5a_Repair Roof_B3010_Specifications_Final.pdf

MOUNTAIN HOME AIR FORCE BASE

MOUNTAIN HOME, IDAHO

100 Percent

SPECIFICATIONS

for the construction of the

REPAIR ROOF MUNITIONS STORAGE FACILITY 3010

Project No. QYZH 12-0066

CH2M HILL

Boise, Idaho

October 2016

© CH2M HILL 2016. All rights reserved.

This document and the ideas and designs incorporated herein, as an instrument of professional service, is the property of CH2M HILL and is not to be used in whole or part, for any other project without the written authorization of CH2M HILL.

Project No. 679700 Copy No.

MHAFB REPAIR ROOF MUNITIONS STORAGE FACILITY 3010

PW\DEN001\679700\679700 TABLE OF CONTENTS

OCTOBER 21, 2016 00 01 10 - iii

TABLE OF CONTENTS

Pages

SPECIFICATIONS

DIVISION 00—PROCUREMENT REQUIREMENTS

00 31 24 Available Information .............................................................. 1- 1 Supplement: Environmental Sampling Report

DIVISION 01—GENERAL REQUIREMENTS

01 00 00 General Requirements .............................................................. 1- 8 01 31 13 Project Coordination ................................................................ 1- 5 Supplement: Base Civil Engineer Work Clearance Request (Dig Permits) 01 33 00 Submittal Procedures ............................................................... 1- 6 Supplement: Material Approval Submittal Form Supplement: Construction Data Sheet Supplement: MHAFB Contractor As-Built Drawing

Standards Supplement: Schedule of Material Submittals 01 35 43 MHAFB Environmental Specifications ................................... 1- 16 Attachment 1: MHAFB Contractors Hazardous Materials Reporting Form Attachment 2: MHAFB Contractor Hazardous Materials Monthly Usage Reporting Form Attachment 3: MHAFB Contractor Site Specific Contingency Plan Attachment 4: Service Order Form Attachment 5: NRC Form 241 01 42 13 Abbreviations and Acronyms .................................................. 1- 5 01 50 00 Temporary Facilities and Controls .......................................... 1- 7 Supplement: Project Sign 01 57 13 Temporary Erosion and Sediment Control .............................. 1- 4

DIVISION 02—EXISTING CONDITIONS

02 41 00 Demolition ............................................................................... 1- 6

DIVISION 07—THERMAL AND MOISTURE PROTECTION

07 14 00 Fluid-Applied Waterproofing .................................................. 1- 11

REPAIR ROOF MUNITIONS STORAGE FACILITY 3010 MHAFB

Pages

TABLE OF CONTENTS PW\DEN001\679700\679700

00 01 10 - iv OCTOBER 21, 2016

DIVISION 31—EARTHWORK

31 23 23 Fill and Backfill ....................................................................... 1- 7 31 23 23.15 Trench Backfill ........................................................................ 1- 8 31 32 19.16 Geotextile ................................................................................. 1- 7

DIVISION 33—UTILITIES

33 41 01 Drainage Piping ....................................................................... 1- 3 Data Sheet: Polyvinyl Chloride (PVC)

END OF SECTION

PW\DEN001\679700\679700 AVAILABLE INFORMATION

OCTOBER 21, 2016 00 31 24 - 1

SECTION 00 31 24

AVAILABLE INFORMATION

PART 1 GENERAL (NOT USED)

PART 2 PROJECTS (NOT USED)

PART 3 EXECUTION

3.01 SUPPLEMENT

A. The supplement listed below, following “End of Section,” is a part of this specification. This supplement is provided for informational purposes only.

