Atchmt 1 - Middle East Gulf Region SOW (28 Sep 21).pdf

Statement of Work for

Contracted Laboratory Services Middle East Region 28 September , 2021

Contents

C-1.0 General Description:

C-1.0.1 Service Locations:

C-1.1 Facilities:

C-1.1.1 Facility Country Restriction:

C-1.2 Specifications, Standards and Handbooks:

C-1.3 Scheduling of Services:

C-2.0 Contractor Deliverables:

C-2.1 Contract Compliance Plan:

C-2.2 Laboratory Test Reports:

C-2.3 Contract Contingency Plan:

C-2.4 Contract Training Plan:

C-2.5 Safety Plan:

C-2.6 Transportation Plan:

C-2.7 Laboratory Equipment Plan:

C-2.8 Monthly Reporting:

C-3.0 Laboratory Requirements:

C-3.1 Operating Hours:

C-3.2 Staffing:

C-3.3 Knowledge and Skills:

C-3.4 Access:

C-3.5 Epoxy Lined Sample Cans:

C-3.6 Thermal Oxidation Stability Failures:

C-3.7 Ellipsometric Tube Deposit Rater (ETR):

C-3.8 Turn-around Times:

C-3.8.1 Sample Testing Turnaround Times:

C-3.9 Retain samples:

C-4.0 Transportation Performance Requirements:

C-5.0 Secured Fuels Performance Requirements:

C-6.0 Surveyor Duties:

C-6.1 Third party witness:

C-6. 2 Sampling of petroleum products:

C-6. 3 Gauging of Petroleum Products:

C-7.0 Joint Contingency Contracting System (JCCS) Requirement:

C-8.0 Sample Shipment:

Attachment 1: Products

Attachment 2: Series Testing Requirements

Attachment 3: Testing Requirements

Page | 1

C-1.0 General Description: This Statement of Work (SOW) provides the requirements for laboratory testing services in multiple locations throughout the Middle East region. The contractor will be responsible for the laboratory testing of government owned petroleum products in accordance with the specifcations as described herein, and transportation of samples from contracted locations to the contractor’s laboratory. Government owned products mentioned in this SOW may also be shipped to the contractor’s laboratory for testing. The countries in the Middle East Region are divided into the following sub-regions:

1. Gulf region: Kuwait, United Arab Emirates (UAE), Jordan, Bahrain and Oman.

2. Qatar region: Qatar.

3. Iraq region: Iraq.

C-1.0.1 Service Locations: When ordered, the contractor shall be able to provide services required in this SOW to DLA Energy in each of the locations listed below. Contractor facilities must be located within the Middle East region and meet the required turn-around times listed in C-3.8.

Gulf Region Qatar Region Kuwait Qatar

Ali Al Salem Air Base Port of Mesaieed

Camp Buehring Al Udeid Air Base

Al Jaber Air Base Camp As Sayliyah

Camp Arifjan Iraq Region

KNB Naval Base Iraq United Arab Emirates (UAE) Erbil/International Airport

Abu Dhabi Bashur

Dubai Baghdad

Jebel Ali Al Asad AB

Fujairah Taqaddum

Al Dhafra Air Base Taji

Bahrain Mahkmour

Sitra Mosul Dam

Isa AB Zaweta

NSA Bahrain Kara Soar Complex

Oman Qwest

Salalah Tikrit

Thumrait AB

Left Blank

Masirah AB

Al Musanah AB

Duqm

Jordan

Mwaffaq As-Salti Air Base/Azraq Air Base

Northern Integration Site

Al Quwayrah

Prince Hassan Air Base (H5)

Joint Training Center (JTC)

King Abdullah Special Operations

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C-1.1 Facilities: The contractor shall have facilities that meet the required turn-around times in section C-3.8 and

3.8.1. The contractor shall provide the location(s) of the facility where the product shall be tested, facility testing capabilities and contact information.

C-1.1.1 Facility Country Restriction: Contractors shall not use laboratories located within Saudi Arabia for laboratory testing of fuel product from Kuwait, United Arab Emirates (UAE), Qatar, Jordan, Bahrain, Iraq or Oman. DLA Energy Quality Assurance Representatives (QAR) have a difficult time with gaining access to many locations within Saudi Arabia to be able to witness testing or conducting periodic site visits.

C-1.2 Specifications, Standards and Handbooks: At each laboratory, the contractor shall retain a copy of all required specifications, standards, test methods, handbooks, etc., per this SOW and perform services in accordance with testing requirements. Military Specifications referenced in Attachment 1 for petroleum product types can be obtained at http://quicksearch.dla.mil or https://assist.dla.mil but can also be requested in writing to the Contracting Officer (CO) or Contracting Officer’s Representative (COR).

C-1.3 Scheduling of Services: After the CO authorizes a task order, the COR or QAR will contact the laboratory to schedule the testing. The contractor shall not perform services under this SOW without a task order or direct authorization from the CO. If a task order was not received, the contractor shall contact the CO or COR prior to any testing. Only the CO can formally, either in writing or verbally, authorize testing and create an obligation.

C-2.0 Contractor Deliverables: All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for government review upon request at any time during the contract performance period.

C-2.1 Contract Compliance Plan: The contractor is responsible for compliance with all contract performance requirements. The contractor is responsible for all actions taken by any sub-contractor utilized under this contract. The contractor shall be ISO 9001 and /or ISO/IEC 17025 certified.

C-2.2 Laboratory Test Reports: The contractor shall maintain records evidencing all analysis performed under this contract. All samples tested shall be documented with a detailed report. Reports shall be complete and legible containing information pertaining but not limited to: Lab Name, Date of test, Test Method, Test Name, Test Results, Test Units and signature certifying results.

