Attachment I Statement of Work.pdf

Statement of Work for

Contracted Laboratory Services

South Pacific Region 23 November 2020

Contents C-1.0 General Description:

C-1.0.1 Service Locations:

C-1.1 Specifications, Standards and Handbooks:

C-1.2 Facilities:

C-1.3 Scheduling of Services:

C-2.0 Contractor Detailed Plans:

C-2.1 Contract Compliance Plan:

C-2.2 Contract Contingency Plan:

C-2.3 Contract Training Plan:

C-2.4 Laboratory Testing Plan:

C-2.5 Safety Plan:

C-2.6 Transportation Plan:

C-2.7 Laboratory Equipment Plan:

C-3.0 Operating Hours:

C-3.1 Staffing:

C-3.2 Knowledge and Skills:

C-4.0 Information and Records Management:

C-4.1 Monthly Reporting Deliverable:

C-5.0 Laboratory Performance Requirements:

C-5.1 Testing Capabilities Deliverable:

C-5.2 Access:

C-5.3 Laboratories:

C-5.3.1 Epoxy Lined Sample Cans:

C-5.4 Product Testing:

C-5.4.1 Ellipsometric Tube Deposit Rater (ETR):

C-5.5 Sample Testing Turnaround Times:

C-5.6 Retain samples:

C-6.0 Transportation Performance Requirements:

C-7.0 Secured Fuels Performance Requirements:

C-8.0 Surveyor Duties:

Attachment 1: Products to be Tested Attachment 2: Series Testing Requirements Attachment 3: Approved Testing Methods Attachment 4: Annual Estimates by Location:

Attachment 5: Sample Shipment

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C-1.0 General Description:

This Statement of Work (SOW) is established to identify the Contractor responsibilities for the period of performance identified in the solicitation and resultatnt contract(s). The Contractor will be responsible for the laboratory testing of government-owned petroleum products in accordance with the specifcations as described herein, and transportation of samples from specified locations to laboratory. Government-owned products mentioned in this SOW located outside the service locations in section C-1.0.1 may be shipped to the Contractor’s laboratory for testing; however the Contractor will not provide transportation unless requested by DLA Energy separately.

C-1.0.1 Service Locations:

The Contractor shall be able to provide requested service of this SOW to the requiring location in the table below. Other locations may be added by future modification. The Contractor shall have a facility in the same country as the locations in the below tables to provide the services required. Addresses can be furnished at contract award if requested.

Guam Philippines Anderson AFB DFSP Subic Bay II (Free Zone) DFSP Guam DFSP Guam II

C-1.1 Specifications, Standards and Handbooks:

The Contractor shall maintain all of the required specifications, standards, test methods, handbooks, etc., per this SOW and perform services in accordance with testing requirements. Military Specifications referenced in Attachment 1 for petroleum product types can be obtained at http://quicksearch.dla.mil or https://assist.dla.mil but can also be supplied by the Contracting Officer (CO) or Contracting Officer’s Representative (COR) if requested in writing.

C-1.2 Facilities:

The Contractor shall have facilities in accordance with paragraph C-1.0.1 to meet the required turn-around times in section C-5.5, provide the location(s) of the facility where the product shall be tested, facility testing capabilities and contact information. If testing of products requirements cannot be accomplished locally, i.e., in the same location or origin, the Contractor shall submit an exemption request with a detailed plan on where the samples shall be tested and how the location shall meet coordinated turn-around times.

C-1.3 Scheduling of Services:

The Contractor shall not perform petroleum testing without a task order from the CO. If a task order was not received, the Contractor shall contact the CO or COR prior to any testing. Only the CO can obligate DLA Energy or verbally authorize testing.

C-2.0 Contractor Detailed Plans:

All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The Government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for Government review upon request at any time during the contract performance period.

C-2.1 Contract Compliance Plan:

The Contractor is responsible for ensuring compliance with all contract performance requirements. The Contractor shall develop an inspection system acceptable to the Government for monitoring overall contract performance. ISO 9001 and/or ISO/IEC 17025 can be considered acceptable with proper certification. The Contract Compliance Plan (CCP) shall include performance requirements for all of the services and specific tasks listed in this SOW and the Contractor’s own performance based plans. The CCP shall include time specific checklists for evaluation of all operational requirements. The CCP shall address procedures for corrective actions including the resolution of any Corrective Action Requests (CAR) and Quality Deficiency Reports (QDR) generated by the Government. Contractor laboratory facilities and personnel and equipment shall be vetted by a DLA Energy Quality representative prior to or during the first order of the performance period unless laboratory was vetted under a previous DLA Energy contract. DLA Energy Quality representatives will conduct periodic site visits to ensure contract compliance. Contractors which have to sub-contract certain test methods or tasks out, due to whatever circumstances, must inform the contracting officer during the offer period, request for an exception, deviation or waiver (EDW) for that particular task, and have the DLA Energy representative in the region vet that/those processes before

Page | 2 or during the first order. The Contractor is responsible for all actions taken by any sub-contractor utilized under this contract.

