dark Yellowish Brown

Clayey Sand SC 100.0 100.0 100.0 98.5 93.8 86.1 62.4 36.0 25.1 17.3 Visual Class, Sieve Hydro

BH20-04

D-5

6.5'-8.5' SM 100.0 100.0 100.0 100.0 100.0 99.6 95.9 87.1 74.0 45.9 Visual Class, Sieve Hydro

BH20-06

D-8

13.0'-14.5' 2.5Y 6/3 Light Yellowish Brown Silty

Sand SM 100.0 100.0 100.0 100.0 100.0 99.5 97.3 92.7 59.3 24.1 Visual Class, Sieve Hydro

2.5Y 6/3 Light Yellowish Brown Silty Sand

0 20 40 60 80 100

CH

or

O H

CL

or

O L

ML or OL

MH or OH

"U " L ine

"A " L ine

ATTERBERG LIMITS RESULTS

ASTM D4318

P L A S T I C I T Y

I N D E X

LIQUID LIMIT

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-1

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

A T

E D

F R

O M

O R

IG

IN

A L

R E

P O

R T

A

T T

E R

B E

R G

L

IM

IT

S

B

IG

B

E N

D R

W C

O

LL

E .G

P J

T E

R R

A C

O N

_D A

T A

T E

M P

LA

T

E .G

D T

/2

8/

PH21-01

PH21-02

PH21-06B

LL

Boring ID Depth PIPL

8 - 9.5 4 - 4.5 4 - 4.5

CL

CL

CL

Lean Clay with Sand

Sandy Lean Clay

Sandy Lean Clay

DescriptionUSCSFines

82.8 60.7 60.2

CL-ML

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

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E N

T F

IN

E

R B

Y W

E

IG

H T

P E

R C

E N

T C

O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-1

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

A T

E D

F R

O M

O R

IG

IN

A L

R E

P O

R T

G

R A

IN

S

IZ

E

: U S

C S

B

IG

B E

N D

R W

C O

LL

E

.G P

J T

E R

R A

C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 98.53 93.82 86.08 62.39 36.02 25.06 17.26

100.0 99.36 90.16 58.98 16.03

100.0 91.62 63.86 31.09 5.8

1/2" 3/8" #4 #10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

BH20-01

BH20-02

BH20-03

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

Silty Sand (SM)

Clayey Sand (SC)

2.5Y 6/2 Light Grayish Brown

2.5Y 6/2 Light Grayish Brown

10YR 4/4 Dark Yellowish Brown

#10 #20 #40 #80 #200

2.5 10.6 5.0

3.3 5.5 12.3

94.2 84.0 76.6

0.0 0.0 0.0

9 - 10 8 - 10 3 - 4

0.0 0.0 6.2

SP-SC

SM

SC

0.384 0.185 0.798

0.173 0.1 0.265

0.087 0.034 0.002

4.43 5.45 351.77

0.90 1.58 38.79

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

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IN

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R B

Y W

E

IG

H T

P E

R C

E N

T C

O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-2

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

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F R

O M

O R

IG

IN

A L

R E

P O

R T

G

R A

IN

S

IZ

E

: U S

C S

B

IG

B E

N D

R W

C O

LL

E

.G P

J T

E R

R A

C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 97.81 89.36 75.93 51.86 15.26

100.0 99.53 97.26 92.68 59.33 24.12

100.0 99.6 95.93 87.11 73.99 45.92

#4 #10 #20 #40 #80 #200

#4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

BH20-04

BH20-06

PH21-01

USCS% CLAY% FINES

D60

Silty Sand (SM)

Silty Sand (SM)

Clayey Sand (SC)

2.5Y 6/3 Light Yellowish Brown

2.5Y 6/3 Light Yellowish Brown

2.5Y 4/3 Olive Brown

#4 #10 #20 #40 #80 #200

37.0 16.1 6.1

8.9 8.1 9.2

54.1 75.9 84.7

0.0 0.0 0.0

6.5 - 8.5 13 - 14.5

1.7 - 2

0.0 0.0 0.0

SM

SM

SC

0.116 0.183 0.241

0.035 0.087 0.107

0.008 0.01 0.008

15.05 18.60 29.93

1.34 4.18 5.88

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

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IN

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E

IG

H T

P E

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E N

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O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-3

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

A T

E D

F R

O M

O R

IG

IN

A L

R E

P O

R T

G

R A

IN

S

IZ

E

: U S

C S

B

IG

B E

N D

R W

C O

LL

E

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J T

E R

R A

C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.4 97.15 90.76 82.75

100.0 99.72 95.29 64.63 15.06

100.0 98.54 76.81 29.41 14.36 7.88

#10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-01

PH21-01

PH21-01

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

Silty, Clayey Sand (SC-SM)

Lean Clay with Sand (CL)

10YR 4/2 Dark Grayish Brown

2.5Y 5/2 Grayish Brown

2.5Y 5/1 Gray

#4 #10 #20 #40 #80 #200

2.8 7.9 62.7

5.1 7.1 20.0

92.1 84.9 17.2

0.0 0.0 0.0

3 - 4.1

5.5 - 5.9 8 - 9.5

0.0 0.0 0.0

SP-SC

SC-SM

CL

0.665 0.166 0.036

0.429 0.098 0.014

0.1 0.036

6.65 4.60

2.77 1.59

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

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IG

H T

P E

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E N

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O A

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B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-4

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

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V A

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IF

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IN

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C S

B

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B E

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J T

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C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 98.94 85.67 43.3 7.51

100.0 98.6 86.85 43.71 5.76

100.0 97.73 88.52 49.9 5.7

#10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-01

PH21-01

PH21-01

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

Poorly Graded Sand with Clay (SP-SC)