Thermal Stability test reports shall include the following additional data:

1. Type of tester used.

2. Tube manufacturer and serial number.

3. Rating method: Visual Tube Rater (VTR), Interferometric Tube Rater (ITR), or Ellipsometric Tube Rater (ETR).

Any reports not containing the appropriate information shall be corrected and resubmitted by the contractor.

C-2.2.1 Laboratory Test Report Additional Email Addresses: The contractor shall be responsible for emailing all test results to the organizational email address of: dlaenergylaboratoryreports@dla.mil, COR, and QAR (CO when requested).

C-2.3 Contract Contingency Plan: The contract contingency plan shall outline contractor actions to ensure there is no significant interruption of services resulting from labor disputes, catastrophic failure of equipment, or the effects of natural disasters/emergencies. The plan shall provide specific details regarding labor issues that may result from potential strike actions, world events, world actions, military contingency and war time manning requirements.

C-2.4 Contract Training Plan: The contractor shall provide a detailed plan that identifies employee training

Page | 3 requirements and procedures necessary to maintain proficiency. The plan shall identify length of training, training sources and a brief description of courses such as safety, environmental protection and job qualification training. The contractor is responsible for ensuring all individual training requirements are accomplished. The contractor must demonstrate current participation in a proficiency program or suitable means to verify laboratory performance.

C-2.5 Safety Plan: The contractor shall provide a detailed plan outlining the policy, procedures and actions necessary to maintain a safe working environment for employees and visitors. The plan shall cover the products stored, handled, Safety Data Sheets (SDS) and guidelines regarding the safe handling of such products and shall be maintained and updated over the course of the contract.

C-2.6 Transportation Plan: The contractor is required to submit a plan for review to transport the petroleum samples to an approved laboratory for testing or shipping (contractor supplied transport, third party delivery service, etc.) and how they plan on tracking the chain of custody to the contractor’s facility. Product quality must be preserved and not altered by shipment. DLA Energy or it’s subcontractor(s) do not have the ability or certification to ship or package fuel samples.

C-2.7 Laboratory Equipment Plan: The contractor will furnish, and update annually to the CO and COR, the status by name, model and serviceability of all equipment used in laboratory testing. Equipment that malfunctions or is non-serviceable shall be reported to the CO and COR within 48 hours with a mitigation plan to provide testing capability.

C-2.8 Monthly Reporting: The contractor shall provide a monthly written report to the CO and COR with the number of laboratory tests performed, what testing was included and the location.

C-3.0 Laboratory Requirements: The below are general requirements for all contractor laboratories. Laboratories are required to have the listed referee test methods which is referenced in the product specifications and international test methods (ASTM, EI, etc.).

C-3.1 Operating Hours: The contractor shall be responsible for adjusting hours of operation to meet workload demands and turn-around times in section C-3.8.

C-3.2 Staffing: The contractor shall provide sufficient staff to accomplish all functions and tasks to include simultaneous operations of performing multiple tests at a time, and provide the contact information for laboratory manager or assistant laboratory manager if the laboratory is not manned 24 hours, seven days a week.

C-3.3 Knowledge and Skills: The contractor shall ensure that personnel assigned to all tasks have the requisite knowledge and skills to meet the performance standards and comply with all applicable country laws, state laws, regulations, and codes. All supervisors and key employees shall be able to read and understand English so they can understand and follow oral or written instructions directions, directives, regulations, and operating procedures. All supervisors and contractor key employees shall be capable of writing in English to compose the required detailed reports.

C-3.4 Access: The contractor shall allow DLA Energy representatives to witness testing or sampling. It shall provide the applicable information for access, provide follow-up to obtain access (for personnel and vehicles) to all facilities that product is tested or sampled. For areas that require special admission the contractor will assist gaining access.

C-3.5 Epoxy Lined Sample Cans: The contractor shall maintain a supply of 10 unused epoxy lined fuel sample shipping containers to be provided to DLA Energy personnel per request. Sample containers shall be stored to ensure they are clean and free from all substances that might contaminate the product being sampled. Containers must meet the following specifics: Complies with ASTM D-4306, height not to exceed 9 inches, diameter not to exceed 7 inches, capacity 1 USG, Bung Plug ¾” with lock-wire hole, carrying handle able to be shipped as hazardous material.

C-3.6 Thermal Oxidation Stability Failures: If a failure occurs using an ALCOR (PAC) Mark IV, the retest shall not be conducted on any ALCOR (PAC) Mark IV model.

C-3.7 Ellipsometric Tube Deposit Rater (ETR): The contractor shall perform ASTM D3241 Annex 3 ETR within the testing turn-around times in section C-3.8.1 Sample Testing Turnaround Times. ETR is the preferred method and shall be treated as the referee method.

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C-3.8 Transportation Turn-around Times: The contractor shall be responsible for transportating the sample from the location in paragraph C-1.0.1 to contractor’s laboratory.. Turn-around time starts when the contractor is notified the sample is prepared for transportation from sample location to the servicing laboratory. Turn-around time ends when fuel sample reaches the laboratory. DLA Energy will give the contractor at least 12 hours of advance notice of the sample being prepared for transportation (prime contractor is responsible for any sub-contractor actions). The 12 hours of advance notice is not included in the turn-around time. If transportation cannot be completed within the turn-around time the contractor shall immediately notify the CO and COR. The contractor shall specify the problem and the estimated completion date and time.

C-3.8.1 Sample Testing Turnaround Times: Sample Testing turn-around times are defined as follows: contractor receives a sample at its laboratory, performs testing, and submits the test reports to the responsible office. The Testing Turnaround Times are listed below. Turn-around time ends when testing results are completed and delivered to DLA Energy. If testing cannot be completed within the turn-around time the contractor will immediately notify the COR, QAR and CO in writing. The contractor’s notification shall specify the reason it is unable to meet the Turnaround Time and provide the estimated completion date and time.