C-2.2 Contract Contingency Plan:

The Contract Contingency Plan shall outline Contractor actions to ensure there is no significant interruption of services resulting from labor disputes, catastrophic failure of equipment, or the effects of natural disasters/emergencies. The plan shall provide specific details regarding labor issues that may result from potential world events, world actions, military contingency and war time manning requirements as well as subcontracting that may be required to meet emergent manning requirements, and the replacement of equipment anticipated to be out of service for more than 48 hours.

C-2.3 Contract Training Plan:

The Contractor shall provide a detailed plan that identifies employee training requirements and procedures necessary to maintain proficiency. The plan shall identify length of training, training sources and a brief description of courses such as safety, environmental protection and job qualification training. The Contractor is responsible for ensuring all individual training requirements are accomplished. The Contractor must demonstrate current participation in a proficiency program or suitable means to verify laboratory performance.

C-2.4 Laboratory Testing Plan:

The Contractor shall maintain detailed plans regarding the required characteristic tests as presented in Attachments 2 and 3.

Contractor shall maintain all of the necessary testing standards and specifications, as noted in paragraph C-1.1 above. If the Contractor is unable to provide certain specification tests, as listed in the maintained standards and specifications, the Contractor must request an exception, deviation or waiver (EDW) during the solicitation process and after award if any changes have occurred. EDW request should be detailed with the cause of such request and the Contractor’s means of correcting the deficiency. If the Contractor plans on using a subcontractor to perform certain tests and/or functions, the Contractor must provide that information in their plan.. The Contractor must also ensure they either possess or have access to all referee methods described in the various specifications. If the Contractor plans on using another laboratory for either normal sample testing as described in this SOW or for referee method support, the Contractor must be able to adhere to the turnaround times listed in C-5.5 below.

C-2.5 Safety Plan:

The Contractor shall provide a detailed plan outlining the policy, procedures and actions necessary to maintain a safe working environment for employees and visitors. The plan shall cover the products stored, handled, Safety Data Sheets (SDS) and guidelines regarding the safe handling of such products and shall be maintained and updated over the course of the contract.

C-2.6 Transportation Plan:

The Contractor is required to submit a plan for review to transport the petroleum samples to an approved laboratory for testing or shipping (Contractor supplied transport, third party delivery service, etc.) and how they plan on tracking the chain of custody to the Contractor’s facility. Product quality must be preserved and not altered by shipment. DLA Energy or its storage terminal contractor(s) do not have the ability or certification to ship or package fuel samples.

C-2.7 Laboratory Equipment Plan:

The Contractor will furnish annually to the CO directly the status by name, model and serviceability of all equipment used in laboratory testing. Equipment that malfunctions or is non-serviceable will be reported to the CO within 48 hours with miagration plan to provide testing capability.

C-3.0 Operating Hours:

The Contractor shall be responsible for adjusting hours of operation to avoid overtime to provide highest level of service to meet workload demands and turnaround times in section C-5.5.

C-3.1 Staffing:

The Contractor shall provide sufficient staffing to accomplish all functions and tasks to include simultaneous operations of performing multiple tests at a time. The Contractor’s staff shall be able to communicate in English and flexible and fully capable of meeting the demands of written orders or oral requests made by DLA Energy representatives. The Contractor shall provide the contact information for a Laboratory Manager or an Assistant Laboratory Manager if the laboratory is not manned 24 hours, seven days a week.

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C-3.2 Knowledge and Skills:

The Contractor shall ensure that personnel assigned to all tasks have the requisite knowledge and skills to meet the performance standards for those tasks and comply with all applicable Country, Federal and state laws, regulations and codes.

All supervisors and key employees shall be able to read and understand English so they can understand and follow oral or written instructions directions, directives, regulations, operating procedures and be capable of writing in English to compose required detailed reports.