Poorly Graded Sand with Clay (SP-SC)

2.5Y 6/2 Light Brownish Gray

2.5Y 4/3 Olive Brown

2.5Y 4/3 Olive Brown

#10 #20 #40 #80 #200

1.8 2.2 3.2

3.9 3.6 4.3

94.3 94.2 92.5

0.0 0.0 0.0

18 - 19.5 28 - 28.5 38 - 39.5

0.0 0.0 0.0

SP-SC

SP-SC

SP-SC

0.225 0.249 0.253

0.121 0.131 0.13

0.082 0.083 0.08

2.76 3.01 3.17

0.80 0.84 0.84

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

R C

E N

T F

IN

E

R B

Y W

E

IG

H T

P E

R C

E N

T C

O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-5

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

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IN

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P

LA

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 96.17 90.23 84.23 73.93 60.68

100.0 96.96 95.1 93.83 91.51 83.1 55.17 14.48

100.0 97.57 95.49 89.25 63.42 27.64 17.62 13.03

#4 #10 #20 #40 #80 #200

1/2" 3/8" #4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-02

PH21-02

PH21-02

USCS% CLAY% FINES

D60

Clayey Sand (SC)

Clayey Sand (SC)

Sandy Lean Clay (CL)

10YR 4/4 Dark Yellowish Brown

2.5Y 5/1 Gray

2.5Y 4/1 Dark Gray

1/2" 3/8" #4 #10 #20 #40 #80 #200

3.4 6.8 37.7

9.7 7.7 23.0

82.5 80.6 39.3

0.0 0.0 0.0

1 - 2 3 - 4

4 - 4.5

4.5 4.9 0.0

SC

SC

CL

0.796 0.209 0.072

0.445 0.105 0.014

0.006 0.034

139.67 6.07

43.67 1.53

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-6

15080 A Cir Omaha, NE

LA

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.89 94.88 73.63 19.12 4.11

100.0 98.67 90.35 52.86 6.8

100.0 99.88 97.59 63.76 9.51

#4 #10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-02

PH21-02

PH21-02

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

Poorly Graded Sand with Clay (SP-SC)

Poorly Graded Sand (SP)

2.5Y 6/2 Light Brownish Gray

2.5Y 5/3 Light Olive Brown

2.5Y 5/2 Grayish Brown

#10 #20 #40 #80 #200

4.3 2.5 0.8

5.2 4.4 3.3

90.5 93.2 95.9

0.0 0.0 0.0

8.6 - 9.5 18 - 19.5 23 - 24.5

0.0 0.0 0.0

SP-SC

SP-SC

SP

0.169 0.212 0.343

0.104 0.117 0.214

0.076 0.08 0.106

2.24 2.66 3.24

0.85 0.80 1.26

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-7

15080 A Cir Omaha, NE

LA

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.63 93.2 45.66 6.03

100.0 99.79 95.57 77.71 44.26 6.15

100.0 95.06 51.26 10.8 4.04

#10 #20 #40 #80 #200

#4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-02

PH21-03

PH21-03

USCS% CLAY% FINES

D60

Poorly Graded Sand (SP)

Poorly Graded Sand with Silt (SP-SM)

Poorly Graded Sand with Clay (SP-SC)

2.5Y 5/2 Grayish Brown

2.5Y 4/3 Olive Brown

2.5Y 4/3 Olive Brown

#10 #20 #40 #80 #200

1.6 3.6 2.5

2.4 2.5 3.6

96.0 93.8 94.0

0.0 0.0 0.0

33 - 34.5 28 - 29.5 33 - 34.5

0.0 0.0 0.0

SP

SP-SM

SP-SC

0.488 0.27 0.233

0.271 0.13 0.127

0.162 0.082 0.082

3.01 3.29 2.85

0.92 0.76 0.85

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-8

15080 A Cir Omaha, NE

LA

B

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/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 98.17 84.23 40.75 4.21

100.0 99.92 97.32 80.1 35.19 2.74

100.0 96.62 51.85 9.6 2.97

#10 #20 #40 #80 #200

#4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-03

PH21-04

PH21-04

USCS% CLAY% FINES

D60

Poorly Graded Sand (SP)

Poorly Graded Sand (SP)

Poorly Graded Sand (SP)

10YR 5/2 Grayish Brown

2.5Y 6/1 Gray

2.5Y 6/1 Gray

#10 #20 #40 #80 #200

0.6 0.6 1.5

2.3 2.2 2.7

97.0 97.3 95.8

0.0 0.0 0.0

38 - 39.5 18 - 19.5 28 - 29.5

0.0 0.0 0.0

SP

SP

SP

0.482 0.289 0.263

0.273 0.156 0.139

0.181 0.091 0.086

2.66 3.17 3.06

0.85 0.93 0.85

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-9

15080 A Cir Omaha, NE

LA

B

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.86 99.01 53.08

100.0 98.43 68.23 7.89 2.41

100.0 97.96 75.17 33.08 3.82

#20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-05

PH21-05

PH21-05

USCS% CLAY% FINES

D60

Poorly Graded Sand (SP)

Poorly Graded Sand (SP)

Sandy Silt (ML)

2.5Y 5/1 Gray

2.5Y 5/1 Gray

Gley 1 4/N Dark Gray

#10 #20 #40 #80 #200

1.2 0.2 43.5

2.7 2.2 9.5

96.2 97.6 46.9

0.0 0.0 0.0

18 - 19.5 23 - 24.5 63 - 64.5

0.0 0.0 0.0

SP

SP

ML

0.312 0.378 0.086

0.164 0.247 0.041

0.09 0.185 0.006

3.46 2.04 14.01

0.96 0.87 3.20

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-10

15080 A Cir Omaha, NE

LA

B

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 94.3 91.79 83.46 72.38 53.0 32.71 14.03 7.01