TESTING TURNAROUND TIMES

A level/Full spec testing 36 hours B-1, B-2, B-3 Testing 24 hours C-level Testing 8 hours Individual Testing 8 hours Expedite Request 6 hours Secured Fuel Performance (See Section C-5.0)

8 hours

C-3.9 Retain samples: After analysis, the contractor shall retain samples for a minimum of 45 days. In the event of a suspected quality issue or dispute, a longer sample retention period may be requested by DLA Energy. The contractor shall be responsible for disposal of excess fuel samples and sample containers.

C-4.0 Transportation Performance Requirements: The contractor shall be responsible for packing and transporting all petroleum samples from a job site to the laboratory in accordance with laws and regulations. When requested, by DLA Energy personnel, the contractor shall be able to provide an epoxy line sample can, detailed in C-3.6 for replacement. When sample transportation is not required of the contractor, they shall be notified in advance.

C-5.0 Secured Fuels Performance Requirements: Due to mission demands, DLA Energy may request petroleum testing services under Attachment 2 from MIL-STD-3004-1 table XII. DLA Energy will provide the contractor with as much advance notice as possible as the turn-around time shall not exceed 8 hours once the laboratory is in receipt of the sample(s). After a task order is issued, the QAR will coordinate the specifics/logistics required for the secured fuels testing services.

C-6.0 Surveyor Duties: When ordered, the contractor shall perform Surveyor Duties at any of the locations identified in section C-1.0.1. The contractor shall ensure all specifications, regulations, ASTM, API MPMS are followed when a DLA Energy representative is not available at locations mentioned in C-1.0.1. Personnel shall be International Federation of Inspection Agencies or TIC council or equivalent certified to perform the duties defined in the following subparagraphs.

C-6.1 Third party witness: When ordered, the contractor shall act as a third party witness to observe operations and report findings to the DLA Energy point of contact with a detailed report within 24 hours. DLA Energy will provide written instructions specific to the operations and objectives in the task order. The following are examples of operations commonly performed: Tank to tank transfers, off-loading vessels, barges, tank trucks, containers, loading vessels, barges, tank trucks, containers.

TRANSPORTATION TURN AROUND TIMES

All locations 24 hours

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C-6. 2 Sampling of petroleum products: When ordered, the contractor shall perform the sampling service from any of the following :

Category 1: vessels or barges Category 2: pipelines, tank trucks, storage tanks, or any containers that may hold fuel.

Procedures shall be performed in accordance with API MPMS and/or ASTM D4057. The contractor shall supply all equipment and material needed to perform tasks.

C-6. 3 Gauging of Petroleum Products: When ordered, the contractor shall perform gauging of vessels (to include bunkers), barges, tank trucks, storage tanks, or any containers that may hold fuel. The contractor shall supply all equipment and material need to perform task.

C-7.0 Joint Contingency Contracting System (JCCS) Requirement: All non-U.S. offerors and all proposed non- U.S. subcontractors must be registered online in the JCCS website (https://www.jccs.gov/).

C-8.0 Sample Shipment: The contractor shall, upon request, be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of request and arrive to the below laboratory within five calendar days.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra Rd San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

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Attachment 1: Products Specifications shall dictate the testing required and the contractor shall develop a plan based on product specifications (A level testing) and MIL-STD-3004-1 (B-1, B-2, B-3, C test). MIL-STD_3004-1 describes products to be tested, types of testing required and additional information as required. All referenced material can be obtained at http://quicksearch.dla.mil/, https://assist.dla.mil/, or by contacting CO, COR, or QAR.

Jet Fuels

Aviation Turbine Fuel, Kerosene Types, Grade JET A, (Specification: ASTM D1655 latest version)

Aviation Turbine Fuel, Kerosene Types, Grade JET A-1, NATO F-35, (Specification: DEF Stan 91-091 latest version)

Aviation Turbine Fuel, Kerosene Types, Grade JP-8, NATO F-34 (Specification: MIL-DTL-83133, latest version) Aviation Turbine Fuel, Grade JP-5, NATO F-44 (Specification: MIL-DTL-5624, latest version)

Aviation Turbine Fuel, Thermally Stable, Grade JPTS (Specification: MIL-DTL-25524, latest version)

Aviation Gasoline, Low Lead, Grade 100LL, NATO F-18 (Specification: ASTM D910, latest version)

Diesel Fuels

Diesel Fuel, Naval Distillate Fuel, NATO F-76 (Specification: MIL-DTL-16884, latest versions)

Diesel Fuel Oil, Grades: Ultra-low sulfur No.1 & No. 2; Low Sulfur No.1 & No. 2 (Specification: ASTM D975, latest version) Diesel Fuel Oil (Specification: EN 590, latest version)

Marine Residual Fuel Oil, Grades: RME-180, RME-380(Specification: ISO 8217, latest version)

Marine Diesel Fuel Oil, Grades: MGO (Specification: ISO 8217, latest version)

Unleaded Fuels

Fuel, Automotive Spark Ignition Engine Grades Regular, Midgrade, Premium (Specification: ASTM D4814, latest version) Fuel, Automotive Spark Ignition Engine (Specification: EN 228, latest version)

Additives

Fuel System Icing Inhibitor (FSII), High Flash (Specification: MIL-DTL-85470, latest version)

Corrosion Inhibitor (CI) (Specification: MIL-PRF-25017, latest version)

Lube Oils

Lubrication Oil, Steam Turbine and Gear, Grade LTL MIL Symbol 2190 (Specification: MIL-PRF-17331, latest version)

Lubrication Oil, Shipboard Internal Combustion, High Output Diesel, Grade LO6, MIL Symbol 9250 (Specification: MIL-PRF-9000, latest version)

Lubrication Oil, Catapult Launch Engine, Grade CLB, (Specification: MIL-PRF-32644, latest version)

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Attachment 2: Series Testing Requirements The list below provides tests by name and methods that shall be required to be performed on petroleum products at the contractor’s laboratory in accordance with product specifications MIL-STD-3004-1, specifications, and authorized test methods. The contractor shall indicate if they cannot perform authorized method or submit a formal exception request to the DLA Energy CO for acceptance. Tests shall be requested by series or individually by a DLA Energy representative as situation warrants.