C-4.0 Information and Records Management:

The Contractor shall maintain records evidencing all services performed containing a complete description held or generated by the Contractor. Records shall be open and readily available to DLA Energy for inspection, review, and audit for the duration of the contract and any subsequent and contiguous contract periods. In addition, special reports may be requested for audits, inspections, reviews and research. On expiration of the contract, all records except personnel files, training records, equipment records and non-proprietary company management records shall be deemed the property of the government and turned over to the Government.

C-4.1 Monthly Reporting Deliverable:

The Contractor shall report monthly to the CO and COR the number of laboratory tests performed, what testing was included and the location.

C-5.0 Laboratory Performance Requirements:

The Contractor shall maintain records evidencing all analysis performed under this contract. All samples tested shall be documented with a detailed report. Reports shall be complete and legible containing information pertaining but not limited to: Lab Name, Test Method, Test Name, Test Results, Test Units, Test Limits. Reports not containing the appropriate information will need to be corrected and resubmitted by the Contractor for approval.

C-5.1 Testing Capabilities Deliverable:

The Contractor must keep CO and COR apprised of any changes to services and proficiencies. Any changes will be reported within 48 hours in writing with a full description of changes and impact to testing. Annually, the Contractor shall provide CO with a list of testing capabilities, locations testing can be completed and a point of contact.

C-5.2 Access:

The Contractor shall allow DLA Energy Representatives to witness testing or sampling and provide applicable information for access, as well as provide follow-up to obtain access (for personnel and vehicles) to all facilities that product is tested or sampled. For areas that require special admission the Contractor will assist gaining access.

C-5.3 Laboratories:

The laboratories shall have a system of calibration equivalent to ISO 10012-1 or 17025. All testing shall be performed in accordance with the appropriate international or local test methods that have been approved for use by DLA Energy and listed in this SOW. Laboratories are required to have the listed referee test methods as referenced in the product specifications and international test methods (ASTM, IP, etc.).

C-5.3.1 Epoxy Lined Sample Cans:

The Contractor shall maintain a supply of 10 unused epoxy lined fuel sample shipping containers to be provided to DLA Energy personnel per request. Sample containers shall be stored to ensure they are clean and free from all substances that might contaminate the product being sampled. Containers must meet the following specifics: Complies with ASTM D- 4306, height not to exceed 9 inches, diameter not to exceed 7 inches, capacity 1 USG, Bung Plug ¾” with lock-wire hole, carrying handle able to be shipped as hazardous material.

C-5.4 Product Testing:

Employees must follow all mentioned, laboratory related reference materials listed in this SOW attachments. Samples

Page | 4 which fail initial testing shall be retested immediately within 1 hour and prior to submission of any test results. The Contractor shall immediately report any delays to the CO, COR and Quality Assurance Representative (QAR) for resolution.

C-5.4.1 Ellipsometric Tube Deposit Rater (ETR):

The Contractor shall have the ability to perform ASTM D3241 Annex 3 ETR within the testing turnaround time in section C-5.5 Sample Testing Turnaround Times when a request is made. ETR is the preferred method and shall be treated as the referee method.

C-5.5 Sample Testing Turnaround Times:

Turnaround time starts when the Contractor is notified that the sample is prepared for transportation from sample location to the servicing laboratory. DLA Energy will give the Contractor at least 12 hours of advance notice when sample will be ready. (prime Contractor is responsible for any sub-Contractor actions). Turnaround times ends when the Contractor submits the test reports to the responsible office. All testing requested, per order, shall be completed within the turn-around time listed below. Turnaround time ends when testing results are completed and delivered to DLA Energy. If testing cannot be completed within the turnaround time due to an unusually long processing time as stated within the test method or some other issue which evolves during the process, the Contractor will immediately notify the CO and COR. The Contractor will specify the problem and the estimated completion date and time.

Maximum Turn-around Hours Chart A level/Full spec testing 48 hours B-1, B-2, B-3 Testing 36 hours C-level Testing 24 hours Individual Tests 5 hours Secured Fuels Testing 8 hours Expedite Request 12 hours

C-5.6 Retain samples:

Samples shall be retained, after analysis, for a minimum of 45 days. In the event of a suspected quality issue or dispute a longer sample retention period may be requested by DLA Energy. The Contractor shall be responsible for disposal of excess fuel samples and sample containers.

C-6.0 Transportation Performance Requirements:

The Contractor shall be responsible for packing and transporting all petroleum samples from job site in paragraph C-1.0.1 to the laboratory in accordance with state, federal, and local laws and regulations. When sample transportation is not required, the Contractor will be notified (sample delivered to laboratory by another person). DLA Energy or its storage terminal contractor do not have the ability or certification to ship or package fuel samples.

