B08_Att_6_Environmental_Report.pdf
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This document is an analytical report that contains environmental test data for soil samples collected from the China Beach area. The report provides the results of laboratory analysis for total petroleum hydrocarbons (TPH), RCRA metals, and polycyclic aromatic hydrocarbons (PAHs) for 12 soil samples. The samples were collected from various depths at 6 different boring locations. The results indicate low to moderate levels of metals, with some detections of PAHs, but no significant detections of TPH. The report includes quality assurance information, such as laboratory control sample and matrix spike recoveries. Overall, the report provides detailed analytical data to characterize the environmental conditions of the soil at the China Beach site.
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Analytical Sciences
Report Date: September 18, 2018
Laboratory Report
Project Name:
Lab Project Number:
China Beach
8090551
This 24 page report of analytical data has been reviewed and approved for release.
Scott Stephens
Miller Pacific Engineering - Novato
Novato, CA 94947
504 Redwood Blvd., Suite 220
1650.116
Laboratory Director
Michele Peters
P.O. Box 750336
Petaluma, CA 94975-0336
Telephone: (707) 769-3128
110 Liberty Street
Petaluma, CA
94952
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-01 B5 0.5-1' ND .05
Motor Oil 540 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/14/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-02 B5 1.5-2' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-03 B5 3-3.5' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-04 B6 0.5-1' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
CA Lab Accreditation #: 2303Lab Project#: 8090551
Diesel8090551-06 B6 3-3.5' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-07 B8 0.5-1' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-08 B8 1-1.5' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-09 B8 2.5-3' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Diesel8090551-10 B9 0.5-1' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-11 B9 1-1.5' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
TPH Diesel & Motor Oil
Diesel8090551-12 B9 2.5-3' ND .05
Motor Oil ND 50
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/13/18
EPA 8015B
B017977Date Sampled:
Date Received:
CAM Metals
Antimony (Sb)8090551-01 B5 0.5-1' ND .05
Arsenic (As) ND .51
Barium (Ba) 210 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 20 1.5
Cobalt (Co) 24 1.5
Copper (Cu) 46 2.0
Lead (Pb) ND .03
Molybdenum (Mo) ND .01
Nickel (Ni) 25 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 110 2.0
Zinc (Zn) 50 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-02 B5 1.5-2' ND .05
Arsenic (As) 2 .9 1.5
Barium (Ba) 72 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 120 1.5
Cobalt (Co) 12 1.5
Copper (Cu) 11 2.0
Lead (Pb) 4 .5 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 140 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 32 2.0
Zinc (Zn) 34 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-03 B5 3-3.5' ND .05
Arsenic (As) 2 .7 1.5
Barium (Ba) 81 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 130 1.5
Cobalt (Co) 12 1.5
Copper (Cu) 12 2.0
Lead (Pb) 4 .3 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 150 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 32 2.0
Zinc (Zn) 29 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-04 B6 0.5-1' ND .05
Arsenic (As) ND .51
Barium (Ba) 180 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 15 1.5
Cobalt (Co) 24 1.5
Copper (Cu) 33 2.0
Lead (Pb) ND .03
Molybdenum (Mo) ND .01
Nickel (Ni) 18 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 110 2.0
Zinc (Zn) 48 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-05 B6 1-1.5' ND .05
Arsenic (As) ND .51
Barium (Ba) 150 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 15 1.5
Cobalt (Co) 22 1.5
Copper (Cu) 31 2.0
Lead (Pb) ND .03
Molybdenum (Mo) ND .01
Nickel (Ni) 18 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 97 2.0
Zinc (Zn) 43 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-06 B6 3-3.5' ND .05
Arsenic (As) 3 .5 1.5
Barium (Ba) 230 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 170 1.5
Cobalt (Co) 17 1.5
Copper (Cu) 17 2.0
Lead (Pb) 3 .5 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 250 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 33 2.0
Zinc (Zn) 29 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-07 B8 0.5-1' ND .05
Arsenic (As) 4 .0 1.5
Barium (Ba) 71 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 170 1.5
Cobalt (Co) 21 1.5
Copper (Cu) 19 2.0
Lead (Pb) 3 .7 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 280 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 35 2.0
Zinc (Zn) 34 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-08 B8 1-1.5' ND .05
Arsenic (As) 4 .2 1.5
Barium (Ba) 150 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 220 1.5
Cobalt (Co) 18 1.5
Copper (Cu) 22 2.0
Lead (Pb) 4 .6 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 300 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 40 2.0
Zinc (Zn) 48 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-09 B8 2.5-3' ND .05
Arsenic (As) 5 .9 1.5
Barium (Ba) 210 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 34 1.5
Cobalt (Co) 13 1.5
Copper (Cu) 44 2.0
Lead (Pb) 8 .4 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 55 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 32 2.0
Zinc (Zn) 65 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-10 B9 0.5-1' ND .05
Arsenic (As) 3 .6 1.5
Barium (Ba) 96 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 150 1.5
Cobalt (Co) 15 1.5
Copper (Cu) 15 2.0
Lead (Pb) 7 .8 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 210 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 37 2.0
Zinc (Zn) 38 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-11 B9 1-1.5' ND .05
Arsenic (As) 3 .2 1.5
Barium (Ba) 120 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 130 1.5