1. A Series (Specification testing in accordance with Attachment 1 and MIL-STD-3004-1)

2. B-1 Series (MIL-STD-3004-1 list tests required in group)

3. B-2 Series (MIL-STD-3004-1 list tests required in group)

4. B-3Series (MIL-STD-3004-1 list tests required in group)

5. C Series (MIL-STD-3004-1 list tests required in group)

Individual Tests: Individual tests may be requested from any test included in the A, B or C series specification, MIL-STD- 3004-1 or from the tables below.

Note: Tests are grouped by physical or chemical property and do not imply equivalency. Verify that the test is appropriate to the product specification prior to analysis.

1. Secured Fuel Series Testing Requirements and Specification Limits JP-5 Jet A Jet A-17 JP-8 F-24

Min. Max. Min. Max. Min. Max. Min. Max. Min. Max.

Appearance

Gravity, API @ 60 °F D1298/D4052

36.0 48.0 37.0 51.0 37.0 51.0 37.0 51.0 37.0 51.0

Density at 15°C (kg/m3) 788 845 775 840 775 840 775 840 775 840

Weight: lb/USG Calculated 6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0 6.5 7.0

Distillation (°C) D863

10% Recovered 205 205 205 205 205 20% Recovered Report Report

50% Recovered Report Report Report Report Report 90% Recovered Report Report Report Report Report Final Boiling Point 300 300 300 300 300 Freezing point, °C D5972/D2386

-46

-40

-47

-47

-40

Flash point, °C D93/D56 60 38 38 38 38

Particulate Matter (mg/L) D2276, D5452, Appendix C of MIL- DTL- 83133

0.5

Conductivity (pS/m) D2624 Report Report 50 700 50 700

Copper strip corrosion D130 No.1 No.1 No.1 No.1 No.1

Water reaction D1094 1b

Existent gum (mg/100 mL) D381 7 7 7 7 7 FSII, (vol %) D5006 0.07 0.20 0.04 0.15 0.04 0.15

Thermal Stability D3241

Change in pressure drop, mm Hg 25 25 25 25 25 One of the tube deposit rating methods shall be run:

(1) Ellipsometer (ETR) (nm) or Interferometer (ITR) (nm)

(2) Heater tube deposit, Visual Tube Rating (VTR)

< 3

Fatty Acid Methyl Ester (FAME)

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2. Jet A & Jet A-1 (NATO F35) Series Testing Requirements for Specifications ASTM D1655 and Def Stan 91-

A Series Characteristics Def Stan

91-091

ASTM

D1655

B-1 Series

B-2 Series

B-3 Series

C-Series

Appearance X X X X X X Color (Visual) X X X X X X Density or API Gravity X X X X X X Particulate Contamination/Particulate Matter

X X X X X

Particle Count X X Total Acidity X X X Aromatics X X Total Sulfur X X Mercaptan Sulfur X X Doctor Test X X Distillation X X X X X Viscosity X X Smoke Point X X Naphthalenes X X Specific Energy X X Hydrogen Content X Calculated Cetane Index X Copper Strip Corrosion X X X X X Freezing Point X X X X X Existent Gum X X X X X Flash Point X X X X X X Water Reaction Lead Content (if present) X X X X

FSII X X X X X

Particulate Contamination/Particulate Matter with Filtration Time

MSEP X X X X X

Electrical Conductivity X X X X X Thermal Stability X X X X Color (Saybolt) X X X Peroxide Number X

FAME X X X X X

Lubricity X

X

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3. JP8 (NATO F34) Series Testing Requirements for Specifications MIL DTL 83133

Characteristics MIL DTL

83133 B-1

Series B-2

Series

Appearance X X X X X Color (Visual) X X X X X Density or API Gravity X X X X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Viscosity X Smoke Point X Naphthalenes X Specific Energy X Hydrogen Content X Calculated Cetane Index X Copper Strip Corrosion X X X X Freezing Point X X X X Existent Gum X X X X Flash Point X X X X X Water Reaction X X X Lead Content (if present) X X X

FSII X X X X

Particulate Contamination/Particulate Matter with Filtration Time

X X X X

MSEP X X X X

Electrical Conductivity X X X X Thermal Stability X X X Color (Saybolt) X X Peroxide Number

FAME X X X X

Lubricity

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4. JP5 (NATO F44) Series Testing Requirements for Specifications MIL DTL 5624

Characteristics MIL DTL

B-1

B-2 Series B-3 Series C- Series

Color (Visual) X X X X X Density or API Gravity X X X X X Particulate Contamination/Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Viscosity X Smoke Point X Naphthalenes X Specific Energy X Hydrogen Content X Calculated Cetane Index X Copper Strip Corrosion X X X X Freezing Point X X X X Existent Gum X X X X Flash Point X X X X X Water Reaction Lead Content (if present) X X X

FSII X X X X

Particulate Contamination/Particulate Matter with Filtration Time

X X X X

MSEP X

Electrical Conductivity X Thermal Stability X X X Color (Saybolt) X X Peroxide Number

FAME X X X X

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5. F-76 Series Testing Requirements for Specifications MIL-DTL-16884