C-7.0 Secured Fuels Performance Requirements:

Due to mission demands the DLA Energy CO, the COR or the QAR may request special petroleum sampling, handling and testing for distinguished visitors. Fuel testing will be from A, B, C series or individual tests in Attachment 2 IAW with MIL-STD-3004-1 Table XII. DLA Energy will provide the Contractor with as much advance notice as possible as the turnaround time shall not exceed 8 hours. Specifics shall be given as guidance if a requirement is requested under this section.

C-8.0 Surveyor Duties:

1. The Contractor shall be capable of respresenting DLA Energy to ensure all specifications, regulations, ASTM, API MPMS are followed when a DLA Energy representative is not available at locations mentioned in C-1.0.1.

Personnel shall be International Federation of Inspection Agencies or TIC council or equivalent certified to perform the duties defined in the following subparagraphs.

1.1 Third party witness. The Contractor shall act as a third party witness to observe operations and report findings to DLA Energy point of contact with a detailed report within 24 hours. DLA Energy will provide written instructions specific to the operations and objectives in the Task Order. The following are examples of operations commonly preformed: Tank to tank transfers, off-loading vessels, barges, tank trucks, containers, loading vessels, Page | 5 barges, tank trucks, containers.

1.2 Sampling of petroleum products. The Contractor shall be capablity of performing sampling in accordance with API MPMS and/or ASTM D4057 when requested of pipelines, vessels, barges, tank trucks, storage tanks, or any containers that may hold fuel. The Contractor shall supply all equipment and material need to perform task.

1.3 Gauging of petroleum products. The Contractor shall be capablity of performing gauging of vessels (to include bunkers), barges, tank trucks, storage tanks, or any containers that may hold fuel. The Contractor shall supply all equipment and material need to perform task.

1.4 Cargo Inspection of petroleum products. The Contractor shall oversee operations to include: Gauging, Sampling, Atmospheric Measuring, Tank cleanliness, Lightering transfers and complete certified detailed reports within 24 hours. The Contractor shall supply all equipment and material need to perform task.

2. The Contractor will have the authority to stop any operations that are thought to be unsafe but must immediately contact the POC named on the Task Order to explain why.

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Attachment 1: Products to be Tested The following are products, which are utilized by DLA Energy and its customers that may require testing at the Contractor’s facility(ies) per the requirements set forth in this SOW. The Contractor must be familiar with all of the product specifications listed below and develop operating procedures and/or checklists to allow their technicians to perform the proper tests and complete the tasks as requested per the task order and in a timely manner. All referenced material can be obtained at http://quicksearch.dla.mil/ or https://assist.dla.mil/ or by contacting the CO or the COR.

1) Aviation Turbine Fuel, Grade JET A (Specification: ASTM D1655 latest version) and JET A-1, NATO F-35 (DEF

Stan 91-091 latest version)

2) Turbine Fuel, Aviation, Kerosene Types, NATO F-34 (JP8) (Specification: MIL-DTL-83133 latest version)

3) Turbine Fuel, Aviation, Grade JP5 NATO F-44 (Specification: MIL-DTL-5624 latest version)

4) Fuel, Navy Distillate NATO F-76 (Specification: MIL-DTL-16884 latest version)

5) Inhibitor, Fuel System Icing, High Flash (FSII) (Specification: MIL-DTL-85470 latest version)

6) Marine Residual Fuel Oil Grade (RME-180/380) (Specification: ISO 8217 latest version)

7) Lubrication Oil, Steam Turbine and Gear (LTL) MIL Symbol 2190 (Specification: MIL-PRF-17331 latest version)

8) Lubrication Oil, (LO6), MIL Symbol 9250, Shipboard Internal Combustion, High Output Diesel

(Specification: MIL-PRF-9000 latest version)

9) Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590, latest version

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Attachment 2: Series Testing Requirements

1. Secured Fuel Series Testing Requirements for Aviation Fuel

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2. Jet A & Jet A-1 (NATO F35) Series Testing Requirements for Specifications ASTM D1655 and Def Stan 91-

A Series Characteristics ASTM

D1655 Def Stan 91-091

B-1 Series

B-2 Series

B-3 Series

C-Series

Appearance/Workmanship X X X X X X Color (Visual) X X X X X X Particulate Contamination/Particulate Matter

X X X X X

Particle Count (Particulate) X Total Acidity X X X Aromatics X X Total Sulfur X X Mercaptan Sulfur X X Doctor Test X X Distillation X X X X X Flash Point X X X X X X API Gravity or Density at 15°C