Cobalt (Co) 14 1.5
Copper (Cu) 14 2.0
Lead (Pb) 5 .4 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 190 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 34 2.0
Zinc (Zn) 34 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Antimony (Sb)8090551-12 B9 2.5-3' ND .05
Arsenic (As) 2 .5 1.5
Barium (Ba) 47 2.0
Beryllium (Be) ND .500
Cadmium (Cd) ND .500
Chromium (Cr) 53 1.5
Cobalt (Co) 6 .5 1.5
Copper (Cu) 16 2.0
Lead (Pb) 3 .2 3.0
Molybdenum (Mo) ND .01
Nickel (Ni) 62 2.0
Selenium (Se) ND .05
Silver (Ag) ND .01
Thallium (Tl) ND .05
Vanadium (V) 25 2.0
Zinc (Zn) 20 5.0
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/12/18
EPA 6010B
B017982Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-01 B5 0.5-1' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-02 B5 1.5-2' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Mercury
Mercury (Hg)8090551-03 B5 3-3.5' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-04 B6 0.5-1' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-05 B6 1-1.5' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-06 B6 3-3.5' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Mercury (Hg)8090551-07 B8 0.5-1' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-08 B8 1-1.5' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-09 B8 2.5-3' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-10 B9 0.5-1' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Mercury (Hg)8090551-11 B9 1-1.5' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Compound NameLab# Sample ID Result (mg/kg) RDL (mg/kg)
Mercury
Mercury (Hg)8090551-12 B9 2.5-3' ND .100
Date Analyzed:
Method:
QC Batch:08/31/18
09/05/18
09/11/18
EPA 7471A
B017991Date Sampled:
Date Received:
Quality Assurance Report
Result Limit
Reporting
Units Level Spike
Result Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TPH Diesel & Motor Oil
Batch B017977 - EPA 3550B GC
Blank (B017977-BLK1) Prepared: 09/06/18 Analyzed: 09/13/18
Diesel mg/kgND 5.0
Motor Oil mg/kgND 50
LCS (B017977-BS1) Prepared: 09/06/18 Analyzed: 09/13/18
Diesel mg/kg 227 65-135110249 5.0
LCS Dup (B017977-BSD1) Prepared: 09/06/18 Analyzed: 09/13/18
Diesel mg/kg 227 3065-135111 0.8251 5.0
Matrix Spike (B017977-MS1) Prepared: 09/06/18 Analyzed: 09/13/18 Source: 8090551-02
Diesel mg/kg 226 ND 65-13589200 5.0
Matrix Spike Dup (B017977-MSD1) Prepared: 09/06/18 Analyzed: 09/13/18 Source: 8090551-02
Diesel mg/kg 225 ND 3065-13589 0.2200 5.0
Reporting
Units Level Spike
Result Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
CAM Metals
Batch B017982 - EPA 3050B
Blank (B017982-BLK1) Prepared & Analyzed: 09/10/18
Antimony (Sb) mg/kgND 5.0
Arsenic (As) mg/kgND 1.5
Barium (Ba) mg/kgND 2.0
Beryllium (Be) mg/kgND 0.50
Cadmium (Cd) mg/kgND 0.50
Chromium (Cr) mg/kgND 1.5
Cobalt (Co) mg/kgND 1.5
Copper (Cu) mg/kgND 2.0
Lead (Pb) mg/kgND 3.0
Molybdenum (Mo) mg/kgND 1.0
Nickel (Ni) mg/kgND 2.0
Selenium (Se) mg/kgND 5.0
Silver (Ag) mg/kgND 1.0
Thallium (Tl) mg/kgND 5.0
Vanadium (V) mg/kgND 2.0
Zinc (Zn) mg/kgND 5.0
LCS (B017982-BS1) Prepared & Analyzed: 09/10/18
Antimony (Sb) mg/kg 25.0 70-1309924.6 5.0
Arsenic (As) mg/kg 25.0 70-1309824.4 1.5
Barium (Ba) mg/kg 25.0 70-13010526.3 2.0
Beryllium (Be) mg/kg 25.0 70-13010626.5 0.50
Cadmium (Cd) mg/kg 25.0 70-1309724.2 0.50
Chromium (Cr) mg/kg 25.0 70-13010425.9 1.5
Cobalt (Co) mg/kg 25.0 70-13010726.8 1.5
Copper (Cu) mg/kg 25.0 70-13010425.9 2.0
Lead (Pb) mg/kg 25.0 70-13010426.1 3.0
Molybdenum (Mo) mg/kg 25.0 70-13010426.0 1.0
Nickel (Ni) mg/kg 25.0 70-13010225.6 2.0
Selenium (Se) mg/kg 25.0 70-1309423.5 5.0
Silver (Ag) mg/kg 6.25 70-130986.11 1.0
Thallium (Tl) mg/kg 25.0 70-13010726.7 5.0
Vanadium (V) mg/kg 25.0 70-13010325.9 2.0
Zinc (Zn) mg/kg 25.0 70-13010526.2 5.0
Units Level Spike
Result Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
CAM Metals
Batch B017982 - EPA 3050B
LCS Dup (B017982-BSD1) Prepared & Analyzed: 09/10/18
Antimony (Sb) mg/kg 25.0 2070-130100 124.9 5.0
Arsenic (As) mg/kg 25.0 2070-13098 0.524.5 1.5
Barium (Ba) mg/kg 25.0 2070-130105 0.0826.4 2.0
Beryllium (Be) mg/kg 25.0 2070-130106 0.326.5 0.50
Cadmium (Cd) mg/kg 25.0 2070-13097 0.324.3 0.50
Chromium (Cr) mg/kg 25.0 2070-130104 0.0925.9 1.5
Cobalt (Co) mg/kg 25.0 2070-130107 0.0626.8 1.5
Copper (Cu) mg/kg 25.0 2070-130104 0.0725.9 2.0
Lead (Pb) mg/kg 25.0 2070-130104 0.426.0 3.0
Molybdenum (Mo) mg/kg 25.0 2070-130104 0.0926.0 1.0
Nickel (Ni) mg/kg 25.0 2070-130103 0.0425.6 2.0
Selenium (Se) mg/kg 25.0 2070-13094 0.323.6 5.0
Silver (Ag) mg/kg 6.25 2070-13097 16.05 1.0
Thallium (Tl) mg/kg 25.0 2070-130106 0.226.6 5.0
Vanadium (V) mg/kg 25.0 2070-130103 0.225.8 2.0
Zinc (Zn) mg/kg 25.0 2070-130105 0.0926.2 5.0
Units Level Spike
Result Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Mercury
Batch B017991 - EPA 7471A Prep
Blank (B017991-BLK1) Prepared: 09/10/18 Analyzed: 09/11/18
Mercury (Hg) mg/kgND 0.10
LCS (B017991-BS1) Prepared: 09/10/18 Analyzed: 09/11/18
Mercury (Hg) mg/kg 0.300 70-1301000.299 0.10
LCS Dup (B017991-BSD1) Prepared: 09/10/18 Analyzed: 09/11/18
Mercury (Hg) mg/kg 0.300 2070-130108 80.324 0.10
Matrix Spike (B017991-MS1) Prepared: 09/10/18 Analyzed: 09/11/18 Source: 8090551-02
Mercury (Hg) mg/kg 0.247 ND 60-1401340.331 0.10
Matrix Spike Dup (B017991-MSD1) Prepared: 09/10/18 Analyzed: 09/11/18 Source: 8090551-02
Mercury (Hg) mg/kg 0.242 ND 2060-140133 10.321 0.10
Notes and Definitions
Relative Percent DifferenceRPD
Analyte NOT DETECTED at or above the reporting detection limit (RDL)ND
Reporting Detection LimitRDL
NR Not Reported
Work Order:
Report Cr eated for: Analytical Sciences
110 Liberty Street Petaluma, CA 94952
Project Contact: Michele Peters
Project: 8090551; China Beach Project P.O.:
Project Received: 09/07/2018
Analytical Report reviewed & approved for release on 09/17/2018 by:
Yen Cao
1809251
The report shall not be reproduced except in full, without the written approval of the laboratory. The analytical results relate only to the items tested. Results reported conform to the most current NELAP standards, where applicable, unless otherwise stated in the case narrative.