100.0 99.42 97.18 76.94 39.77 17.34

100.0 99.08 97.84 94.15 78.46 26.26 10.19

3/4" 1/2" 3/8" #4 #10 #20 #40 #80 #200

#4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-05

PH21-05

PH21-05

USCS% CLAY% FINES

D60

Poorly Graded Sand with Silt (SP-SM)

Silty Sand (SM)

Well Graded Sand with Silt and Gravel

(SW-SM)

Gley 1 5/N Gray

2.5Y 5/1 Gray

2.5Y 4/1 Dark Gray

3/8" #4 #10 #20 #40 #80 #200

10.2

7.0

12.1 5.3

88.9 82.7 76.4

0.0 0.0 0.0

74.5 - 76 78 - 79.5

84.1 - 84.5

0.9 0.0 16.5

SP-SM

SM

SW-SM

0.314 0.287 1.158

0.191 0.123 0.375

0.036 0.109

4.22 7.98 10.63

1.57 1.46 1.12

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-11

15080 A Cir Omaha, NE

LA

B

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 98.85 98.51 95.77 88.76 44.68 19.64

100.0 99.92 99.22 95.67 64.4

100.0 99.96 99.52 90.36 51.5 7.85

3/8" #4 #10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-06

PH21-06

PH21-06

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

Sandy Silt (ML)

Silty Sand (SM)

2.5Y 4/3 Olive Brown

2.5Y 5/1 Gray

2.5Y 3/1 Very Dark Gray

#4 #10 #20 #40 #80 #200

3.6 49.5 11.1

4.2 14.9 8.5

92.2 35.6 79.2

0.0 0.0 0.0

23 - 24.5 48 - 49.5 53 - 53.7

0.0 0.0 1.1

SP-SC

ML

SM

0.217 0.069 0.243

0.117 0.038 0.108

0.078 0.027

2.77 9.12

0.80 1.80

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-12

15080 A Cir Omaha, NE

LA

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/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.49 99.31 98.77 94.93 59.76 12.62

100.0 99.61 91.62 19.89 4.76

100.0 99.91 99.8 99.36 96.57 51.34

3/8" #4 #10 #20 #40 #80 #200

#10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-06

PH21-06

PH21-06

USCS% CLAY% FINES

D60

Sandy Silt (ML)

Poorly Graded Sand (SP)

Clayey Sand (SC)

2.5Y 3/1 Very Dark Gray

2.5Y 3/1 Very Dark Gray

2.5Y 3/2 Very Dark Grayish Brown

#4 #10 #20 #40 #80 #200

37.9 2.3 4.8

13.5 2.4 7.9

48.7 95.2 86.9

0.0 0.0 0.0

53.7 - 54.5 58 - 60

63.5 - 65

0.0 0.0 0.5

ML

SP

SC

0.089 0.291 0.181

0.042 0.203 0.104

0.102 0.036

2.87 5.09

1.40 1.67

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

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GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-13

15080 A Cir Omaha, NE

LA

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D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 96.02 96.02 95.12 94.61 93.85 87.47 48.69 15.21

100.0 93.62 93.62 88.62 76.44 39.41 17.01 11.38 9.26

100.0 98.85 91.02 82.5 72.34 36.29 12.05 8.3

3/4" 1/2" 3/8" #4 #10 #20 #40 #80 #200

3/4" 1/2" 3/8" #4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-06

PH21-06

PH21-06

USCS% CLAY% FINES

D60

Well Graded Sand with Silt (SW-SM)

Well Graded Sand with Clay (SW-SC)

Silty Sand (SM)

10YR 5/2 Grayish Brown

10YR 5/2 Grayish Brown

2.5Y 4/2 Dark Grayish Brown

1/2" 3/8" #4 #10 #20 #40 #80 #200

8.3 3.2 9.4

6.0 5.8

82.7 79.4 79.9

0.0 0.0 0.0

69 - 69.5 73 - 73.8

73.8 - 74.5

9.0 11.4 4.9

SW-SM

SW-SC

SM

0.67 1.368 0.231

0.34 0.635 0.11

0.112 0.102 0.034

6.01 13.43 6.78

1.55 2.90 1.54

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

R C

E N

T F

IN

E

R B

Y W

E

IG

H T

P E

R C

E N

T C

O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-14

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

A T

E D

F R

O M

O R

IG

IN

A L

R E

P O

R T

G

R A

IN

S

IZ

E

: U S

C S

B

IG

B E

N D

R W

C O

LL

E

.G P

J T

E R

R A

C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.02 86.16 44.78 14.5

100.0 99.65 98.48 95.96 90.82 75.41 60.21

100.0 99.76 98.89 90.88 61.34 25.41 7.72

#10 #20 #40 #80 #200

3/8" #4 #10 #20 #40 #80 #200

% Finer% Finer% Finer

% SILT

CC

D10

PH21-06

PH21-06B

PH21-06B

USCS% CLAY% FINES

D60

Poorly Graded Sand with Silt (SP-SM)

Sandy Lean Clay (CL)

Silty Sand (SM)