X X X X X X

Freezing Point X X X X X Viscosity at minus 20°C X X Smoke Point X X Naphthalenes X X Specific Energy (Net Heat of Cumbusiton)

X X

Copper Strip X X X X X Thermal Stability X X X X Existent Gum X X X X X Microseparometer X X Electrical Conductivity X X X X X Lubricity X Color, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X X

Fuel System Icing Inhibitor X X X X X

FAME X X X X X

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3. JP8 (NATO F34) Series Testing Requirements for Specifications MIL DTL 83133

Characteristics MIL DTL 83133

B-1 Series

B-2 Series

B-3

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API Gravity or Density at 15°C

X X X X X

Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Naphthalenes X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X X X X Electrical Conductivity X X X X Lubricity Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

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4. JP5 (NATO F44) Series Testing Requirements for Specifications MIL DTL 5624

Characteristics MIL DTL 5624 B-1

Series B-2

Series B-3

C- Series

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/ Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API or Density at 15 deg. C X X X X X Vapor Pressure X Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X Electrical Conductivity X Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

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5. F-76 Series Testing Requirements for Specifications MIL-DTL-16884

Characteristics MIL F 16884 B-1

Series B-2

Series B-3

Series C-

Series

Appearance/Workmanship X X X X X Demulsification X API Gravity or Density at 15°C X X X X X Distillation X X X Cloud Point X X Color X X X X X Flashpoint X X X X X Particulate Contamination X X X Pour Point X X Viscosity at 40°C X X Acid Number X Ash X Aromatics X Carbon Residue X X X Copper Strip Corrosion X X Hydrogen Content X Ignition Quality (Cetane Number, Cetane Index, or Derived Cetane Number)

X X

Storage Stability X X Sulfur Content X X X Trace Metals (Ca, Pb, Na, K and V) X Lubricity X Water and Sediment X X

FAME X X X X

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6. Fuel System Icing Inhibitor (FSII) (NATO S-1745) Series Testing Requirements for Specifications MIL-

DTL-85470

7. Marine Residual Fuel Oil (RME 180/380) Series Testing Requirements for Specification ISO 8217

Characteristics MIL DTL 85470 B-1

Series B-2

B-3 Series C-Series

Acid Number X X Color, Platinum Cobalt X Distillation X X Ethylene Glycol X X pH of 25 % solution in water X X Relative density X X X Water (mass %) X X Flash point X X Appearance/Workmanship X X X

A Series Characteristics ISO 8217 B-1

Series B-2

Series B-3

Kinematic Viscosity at 50°C X X X X X

Density at 15°C X X X X X Calculated Carbon Aromaticity

Index X X

Sulfur X X Flash point X X X X X

Hydrogen sulfide X X Acid Number X X

Total Sediment aged X X X Carbon Residue X X X

Pour Point X X Water X X X Ash X X

Vanadium X Sodium X X

Aluminum plus silicon X Used lubricating oils X

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8. Lubrication Oil (LTL) (NATO O-250) Series Testing Requirements for Specification MIL PRF 17331

Characteristics MIL PRF

17331 B-1

Series B-2

Series B-3

Sulfur X n/a Acid Number X n/a Corrosion X X n/a Corrosion, Copper Strip X n/a Water content, mass% X X X n/a X Gravity X X n/a X Flash point X X X n/a Pour Point X X n/a Viscosity (per MIL PRF 17331) X X n/a Viscosity @100°C X X n/a Viscosity @ 40°C X X n/a X Emulsion test X X X n/a Total sludge, iron and copper X n/a Foam Test X X X n/a X Cleanliness (Solid Particle Contamination)

X n/a

Neutralization number (acid/base) X X n/a Appearance (to include visual sediment & water)

X X n/a X

Solid contaminants X X X n/a

9. Lubrication Oil (LO6) (NATO O-278) Series Testing Requirements for Specification MIL PRF 9000

Characteristics MIL PRF 9000 B-1

Series B-2

Series B-3

Series C-Series n/a X Appearance/Workmanship X X X Flash point X X X n/a Foam (stability only) X X X n/a Gravity X X n/a X Metals/Elements:Calcium, Magnesium, Zinc, Phosphorus

X n/a

Pour Point X X n/a Sulfur X n/a Total base number X n/a Viscosity index X n/a Viscosity at 100°C X n/a Viscosity at 40°C X X n/a Neutralization number (acid/base) X X n/a Solid contaminants X X n/a Emulsion test X X n/a Water (by centrifuge) X X n/a X