Analytical Report
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Project Manager
McCampbell Analytical, Inc.
"When Quality Counts"
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Glossary of Terms & Qualif ier Defin itions
Client: Analytical Sciences Project: 8090551; China Beach WorkOrder : 1809251
McCampbell Analytical, Inc.
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Glos sary Abbreviatio n
95% Interval 95% Confident Interval c Serial Dilution Percent Difference
DF Dilution Factor
DI WET (DISTLC) Waste Extraction Test using DI water
DISS Dissolved (direct analysis of 0.45 µm filtered and acidified water sample)
DLT Dilution Test (Serial Dilution)
DUP Duplicate
EDL Estimated Detection Limit
ERS External reference sample. Second source calibration verification.
ITEF International Toxicity Equivalence Factor
LCS Laboratory Control Sample
MB Method Blank
MB % Rec % Recovery of Surrogate in Method Blank, if applicable
MDL Method Detection Limit
ML Minimum Level of Quantitation
MS Matrix Spike
MSD Matrix Spike Duplicate
N/A Not Applicable
ND Not detected at or above the indicated MDL or RL
NR Data Not Reported due to matrix interference or insufficient sample amount.
PDS Post Digestion Spike
PDSD Post Digestion Spike Duplicate
PF Prep Factor
RD Relative Difference
RL Reporting Limit (The RL is the lowest calibration standard in a multipoint calibration.)
RPD Relative Percent Deviation
RRT Relative Retention Time
SPK Val Spike Value
SPKRef Val Spike Reference Value
SPLP Synthetic Precipitation Leachate Procedure
ST Sorbent Tube
TCLP Toxicity Characteristic Leachate Procedure
TEQ Toxicity Equivalents
WET (STLC) Waste Extraction Test (Soluble Threshold Limit Concentration)
Glossary of Terms & Qualif ier Defin itions
Client: Analytical Sciences Project: 8090551; China Beach WorkOrder : 1809251
McCampbell Analytical, Inc.
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Analytica l Qualif iers
S Surrogate spike recovery outside accepted recovery limits.
a1 Sample diluted due to matrix interference.
a2 Sample diluted due to cluttered chromatogram.
a3 Sample diluted due to high organic content.
a4 Reporting limits raised due to the sample's matrix prohibiting a full volume extraction.
c1 Surrogate recovery outside of the control limits due to the dilution of the sample.
Qual ity Control Qua li fiers
F2 LCS/LCSD recovery and/or RPD is out of acceptance criteria.
F10 MS/MSD outside control limits. Physical or chemical interferences exist due to sample matrix.
Analytical Report
McCampbell Analytical, Inc.
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B5 0.5-1' 1809251-001A Soil 08/31/2018 14:45 GC40 09101814.d 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.20 200 09/10/2018 16:45 a-BHC ND 0.20 200 09/10/2018 16:45 b-BHC ND 0.20 200 09/10/2018 16:45 d-BHC ND 0.20 200 09/10/2018 16:45 g-BHC ND 0.20 200 09/10/2018 16:45
Chlordane (Technical) ND 5.0 200 09/10/2018 16:45 a-Chlordane ND 0.20 200 09/10/2018 16:45 g-Chlordane ND 0.20 200 09/10/2018 16:45 p,p-DDD ND 0.20 200 09/10/2018 16:45 p,p-DDE ND 0.20 200 09/10/2018 16:45 p,p-DDT ND 0.20 200 09/10/2018 16:45
Dieldrin ND 0.20 200 09/10/2018 16:45
Endosulfan I ND 0.20 200 09/10/2018 16:45
Endosulfan II ND 0.20 200 09/10/2018 16:45
Endosulfan sulfate ND 0.20 200 09/10/2018 16:45
Endrin ND 0.20 200 09/10/2018 16:45
Endrin aldehyde ND 0.20 200 09/10/2018 16:45
Endrin ketone ND 0.20 200 09/10/2018 16:45
Heptachlor ND 0.20 200 09/10/2018 16:45
Heptachlor epoxide ND 0.20 200 09/10/2018 16:45
Hexachlorobenzene ND 2.0 200 09/10/2018 16:45
Hexachlorocyclopentadiene ND 4.0 200 09/10/2018 16:45
Methoxychlor ND 0.20 200 09/10/2018 16:45
Toxaphene ND 10 200 09/10/2018 16:45
Surrogates REC (%) LimitsQualifiers
Analytical Comments: c1,a3Analyst(s): LT
Decachlorobiphenyl 246 70-130S 09/10/2018 16:45
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(Cont.)