1. Environmental Sampling Report.

FINAL In sp e c t i on Repo r t

Environmental Sampling Report

QYZH 12-0066

Munitions Storage Area Facility 3010

Mountain Home AFB, Idaho

Prepared for

Mountain Home AFB, Idaho

October 21, 2016

Contents

Section Page

Introduction

Inspection Methodology

Asbestos Inspection

Lead-Based Paint Inspection

Pesticide Inspection

Findings

Asbestos

Lead-Based Paint

Pesticides

Recommendations

Appendixes

A Asbestos and Lead-Based Paint Building Inspector Certificates B Pictures C Laboratory Accreditations D Laboratory Results and COCs

I

Introduction

Facility 3010 is an existing earth covered magazine (ECM) munitions storage facility. The existing concrete structure is believed to be coated with a waterproof membrane, covered by earth. The earthen cover is sloped, with a 2 foot minimum thickness at the top. A 4 inch thick gunite coating has been applied to the earth mound cover, this gunite shell has failed and developed severe cracks over time, which permits erosion of the soils below. Mountain Home Air Force Base (MHAFB) desires to remove the existing earthen cover and gunite shell, as well as the existing waterproof membrane covering the ECM structure itself, in order to provide a new waterproof membrane, replacement and recompaction of earthen soil cover, and installation of a new separation geotextile and geocell grid filled with crushed aggregate to prevent erosion.

Scope of Work & Survey Limitations MHAFB contacted CH2M to perform a limited environmental inspection on Building 3010 in the Munitions Storage Area (MSA). The environmental inspection is limited to the roof structure and associated venting, as shown in the “Statement of Work” dated 5 February 2016. Inspection efforts included sampling and analysis of the following materials associated with the roofing system:

• asbestos containing buildings materials (ACBMs) in waterproofing membrane

• lead-based paint (LBP) on exposed ventilation shafts

• pesticides in earthen cover

Inspection Methodology

On July 30 and August 16, 2016, Michael Wirtz performed environmental inspections on the roof structure of Building 3010 for the presence of ACBM, LBP, and pesticides. Mr. Wirtz is a trained and certified AHERA Building Inspector and United State Environmental Protection Agency (USEPA) certified lead based paint building inspector (see Appendix A).

Asbestos Inspection

In order to expose the waterproof membrane, Mr. Wirtz had to cut through 4-inch thick gunite using a hand held concrete saw, and under a hot work permit set by the MHAFB Fire Department. Once a section of gunite was removed, Mr. Wirtz dug through approximately 3 inches of soil to expose a canvas and plastic sheet layer followed by approximately 27 inches of soil to the waterproof membrane (see Appendix B). Directly on top of the concrete roof structure of the ECM was membrane coating. Three samples were collected for the potential presence of asbestos: one sample of the membrane, a sample of the plastic sheet, and a sample of the canvas.

The suspect ACBM samples were sent to TestAmerica Laboratory in Nashville, TN (TestAmerica) for analysis using Chain-of-Custody (COC) sample tracking procedures.

TestAmerica is a National Voluntary Laboratory Accreditation Program (NVLAP) accredited asbestos laboratory. Laboratory accreditations are provided in Appendix C.

Samples were analyzed using polarized light microscopy (PLM), EPA Method 600/R- 93/116.

Lead-Based Paint Inspection

A LBP inspection was also conducted on the roof structure of Building 3010. Two bulk samples of suspect LBP were collected with a cutter or other tool, as appropriate. One sample was collected from the vent (sample ID 3010-LBP-01-vent), and one from the waterproof membrane (sample ID 3010-LBP-02-tar). Representative photographs of the waterproofing membrane and vent are provided in Appendix B. The lead samples were placed into a clean plastic bag with the sample identification written on the outside of the bag.

All suspect LBP samples were sent to TestAmerica Laboratory in Nashville, TN (TestAmerica) for analysis using COC sample tracking procedures. Samples were analyzed using EPA Method SW 846 6010B.

Pesticide Inspection

After a gunite section was removed and a hole was dug exposing the top of the ECM structure (approximately 30 inches deep soil layer), a sample was collected along the entire depth of the hole and analyzed for pesticides using EPA Method 8081. A 4-ouce glass jar was used to collect the sample by scrapping the edge of the jar along the entire depth of the hole to fill the jar. Refer to Appendix B for photographs.

Findings

Asbestos

All of the asbestos samples were non-detect (ND) for the presence of asbestos. Laboratory results and COCs are included in Appendix D.

Lead-Based Paint

One of the samples exceeded 5,000 mg/kg. The brown paint on the vent (Sample ID 3010- LBP-01-vent) has a lead concentration of 8,600 mg/kg. Approximately 100 ft2 of painted surface is on the vent. The other sample was below 5,000 mg/kg. Laboratory results and COCs are included in Appendix D.