6. Fuel System Icing Inhibitor (FSII) (NATO S-1745) Series Testing Requirements for Specifications MIL-

DTL-85470

Characteristics MIL F

16884 B-1

Series B-2

B-3 Series C-Series

Color X X X X X Density or API Gravity X X X X X Distillation X X X Flash Point X X X X X Carbon Residue X X X Cloud Point X X Pour point X X Copper Strip Corrosion X X Viscosity X X Water and Sediment X X X X Storage Stability X X Sulfur X X X Fatty Acid Methyl Ester (FAME) X X X Lubricity X X X Demulsification X Particulate Contamination/Particulate Matter

X X X

Acid Number X Ash X Aromatics X Hydrogen Content X Ignition Quality (Cetane Number), referee

X

Ignition Quality (Cetane Index) X X Ignition Quality (Derived Cetane Number)

X

Trace Metals (Ca, Pb, Na, K and V) X

A Series Characteristics MIL DTL 85470 B-1

Series B-2

Series B-3 Series C-Series

Appearance X n/a X n/a X Acid Number X n/a X n/a Color, Platinum Cobalt X n/a n/a Distillation X n/a X n/a Ethylene Glycol X n/a X n/a pH of 25% solution in water X n/a X n/a Relative Density X n/a X n/a X Water (mass%) X n/a X n/a Flash Point X n/a n/a X

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7. Marine Residual Fuel Oil (RME 180, RME 380) Series Testing Requirements for Specification ISO 8217

Characteristics ISO 8217 B-1

Series B-2

Series B-3

Series C-Series

Appearance X X X X X Kinematic Viscosity X X X X X Density X X X X X Calculated Carbon Aromaticity Index (CCAI) X X Sulfur X X Flash Point X X X X X Hydrogen Sulfide X X Acid Number X X Total Sediment, aged X X X Carbon Residue X X X Pour Point X X Water X X X Ash X X Vanadium X Sodium X X Aluminum plus silicon X Used lubricating Oil X Cetane Index Oxidation Stability

FAME

Cloud Point Cold Filter Plugging Point

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8. Marine Gas Oil (MGO) Grade DMA Series Testing Requirements for Specification ISO 8217

Characteristics

ISO 8217

B-1

Series B-2

Series B-3

Series C-Series

Appearance X X X X X Kinematic Viscosity X X Density X X X X Calculated Carbon Aromaticity Index

(CCAI)

Sulfur X X Flash Point X X X X X Hydrogen Sulfide X Acid Number X X Total Sediment, aged Carbon Residue X X X Pour Point X X Water X Ash X Vanadium Sodium Aluminum plus silicon Used lubricating Oil Cetane Index X X Oxidation Stability X X X

FAME X X X

Cloud Point X Cold Filter Plugging Point X Lubricity X

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9. Lubrication Oil (LTL) (NATO O-250) Series Testing Requirements for Specification MIL PRF 17331

Characteristics MIL PRF

17331 B-1

Series B-2

Series

Appearance X X X n/a X Sulfur X n/a Acid Number (Neutralization number) X X n/a Corrosion X n/a Copper strip corrosion X X n/a Oil Compatibility X n/a Water Content X X X n/a X API Gravity X X X n/a X Flash Point X X X n/a Pour Point X X n/a Viscosity @ 4.4°C X n/a Viscosity @100°C X X X n/a Viscosity @40°C X X X n/a Emulsion Test X X X n/a Oxidation (Total Sludge, iron and copper) X n/a Oxidation by RPVOT X n/a Scuffing load capacity (FZG) X n/a Wear test X n/a Homogeneity X Foam test X X X Solid particle contamination (Cleanliness) X X X Thermal stability (Copper appearance, steel appearance, sludge)

X

Coking tendency X

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10. Lubrication Oil (LO6) (NATO O-278) Series Testing Requirements for Specification MIL PRF 9000

Characteristics MIL PRF 9000 B-1

Series B-2

Series B-3

Series C-Series

Appearance X X X X Sulfated Ash X X X n/a Copper strip corrosion X n/a Flash point X X X n/a Foam (stability only) X X X n/a Gravity X X X n/a X Barium X n/a Calcium X n/a Magnesium X n/a Zinc X n/a Phosphorus X n/a Nitrogen X n/a Pour Point X X n/a Rust prevention X n/a Sulfur X n/a Total base number (Neutralization number)

X X n/a

Viscosity index X n/a Viscosity @ 100°C X X X n/a Viscosity @ 40°C X n/a

11. Lubrication Oil (CLB) Series Testing Requirements for Specification MIL PRF 32644

A Series Characteristics MIL PRF 32644 B-1

Series B-2

Series B-3

Series C-Series

Appearance/Workmanship X X X n/a X Viscosity @ 40°C X X X n/a Viscosity @100°C X X X n/a Viscosity @150°C X n/a Viscosity Index X X X n/a Flash Point X X X n/a Pour Point X X X n/a Sulfur X X X n/a Acid Number (Neutralization number) X X X n/a Density X X X n/a API Gravity X X X n/a X Ash Content X X X n/a Trace Sediment X X n/a Copper strip corrosion X X X n/a Foam X X X n/a Oxidation Stability X n/a Four-Ball Wear Test X n/a Four-Ball EP Test X n/a

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12. Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590

Characteristics ASTM

D975

EN 590 B-1

Series B-2

Series B-3

Series C-Series

Appearance/Workmanship X X X X X X Flash point X X X X X X Water and Sediment X X X Distillation X X Kinematic Viscosity @ 40°C X X X Ash X X X Sulfur X X X X Copper strip corrosion X X Cetane number X X Cetane index X X Aromaticity X Cloud Point X X X X