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B5 1.5-2' 1809251-002A Soil 08/31/2018 14:45 GC23 09071849.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 05:18 a-BHC ND 0.0010 1 09/08/2018 05:18 b-BHC ND 0.0010 1 09/08/2018 05:18 d-BHC ND 0.0010 1 09/08/2018 05:18 g-BHC ND 0.0010 1 09/08/2018 05:18
Chlordane (Technical) ND 0.025 1 09/08/2018 05:18 a-Chlordane ND 0.0010 1 09/08/2018 05:18 g-Chlordane ND 0.0010 1 09/08/2018 05:18 p,p-DDD ND 0.0010 1 09/08/2018 05:18 p,p-DDE ND 0.0010 1 09/08/2018 05:18 p,p-DDT ND 0.0010 1 09/08/2018 05:18
Dieldrin ND 0.0010 1 09/08/2018 05:18
Endosulfan I ND 0.0010 1 09/08/2018 05:18
Endosulfan II ND 0.0010 1 09/08/2018 05:18
Endosulfan sulfate ND 0.0010 1 09/08/2018 05:18
Endrin ND 0.0010 1 09/08/2018 05:18
Endrin aldehyde ND 0.0010 1 09/08/2018 05:18
Endrin ketone ND 0.0010 1 09/08/2018 05:18
Heptachlor ND 0.0010 1 09/08/2018 05:18
Heptachlor epoxide ND 0.0010 1 09/08/2018 05:18
Hexachlorobenzene ND 0.010 1 09/08/2018 05:18
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 05:18
Methoxychlor ND 0.0010 1 09/08/2018 05:18
Toxaphene ND 0.050 1 09/08/2018 05:18
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 123 70-130 09/08/2018 05:18
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B5 3-3.5' 1809251-003A Soil 08/31/2018 14:45 GC23 09071862.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 08:43 a-BHC ND 0.0010 1 09/08/2018 08:43 b-BHC ND 0.0010 1 09/08/2018 08:43 d-BHC ND 0.0010 1 09/08/2018 08:43 g-BHC ND 0.0010 1 09/08/2018 08:43
Chlordane (Technical) ND 0.025 1 09/08/2018 08:43 a-Chlordane ND 0.0010 1 09/08/2018 08:43 g-Chlordane ND 0.0010 1 09/08/2018 08:43 p,p-DDD ND 0.0010 1 09/08/2018 08:43 p,p-DDE ND 0.0010 1 09/08/2018 08:43 p,p-DDT ND 0.0010 1 09/08/2018 08:43
Dieldrin ND 0.0010 1 09/08/2018 08:43
Endosulfan I ND 0.0010 1 09/08/2018 08:43
Endosulfan II ND 0.0010 1 09/08/2018 08:43
Endosulfan sulfate ND 0.0010 1 09/08/2018 08:43
Endrin ND 0.0010 1 09/08/2018 08:43
Endrin aldehyde ND 0.0010 1 09/08/2018 08:43
Endrin ketone ND 0.0010 1 09/08/2018 08:43
Heptachlor ND 0.0010 1 09/08/2018 08:43
Heptachlor epoxide ND 0.0010 1 09/08/2018 08:43
Hexachlorobenzene ND 0.010 1 09/08/2018 08:43
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 08:43
Methoxychlor ND 0.0010 1 09/08/2018 08:43
Toxaphene ND 0.050 1 09/08/2018 08:43
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 123 70-130 09/08/2018 08:43
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B6 0.5-1' 1809251-004A Soil 08/31/2018 14:00 GC23 09071863.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0050 5 09/08/2018 08:59 a-BHC ND 0.0050 5 09/08/2018 08:59 b-BHC ND 0.0050 5 09/08/2018 08:59 d-BHC ND 0.0050 5 09/08/2018 08:59 g-BHC ND 0.0050 5 09/08/2018 08:59
Chlordane (Technical) ND 0.12 5 09/08/2018 08:59 a-Chlordane ND 0.0050 5 09/08/2018 08:59 g-Chlordane ND 0.0050 5 09/08/2018 08:59 p,p-DDD ND 0.0050 5 09/08/2018 08:59 p,p-DDE ND 0.0050 5 09/08/2018 08:59 p,p-DDT ND 0.0050 5 09/08/2018 08:59
Dieldrin ND 0.0050 5 09/08/2018 08:59
Endosulfan I ND 0.0050 5 09/08/2018 08:59
Endosulfan II ND 0.0050 5 09/08/2018 08:59
Endosulfan sulfate ND 0.0050 5 09/08/2018 08:59
Endrin ND 0.0050 5 09/08/2018 08:59
Endrin aldehyde ND 0.0050 5 09/08/2018 08:59
Endrin ketone ND 0.0050 5 09/08/2018 08:59
Heptachlor ND 0.0050 5 09/08/2018 08:59
Heptachlor epoxide ND 0.0050 5 09/08/2018 08:59
Hexachlorobenzene ND 0.050 5 09/08/2018 08:59
Hexachlorocyclopentadiene ND 0.10 5 09/08/2018 08:59
Methoxychlor ND 0.0050 5 09/08/2018 08:59
Toxaphene ND 0.25 5 09/08/2018 08:59
Surrogates REC (%) Limits
Analytical Comments: a3Analyst(s): LT
Decachlorobiphenyl 112 70-130 09/08/2018 08:59
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B6 1-1.5' 1809251-005A Soil 08/31/2018 14:00 GC23 09071864.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0050 5 09/08/2018 09:15 a-BHC ND 0.0050 5 09/08/2018 09:15 b-BHC ND 0.0050 5 09/08/2018 09:15 d-BHC ND 0.0050 5 09/08/2018 09:15 g-BHC ND 0.0050 5 09/08/2018 09:15
Chlordane (Technical) ND 0.12 5 09/08/2018 09:15 a-Chlordane ND 0.0050 5 09/08/2018 09:15 g-Chlordane ND 0.0050 5 09/08/2018 09:15 p,p-DDD ND 0.0050 5 09/08/2018 09:15 p,p-DDE ND 0.0050 5 09/08/2018 09:15 p,p-DDT ND 0.0050 5 09/08/2018 09:15
Dieldrin ND 0.0050 5 09/08/2018 09:15
Endosulfan I ND 0.0050 5 09/08/2018 09:15
Endosulfan II ND 0.0050 5 09/08/2018 09:15
Endosulfan sulfate ND 0.0050 5 09/08/2018 09:15
Endrin ND 0.0050 5 09/08/2018 09:15
Endrin aldehyde ND 0.0050 5 09/08/2018 09:15
Endrin ketone ND 0.0050 5 09/08/2018 09:15
Heptachlor ND 0.0050 5 09/08/2018 09:15
Heptachlor epoxide ND 0.0050 5 09/08/2018 09:15
Hexachlorobenzene ND 0.050 5 09/08/2018 09:15