Pesticides

No pesticides are present in the soil mound covering Building 3010. Laboratory results and COCs are included in Appendix D.

Recommendations

If impacted during the renovation process, the brown paint on the vent of Building 3010 should be abated by a trained professional. Any welding on the vent should be done only after the brown paint and any sub layer are removed exposing bare metal.

Appendix A

Asbestos and Lead-Based Paint Building Inspector Certificates

Appendix B

Pictures

PHOTO LOG

APPENDIX B CH2M HILL, INC 1

3010 Hole to Top of ECM

3010 Exposed Roof of ECM with Tar and Bare Concrete Under Tar

PHOTO LOG

2 CH2M HILL, INC APPENDIX B

3010 Roof After Sampling

3010 Vent Pipe

Appendix C

Laboratory Accreditations

Appendix D

Laboratory Results and COCs

ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177

TestAmerica Job ID: 490-108994-1 TestAmerica Sample Delivery Group: 2999, 3007, 3010 Client Project/Site: MHAFB MSA

For:

CH2M Hill, Inc.

322 E. Front St.

Suite 200 Boise, Idaho 83702

Attn: Mike Wirtz

Authorized for release by:

8/10/2016 12:58:11 PM

Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm http://www.testamericainc.com mailto:roxanne.cisneros@testamericainc.com

Table of Contents

Client: CH2M Hill, Inc.

Project/Site: MHAFB MSA

TestAmerica Job ID: 490-108994-1

SDG: 2999, 3007, 3010

TestAmerica Nashville

8/10/2016

Cover Page

Table of Contents

Sample Summary

Case Narrative

Definitions

Method Summary

Certification Summary

Subcontract Data

Chain of Custody

Receipt Checklists

Sample Summary TestAmerica Job ID: 490-108994-1Client: CH2M Hill, Inc.

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-108994-1 2999-AS-01-Roof Solid 07/28/16 00:01 08/03/16 09:55

490-108994-2 3007-AS-01-Tar Solid 07/28/16 00:01 08/03/16 09:55

490-108994-3 3007-AS-02-Tar Solid 07/28/16 00:01 08/03/16 09:55

490-108994-4 3007-AS-03-sub layer plastic Solid 07/28/16 00:01 08/03/16 09:55

490-108994-5 3007-AS-04-Cloth sub layer Solid 07/28/16 00:01 08/03/16 09:55

490-108994-6 3010-AS-01-tar Solid 07/29/16 00:01 08/03/16 09:55

490-108994-7 3010-AS-02-fabric Solid 07/29/16 00:01 08/03/16 09:55

490-108994-8 3010-AS-03-plastic Solid 07/29/16 00:01 08/03/16 09:55

TestAmerica Nashville

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Case Narrative Client: CH2M Hill, Inc. TestAmerica Job ID: 490-108994-1 Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Job ID: 490-108994-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative 490-108994-1

Comments

No additional comments.

Receipt

The samples were received on 8/3/2016 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 19.9º C.

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TestAmerica Nashville Page 4 of 14 8/10/2016

Definitions/Glossary

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Nashville

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Method Summary

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Method Method Description LaboratoryProtocol

NONESubcontract -

Asbestos

General Sub Contract Method EMLab FL

Protocol References:

NONE = NONE

Laboratory References:

EMLab FL = EMLab P&K - Fort Lauderdale, 6301 NW 5th Way, Suite 2850, Fort Lauderdale, FL 33309, TEL (954)776-8400

TestAmerica Nashville

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Certification Summary Client: CH2M Hill, Inc. TestAmerica Job ID: 490-108994-1 Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Laboratory: TestAmerica Nashville The certifications listed below are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Utah TN000328NELAP 07-31-16 *

Laboratory: EMLab P&K - Fort Lauderdale All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

AIHA-LAP, LLC 173067EMLAP 03-01-18

AIHA-LAP, LLC IHLAP 173067 03-01-18

TestAmerica Nashville

* Certification renewal pending - certification considered valid.