10YR 5/2 Grayish Brown

2.5Y 5/1 Gray

2.5Y 5/2 Grayish Brown

3/8" #4 #10 #20 #40 #80 #200

7.7 40.5 8.5

19.7 6.0

92.0 39.4 85.5

0.0 0.0 0.0

78 - 79.5 4 - 4.5 8 - 9.5

0.2 0.4 0.0

SP-SM

CL

SM

0.412 0.074 0.247

0.201 0.02 0.117

0.084 0.032

4.90 7.63

1.17 1.72

0.0010.010.1110100

3/4 1/23/8 30 403 60

HYDROMETERU.S. SIEVE OPENING IN INCHES

16 20

U.S. SIEVE NUMBERS

44 10063 2 10 14 506 2001.5 81 140

P E

R C

E N

T F

IN

E

R B

Y W

E

IG

H T

P E

R C

E N

T C

O A

R S

E R

B Y

W E

IG

H

T

GRAIN SIZE DISTRIBUTION

ASTM D422 / ASTM C136

PROJECT NUMBER: 05215156

PROJECT: Big Bend RW Collector Pipe

Replacement FFP Pilot Hole

SITE: BIA Rd 4 and Native American Scenic Byway

Fort Thompson, SD

CLIENT: US Army Corps of Engineers (USACE) Omaha, NE

EXHIBIT: B-15

15080 A Cir Omaha, NE

LA

B

O R

A T

O R

Y T

E S

T S

A R

E N

O T

V A

LI

D

IF

S

E P

A R

A T

E D

F R

O M

O R

IG

IN

A L

R E

P O

R T

G

R A

IN

S

IZ

E

: U S

C S

B

IG

B E

N D

R W

C O

LL

E

.G P

J T

E R

R A

C O

N _D

A T

A T

E M

P

LA

T E

.G D

T

/2 8/

D30

% SAND% GRAVEL% COBBLES

COEFFICIENTS

coarse

BORING ID

CU

SOIL DESCRIPTION

REMARKS

GRAIN SIZE

DEPTH

SILT OR CLAYCOBBLES

GRAVEL SAND

mediumfine coarse fine

SieveSieveSieve

100.0 99.2 87.24 44.56 8.06

% Finer% Finer% Finer

% SILT

CC

D10

PH21-06B

USCS% CLAY% FINES

D60

Poorly Graded Sand with Clay (SP-SC)

2.5Y 5/2 Grayish Brown

#10 #20 #40 #80 #200

3.5 4.591.90.013 - 14.5 0.0 SP-SC

0.246 0.127 0.079

3.13 0.83

Appendix D: HTRW Report

DEPARTMENT OF THE ARMY

CORPS OF ENGINEERS, OMAHA NE

1616 CAPITOL AVENUE

OMAHA NE 68102-4901

CENWO-EDG-S 2 July 2021

MEMORANDUM FOR RECORD

SUBJECT: Big Bend Dam, Fort Thompson, South Dakota, Soil, Groundwater and Investigative Derived Waste (IDW) Sampling.

1. Introduction. Past use of diesel fuel in piezometers to prohibit freezing during winter months has caused concern about the condition of the groundwater and soil in the vicinity of the wells.

2. Scope of Work. This environmental sampling event is to test the soil and groundwater for total petroleum hydrocarbons with diesel range organics (TPH-DRO) from 12 soil borings located near piezometers and relief wells at the site. Testing will be required if contamination is suspected. Sampling will be taken from IDW samples and tested.

3. Sampling Activities. The sampling team included the three man drill crew and a geologist. Soil samples were collected during 1-18 June 2020 and the locations of these samples are in Enclosure 1.

a. Soil samples were collected from each boring at the upper limit of the groundwater. The sampling list is in Enclosure 2.

b. Groundwater was collected as a grab sample from the bottom of the boring.

c. IDW samples were taken at boring location BBSD-11A and BBSD-12A these were tested 10 May 2021 .The laboratory report is Enclosure 5.

4. Analytical Data. Soil, groundwater, and IDW was analyzed using EPA SW-846 methods for TPH-DRO (8015C). CT Laboratories in Baraboo, Wisconsin provided the sample analysis.

a. A manual stage 2A validation of the laboratory data was performed in accordance with the DoD General Data Validation Guidelines and Quality Systems Manual V5.1. Results of the data validation are found in Enclosure 4.

Based on the results of the validation, data are usable for the purpose of making a decision regarding the presence or absence of contamination and concentrations where special handling is required at the site. IDW data were not validated.

REPLY TO

ATTENTION OF

CENWO-EDG-S

SUBJECT: Big Bend Dam, Fort Thompson, South Dakota, Soil, Groundwater and Investigative Derived Waste (IDW) Sampling.

b. A detection above the Regional Screening Level (RSL) for TPH-DRO was noted at boring location BBSD-11A and BBSD-12A. The cuttings from these borings were collected in drums as IDW. Refer to Enclosure 3 for the combined laboratory analytical report.

Detected Analyte Table Derived from the Laboratory Analytical Report

Sampling Completed 18 June 2020

Sample ID DRO Matrix Method Container BBSD-01A 9.70 mg/kg J6

Soil

SW846 8015C

4 ounce glass jar No preservatives 14 day hold time

BBSD-02A 6.93 J

BBSD-00A1 <17 U5

BBSD-03A 7.05 J

BBSD-04A <18 U

BBSD-05A <18 U

BBSD-05A-MS 224

BBSD-05A-MSD 209

BBSD-06A <19 U

BBSD-07A <19 U

BBSD-08A <18 U

BBSD-XXA2 <18 U

BBSD-09A 7.50 J

BBSD-10A 7.24 J

BBSD-11A 96.9

BBSD-12A 2830

BBSD-01B 110 ug/L J

Water 1 liter amber glass jar

No preservatives 7 day hold time

BBSD-02B 480

BBSD-00B3 440

BBSD-03B 270

BBSD-04B 200 J

BBSD-05B 1200

BBSD-05B-MS 3890

BBSD-05B-MSD 3860

BBSD-06B 260 J

BBSD-07B 520 J

BBSD-08B 74 J

BBSD-XXB4 67 J

BBSD-09B 290 J

BBSD-10B 420

BBSD-11B 300

BBSD-12B 27,000

1 – Duplicate sample for BBSD-02A 2 – Duplicate sample for BBSD-08A 3 – Duplicate sample for BBSD-02B 4 – Duplicate sample for BBSD-08B 5 - Analyte concentration was below detection limit 6 – Estimated value

CENWO-EDG-S

SUBJECT: Big Bend Dam, Fort Thompson, South Dakota, Soil, Groundwater and Investigative Derived Waste (IDW) Sampling.

