Attachment_6_-_Analyte_List.pdf

ATTACHMENT 6

ANALYTE LIST

EPA 8260 Compounds to be Tested

DLR DLR

(µg/L) (µg/L)

Acetone -- cis-1,3-Dichloropropene -- Benzene 0.5 trans-1,3-Dichloropropene -- Bromochloromethane 0.5 Di-isopropylether (DIPE) 3.0 Bromodichloromethane 1.0 Ethanol -- Bromoform 1.0 Ethyl Tert Butyl Ether 3.0 Bromomethane 0.5 Ethylbenzene 0.5 2-Butanone (MEK) 5.0 2-Hexanone (Methyl Butyl Ketone) -- Carbon Disulfide 0.5 Hexachlorobutadiene 0.5 Carbon Tetrachloride 0.5 Iodomethane (Methyl Iodide) -- Chlorobenzene 0.5 Methyl Tert Butyl Ether (MTBE) 3.0 Chlorodifluoromethane* -- 4-Methyl-2-Pentanone (MIBK) -- Chloroethane 0.5 Methylene Chloride (Dichloromethane) 0.5 Chloroform 1.0 Naphthalene 0.5 Chloromethane 0.5 Styrene 0.5 Dibromochloromethane 1.0 Tert-Amyl Methyl Ether 3.0 1,2-Dibromo-3-chloropropane (DBCP) -- Tertiary butyl alcohol 2.0 1,2-Dibromoethane (EDB) -- 1,1,1,2-Tetrachloroethane 0.5 Dibromomethane 0.5 1,1,2,2-Tetrachloroethane 0.5 1,2-Dichlorobenzene 0.5 Tetrachloroethene (PCE) 0.5 1,3-Dichlorobenzene 0.5 Toluene 0.5 1,4-Dichlorobenzene 0.5 1,2,4-Trichlorobenzene 0.5 trans-1,4-Dichloro-2-butene -- 1,1,1-Trichloroethane 0.5 Dichlorofluoromethane* -- 1,1,2-Trichloroethane 0.5 Dichlorodifluoromethane 0.5 Trichloroethene (TCE) 0.5 1,1-Dichloroethane 0.5 Trichlorofluoromethane 10 1,2-Dichloroethane 0.5 1,2,3-Trichloropropane -- 1,1-Dichloroethene 0.5 Vinyl Acetate --cis-1,2-Dichloroethene 0.5 Vinyl chloride 0.5 trans-1,2-Dichloroethene -- Xylenes (Total) 0.5 1,2-Dichloropropane 0.5

Unknown chromatographic peaks shall be reported, flagged and tracked for potential comparison to subsequent unknown peaks that may be observed in future sampling events.

Identification of unknown chromatographic peaks that recur in subsequent sampling events may be required.

DLR = California Code of Regulations, Title 22, Section 64400, Article 34, Detection Limits for Purposes of Reporting (DLRs) -- = DLRs are not available or does not apply

* = Constituents not part of standard EPA 8260B analysis list; however need to be included, if possible

ATTACHMENT 5 (continued)

EPA 8260 (extended list) Compounds to be Tested:

DLR DLR

(µg/L) (µg/L)