Hexachlorocyclopentadiene ND 0.10 5 09/08/2018 09:15
Methoxychlor ND 0.0050 5 09/08/2018 09:15
Toxaphene ND 0.25 5 09/08/2018 09:15
Surrogates REC (%) Limits
Analytical Comments: a3Analyst(s): LT
Decachlorobiphenyl 122 70-130 09/08/2018 09:15
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B6 3-3.5' 1809251-006A Soil 08/31/2018 14:00 GC23 09071850.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 05:34 a-BHC ND 0.0010 1 09/08/2018 05:34 b-BHC ND 0.0010 1 09/08/2018 05:34 d-BHC ND 0.0010 1 09/08/2018 05:34 g-BHC ND 0.0010 1 09/08/2018 05:34
Chlordane (Technical) ND 0.025 1 09/08/2018 05:34 a-Chlordane ND 0.0010 1 09/08/2018 05:34 g-Chlordane ND 0.0010 1 09/08/2018 05:34 p,p-DDD 0.0017 0.0010 1 09/08/2018 05:34 p,p-DDE ND 0.0010 1 09/08/2018 05:34 p,p-DDT ND 0.0010 1 09/08/2018 05:34
Dieldrin ND 0.0010 1 09/08/2018 05:34
Endosulfan I ND 0.0010 1 09/08/2018 05:34
Endosulfan II ND 0.0010 1 09/08/2018 05:34
Endosulfan sulfate ND 0.0010 1 09/08/2018 05:34
Endrin ND 0.0010 1 09/08/2018 05:34
Endrin aldehyde ND 0.0010 1 09/08/2018 05:34
Endrin ketone ND 0.0010 1 09/08/2018 05:34
Heptachlor ND 0.0010 1 09/08/2018 05:34
Heptachlor epoxide ND 0.0010 1 09/08/2018 05:34
Hexachlorobenzene ND 0.010 1 09/08/2018 05:34
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 05:34
Methoxychlor ND 0.0010 1 09/08/2018 05:34
Toxaphene ND 0.050 1 09/08/2018 05:34
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 113 70-130 09/08/2018 05:34
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B8 0.5-1' 1809251-007A Soil 08/31/2018 11:30 GC23 09071865.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0020 2 09/08/2018 09:30 a-BHC ND 0.0020 2 09/08/2018 09:30 b-BHC ND 0.0020 2 09/08/2018 09:30 d-BHC ND 0.0020 2 09/08/2018 09:30 g-BHC ND 0.0020 2 09/08/2018 09:30
Chlordane (Technical) ND 0.050 2 09/08/2018 09:30 a-Chlordane ND 0.0020 2 09/08/2018 09:30 g-Chlordane ND 0.0020 2 09/08/2018 09:30 p,p-DDD ND 0.0020 2 09/08/2018 09:30 p,p-DDE ND 0.0020 2 09/08/2018 09:30 p,p-DDT ND 0.0020 2 09/08/2018 09:30
Dieldrin ND 0.0020 2 09/08/2018 09:30
Endosulfan I ND 0.0020 2 09/08/2018 09:30
Endosulfan II ND 0.0020 2 09/08/2018 09:30
Endosulfan sulfate ND 0.0020 2 09/08/2018 09:30
Endrin ND 0.0020 2 09/08/2018 09:30
Endrin aldehyde ND 0.0020 2 09/08/2018 09:30
Endrin ketone ND 0.0020 2 09/08/2018 09:30
Heptachlor ND 0.0020 2 09/08/2018 09:30
Heptachlor epoxide ND 0.0020 2 09/08/2018 09:30
Hexachlorobenzene ND 0.020 2 09/08/2018 09:30
Hexachlorocyclopentadiene ND 0.040 2 09/08/2018 09:30
Methoxychlor ND 0.0020 2 09/08/2018 09:30
Toxaphene ND 0.10 2 09/08/2018 09:30
Surrogates REC (%) Limits
Analytical Comments: a3Analyst(s): LT
Decachlorobiphenyl 119 70-130 09/08/2018 09:30
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3DJH����RI���
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B8 1-1.5' 1809251-008A Soil 08/31/2018 11:30 GC23 09071866.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 09:46 a-BHC ND 0.0010 1 09/08/2018 09:46 b-BHC ND 0.0010 1 09/08/2018 09:46 d-BHC ND 0.0010 1 09/08/2018 09:46 g-BHC ND 0.0010 1 09/08/2018 09:46
Chlordane (Technical) ND 0.025 1 09/08/2018 09:46 a-Chlordane ND 0.0010 1 09/08/2018 09:46 g-Chlordane ND 0.0010 1 09/08/2018 09:46 p,p-DDD ND 0.0010 1 09/08/2018 09:46 p,p-DDE ND 0.0010 1 09/08/2018 09:46 p,p-DDT ND 0.0010 1 09/08/2018 09:46
Dieldrin ND 0.0010 1 09/08/2018 09:46
Endosulfan I ND 0.0010 1 09/08/2018 09:46
Endosulfan II ND 0.0010 1 09/08/2018 09:46
Endosulfan sulfate ND 0.0010 1 09/08/2018 09:46
Endrin ND 0.0010 1 09/08/2018 09:46
Endrin aldehyde ND 0.0010 1 09/08/2018 09:46
Endrin ketone ND 0.0010 1 09/08/2018 09:46
Heptachlor ND 0.0010 1 09/08/2018 09:46
Heptachlor epoxide ND 0.0010 1 09/08/2018 09:46
Hexachlorobenzene ND 0.010 1 09/08/2018 09:46
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 09:46
Methoxychlor ND 0.0010 1 09/08/2018 09:46
Toxaphene ND 0.050 1 09/08/2018 09:46
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 121 70-130 09/08/2018 09:46
&$�(/$3��������1(/$3�����25(/$3
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B8 2.5-3' 1809251-009A Soil 08/31/2018 11:30 GC23 09071868.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 10:18 a-BHC ND 0.0010 1 09/08/2018 10:18 b-BHC ND 0.0010 1 09/08/2018 10:18 d-BHC ND 0.0010 1 09/08/2018 10:18 g-BHC ND 0.0010 1 09/08/2018 10:18
Chlordane (Technical) ND 0.025 1 09/08/2018 10:18 a-Chlordane ND 0.0010 1 09/08/2018 10:18 g-Chlordane ND 0.0010 1 09/08/2018 10:18 p,p-DDD ND 0.0010 1 09/08/2018 10:18 p,p-DDE ND 0.0010 1 09/08/2018 10:18 p,p-DDT ND 0.0010 1 09/08/2018 10:18
Dieldrin ND 0.0010 1 09/08/2018 10:18
Endosulfan I ND 0.0010 1 09/08/2018 10:18
Endosulfan II ND 0.0010 1 09/08/2018 10:18