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10. Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590

Characteristics ASTM

D975

EN 590 B-1

Series B-2

Series B-3

Flash point X X X X X X Water and Sediment X X Distillation X X X X Kinematic Viscosity X X X Ash X X Sulfur X X X Copper strip corrosion X X X Cetane number X X Cetane index X X X Aromaticity X Cloud Point X X X X

LTFT/CFPP X X

Ramsbottom Carbon Residue

X X

Lubricity X Conductivity X API Gravity or Density at 15°C

X X X X X X

Polycyclic aromatic hydrocarbons

X X

Manganese content X X Water Content X X X Total Contamination X X

FAME X X X

Oxidation stability X X Appearance/Workmanship X X X X X X Pour Point X X X

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Attachment 3: Approved Testing Methods

Table 1: Aviation Turbine Fuels

Def Stan 91-

Jet A/A-1

(ASTM

D1655)

JP-8 (MIL-DTL-

83133)

JP-5 (MIL-

DTL-

5624)

Appearance Visual Visual Visual

ASTM D6986

Visual

Color (Visual) Visual Visual Visual Visual Density or API

Gravity

IP365,

D4052

D1298, IP 160,

D4052, IP

D1298, IP160, D4052

(referee), IP 365, D7777

D1298, D4052, D7777

Particulate Matter

IP 423,

D5452, IP 216, D2276,

IP 423, D5452

(referee)

D2276, D5452 (referee), IP 423

D2276, D5452 (referee)

Particle Count

IP 564, IP 565,

IP 577

IP 564, IP 565, IP

577, D7619

D8166, IP 564, IP 565,

IP 577

D7619 (referee)

D8166, IP 564, IP

565, IP 577

D7619 (referee)

Total Acidity IP 354, D3242 IP 354, D3242 IP 354, D3242 D3242

Aromatics IP 156, D1319, IP 436, D6379

IP 156, D1319, IP

436, D6379

IP 156, D1319 (referee), IP 436, D6379

D1319 (referee), D6379

Total Sulfur IP 336 D1266 D2622, D4294, D5453, IP

D129, D1266, D2622, D3120, D4294 (referee) , D5453, or IP

D129, D1266, D2622, D3120, D4264 (referee), D5453

Mercaptan Sulfur

IP 342, D3227 IP 342, D3227 IP 342, D3227 (referee) D3227

Doctor Test IP 30 D4952 D4952 D4952

Distillation IP 123, D86 D86, D2887, IP 406, D7344, D7345, IP

D86 (referee), D2887, IP 406, IP 123, D7345

D86 (referee) , D7345, D2887

Viscosity IP 71, D445 IP 71 Section 1, D445, D7042, D7945

IP 71 Section 1, D445 (referee), D7042, D7945

D445

Smoke Point IP 598, D1322 IP 598, D1322 IP 598, D1322 IP 598, D1322

Naphthalenes D1840 D1840 D1840 D1840

Specific Energy

D3338, D4809 (referee), IP 12, IP 355

D3338, D4529, D4809 (referee), IP

D3338, D4529, D4809 (referee), IP 12

D3338, D3338M, D4529, D4809 (referee)

Hydrogen Content

N/A

D3343, D3701, D3343, D3701, D5291, D7171 (referee)

D3701, D5291, D7171 (referee)

Calculated Cetane Index

D976, D4737 D976, D4737 D976, D4737

Copper Strip Corrosion

IP 154, D130 D130 D130, IP 154 D130

Freezing Point IP 16, D2386 D5972, IP 435, D7153, IP 529, D7154, IP

528, D2386, IP 16

D2386 (referee), IP 16, D5972, IP

435, D7153, IP

529, D7154, IP

D2386 (referee), D5972, D7153, D7154

Existent Gum IP 540 D381, IP 540 D381(referee), IP540 D381(referee), IP

Flash Point IP 170 D56, D93, D3828, IP 170, IP 523

D56, D93(referee), D3828, IP 170

D56, D93 (referee), Page | 16

D3828

Lead Content N/A N/A N/A N/A FSII IP 424, D5006 D5006 D5006 (referee), IP 424 D5006

Filtration Time N/A N/A D2276, D5452 (referee)

D2276, D5452( referee)

MSEP D3948 D3948 D3948,

D7224 (referee)

D3948, D7224 (referee)

Electrical Conductivity

IP 274,

D2624

D2624 D2624, IP 274 D2624

Thermal Stability

IP 323. D3241 D3241 (Annex A3 is referee) See C- 5.4.1

D3241 (Annex A3 is considered referee) See C-5.4.1;