Acetone -- 2,2-Dichloropropane 0.5 Acetonitrile -- 1,1-Dichloropropene 0.5 Acrolein -- cis-1,3-Dichloropropene -- Acrylonitrile -- trans-1,3-Dichloropropene -- Allyl Chloride (3-Chloroprene) -- Di-Isopropyl ether (DIPE) 3.0 Benzene 0.5 Ethanol -- Bromochloromethane 0.5 Ethyl tert-Butyl ether (ETBE) 3.0 Bromodichloromethane 1.0 Ethylbenzene 0.5 Bromoform 1.0 Ethyl methacrylate -- Bromomethane (Methyl Bromide) 0.5 Hexachlorobutadiene 0.5 2-Butanone (MEK) 5.0 2-Hexanone (Methyl Butyl Ketone) -- Carbon Disulfide 0.5 Iodomethane (Methyl Iodide) -- Carbon Tetrachloride 0.5 Isobutyl Alcohol (isobutanol) -- Chlorobenzene 0.5 Methacrylonitrile -- Chlorodifluromethane* -- Methyl Methacrylate -- Chloroethane (Ethyl Chloride) 0.5 Methyl Tert Butyl Ether (MTBE) 3.0 Chloroform 1 4-Methyl-2-Pentanone (MIBK) 5.0 Chloromethane (Methyl Chloride) 0.5 Methylene Chloride (Dichloromethane) 0.5 Chloroprene -- Naphthalene 0.5 Dibromochloromethane 1.0 Propionitrile (Ethyl Cyanide) -- 1,2-Dibromo-3-chloropropane (DBCP) -- Styrene 0.5 1,2-Dibromoethane (EDB) -- tert-butyl alcohol 2.0 Dibromomethane (Methylene Bromide) 0.5 tert-Amyl methyl ether (TAME) 3.0 1,2-Dichlorobenzene 0.5 1,1,1,2-Tetrachloroethane 0.5 1,3-Dichlorobenzene 0.5 1,1,2,2-Tetrachloroethane 0.5 1,4-Dichlorobenzene 0.5 Tetrachloroethene (PCE) 0.5 trans-1,4-Dichloro-2-butene -- Toluene 0.5 Dichlorofluromethane* -- 1,2,4-Trichlorobenzene 0.5 Dichlorodifluoromethane 0.5 1,1,1-Trichloroethane 0.5 1,1- Dichloroethane 0.5 1,1,2-Trichloroethane 0.5 1,2-Dichloroethane 0.5 Trichloroethene (TCE) 0.5 1,1-Dichloroethene 0.5 Trichlorofluoromethane (CFC-11) 5.0 cis-1,2-Dichloroethene 0.5 1,2,3-Trichloropropane --trans-1,2-Dichloroethene -- Vinyl Acetate -- 1,2-Dichloropropane 0.5 Vinyl chloride 0.5 1,3-Dichloropropane 0.5 Xylenes (Total) 0.5

Unknown chromatographic peaks shall be reported, flagged and tracked for potential comparison to subsequent unknown peaks that may be observed in future sampling events. Identification of unknown chromatographic peaks that recur in subsequent sampling events may be required.

DLR = California Code of Regulations, Title 22, Section 64400, Article 34, Detection Limits for Purposes of Reporting (DLRs) -- = DLRs are not available or does not apply

* = Constituents not part of standard EPA 8260B analysis list; however need to be included, if possible

EPA 8270 Compounds to be Tested:

DLR DLR DLR

(µg/L) (µg/L) (µg/L)

Acenaphthene 5.0 p-(Dimethylamino)azobenzene -- 1-Naphthylamine -- Acenaphthylene 5.0 7,12-Dimethylbenz(a)anthracene 5.0 2-Naphthylamine -- Acetophenone -- 3,3'-Dimethylbenzidine -- 2-Nitroaniline -- 2-Acetylaminofluorene (2-AAF) -- 2,4-Dimethylphenol (m-Xylenol) 5.0 3-Nitroaniline -- 4-Aminobiphenyl -- Dimethyl phthalate 5.0 4-Nitroaniline -- Anthracene 5.0 1,3-Dinitrobenzene -- Nitrobenzene -- Benzo(a)anthracene 10 4,6-Dinitro-o-cresol (2-Methyl-4,6-dinitrophenol) -- 2-Nitrophenol 5.0 Benzo(b)fluoranthene 10 2,4-Dinitrophenol 5.0 4-Nitrophenol 5.0 Benzo(k)fluoranthene 10 2,4-Dinitrotoluene 5.0 N-Nitrosodi-n-butylamine -- Benzo(ghi)perylene 10 2,6-Dinitrotoluene 5.0 N-Nitrosodimethylamine -- Benzo(a)pyrene -- Di-n-octylphthalate 5.0 N-Nitrosodiethylamine -- Benzyl Alcohol -- Diphenylamine -- N-Nitrosodiphenylamine -- Benzyl butyl phthalate 10 Ethyl methanesulfonate -- N-Nitrosodi-n-propylamine --bis(2-chloroethoxy)methane 5.0 Famphur -- N-Nitrosomethylethylamine --bis(2-chloroethyl)ether -- Fluoranthene 5.0 N-Nitrosopiperidine --bis(2-chloroisopropyl)ether 5.0 Fluorene 5.0 N-Nitrosopyrrolidine --bis(2-ethylhexyl)phthalate -- Hexachlorobenzene 0.5 5-Nitro-o-toluidine -- 4-Bromophenyl phenyl ether 5.0 Hexachlorocyclopentadiene 1.0 Pentachlorobenzene -- 4-Chloroaniline -- Hexachloroethane 5.0 Pentachlonitrobenzene -- Chlorobenzilate -- Hexachloropropene -- Pentachlorophenol 0.2 4-choro-3-methylphenol 5.0 Indeno(1,2,3-c,d)pyrene 10 Phenacetin -- 2-Chloronapthalene 5.0 Isodrin -- Phenanthrene 5.0 2-Chorophenol 5.0 Isophorone 10 Phenol 5.0 4-Chlorophenyl phenyl ether 5.0 Isosafrole -- p-Phenylenediamine -- Chrysene 5.0 Kepone -- 1,4-Phenylenediamine -- Diallate -- Methapyrilene -- Pronamide -- Dibenzo(a,h)anthracene 5.0 3-Methylcholanthrene -- Pyrene 5.0 Dibenzofuran -- Methyl methane sulfonate -- Safrole -- Di-n-butylphthalate 5.0 2-Methylnaphthalene -- 1,2,4,5-Tetrachlorobenzene -- 3,3'-Dichlorobenzidine 20 2-Methylphenol (o-Cresol) -- 2,3,4,6-Tetrachlorophenol -- 2,4-Dichlorophenol 5.0 3-Methylphenol (m-Cresol) -- o-Toluidine -- 2,6-Dichlorophenol -- 4-Methylphenol (p-Cresol) -- 2,4,5-Trichlorophenol 5.0 Diethyl phthalate 5.0 1,4-Naphthoquinone -- 0,0,0-Triethyl phosphorothioate --