5. Interpretation and Evaluation.

a. The soil sample taken at BBSD-12A was analyzed at 2830 mg/kg and the groundwater from the same location was analyzed at 27,000 ug/L. The soil sample taken at BBSD-11A was analyzed at 96.9 mg/kg. This sampling event occurred during the June 2020 borings. Excavated soils with TPH concentrations greater than 10 mg/kg must be disposed of in accordance with the permitting requirements of the SDDNR Waste Management Program.

b. The groundwater sample taken from the BBSD- 12B location was analyzed at 27,000 ug/L. If dewatering is required during construction, groundwater in this area must be containerized and sampled for disposal procedures.

c. During construction, excavated contaminated soil must be stockpiled and tested for contamination of TPH-DRO, BTEX and Naphthalene prior to disposition for acceptance to landfills.

d. IDW cuttings were sampled 10 May 2021 The Laboratory report shows concentrations of TPH-DRO above the RSL (see Enclosure 5). This waste will require disposal in accordance with the permitting requirements of the SDDNR Waste Management Program. Undisturbed contaminated soil requires no special handling instructions. Tier I action levels* for soils are as follows:

Chemical of Concern Action Level IDW Chemical Concentrations Benzene 0.2 ppm U* Toluene 15 ppm U

Ethylbenzene 10 ppm U Xylenes 300 ppm U

Naphthalene 25 ppm U TPH-DRO 10 ppm 17.9 J*

* Taken from SDDNR Petroleum Assessment and Cleanup Handbook (Chapter 4)

*U- Analyte concentration was below detection limit.

*J- Estimated Value

6. Point of contact for this memorandum is the undersigned at (402) 995-2285.

5 Enclosures Marc Anderson

1. Sampling Location Map Environmental Scientist

2. Sampling List Military Munitions and Environmental Science

3. Laboratory Report June 2020 sampling

4. Laboratory Data Validation June 2020

5. Laboratory Report IDW Sample May 2021

ENCLOSURE 1

SAMPLING LOCATION MAP

This page was intentionally left blank.

@A

@A

@A

@A

@A @A @A @A

@A @A @A

@A

@A @A

@A @A

@A

@A

@A@A

@A @A @A@A @A @A

@A

@A

@A

@A

@A

@A

@A

@A

@A

@A

BH20-12

BH20-11

BH20-10

BH20-09

BH20-08

BH20-07

BH20-06

BH20-05

BH20-04

BH20-03

BH20-02

BH20-01

RW-68

RW-67

RW-66

RW-67A

RW-66B

RW-68B

RW-68A

RW-67B

RW-66C

RW-66A

PZ-24

PZ-22

PZ-21

PZ-19

PZ 30

PZ 29

PZ 28

PZ 27

PZ 26

J970R J662R

J474R

J320RJ171R

H810R

H560R

PZ-25R

J662Ra J474Rb

J320RbJ171Rb

H810Ra

H560Ra

J970Ra

J662Rb

J320Ra

H1060RH1060Rb

D760Rba

J970Rba-12

H810Rba-12

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community

LEGEND

&= Soil Boring (As-Drilled)

&% Existing Relief Well

@A Existing Piezometer

&= Historical Soil Boring

Relief Well Collector Pipe

Proposed Extension

Toe Drain

Connector Pipe

³

_̂ South Dakota

Nebraska

Iowa

MinnesotaPierrePierre

U.S. Army Corps of Engineers Omaha District

Big Bend Dam Fort Thompson, SD

Soil Boring Location Map

July 2020 FIGURE 1

100 0 10050 Ft

ENCLOSURE 2

SAMPLING LIST

JUNE 2020

Sample ID DRO Matrix Method Container BBSD-01A 9.70 mg/kg

Soil

SW846 8015C

4 ounce glass jar No preservatives 14 day hold time

BBSD-02A 6.93

BBSD-00A1 <17

BBSD-03A 7.05

BBSD-04A <18

BBSD-05A <18

BBSD-05A-MS 224

BBSD-05A-MSD 209

BBSD-06A <19

BBSD-07A <19

BBSD-08A <18

BBSD-XXA2 <18

BBSD-09A 7.50

BBSD-10A 7.24

BBSD-11A 96.9

BBSD-12A 2830

BBSD-01B 110 ug/L

Water 1 liter amber glass jar

No preservatives 7 day hold time

BBSD-02B 480

BBSD-00B3 440

BBSD-03B 270

BBSD-04B 200

BBSD-05B 1200

BBSD-05B-MS 3890

BBSD-05B-MSD 3860

BBSD-06B 260

BBSD-07B 520

BBSD-08B 74

BBSD-XXB4 67

BBSD-09B 290

BBSD-10B 420

BBSD-11B 300

BBSD-12B 27,000

1 – Duplicate sample for BBSD-02A 2 – Duplicate sample for BBSD-08A 3 – Duplicate sample for BBSD-02B 4 – Duplicate sample for BBSD-08B

*Sampling event occurred June 2020

ENCLOSURE 3

LABORATORY REPORT

JUNE 2020

ANALYTICAL SUMMARY REPORT

This report at a minimum contains the following information:

Analytical Report of Test Results Description of QC Qualifiers Chain of Custody (copy) Quality Control Summary (if applicable) Case Narrative (if applicable) Correspondence with Client (if applicable)

This report has been specifically prepared to satisfy project or program requirements. These results are in compliance with NELAC requirements for parameters where accreditation is required or available, unless otherwise noted in the case narrative.