IP 323

D3241 (Annex A3 is referee) See C-5.4.1

Color (Saybolt) D156, D6045 D156 D156 (referee) , D6045

D156 (referee), D6045

Peroxide Number

D3703 N/A N/A

FAME IP 585, IP 590 D7797, IP 583,

IP 585 (referee), IP

590, IP 599

D7797, IP 583,

IP 585 (referee), IP 590, IP 599

D7797, IP 583, IP

(referee), IP 590, IP 599

Lubricity D5001 D5001 N/A N/A

Table 2: Marine Diesel

F-76 (MIL-DTL-16884)

Appearance D4176

Color (Visual) D1500 (referee), D6045 Density or API Gravity D1298 (referee), D4052, D287, D7777

Distillation D86 (referee), D2887 Flash Point D93(referee), D6450, D3828

Carbon Residue D524(referee), D189, D4530 Cloud Point D2500(referee), D5771, D5772, D5773 Pour point D97(referee), D5949, D5950, D5985

Copper Strip Corrosion D130 Viscosity D445, D7042

Water and Sediment D2709 Particulate D6217

Storage Stability D5304 (referee), D2274 Sulfur D5354(referee), D1266, D2622, D3120, D7039

Fatty Acid Methyl Ester (FAME) BS EN 14078, IP579, D7963 Lubricity D6079 (referee), D7688

Demulsification D1401 Particulate Contamination D6217 (referee), D5452

Acid Number D974 (referee), D664 Ash D482

Aromatics D6591 (referee), D2425 Hydrogen Content D7171 (referee), D4808, D5291

Ignition Quality (Cetane Number, Cetane Index or Derived Cetane

Number)

D613 (referee), D976, D6890, D7170

Trace Metals (Ca, Pb, Na, K and V) D7111 (referee), D3605

Page | 17

Table 3: Fuel System Icing Inhibitor

MIL-DTL-85470

Appearance Visual

Acid Number D1613 Color, Platinum Cobalt D1209 (referee), E450

Distillation D1078 Ethylene Glycol Per specification pH of 25% solution in water E70 Relative Density D891 (referee), D4052 Water (mass%) D1364 (referee), E1064, E203

Flash Point D93 (referee), D56, D3828

Table 4: Marine Residual Fuel Oil (RME180/380)

ISO 8217

Kinematic Viscosity ISO 3104 Density ISO 3675, ISO 12185

Calculated Carbon Aromaticity Index (CCAI)

Specification

Sulfur ISO 8754, ISO 14596, D4264 Flash Point ISO 2719

Hydrogen Sulfide IP570 Acid Number D664

Total Sediment, aged ISO 10307-2 Carbon Residue ISO 10370

Pour Point ISO 3016 Water ISO 3733

Ash ISO 6245 Vanadium IP 501 (referee), IP 470, ISO 14597

Sodium IP 501 (referee), IP 470 Aluminum plus silicon IP 501 (referee), IP 470, ISO 10478

Used lubricating Oil (ULO) IP 501 (referee), IP 470, IP 500 Cetane Index ISO 4264

Table 5: Lubrication Oil (LTL) (NATO O-250)

MIL-PRF-17331

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481, D7751

Acid Number D974 (referee), ASTM D664 Corrosion D665, Procedure B

Corrosion, Copper Strip D130 Water Content D6304 (referee), ASTM D7546 API Gravity D287, D1298 (referee), D4052 Flash Point D92, D93 (referee) Pour Point D97 (referee), D5950, D5949

Viscosity @ 4.4°C D445 (referee), D7042 Viscosity @100°C D445 (referee), D7042 Viscosity @40°C D445 (referee), D7042

Emulsion Test D1401 Total Sludge, iron and copper D4310

Foam test D892 Cleanliness (Solid Particle Contamination) D4898

Neutralization number (acid/base) D974 Appearance (to include visual sediment & water) Visual

Page | 18

Table 6: Lubrication Oil (LO6) (NATO O-278)