Endosulfan sulfate ND 0.0010 1 09/08/2018 10:18
Endrin ND 0.0010 1 09/08/2018 10:18
Endrin aldehyde ND 0.0010 1 09/08/2018 10:18
Endrin ketone ND 0.0010 1 09/08/2018 10:18
Heptachlor ND 0.0010 1 09/08/2018 10:18
Heptachlor epoxide ND 0.0010 1 09/08/2018 10:18
Hexachlorobenzene ND 0.010 1 09/08/2018 10:18
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 10:18
Methoxychlor ND 0.0010 1 09/08/2018 10:18
Toxaphene ND 0.050 1 09/08/2018 10:18
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 122 70-130 09/08/2018 10:18
&$�(/$3��������1(/$3�����25(/$3
1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B9 0.5-1' 1809251-010A Soil 08/31/2018 10:30 GC40 09141817.d 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0020 2 09/14/2018 14:07 a-BHC ND 0.0020 2 09/14/2018 14:07 b-BHC ND 0.0020 2 09/14/2018 14:07 d-BHC ND 0.0020 2 09/14/2018 14:07 g-BHC ND 0.0020 2 09/14/2018 14:07
Chlordane (Technical) ND 0.050 2 09/14/2018 14:07 a-Chlordane ND 0.0020 2 09/14/2018 14:07 g-Chlordane ND 0.0020 2 09/14/2018 14:07 p,p-DDD ND 0.0020 2 09/14/2018 14:07 p,p-DDE ND 0.0020 2 09/14/2018 14:07 p,p-DDT 0.0021 0.0020 2 09/14/2018 14:07
Dieldrin ND 0.0020 2 09/14/2018 14:07
Endosulfan I ND 0.0020 2 09/14/2018 14:07
Endosulfan II ND 0.0020 2 09/14/2018 14:07
Endosulfan sulfate ND 0.0020 2 09/14/2018 14:07
Endrin ND 0.0020 2 09/14/2018 14:07
Endrin aldehyde ND 0.0020 2 09/14/2018 14:07
Endrin ketone ND 0.0020 2 09/14/2018 14:07
Heptachlor ND 0.0020 2 09/14/2018 14:07
Heptachlor epoxide ND 0.0020 2 09/14/2018 14:07
Hexachlorobenzene ND 0.020 2 09/14/2018 14:07
Hexachlorocyclopentadiene ND 0.040 2 09/14/2018 14:07
Methoxychlor ND 0.0020 2 09/14/2018 14:07
Toxaphene ND 0.10 2 09/14/2018 14:07
Surrogates REC (%) Limits
Analytical Comments: a1,a2Analyst(s): KX
Decachlorobiphenyl 110 70-130 09/14/2018 14:07
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B9 1-1.5' 1809251-011A Soil 08/31/2018 10:30 GC23 09071851.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 05:50 a-BHC ND 0.0010 1 09/08/2018 05:50 b-BHC ND 0.0010 1 09/08/2018 05:50 d-BHC ND 0.0010 1 09/08/2018 05:50 g-BHC ND 0.0010 1 09/08/2018 05:50
Chlordane (Technical) ND 0.025 1 09/08/2018 05:50 a-Chlordane ND 0.0010 1 09/08/2018 05:50 g-Chlordane ND 0.0010 1 09/08/2018 05:50 p,p-DDD ND 0.0010 1 09/08/2018 05:50 p,p-DDE ND 0.0010 1 09/08/2018 05:50 p,p-DDT ND 0.0010 1 09/08/2018 05:50
Dieldrin ND 0.0010 1 09/08/2018 05:50
Endosulfan I ND 0.0010 1 09/08/2018 05:50
Endosulfan II ND 0.0010 1 09/08/2018 05:50
Endosulfan sulfate ND 0.0010 1 09/08/2018 05:50
Endrin ND 0.0010 1 09/08/2018 05:50
Endrin aldehyde ND 0.0010 1 09/08/2018 05:50
Endrin ketone ND 0.0010 1 09/08/2018 05:50
Heptachlor ND 0.0010 1 09/08/2018 05:50
Heptachlor epoxide ND 0.0010 1 09/08/2018 05:50
Hexachlorobenzene ND 0.010 1 09/08/2018 05:50
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 05:50
Methoxychlor ND 0.0010 1 09/08/2018 05:50
Toxaphene ND 0.050 1 09/08/2018 05:50
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 114 70-130 09/08/2018 05:50
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/7/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8081A
Unit : mg/kg
Organochlorine Pesticides
B9 2.5-3' 1809251-012A Soil 08/31/2018 10:30 GC23 09071852.D 164535
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
Aldrin ND 0.0010 1 09/08/2018 06:05 a-BHC ND 0.0010 1 09/08/2018 06:05 b-BHC ND 0.0010 1 09/08/2018 06:05 d-BHC ND 0.0010 1 09/08/2018 06:05 g-BHC ND 0.0010 1 09/08/2018 06:05
Chlordane (Technical) ND 0.025 1 09/08/2018 06:05 a-Chlordane ND 0.0010 1 09/08/2018 06:05 g-Chlordane ND 0.0010 1 09/08/2018 06:05 p,p-DDD ND 0.0010 1 09/08/2018 06:05 p,p-DDE ND 0.0010 1 09/08/2018 06:05 p,p-DDT ND 0.0010 1 09/08/2018 06:05
Dieldrin ND 0.0010 1 09/08/2018 06:05
Endosulfan I ND 0.0010 1 09/08/2018 06:05
Endosulfan II ND 0.0010 1 09/08/2018 06:05
Endosulfan sulfate ND 0.0010 1 09/08/2018 06:05
Endrin ND 0.0010 1 09/08/2018 06:05
Endrin aldehyde ND 0.0010 1 09/08/2018 06:05
Endrin ketone ND 0.0010 1 09/08/2018 06:05
Heptachlor ND 0.0010 1 09/08/2018 06:05
Heptachlor epoxide ND 0.0010 1 09/08/2018 06:05
Hexachlorobenzene ND 0.010 1 09/08/2018 06:05
Hexachlorocyclopentadiene ND 0.020 1 09/08/2018 06:05
Methoxychlor ND 0.0010 1 09/08/2018 06:05
Toxaphene ND 0.050 1 09/08/2018 06:05
Surrogates REC (%) Limits
Analyst(s): LT
Decachlorobiphenyl 118 70-130 09/08/2018 06:05
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B5 0.5-1' 1809251-001A Soil 08/31/2018 14:45 GC21 09101823.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene ND 0.21 20 09/10/2018 19:33
Acenaphthene ND 0.21 20 09/10/2018 19:33
Acenaphthylene ND 0.21 20 09/10/2018 19:33