1230 Lange Court • Baraboo, WI 53913 • 608-356-2760 www.ctlaboratories.com

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 1 of 18

Project Name: BIG BEND DAM TOE DRAIN REPLACEMENT

Contract #: 3357 Folder #: 153747

Project #:

USACE - OMAHA

Project Phase: FORT THOMPSON, SD

ANALYTICAL SAMPLE DATA

TOM WEIRAUCH

SUITE 9000

Purchase Order #:

Project Name: BIG BEND DAM TOE DRAIN REPLACEMENT

Contract #:

Folder #:

1616 CAPITOL AVE Date Received: 06/04/2020

Arrival Temperature: 3.2 Report Date: 06/18/2020

OMAHA, NE 68102-9000

USACE - OMAHA

Reprint Date:

Project #:

Project Phase:

06/19/2020

FORT THOMPSON, SD

153747

CT LAB#: 427712

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1105

Analyte

Sample Description: BBSD-01B

DOD

LOD

Client Sample #:

Organic Results ug/L110 6/9/20 JJYDiesel Range Organics 06/08/2020 10:30 13:49J200 EPA 8015C100 1.0020034 % Recovery71 6/9/20 JJYSURR: Octacosane 06/08/2020 10:30 13:49 EPA 8015C1.0014260 % Recovery63 6/9/20 JJYSurr: Triacontane 06/08/2020 10:30 13:49 EPA 8015C1.0014029

CT LAB#: 427714

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/03/2020 0845

Analyte

Sample Description: BBSD-03B

DOD

LOD

Client Sample #:

Organic Results ug/L270 6/9/20 JJYDiesel Range Organics 06/08/2020 10:30 14:17200 EPA 8015C100 1.0020034 % Recovery81 6/9/20 JJYSURR: Octacosane 06/08/2020 10:30 14:17 EPA 8015C1.0014260 % Recovery74 6/9/20 JJYSurr: Triacontane 06/08/2020 10:30 14:17 EPA 8015C1.0014029

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 2 of 18

Contract #: 3357 Folder #: 153747

Project #:

USACE - OMAHA

Project Phase: FORT THOMPSON, SD

CT LAB#: 427715

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/03/2020 1023

Analyte

Sample Description: BBSD-12B

DOD

LOD

Client Sample #:

Organic Results ug/L27000 6/9/20 JJYDiesel Range Organics 06/08/2020 10:30 16:091100 EPA 8015C530 5.001100180 % Recovery26 S 6/9/20 JJYSURR: Octacosane 06/08/2020 10:30 14:45 EPA 8015C1.0014260 % Recovery19 S 6/9/20 JJYSurr: Triacontane 06/08/2020 10:30 14:45 EPA 8015C1.0014029

CT LAB#: 427716

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1244

Analyte

Sample Description: BBSD-02B

DOD

LOD

Client Sample #:

Organic Results ug/L480 6/9/20 JJYDiesel Range Organics 06/08/2020 10:30 15:13250 EPA 8015C130 1.0025042 % Recovery25 S 6/9/20 JJYSURR: Octacosane 06/08/2020 10:30 15:13 EPA 8015C1.0014260 % Recovery20 S 6/9/20 JJYSurr: Triacontane 06/08/2020 10:30 15:13 EPA 8015C1.0014029

CT LAB#: 427717

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1244

Analyte

Sample Description: BBSD-00B

DOD

LOD

Client Sample #:

Organic Results ug/L440 6/9/20 JJYDiesel Range Organics 06/08/2020 10:30 18:02250 EPA 8015C130 1.0025042 % Recovery29 S 6/9/20 JJYSURR: Octacosane 06/08/2020 10:30 18:02 EPA 8015C1.0014260 % Recovery21 S 6/9/20 JJYSurr: Triacontane 06/08/2020 10:30 18:02 EPA 8015C1.0014029

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 3 of 18

Contract #: 3357 Folder #: 153747

Project #:

USACE - OMAHA

Project Phase: FORT THOMPSON, SD

CT LAB#: 427718

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1225

Analyte

Sample Description: BBSD-00A

DOD

LOD

Client Sample #:

Inorganic Results

%82.7 6/15/20 BMMSolids, Percent 13:570.1 EPA 8000C0.1 1.000.10.1

Organic Results mg/kg<17 6/16/20 JJYDiesel Range Organics 06/16/2020 10:30 18:56U46 EPA 8015C17 1.00465.8 % Recovery50 6/16/20 JJYSURR: Octacosane 06/16/2020 10:30 18:56 EPA 8015C1.0012544 % Recovery40 6/16/20 JJYSurr: Triacontane 06/16/2020 10:30 18:56 EPA 8015C1.0013635

CT LAB#: 427719

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/03/2020 0941

Analyte

Sample Description: BBSD-12A

DOD

LOD

Client Sample #:

Inorganic Results

%83.6 6/15/20 BMMSolids, Percent 13:570.1 EPA 8000C0.1 1.000.10.1

Organic Results mg/kg2830 6/17/20 JJYDiesel Range Organics 06/16/2020 10:30 11:56230 EPA 8015C88 5.0023029 % Recovery81 6/17/20 JJYSURR: Octacosane 06/16/2020 10:30 11:56 EPA 8015C5.0012544 % Recovery69 6/17/20 JJYSurr: Triacontane 06/16/2020 10:30 11:56 EPA 8015C5.0013635

CT LAB#: 427720

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1225

Analyte

Sample Description: BBSD-02A

DOD

LOD

Client Sample #:

Inorganic Results

%88.3 6/15/20 BMMSolids, Percent 13:570.1 EPA 8000C0.1 1.000.10.1

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 4 of 18

Contract #: 3357 Folder #: 153747

Project #:

USACE - OMAHA

Project Phase: FORT THOMPSON, SD

CT LAB#: 427720

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1225

Analyte

Sample Description: BBSD-02A

DOD

LOD

Client Sample #:

Organic Results mg/kg6.93 6/16/20 JJYDiesel Range Organics 06/16/2020 10:30 19:52J44 EPA 8015C16 1.00445.5 % Recovery55 6/16/20 JJYSURR: Octacosane 06/16/2020 10:30 19:52 EPA 8015C1.0012544 % Recovery43 6/16/20 JJYSurr: Triacontane 06/16/2020 10:30 19:52 EPA 8015C1.0013635

CT LAB#: 427721

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1025

Analyte

Sample Description: BBSD-01A

DOD

LOD

Client Sample #:

Inorganic Results

%78.9 6/15/20 BMMSolids, Percent 13:570.1 EPA 8000C0.1 1.000.10.1

Organic Results mg/kg9.70 6/16/20 JJYDiesel Range Organics 06/16/2020 10:30 20:19J51 EPA 8015C19 1.00516.3 % Recovery53 6/16/20 JJYSURR: Octacosane 06/16/2020 10:30 20:19 EPA 8015C1.0012544 % Recovery45 6/16/20 JJYSurr: Triacontane 06/16/2020 10:30 20:19 EPA 8015C1.0013635

CT LAB#: 427722

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1418

Analyte

Sample Description: BBSD-03A

DOD

LOD

Client Sample #:

Inorganic Results

%80.0 6/15/20 BMMSolids, Percent 13:570.1 EPA 8000C0.1 1.000.10.1

Organic Results

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 5 of 18

Contract #: 3357 Folder #: 153747

Project #:

USACE - OMAHA

Project Phase: FORT THOMPSON, SD

CT LAB#: 427722

Result Units DL DOD

LOQ

RL DF Qualifier Prep Date/Time

Analysis Date/Time

Analyst Method

Sampled: 06/02/2020 1418

Analyte

Sample Description: BBSD-03A

DOD

LOD

Client Sample #:

mg/kg7.05 6/16/20 JJYDiesel Range Organics 06/16/2020 10:30 20:47J50 EPA 8015C19 1.00506.2 % Recovery54 6/16/20 JJYSURR: Octacosane 06/16/2020 10:30 20:47 EPA 8015C1.0012544 % Recovery45 6/16/20 JJYSurr: Triacontane 06/16/2020 10:30 20:47 EPA 8015C1.0013635

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis 153747 - Page 6 of 18

Notes:

^ Indicates the laboratory is NELAP accredited for this analyte by the indicated matrix and method. DL (detection limit), LOD (limit of detection), loq (limit of quantitation) as defined by most recent DOD QSM version.

Submitted by: Brett M. Szymanski Project Manager 608-356-2760

DescriptionCode QC Qualifiers

B Analyte detected in the associated Method Blank.

C Toxicity present in BOD sample.

D Diluted Out.

E Safe, No Total Coliform detected.

F Unsafe, Total Coliform detected, no E. Coli detected.

G Unsafe, Total Coliform detected and E. Coli detected.

H Holding time exceeded.

I Incubator temperature was outside acceptance limits during test period.

J Estimated value.

L Significant peaks were detected outside the chromatographic window.

M Matrix spike and/or Matrix Spike Duplicate recovery outside acceptance limits.

N Insufficient BOD oxygen depletion.

O Complete BOD oxygen depletion.

P Concentration of analyte differs more than 40% between primary and confirmation analysis.

Q Laboratory Control Sample outside acceptance limits.

R See Narrative at end of report.

S Surrogate standard recovery outside acceptance limits due to apparent matrix effects.

T Sample received with improper preservation or temperature.

U Analyte concentration was below detection limit.

V Raised Quantitation or Reporting Limit due to limited sample amount or dilution for matrix background interference.

W Sample amount received was below program minimum.

X Analyte exceeded calibration range.

Y Replicate/Duplicate precision outside acceptance limits.

Z Specified calibration criteria was not met.

Current CT Laboratories Certifications

Wisconsin (WDNR) Chemistry ID# 157066030 Wisconsin (DATCP) Bacteriology ID# 289 Louisiana NELAP (primary) ID# ACC20190002 Illinois NELAP Lab ID# 200073 Kansas NELAP Lab ID# E-10368 Virginia NELAP Lab ID# 460203 ISO/IEC 17025-2005 A2LA Cert # 3806.01 DoD-ELAP A2LA 3806.01 GA EPD Stipulation ID ACC20190002

All samples were received intact and properly preserved unless otherwise noted. The results reported relate only to the samples tested. This report shall not be reproduced, except in full, without written approval of this laboratory. The Chain of Custody is attached.

This report has been specifically prepared to satisfy project or program requirements. These results are in compliance with NELAC requirements for the parameters where accreditation is required or available, unless noted in the case narrative.