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Approved by:

Approved Signatory Tracy Garcia

Report for:

Ms. Roxanne Cisneros TestAmerica-Nashville, TN 2960 Foster Creighton Drive Nashville, TN 37204

Regarding: Project: 490-108994-1; MHAFB MSA

EML ID: 1580258

All samples were received in acceptable condition unless noted in the Report Comments portion in the body of the report. The results relate only to the items tested. The results include an inherent uncertainty of measurement associated with estimating percentages by polarized light microscopy. Measurement uncertainty data for sample results with >1% asbestos concentration can be provided when requested.

EMLab P&K ("the Company") shall have no liability to the client or the client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall the Company be liable to the client with respect to the Test Results except for the Company's own willful misconduct or gross negligence nor shall the Company be liable for incidental or consequential damages or lost profits or revenues to the fullest extent such liability may be disclaimed by law, even if the Company has been advised of the possibility of such damages, lost profits or lost revenues. In no event shall the Company's liability with respect to the Test Results exceed the amount paid to the Company by the client therefor.

Dates of Analysis:

Asbestos PLM: 08-10-2016

Service SOPs: Asbestos PLM (EPA Methods 600/R-93/116 & 600/M4-82-020, SOP EM-AS-S-1267)

EMLab ID: 1580258, Page 1 of 3EMLab P&K, LLC

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EMLab P&K 6500 McDonough Dr, Suite C-10, Norcross, GA 30093

(866) 871-1984 Fax (954) 776-8485 www.emlab.com

Client: TestAmerica-Nashville, TN C/O: Ms. Roxanne Cisneros Re: 490-108994-1; MHAFB MSA

Date of Sampling: 07-28-2016 Date of Receipt: 08-05-2016 Date of Report: 08-10-2016

ASBESTOS PLM REPORT: EPA-600/M4-82-020 & EPA METHOD 600/R-93-116

Total Samples Submitted: 8 Total Samples Analyzed: 8

Total Samples with Layer Asbestos Content > 1%: 0

Location: 2999-AS-01-Roof (490-108994-1) Lab ID-Version‡: 7330050-1

Sample Layers Asbestos Content Beige Non-Fibrous Material / Black Non-Fibrous Material ND

Sample Composite Homogeneity: Moderate

Location: 3007-AS-01-Tar (490-108994-2) Lab ID-Version‡: 7330051-1

Sample Layers Asbestos Content Gray Cementitious Material ND Black Roofing Tar and Felt ND

Composite Non-Asbestos Content: 40% Cellulose Sample Composite Homogeneity: Poor

Location: 3007-AS-02-Tar (490-108994-3) Lab ID-Version‡: 7330052-1

Sample Layers Asbestos Content Gray Cementitious Material ND Black Roofing Tar and Felt ND

Composite Non-Asbestos Content: 40% Cellulose Sample Composite Homogeneity: Poor

Location: 3007-AS-03-Sub Layer Plastic (490-108994-4) Lab ID-Version‡: 7330053-1

Sample Layers Asbestos Content Black Non-Fibrous Material ND

Tan Powdery Material ND Sample Composite Homogeneity: Moderate

EMLab ID: 1580258, Page 2 of 3EMLab P&K, LLC

The test report shall not be reproduced except in full, without written approval of the laboratory. The report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST, or any agency of the federal government. EMLab P&K reserves the right to dispose of all samples after a period of thirty (30) days, according to all state and federal guidelines, unless otherwise specified.

Inhomogeneous samples are separated into homogeneous subsamples and analyzed individually. ND means no fibers were detected. When detected, the minimum detection and reporting limit is less than 1% unless point counting is performed. Floor tile samples may contain large amounts of interference material and it is recommended that the sample be analyzed by gravimetric point count analysis to lower the detection limit and to aid in asbestos identification.

‡ A "Version" indicated by -"x" after the Lab ID# with a value greater than 1 indicates a sample with amended data. The revision number is reflected by the value of "x".