LTFT/CFPP X X

Carbon Residue X X X Lubricity X X Conductivity X API Gravity or Density at 15°C

X X X X X

Polycyclic aromatic hydrocarbons

X

Manganese content X Water Content X X Total Contamination X

FAME X

Oxidation stability X X

Page | 17

13. Corrosion Inhibitor/Lubricity Inhibitor (CI/LI) (NATA S-1747) Series Testing Requirements for Specification MIL-PRF-25017

Characteristics MIL-PRF-25017 B-1

Series B-2

Series B-3 Series C-Series

Appearance/Workmanship X X X Solubility X Rust X Lubricity (BOCLE) X X Water Separation (MSEP) X X Electrical Conductivity X Ash Content X X Pour Point X X Storage Stability X Fuel Injection Fouling X Emulsification Tendency X Accelerated Stability X Density @ 15℃ X X X Viscosity @ 40℃ X X Flash point X X X Acid Number (Neutralization Number)

X X pH of 25 % solution in water

X X

Metals X X

Page | 18

14. Gasoline, Unleaded (NATO F67) Series Testing Requirements for Specifications ASTM D4814, EN 228

Characteristics ASTM

D4814

EN 228 B-1

Series B-2

Series B-3

Appearance (and visual color)

X X X X X X

Vapor Pressure X X X X Density or API Gravity X X X X X X Distillation X X X X X Driveability Index X Lead Content X X Sulfur X X Silver Strip Corrosion X Copper Strip Corrosion X X X X Gum Content X X X X Oxidation Stability X X X Vapor Liquid Ratio X Antiknock Index X Research Octane Number

(RON)

X X X X

Motor Octane Number

(MON)

X X X X

Manganese Content X X Hydrocarbon type content (olefins and aromatics)

X

Benzene Content X Oxygen Content X X Oxygenate Content X X Vapor Lock Index X X

Page | 19

Attachment 3: Testing Requirements

Table 1: Aviation Turbine Fuels

*Def Stan 91-091

Jet A/A-1

(ASTM D1655)

JPTS

(MIL-DTL- 25524)

JP-8, NATO F-35,

JP-8 +100

( MIL-DTL- 83133)

JP-5

(MIL-DTL- 5624)

Appearance Visual, D4176 Procedure 1

Visual, D4176 Visual, D6986 Visual, D6986 Visual

Color (Visual) D156, D6045, (Note 1)

Visual Visual Visual Visual

Density or API Gravity

IP 365, IP 160,

D4052, D1298

D1298, IP 160,

D4052, IP 365

D1298, D4052 (referee), D7777

D1298, IP160,

D4052, D7777, IP

D1298, D4052 D7777

Particulate Contamination /Particulate Matter

IP 423, D5452

(Note 2), IP 564, IP 565, IP 577

D2276, IP 216

D5452 (referee), IP

D2276, D5452 (referee)

D2276, D5452 D2276, D5452 (referee)

Particle Count IP 564, IP 565, IP 577 (Note 4)

IP 564, IP 565, IP

577, D7619

D8166, IP 564, IP 565,

IP 577, D7619

D8166, IP 564, IP 565,

IP 577, D7619

IP 564, ID 565, IP 577

D7619 (referee)

Total Acidity IP 354, D3242 IP 354, D3242 ASTM D3242 D3242, IP 345 D3242

Aromatics IP 156, D1319 (Note 5), IP 436, D6379 (Note 6)

IP 156, D1319, IP

436, D6379

D1319 (referee), D6379 D1319, IP 156 D1319, D6379

Total Sulfur IP 336, IP 107, IP 243, IP 373, IP, 447, D1266, D2622, D4294, D5453

D1266, D2622, D4294, D5453, IP

D1266, D2622, D3120, D4294 (referee) , D5453, D7039

D129, D1266, D2622, D3120, D4294 (referee), D5453, IP

D129, D1266, D2622, D3120, D4294 (referee), D5453

Mercaptan Sulfur

IP 342, D3227

(Note 7)

IP 342, D3227 D3227 D3227, IP 342 D3227

Doctor Test IP 30, D4952 D4952 D4952 D4952 D4952

Distillation IP 123, IP406 (Note 1), D86, D2887, D7345 (Note 2)

D86, D2887, IP 406,

D7344

D7345, IP 123

D86 (referee), D2887, D7345

D86 (referee), D2887, IP 406, IP 123, D7345

D86 (referee) , D7345, D2887

Viscosity IP 71, D445, D7042 (Note 4), D7945

IP 71 Section 1, D445, D7042, D7945

D445 (referee), D7042, D7945

D445, D7042, D7945, IP 71 Section 1

D445

Smoke Point IP 598, D1322 (Note 12)

IP 598, D1322 D1322 IP 598, D1322 D1322

Naphthalenes D1840 D1840 D1840 D1840 D1840

Specific Energy

D3338, D4529, D4809 (referee), IP 12, see Note 13

D3338, D4529, D4809 (referee), IP

D3338, D4529, D4809 (referee), D3338, D4529, D4809 (referee), IP 12

D3338, D3338M, D4529, D4809 (referee)

Hydrogen Content

N/A D3343, D3701 D3343, D3701, D7171 D3343, D3701, D5291, D7171

D3701, D5291, D7171

Calculated Cetane Index

N/A D4737 Procedure A D976, D4737 D976, D4737 D976, D4737

Page | 20

Copper Strip Corrosion

IP 154, D130

(Note 14)

D130, IP 154 D130 D130, IP 154 D130

Freezing Point IP 16, IP 435, IP528, IP529, D2386 (Note 11), D5972, D7153, D7154

D5972, IP 435, D7153

IP 529,

D7154, IP 528,

D2386, IP 16

D2386 (referee), D5972, D7153, D7154

D2386 (referee), D5972, D7153, D7154, IP 16, IP

435, IP 528, IP 529

D2386 (referee), D5972, D7153, D7154

Existent Gum IP 540, D381 D381, IP 540 D381(referee), IP 540 D381(referee), IP540 D381(referee), IP 540