Anthracene ND 0.21 20 09/10/2018 19:33
Benzo (a) anthracene ND 0.80 20 09/10/2018 19:33
Benzo (a) pyrene ND 0.40 20 09/10/2018 19:33
Benzo (b) fluoranthene ND 0.21 20 09/10/2018 19:33
Benzo (g,h,i) perylene ND 0.40 20 09/10/2018 19:33
Benzo (k) fluoranthene ND 0.21 20 09/10/2018 19:33
Chrysene ND 0.40 20 09/10/2018 19:33
Dibenzo (a,h) anthracene ND 0.40 20 09/10/2018 19:33
Fluoranthene ND 0.21 20 09/10/2018 19:33
Fluorene ND 0.40 20 09/10/2018 19:33
Indeno (1,2,3-cd) pyrene ND 0.40 20 09/10/2018 19:33
2-Methylnaphthalene ND 0.40 20 09/10/2018 19:33
Naphthalene ND 0.21 20 09/10/2018 19:33
Phenanthrene ND 0.80 20 09/10/2018 19:33
Pyrene ND 0.40 20 09/10/2018 19:33
Surrogates REC (%) Limits
Analytical Comments: a4Analyst(s): REB
2-Fluorophenol 108 30-130 09/10/2018 19:33
2-Fluorobiphenyl 115 30-130 09/10/2018 19:33
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B5 1.5-2' 1809251-002A Soil 08/31/2018 14:45 GC21 09101824.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene 0.0016 0.0013 1 09/10/2018 20:00
Acenaphthene ND 0.0013 1 09/10/2018 20:00
Acenaphthylene ND 0.0013 1 09/10/2018 20:00
Anthracene ND 0.0013 1 09/10/2018 20:00
Benzo (a) anthracene ND 0.0050 1 09/10/2018 20:00
Benzo (a) pyrene ND 0.0025 1 09/10/2018 20:00
Benzo (b) fluoranthene 0.0013 0.0013 1 09/10/2018 20:00
Benzo (g,h,i) perylene ND 0.0025 1 09/10/2018 20:00
Benzo (k) fluoranthene ND 0.0013 1 09/10/2018 20:00
Chrysene ND 0.0025 1 09/10/2018 20:00
Dibenzo (a,h) anthracene ND 0.0025 1 09/10/2018 20:00
Fluoranthene 0.0013 0.0013 1 09/10/2018 20:00
Fluorene ND 0.0025 1 09/10/2018 20:00
Indeno (1,2,3-cd) pyrene ND 0.0025 1 09/10/2018 20:00
2-Methylnaphthalene ND 0.0025 1 09/10/2018 20:00
Naphthalene ND 0.0013 1 09/10/2018 20:00
Phenanthrene 0.0060 0.0050 1 09/10/2018 20:00
Pyrene ND 0.0025 1 09/10/2018 20:00
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 96 30-130 09/10/2018 20:00
2-Fluorobiphenyl 79 30-130 09/10/2018 20:00
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B5 3-3.5' 1809251-003A Soil 08/31/2018 14:45 GC21 09101825.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene 0.0018 0.0013 1 09/10/2018 20:27
Acenaphthene ND 0.0013 1 09/10/2018 20:27
Acenaphthylene ND 0.0013 1 09/10/2018 20:27
Anthracene ND 0.0013 1 09/10/2018 20:27
Benzo (a) anthracene 0.0096 0.0050 1 09/10/2018 20:27
Benzo (a) pyrene 0.0076 0.0025 1 09/10/2018 20:27
Benzo (b) fluoranthene 0.0066 0.0013 1 09/10/2018 20:27
Benzo (g,h,i) perylene 0.010 0.0025 1 09/10/2018 20:27
Benzo (k) fluoranthene 0.010 0.0013 1 09/10/2018 20:27
Chrysene 0.010 0.0025 1 09/10/2018 20:27
Dibenzo (a,h) anthracene 0.0097 0.0025 1 09/10/2018 20:27
Fluoranthene 0.0069 0.0013 1 09/10/2018 20:27
Fluorene ND 0.0025 1 09/10/2018 20:27
Indeno (1,2,3-cd) pyrene 0.0094 0.0025 1 09/10/2018 20:27
2-Methylnaphthalene ND 0.0025 1 09/10/2018 20:27
Naphthalene ND 0.0013 1 09/10/2018 20:27
Phenanthrene 0.0072 0.0050 1 09/10/2018 20:27
Pyrene 0.0072 0.0025 1 09/10/2018 20:27
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 90 30-130 09/10/2018 20:27
2-Fluorobiphenyl 77 30-130 09/10/2018 20:27
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B6 0.5-1' 1809251-004A Soil 08/31/2018 14:00 GC21 09101826.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene ND 0.0013 1 09/10/2018 20:54
Acenaphthene ND 0.0013 1 09/10/2018 20:54
Acenaphthylene ND 0.0013 1 09/10/2018 20:54
Anthracene ND 0.0013 1 09/10/2018 20:54
Benzo (a) anthracene ND 0.0050 1 09/10/2018 20:54
Benzo (a) pyrene ND 0.0025 1 09/10/2018 20:54
Benzo (b) fluoranthene ND 0.0013 1 09/10/2018 20:54
Benzo (g,h,i) perylene ND 0.0025 1 09/10/2018 20:54
Benzo (k) fluoranthene ND 0.0013 1 09/10/2018 20:54
Chrysene ND 0.0025 1 09/10/2018 20:54
Dibenzo (a,h) anthracene ND 0.0025 1 09/10/2018 20:54
Fluoranthene ND 0.0013 1 09/10/2018 20:54
Fluorene ND 0.0025 1 09/10/2018 20:54
Indeno (1,2,3-cd) pyrene ND 0.0025 1 09/10/2018 20:54
2-Methylnaphthalene ND 0.0025 1 09/10/2018 20:54
Naphthalene ND 0.0013 1 09/10/2018 20:54
Phenanthrene ND 0.0050 1 09/10/2018 20:54
Pyrene ND 0.0025 1 09/10/2018 20:54
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 93 30-130 09/10/2018 20:54
2-Fluorobiphenyl 82 30-130 09/10/2018 20:54
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B6 1-1.5' 1809251-005A Soil 08/31/2018 14:00 GC21 09101827.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene ND 0.0026 2 09/10/2018 21:21
Acenaphthene ND 0.0026 2 09/10/2018 21:21
Acenaphthylene ND 0.0026 2 09/10/2018 21:21
Anthracene ND 0.0026 2 09/10/2018 21:21
Benzo (a) anthracene ND 0.010 2 09/10/2018 21:21
Benzo (a) pyrene ND 0.0050 2 09/10/2018 21:21
Benzo (b) fluoranthene ND 0.0026 2 09/10/2018 21:21
Benzo (g,h,i) perylene ND 0.0050 2 09/10/2018 21:21