Page 9 of 14 8/10/2016

EMLab P&K 6500 McDonough Dr, Suite C-10, Norcross, GA 30093

(866) 871-1984 Fax (954) 776-8485 www.emlab.com

Client: TestAmerica-Nashville, TN C/O: Ms. Roxanne Cisneros Re: 490-108994-1; MHAFB MSA

Date of Sampling: 07-28-2016 Date of Receipt: 08-05-2016 Date of Report: 08-10-2016

ASBESTOS PLM REPORT: EPA-600/M4-82-020 & EPA METHOD 600/R-93-116

Location: 3007-AS-04-Cloth Sub Layer (490-108994-5) Lab ID-Version‡: 7330054-1

Sample Layers Asbestos Content Tan Fibrous Material ND Tan Powdery Material ND

Composite Non-Asbestos Content: 80% Synthetic Fibers Sample Composite Homogeneity: Moderate

Location: 3010-AS-01-Tar (490-108994-6) Lab ID-Version‡: 7330055-1

Sample Layers Asbestos Content Black Roofing Tar and Felt ND

Composite Non-Asbestos Content: 55% Cellulose Sample Composite Homogeneity: Poor

Location: 3010-AS-02-Fabric (490-108994-7) Lab ID-Version‡: 7330056-1

Sample Layers Asbestos Content Tan Fibrous Material ND Tan Powdery Material ND

Composite Non-Asbestos Content: 80% Synthetic Fibers Sample Composite Homogeneity: Moderate

Location: 3010-AS-03-Plastic (490-108994-8) Lab ID-Version‡: 7330057-1

Sample Layers Asbestos Content Black Non-Fibrous Material ND

Tan Powdery Material ND Sample Composite Homogeneity: Moderate

EMLab ID: 1580258, Page 3 of 3EMLab P&K, LLC

The test report shall not be reproduced except in full, without written approval of the laboratory. The report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST, or any agency of the federal government. EMLab P&K reserves the right to dispose of all samples after a period of thirty (30) days, according to all state and federal guidelines, unless otherwise specified.

Inhomogeneous samples are separated into homogeneous subsamples and analyzed individually. ND means no fibers were detected. When detected, the minimum detection and reporting limit is less than 1% unless point counting is performed. Floor tile samples may contain large amounts of interference material and it is recommended that the sample be analyzed by gravimetric point count analysis to lower the detection limit and to aid in asbestos identification.

‡ A "Version" indicated by -"x" after the Lab ID# with a value greater than 1 indicates a sample with amended data. The revision number is reflected by the value of "x".

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Login Sample Receipt Checklist

Client: CH2M Hill, Inc. Job Number: 490-108994-1

SDG Number: 2999, 3007, 3010

Login Number: 108994

Question Answer Comment

Creator: McBride, Mike

List Source: TestAmerica Nashville

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

TestAmerica Nashville Page 14 of 14 8/10/2016

TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177

TestAmerica Job ID: 490-108996-1 TestAmerica Sample Delivery Group: 2999, 3007, 3010 Client Project/Site: MHAFB MSA

For:

CH2M Hill, Inc.

322 E. Front St.

Suite 200 Boise, Idaho 83702

Attn: Mike Wirtz

Authorized for release by:

8/10/2016 1:08:58 PM

Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm

Project/Site: MHAFB MSA

TestAmerica Job ID: 490-108996-1

SDG: 2999, 3007, 3010

TestAmerica Nashville

8/10/2016

Cover Page

Table of Contents

Sample Summary

Case Narrative

Definitions

Client Sample Results

QC Sample Results

QC Association

Chronicle

Method Summary

Certification Summary

Chain of Custody

Receipt Checklists

TestAmerica Job ID: 490-108996-1Client: CH2M Hill, Inc.

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-108996-1 2999-LBP-01-roof Solid 07/28/16 00:01 08/03/16 09:55

490-108996-2 2999-LBP-02-east vent Solid 07/28/16 00:01 08/03/16 09:55

490-108996-3 2999-LBP-03-west vent Solid 07/28/16 00:01 08/03/16 09:55

490-108996-4 3007-LBP-01-vent Solid 07/28/16 00:01 08/03/16 09:55

490-108996-5 3007-LBP-02-tar Solid 07/28/16 00:01 08/03/16 09:55

490-108996-6 3010-LBP-01-vent Solid 07/29/16 00:01 08/03/16 09:55

490-108996-7 3010-LBP-02-tar Solid 07/29/16 00:01 08/03/16 09:55

TestAmerica Nashville

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Client: CH2M Hill, Inc. TestAmerica Job ID: 490-108996-1 Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Job ID: 490-108996-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative 490-108996-1

Comments

No additional comments.