Flash Point IP 170, IP 523, D56, (Note 3), D3828

D56, D93, D3828, IP 170, IP 523

D56, D93(referee), D3828, IP170

D56, D93 (referee), D3828, IP 170

D56, D93 (referee), D3828

Water Reaction***

N/A N/A N/A N/A N/A

Lead Content D5059 N/A N/A N/A N/A

FSII IP 424,

D5006

D5006 D5006 D5006 D5006

Filtration Time N/A N/A N/A (Appendix A) (Appendix A), D2276, D5452 ( referee)

MSEP D3948, (Note 18)

D3948 D3948, D7224 (referee)

D3948, D7224 (referee, if fully additized)

D3948, D7224 (referee)

Electrical Conductivity

IP 274,

D2624, (Note 19)

D2624, IP 274 D2624 D2624, IP 274 D2624

Thermal Stability

IP 323, D3241,

(Note 15), (Note 16), (Note 17)

D3241 (Annex A3, referee)

D3241 (Annex A3 is referee)

D3241 (Annex A3, referee), IP 323

D3241 (Annex A3, referee)

Color (Saybolt) D156, D6045 D156 D156 (referee), D6045

D156 (referee), D6045 D156 (referee), D6045

Peroxide Number**

N/A N/A N/A N/A N/A

FAME IP 583, IP 585,

IP 590,

IP 599, D7797

D7797, IP 583,

IP 585 (referee), IP

590, IP 599

N/A D7797, IP 583, IP 585

(referee), IP 590, IP

D7797, IP 583, IP 585

(referee), IP 590, IP 599

Lubricity D5001, (Note 20)

D5001 N/A N/A N/A

*Note: Def Stan 90-091 specification’s “numbered Note” reference provides additional guidance for that test property.

**Note: Peroxide Number is not a requirement per the product specification (i.e., MIL-DTL-83133); however, per MIL-STD-3004 specification, the applicable test methods to measure the property are the following: ASTM D3703, ASTM D6447.

***Note: Water Reaction is not a requirement per the product specification (i.e., MIL-DTL-83133); however, per MIL-STD-3004 specification, the applicable test method(s) to measure the property is the following: ASTM D1094.

Page | 21

Table 2: Aviation Gasoline Def Stan

91-090 Leaded AvGas

(ASTM D910)

Appearance Visual, D4176 Visual Color (Visual) Visual Visual Density or API Gravity IP 365, D4052 D1298, IP160, D4052 Distillation IP 123, D86 (Group 2) D86 Copper Strip Corrosion IP 154, D130 D130 Existent Gum IP 131, D381 D381 Vapor Pressure IP 69, D323 D323, D5191 Lead Content IP 270, D3237 D3341, D5059 Potential Gum IP 138, D873 D873 Lean Mixture Octane Number (MON) IP 236, D2700 D2700 Rich Mixture Octane Number (RON) IP 119, D909 D909 Performance Number IP 119, D909 D909 Sulfur Content IP 107, D1266 D1266, D2622 D5453 Dye Content specification (Table 2) D2392 Color (Lovibond) IP 569, IP 17, D2392 IP569 Specific Energy (Net Heat of Combustion)

D4529, D3338, D4809

D4529, D3338

Freezing Point IP 16, D2386 D2386 Conductivity IP 274, D2624 D2624 Oxidation Stability IP 138, D873 D873 Oxidation Stability (Potential Gum) IP 138, D873 D873 Oxidation Stability (Lead Precipitate) D873 D873 Water Reaction IP 289, D1094 D1094

Table 3: Marine Diesel

F-76

(MIL-DTL-16884)

Appearance D4176 Color D1500 (referee), D6045 Density or API Gravity D1298 (referee), D4052, D287, D7777 Distillation D86 (referee), D2887 Flash Point D93 (referee), D6450, D3828 Carbon Residue D524 (referee), D189, D4530 Cloud Point D2500(referee), D5771, D5772, D5773 Pour point D97(referee), D5949, D5950, D5985 Copper Strip Corrosion D130 Viscosity D445, D7042 Water and Sediment D2709 Storage Stability D5304 (referee), D2274 Sulfur D5354 (referee), D1266, D2622, D3120, D7039 Fatty Acid Methyl Ester (FAME) BS EN 14078, IP 579, D7963 Lubricity D6079 (referee), D7688 Demulsification D1401 Particulate Contamination/Particulate Matter D6217 (referee), D5452 Acid Number D974 (referee), D664 Ash D482 Aromatics D6591 (referee), D2425 Hydrogen Content D7171 (referee), D4808, D5291 Ignition Quality (Cetane Number), referee D613 (referee) Ignition Quality (Cetane Index) D976 Ignition Quality (Derived Cetane Number) D6890, D7170 Trace Metals (Ca, Pb, Na, K and V) D7111 (referee), D3605

Page | 22

Table 4: Fuel System Icing Inhibitor

MIL-DTL-85470

Appearance Visual Acid Number D1613 Color, Platinum Cobalt D1209 (referee), E450 Distillation D1078 Ethylene Glycol specification pH of 25% solution in water E70 Relative Density D891 (referee), D4052 Water (mass%) D1364 (referee), E1064, E203 Flash Point D93 (referee), D56, D3828

Table 5: Motor Gasoline

ASTM D4814 EN 228

Appearance Visual, D4176 Visual Vapor Pressure D4953, D5191, D5482 or D6378 EN ISO 13016-1

Density or API Gravity D287, D1298, D4052 EN ISO 3675, EN ISO 12185 (referee) Distillation D86, D7345 EN ISO 3405