MIL-PRF-9000

Appearance/Workmanship Visual

Flash point D92 Foam (stability only) D892

Gravity D287, D1298, D4052 Calcium D4628, D4927, D4951, D6443, D6481

Magnesium D4628, D4927, D4951, D6443 Zinc D4638, D4927, D4951, D6443, D6481

Phosphorus D1091, D4047, D4927, D4951, D6443, D6481 Pour Point D97, D5949, D5950

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481

Total base number D2896 Viscosity index D2270

Viscosity at 100°C D445 Viscosity at 40°C D445

Neutralization number (acid/base) D2896 Ash, sulfated D874

Corrosion, copper strip D130 Table 7: Diesel Fuel Oil

ASTM D975 EN 590

Flash point D93 EN ISO2719

Water and Sediment D2709, D1796 N/A Distillation D86 EN ISO3405, EN ISO3924

Kinematic Viscosity D445 EN ISO3104 Ash D482 EN ISO6245

Sulfur D2622, D5453 EN ISO20846, EN ISO20884, EN

ISO13032

Copper strip corrosion D130 EN ISO2160 Cetane number D613 EN ISO5165, EN15195, EN16144

Cetane index D976 EN ISO4264 Aromaticity D1319 N/A Cloud Point D2500 EN23015

LTFT/CFPP D4539, D6371 EN116, EN16329

Carbon Residue D524 EN ISO10370 Lubricity D6079, D7688 EN ISO12156-1

Conductivity D2624 D4308 API Gravity or Density at 15°C

N/A EN ISO3675, EN ISO12185

Polycyclic aromatic hydrocarbons

N/A EN12916

Manganese content N/A prEN16576 Water Content N/A EN ISO12937

Total Contamination N/A EN12662

FAME N/A EN14078

Oxidation stability N/A EN ISO 12205, EN15751 Appearance/Workmansh ip Visual Visual

Page | 19

Table 8: Reclaimed Fuel Oil (FOR)

MIL-PRF-24951

Flashpoint D93

Explosiveness FED-STD-791 Test Method 1151.1 Water and Sediment D1796

Sediment D473 API Gravity or Density at 60°C D287

Viscosity at 40°C D445 Viscosity at 50°C D88

Pour Point D97 Neutrality FED-STD-791 Test Method 5101

Sulfur Content D129 Ash D482

Trace Metals: Arsenic, Cadmium, Chromium and Lead

EPA SW-846, Method 3040/3050 and proposed method for evaluating solid waste

Total Halogen D808-87

Page | 20

Attachment 4: Annual Estimates by Location:

Table listed below illustrates the annual estimated work by fuel grade to be performed. Attachment 2 defines the tests that makeup a series (slate) in accordance with specifications and/or MIL-STD-3004-1. Individual test shall be requested from any test in the A, B or C series but most common will be retests following a testing failure. Due to unpredictable situations unable to state the exact tests that will be requested but a historical series average.

Guam Jet A/A-1 JP-5 JP-8 F-76 FSII

A-Series 5 A-Series 5 A-Series 5 A-Series 5 A-Series 2

B-1 Series 30 B-1 Series 25 B-1

Series 5 B-1 Series 25 B-1 Series 0

B-2 Series 10 B-2 Series 10 B-2

Series 35 B-2 Series 5 B-2 Series 6

B-3 Series 0 B-3 Series 0 B-3

Series 0 B-3 Series 0 B-3 Series 0

C Series 30 C Series 5 C Series 25 C Series 39 C Series 0

Individual 10 Individual 10 Individual 25 Individual 15 Individual 1

RME LTL LO6 Diesel

A-Series 5 A-Series 3 A-Series 5 A-Series 1

B-1 Series 0 B-1 Series 0 B-1 Series 0 B-1 Series 1

B-2 Series 5 B-2 Series 3 B-2 Series 6 B-2 Series 5

B-3 Series 0 B-3 Series 0 B-3 Series 0 B-3 Series 0

C Series 5 C Series 1 C Series 0 C Series 6

Individual 1 Individual 1 Individual 12 Individual 5

Subic Bay Jet A/A-1 JP-5 JP-8 F-76

A-Series 5 A-Series 5 A-Series 0 A-Series 0

B-1 Series 0 B-1 Series 0 B-1 Series 0 B-1 Series 0

B-2 Series 10 B-2 Series 10 B-2 Series 10 B-2 Series 10

B-3 Series 0 B-3 Series 0 B-3 Series 0 B-3 Series 0

C Series 0 C Series 0 C Series 0 C Series 0

Individual 10 Individual 9 Individual 15 Individual 10

Page | 21

Attachment 5: Sample Shipment

1. Sample Shipment The Contractor shall upon request be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of request and arrive to the below laboratory within five calendar days.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-5083

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-7632

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra RD

San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

DLA Enery Okinawa Laboratory Okinawa Chibana Compound, RTE #74 Bldg. 53145

Chibana Okinawa City, Okinawa, Japan 904-2143

Intentionally Left Blank Intentionally Left Blank