Receipt

The samples were received on 8/3/2016 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 19.9º C.

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TestAmerica Nashville Page 4 of 21 8/10/2016

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Nashville

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Client Sample Results

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-1Client Sample ID: 2999-LBP-01-roof Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 22.3 0.954 0.477 mg/Kg 08/04/16 14:20 08/05/16 01:43 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

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SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-2Client Sample ID: 2999-LBP-02-east vent Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 19.6 0.969 0.484 mg/Kg 08/04/16 14:20 08/05/16 01:47 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

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SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-3Client Sample ID: 2999-LBP-03-west vent Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 23.5 1.00 0.501 mg/Kg 08/04/16 14:20 08/05/16 01:52 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

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SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-4Client Sample ID: 3007-LBP-01-vent Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 298 0.986 0.493 mg/Kg 08/04/16 14:20 08/05/16 02:05 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

Page 9 of 21 8/10/2016

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-5Client Sample ID: 3007-LBP-02-tar Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 7.44 0.992 0.496 mg/Kg 08/04/16 14:20 08/05/16 02:09 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

Page 10 of 21 8/10/2016

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-6Client Sample ID: 3010-LBP-01-vent Matrix: SolidDate Collected: 07/29/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 8600 0.992 0.496 mg/Kg 08/04/16 14:20 08/05/16 02:14 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

Page 11 of 21 8/10/2016

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Lab Sample ID: 490-108996-7Client Sample ID: 3010-LBP-02-tar Matrix: SolidDate Collected: 07/29/16 00:01

Date Received: 08/03/16 09:55

Method: 6010B - Metals (ICP)

RL MDL

Lead 5.47 0.963 0.482 mg/Kg 08/04/16 14:20 08/05/16 02:18 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Nashville

Page 12 of 21 8/10/2016

QC Sample Results

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Method: 6010B - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 490-360454/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 360541 Prep Batch: 360454

RL MDL

Lead ND 0.996 0.498 mg/Kg 08/04/16 14:20 08/05/16 00:42 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-360454/2-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 360541 Prep Batch: 360454

Lead 19.3 19.81 mg/Kg 102 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-360454/3-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 360541 Prep Batch: 360454

Lead 19.9 20.54 mg/Kg 103 80 - 120 4 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Matrix SpikeLab Sample ID: 490-108915-G-5-C MS

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 360541 Prep Batch: 360454

Lead 9.52 19.3 28.22 mg/Kg 97 75 - 125

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-108915-G-5-D MSD

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 360541 Prep Batch: 360454

Lead 9.52 19.5 28.46 mg/Kg 97 75 - 125 1 20

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

TestAmerica Nashville

Page 13 of 21 8/10/2016

QC Association Summary

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Metals

Prep Batch: 360454

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3051A490-108996-1 2999-LBP-01-roof Total/NA

Solid 3051A490-108996-2 2999-LBP-02-east vent Total/NA

Solid 3051A490-108996-3 2999-LBP-03-west vent Total/NA

Solid 3051A490-108996-4 3007-LBP-01-vent Total/NA

Solid 3051A490-108996-5 3007-LBP-02-tar Total/NA

Solid 3051A490-108996-6 3010-LBP-01-vent Total/NA

Solid 3051A490-108996-7 3010-LBP-02-tar Total/NA

Solid 3051AMB 490-360454/1-A Method Blank Total/NA

Solid 3051ALCS 490-360454/2-A Lab Control Sample Total/NA

Solid 3051ALCSD 490-360454/3-A Lab Control Sample Dup Total/NA

Solid 3051A490-108915-G-5-C MS Matrix Spike Total/NA

Solid 3051A490-108915-G-5-D MSD Matrix Spike Duplicate Total/NA

Analysis Batch: 360541

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 6010B 360454490-108996-1 2999-LBP-01-roof Total/NA