153747 - Page 7 of 18

1230 Lange Court • Baraboo , W I 53913 • 608 -356-2760 www.ctlabor atories .com

QC SUMMARY REPORT

USACE - OMAHA Project Name: BIG BEND DAM TOE DRAIN

REPLACEMENT

Project #: SDG #: 0 Folder #: 153747

Duplicate

06/15/2020Analytical Run #: Analysis Date:

13:57Analysis Time:432147

BMM

CTLab #:

Analyst:

Prep Batch #:

427718Parent Sample #:

Prep Date/Time:

SOILMatrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

171971 Method: SW8000C

Solids, Percent % 0 883.0 82.7

Date Printed: 06/19/2020

CTLaboratories LLC 1230 Lange Court • Baraboo, WI 53913 • 608-356-2760 www.ctlaboratories.com

153747 - Page 8 of 18

USACE - OMAHA Project Name: BIG BEND DAM TOE DRAIN

REPLACEMENT

Project #: SDG #: 0 Folder #: 153747

Lab Control Spike Duplicate Water

06/09/2020Analytical Run #: Analysis Date:

16:38Analysis Time:427836

76713

JJY

CTLab #:

Analyst:

Prep Batch #:

427835Parent Sample #:

Prep Date/Time:

LIQUID

JLH

Matrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

171977 Method: SW801506/08/202010:30

Diesel Range Organics ug/L 79 132 4 301980 36 ---2500

Date Printed: 06/19/2020

CTLaboratories LLC 1230 Lange Court • Baraboo, WI 53913 • 608-356-2760

153747 - Page 9 of 18

Project #: SDG #: 0 Folder #: 153747

Lab Control Spike Water

06/09/2020Analytical Run #: Analysis Date:

13:21Analysis Time:427835

76713

JJY

CTLab #:

Analyst:

Prep Batch #:

Parent Sample #:

Prep Date/Time:

LIQUID

JLH

Matrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

171977 Method: SW801506/08/202010:30

Diesel Range Organics ug/L 76 132 301900 36 ---2500

Date Printed: 06/19/2020

CTLaboratories LLC

153747 - Page 10 of 18

Project #: SDG #: 0 Folder #: 153747

Method Blank Water

06/09/2020Analytical Run #: Analysis Date:

12:52Analysis Time:427834

76713

JJY

CTLab #:

Analyst:

Prep Batch #:

Parent Sample #:

Prep Date/Time:

LIQUID

JLH

Matrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

171977 Method: SW801506/08/202010:30

Diesel Range Organics ug/L U 10033 0

Date Printed: 06/19/2020

CTLaboratories LLC 1230 Lange Court • Baraboo, WI 53913 • 608-356-2760

153747 - Page 11 of 18

Project #: SDG #: 0 Folder #: 153747

Lab Control Spike Soil

06/16/2020Analytical Run #: Analysis Date:

18:27Analysis Time:428336

76752

JJY

CTLab #:

Analyst:

Prep Batch #:

Parent Sample #:

Prep Date/Time:

SOLID

JLH

Matrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

172235 Method: SW801506/16/202010:30

Diesel Range Organics mg/kg 77 132 30192 38 ---250

Date Printed: 06/19/2020

CTLaboratories LLC 1230 Lange Court • Baraboo, WI 53913 • 608-356-2760

153747 - Page 12 of 18

Project #: SDG #: 0 Folder #: 153747

Method Blank Soil

06/16/2020Analytical Run #: Analysis Date:

17:59Analysis Time:428335

76752

JJY

CTLab #:

Analyst:

Prep Batch #:

Parent Sample #:

Prep Date/Time:

SOLID

JLH

Matrix:

Prep Analyst:

RPD

Limit

Spike Amount Added

Analyte Units % Recovery

Control Limits

RPDQualifier(s)QC sample result

Parent sample result

172235 Method: SW801506/16/202010:30

Diesel Range Organics mg/kg U 205 0

Date Printed: 06/19/2020

CTLaboratories LLC 1230 Lange Court • Baraboo, WI 53913 • 608-356-2760

153747 - Page 13 of 18

153747

Sample Condition Report

Folder #: 153747 Print Date / Time: 06/04/2020 12:37 Client: USACE - OMAHA Received Date / Time / By: 06/04/2020 11:30 CHB

Project Name: BIG BEND DAM TOE DRAIN REPLACEM Log-In Date / Time / By: 06/04/2020 12:08 JLS Project Phase: FORT THOMPSON, SD Project #: PM: BMS

Coolers: 6380 Temperature: 3.2 C On Ice: Y Custody Seals Present : Y COC Present:? Y Complete? Y

Seal Intact? Y Numbers: DATED AND SIGNED Ship Method: FEDEX EXPRESS Tracking Number: 806531978900 Adequate Packaging: Y Temp Blank Enclosed? Y

Notes: THE SAMPLES WERE RECEIVED IN GOOD CONDITION ON ICE.

TWO CUSTODY SEALS WERE PRESENT AND INTACT UPON RECEIPT - BOTH WERE DATED 6/3/20 AND SIGNED.

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427712 BBSD-01B

AMBER GL 1 / DRO

Total # of Containers of Type ( AMBER GL ) = 1

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427714 BBSD-03B

AMBER GL 1 / DRO

Total # of Containers of Type ( AMBER GL ) = 1

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427715 BBSD-12B

AMBER GL 1 / DRO

Total # of Containers of Type ( AMBER GL ) = 1

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427716 BBSD-02B

AMBER GL 1 / DRO

Total # of Containers of Type ( AMBER GL ) = 1

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427717 BBSD-00B

AMBER GL 1 / DRO

Total # of Containers of Type ( AMBER GL ) = 1

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427718 BBSD-00A

UNPRES GL 1 / DRO,%SOL

Total # of Containers of Type ( UNPRES GL ) = 1

153747 - Page 14 of 18

153747

Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427719 BBSD-12A

UNPRES GL 1 / DRO,%SOL

Total # of Containers of Type ( UNPRES GL ) = 1 Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427720 BBSD-02A

UNPRES GL 1 / DRO,%SOL

Total # of Containers of Type ( UNPRES GL ) = 1 Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427721 BBSD-01A

UNPRES GL 1 / DRO,%SOL

Total # of Containers of Type ( UNPRES GL ) = 1 Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

427722 BBSD-03A

UNPRES GL 1 / DRO,%SOL

Total # of Containers of Type ( UNPRES GL ) = 1

Condition Code Condition Description 1 Sample Received OK

153747 - Page 15 of 18

153747 - Page 16…

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