Driveability Index specification N/A Lead Content D3237 D5059 EN 237

Sulfur D1266, D2622, D3120, D5453, D6920, D7039, D7220

EN ISO 13032, EN ISO 20846 EN ISO 20884

Silver Strip Corrosion D7667, D7671 N/A Copper Strip Corrosion D130 EN ISO 2160

Gum Content D381 EN ISO 6246 Oxidation Stability D525 EN ISO 7536 Vapor Liquid Ratio D5188 N/A

Antiknock Index specification Research Octane Number

(RON)

D2699, D2885 EN ISO5164

Motor Octane Number (MON) D2700, D2885 EN ISO 5163 Manganese Content D3831 EN 16135, EN 16136

Hydrocarbon type content (olefins and aromatics)

N/A EN 15553, EN ISO 22854

Benzene Content N/A EN 238, EN 12177, EN ISO 22854 Oxygen Content D4815 (calculation) EN 1601, EN 13132, EN ISO 22854

Oxygenate Content D4815 (calculation) EN 1601, EN 13132, EN ISO 22854 Vapor Lock Index N/A specification

Page | 23

Table 6: Bunker/Marine Fuel Residual Fuel Oil

RME 180/380

(ISO 8217)

Marine Gas Oil MGO; DMA grade

(ISO 8217)

Appearance Visual Visual

Kinematic Viscosity ISO 3104 ISO 3104 Density ISO 3675, ISO 12185, D4052 ISO 3675, ISO 12185

Calculated Carbon Aromaticity Index

(CCAI)

specification

N/A

Sulfur ISO 8754, ISO 14596, D4264 ISO 8754, ISO 14596, D4264 Flash Point ISO 2719 ISO 2719

Hydrogen Sulfide IP 570 IP 570 Acid Number D664 D664

Total Sediment, aged ISO 10307-2 N/A Carbon Residue ISO 10370, D4530 ISO 10370

Pour Point ISO 3016 ISO 3016 Water ISO 3733 ISO 3733

Ash ISO 6245 ISO 6245 Vanadium IP 501, IP 470, ISO 14597, D5863 N/A

Sodium IP 501, IP 470 N/A Aluminum plus silicon IP 501, IP 470, ISO 14597, D5184 N/A

Used lubricating Oil IP 501, IP 470, IP 500 N/A Cetane Index N/A ISO 4264

Oxidation Stability N/A ISO 12205

FAME N/A IP 579, D7963

Cloud Point N/A ISO 3015 Cold Filter Plugging Point N/A IP 309, IP 612

Lubricity N/A ISO 12156

Table 7: Lubrication Oil (LTL) (NATO O-250)

MIL-PRF-17331

Appearance specification (visual) Sulfur D129, D1552, D2622, D4927 (referee), D4951, D6443, D6481, D7751

Acid Number (Neutralization number) D974, D664 Corrosion D665, Procedure B Copper strip corrosion D130 Oil Compatibility specification, D7155 Water Content D6304 (referee), D7546 API Gravity D287, D1298 (referee), D4052 Flash Point D92, D93 (referee) Pour Point D97 (referee), D5949, D5950 Viscosity @ 4.4°C D445 (referee), D7042 Viscosity @100°C D445 (referee), D7042 Viscosity @40°C D445 (referee), D7042 Emulsion Test D1401 Oxidation (Total Sludge, iron and copper)

D4310

Oxidation by RPVOT D2272 Scuffing load capacity (FZG) D5182 Wear test D4172 Homogeneity specification Foam test D892 Solid particle contamination (Cleanliness)

D4898

Thermal stability (Copper appearance, steel appearance, sludge)

D2070

Coking tendency Appendix A

Page | 24

Table 8: Lubrication Oil (LO6) (NATO O-278)

MIL-PRF-9000

Appearance Visual Sulfated Ash D874 Copper strip corrosion D130 Flash point D92 Foam (stability only) D892 Gravity D287, D1298, D4052 Barium D4628, D4927, D4951 Calcium D4628, D4927, D4951, D6443, D6481

Magnesium D4628, D4927, D4951, D6443 Zinc D4628, D4927, D4951, D6443, D6481 Phosphorus D1091, D4047, D4927, D4951, D6443, D6481 Nitrogen D3228, D4629, D5762 Pour Point D97, D5949, D5950 Rust prevention D6557 Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481 Total base number (Neutralization number)

D2896

Viscosity index D2270 Viscosity @ 100°C D445 Viscosity @ 40°C D445

Table 9: Diesel Fuel Oil

ASTM D975 EN 590

Appearance/Workmanship Visual, D4176 specification Flash point D93 EN ISO 2719 Water and Sediment D2709 N/A Distillation D86 EN ISO 3405, EN ISO 3924 Kinematic Viscosity @ 40°C D445 EN ISO 3104 Ash D482 EN ISO 6245 Sulfur D2622, D5453 EN ISO 20846, EN ISO 20884, EN ISO

13032 Copper strip corrosion D130 EN ISO 2160 Cetane number D613 EN ISO 5165, EN 15195, EN 16144 Cetane index D976 EN ISO 4264 Aromaticity D1319 N/A Cloud Point D2500 EN 23015

LTFT/CFPP D4539, D6371 EN 116, EN 16329

Carbon Residue D524 EN ISO 10370 Lubricity D6079, D7688 EN ISO 12156-1 Conductivity D2624, D4308 N/A API Gravity or Density at 15°C N/A EN ISO 3675, EN ISO 12185 Polycyclic aromatic hydrocarbons N/A EN 12916 Manganese content N/A prEN 16576 Water Content N/A EN ISO 12937 Total Contamination N/A EN 12662

FAME N/A EN 14078

Oxidation stability N/A EN ISO 12205, EN 15751