1,3,5-Trinitrobenzene (sym) --

-- = DLRs are not available or does not apply DLR = California Code of Regulations, Title 22, Section 64400, Article 34, Detection Limits for Purposes of Reporting (DLRs)

EPA 8151A Compounds to be Tested (minimum):

DLR DLR

(µg/L) (µg/L) 2,4-D 10 2,4,5-TP (Silvex) 1.0 2,4,5 T -- Dinoseb 2.0

EPA 8141B Compounds to be Tested (minimum):

DLR DLR

(µg/L) (µg/L) Atrazine 0.5 Methyl Parathion -- Chlorpyrifos 1.0 Parathion (Ethyl Parathion) -- Di - Syston (Disulfoton) 100 Phorate (Thimet) 0.2 Diazinon -- Simazine 1.0 Dimethoate -- Thionazin --

EPA 8080 Compounds to be Tested (minimum):

DLR DLR

(µg/L) (µg/L) Aldrin 0.075 Dieldrin 0.02 Aroclor-1016 -- 4-4'-DDD 0.02 Aroclor-1221 -- 4-4'-DDE 0.01 Aroclor-1232 -- 4-4'-DDT 0.02 Aroclor-1242 -- Endrin 0.1 Aroclor-1248 -- Endrin aldehyde 0.05 Aroclor-1254 -- Endrin Ketone -- Aroclor-1260 -- Endosulfan I 0.01 alpha-BHC 0.01 Endosulfan II 0.01 2 beta-BHC 0.05 Endosulfan sulfate 0.05 2 delta-BHC 0.05 Heptachlor 0.01 2 gamma-BHC 0.2 Heptachlor epoxide 0.01 alpha-Chlordane -- Methoxychlor 10 gamma-Chlordane -- Toxaphene 1.0

DLR = California Code of Regulations, Title 22, Section 64400, Article 34, Detection Limits for Purposes of Reporting (DLRs) -- = DLRs are not available or does not apply

Inorganic Compounds to be Tested (minimum):

DLR DLR

(µg/L) (µg/L)

Aluminum 50 Magnesium Antimony 6.0 Manganese 20 Arsenic 2.0 Mercury 1.0 Barium 100 Nickel 10 Beryllium 1.0 Potassium Cadmium 1.0 Selenium 5.0 Calcium Silver 10 Chromium 10.0 Sodium Chromium VI 1.0 Thallium 1.0 Cobalt Tin Copper 50 Vanadium 3.0 Iron 100 Zinc 50 Lead 5.0 Cyanide --

DLR DLR

(mg/L) (mg/L)

Bicarbonate -- Total Dissolved Solids -- Carbonate -- Total Organic Carbon 0.3 Chloride -- Total Suspended Solids -- Nitrate (as N) 0.4 Total Kjeldahl -- Sulfate 0.5 Biochemical Demand -- Oil and Grease -- Chemical Oxygen Demand --

-- = DLRs are not available or does not apply

DLR = California Code of Regulations, Title 22, Section 64400, Article 34, Detection Limits for Purposes of Reporting (DLRs)