Benzo (k) fluoranthene ND 0.0026 2 09/10/2018 21:21
Chrysene ND 0.0050 2 09/10/2018 21:21
Dibenzo (a,h) anthracene ND 0.0050 2 09/10/2018 21:21
Fluoranthene ND 0.0026 2 09/10/2018 21:21
Fluorene ND 0.0050 2 09/10/2018 21:21
Indeno (1,2,3-cd) pyrene ND 0.0050 2 09/10/2018 21:21
2-Methylnaphthalene ND 0.0050 2 09/10/2018 21:21
Naphthalene ND 0.0026 2 09/10/2018 21:21
Phenanthrene ND 0.010 2 09/10/2018 21:21
Pyrene ND 0.0050 2 09/10/2018 21:21
Surrogates REC (%) Limits
Analytical Comments: a3Analyst(s): REB
2-Fluorophenol 93 30-130 09/10/2018 21:21
2-Fluorobiphenyl 80 30-130 09/10/2018 21:21
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B6 3-3.5' 1809251-006A Soil 08/31/2018 14:00 GC21 09101828.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene 0.0063 0.0013 1 09/10/2018 21:49
Acenaphthene ND 0.0013 1 09/10/2018 21:49
Acenaphthylene ND 0.0013 1 09/10/2018 21:49
Anthracene ND 0.0013 1 09/10/2018 21:49
Benzo (a) anthracene ND 0.0050 1 09/10/2018 21:49
Benzo (a) pyrene ND 0.0025 1 09/10/2018 21:49
Benzo (b) fluoranthene 0.0016 0.0013 1 09/10/2018 21:49
Benzo (g,h,i) perylene ND 0.0025 1 09/10/2018 21:49
Benzo (k) fluoranthene ND 0.0013 1 09/10/2018 21:49
Chrysene ND 0.0025 1 09/10/2018 21:49
Dibenzo (a,h) anthracene ND 0.0025 1 09/10/2018 21:49
Fluoranthene 0.0022 0.0013 1 09/10/2018 21:49
Fluorene ND 0.0025 1 09/10/2018 21:49
Indeno (1,2,3-cd) pyrene ND 0.0025 1 09/10/2018 21:49
2-Methylnaphthalene 0.011 0.0025 1 09/10/2018 21:49
Naphthalene 0.0060 0.0013 1 09/10/2018 21:49
Phenanthrene 0.010 0.0050 1 09/10/2018 21:49
Pyrene 0.0029 0.0025 1 09/10/2018 21:49
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 105 30-130 09/10/2018 21:49
2-Fluorobiphenyl 84 30-130 09/10/2018 21:49
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B8 0.5-1' 1809251-007A Soil 08/31/2018 11:30 GC21 09101829.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene 0.013 0.0013 1 09/10/2018 22:16
Acenaphthene ND 0.0013 1 09/10/2018 22:16
Acenaphthylene ND 0.0013 1 09/10/2018 22:16
Anthracene ND 0.0013 1 09/10/2018 22:16
Benzo (a) anthracene 0.0073 0.0050 1 09/10/2018 22:16
Benzo (a) pyrene ND 0.0025 1 09/10/2018 22:16
Benzo (b) fluoranthene 0.0024 0.0013 1 09/10/2018 22:16
Benzo (g,h,i) perylene ND 0.0025 1 09/10/2018 22:16
Benzo (k) fluoranthene ND 0.0013 1 09/10/2018 22:16
Chrysene 0.0036 0.0025 1 09/10/2018 22:16
Dibenzo (a,h) anthracene ND 0.0025 1 09/10/2018 22:16
Fluoranthene 0.0031 0.0013 1 09/10/2018 22:16
Fluorene ND 0.0025 1 09/10/2018 22:16
Indeno (1,2,3-cd) pyrene ND 0.0025 1 09/10/2018 22:16
2-Methylnaphthalene 0.016 0.0025 1 09/10/2018 22:16
Naphthalene 0.021 0.0013 1 09/10/2018 22:16
Phenanthrene 0.025 0.0050 1 09/10/2018 22:16
Pyrene 0.0051 0.0025 1 09/10/2018 22:16
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 92 30-130 09/10/2018 22:16
2-Fluorobiphenyl 77 30-130 09/10/2018 22:16
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B8 1-1.5' 1809251-008A Soil 08/31/2018 11:30 GC21 09101830.D 164633
Analytes Result DF Date AnalyzedRL
Client ID Lab ID Matr ix Date Collected Instrument Batch ID
1-Methylnaphthalene 0.062 0.0013 1 09/10/2018 22:43
Acenaphthene ND 0.0013 1 09/10/2018 22:43
Acenaphthylene ND 0.0013 1 09/10/2018 22:43
Anthracene ND 0.0013 1 09/10/2018 22:43
Benzo (a) anthracene 0.0090 0.0050 1 09/10/2018 22:43
Benzo (a) pyrene 0.0062 0.0025 1 09/10/2018 22:43
Benzo (b) fluoranthene 0.0061 0.0013 1 09/10/2018 22:43
Benzo (g,h,i) perylene 0.0081 0.0025 1 09/10/2018 22:43
Benzo (k) fluoranthene 0.0060 0.0013 1 09/10/2018 22:43
Chrysene 0.010 0.0025 1 09/10/2018 22:43
Dibenzo (a,h) anthracene 0.0065 0.0025 1 09/10/2018 22:43
Fluoranthene 0.0073 0.0013 1 09/10/2018 22:43
Fluorene 0.0031 0.0025 1 09/10/2018 22:43
Indeno (1,2,3-cd) pyrene 0.0066 0.0025 1 09/10/2018 22:43
2-Methylnaphthalene 0.089 0.0025 1 09/10/2018 22:43
Naphthalene 0.035 0.0013 1 09/10/2018 22:43
Phenanthrene 0.036 0.0050 1 09/10/2018 22:43
Pyrene 0.0085 0.0025 1 09/10/2018 22:43
Surrogates REC (%) Limits
Analyst(s): REB
2-Fluorophenol 96 30-130 09/10/2018 22:43
2-Fluorobiphenyl 73 30-130 09/10/2018 22:43
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1534 Willow Pass Road, Pittsburg, CA 94565-1701
Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 http://www.mccampbell.com / E-mail: main@mccampbell.com"When Quality Counts"
Client: Analytical Sciences
Project: 8090551; China Beach
Date Received: 9/7/18 10:25
Date Prepared: 9/10/18
WorkOrder: 1809251
Extraction Method: SW3550B
Analytical Method: SW8270C-SIM
Unit : mg/kg
Polynuclear Ar omatic Hydrocarbons (PAHs / PNAs) using SIM M ode
B8 2.5-3' 1809251-009A Soil 08/31/2018…
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