Solid 6010B 360454490-108996-2 2999-LBP-02-east vent Total/NA

Solid 6010B 360454490-108996-3 2999-LBP-03-west vent Total/NA

Solid 6010B 360454490-108996-4 3007-LBP-01-vent Total/NA

Solid 6010B 360454490-108996-5 3007-LBP-02-tar Total/NA

Solid 6010B 360454490-108996-6 3010-LBP-01-vent Total/NA

Solid 6010B 360454490-108996-7 3010-LBP-02-tar Total/NA

Solid 6010B 360454MB 490-360454/1-A Method Blank Total/NA

Solid 6010B 360454LCS 490-360454/2-A Lab Control Sample Total/NA

Solid 6010B 360454LCSD 490-360454/3-A Lab Control Sample Dup Total/NA

Solid 6010B 360454490-108915-G-5-C MS Matrix Spike Total/NA

Solid 6010B 360454490-108915-G-5-D MSD Matrix Spike Duplicate Total/NA

TestAmerica Nashville

Page 14 of 21 8/10/2016

Lab Chronicle

Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Client Sample ID: 2999-LBP-01-roof Lab Sample ID: 490-108996-1 Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.524 g 100 mL

Analysis 6010B 1 360541 08/05/16 01:43 BLG TAL NSHTotal/NA

Client Sample ID: 2999-LBP-02-east vent Lab Sample ID: 490-108996-2 Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.516 g 100 mL

Analysis 6010B 1 360541 08/05/16 01:47 BLG TAL NSHTotal/NA

Client Sample ID: 2999-LBP-03-west vent Lab Sample ID: 490-108996-3 Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.499 g 100 mL

Analysis 6010B 1 360541 08/05/16 01:52 BLG TAL NSHTotal/NA

Client Sample ID: 3007-LBP-01-vent Lab Sample ID: 490-108996-4 Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.507 g 100 mL

Analysis 6010B 1 360541 08/05/16 02:05 BLG TAL NSHTotal/NA

Client Sample ID: 3007-LBP-02-tar Lab Sample ID: 490-108996-5 Matrix: SolidDate Collected: 07/28/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.504 g 100 mL

Analysis 6010B 1 360541 08/05/16 02:09 BLG TAL NSHTotal/NA

Client Sample ID: 3010-LBP-01-vent Lab Sample ID: 490-108996-6 Matrix: SolidDate Collected: 07/29/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.504 g 100 mL

Analysis 6010B 1 360541 08/05/16 02:14 BLG TAL NSHTotal/NA

TestAmerica Nashville

Page 15 of 21 8/10/2016

Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Client Sample ID: 3010-LBP-02-tar Lab Sample ID: 490-108996-7 Matrix: SolidDate Collected: 07/29/16 00:01

Date Received: 08/03/16 09:55

Prep 3051A PG108/04/16 14:20 TAL NSH360454

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 0.519 g 100 mL

Analysis 6010B 1 360541 08/05/16 02:18 BLG TAL NSHTotal/NA

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177

TestAmerica Nashville

Page 16 of 21 8/10/2016

SDG: 2999, 3007, 3010Project/Site: MHAFB MSA

Method Method Description LaboratoryProtocol

SW8466010B Metals (ICP) TAL NSH

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177

TestAmerica Nashville

Page 17 of 21 8/10/2016

Project/Site: MHAFB MSA SDG: 2999, 3007, 3010

Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each certification below.

Authority Program EPA Region Certification ID Expiration Date

Utah TN000328NELAP 07-31-16 *

Analysis Method Prep Method Matrix Analyte

The following analytes are included in this report, but certification is not offered by the governing authority:

6010B 3051A Solid Lead

TestAmerica Nashville

* Certification renewal pending - certification considered valid.

Page 18 of 21 8/10/2016

Page 19 of 21 8/10/2016

Page 20 of 21 8/10/2016

Client: CH2M Hill, Inc. Job Number: 490-108996-1

SDG Number: 2999, 3007, 3010

Login Number: 108996

Question Answer Comment

Creator: McBride, Mike

List Source: TestAmerica Nashville

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate

HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

TestAmerica Nashville Page 21 of 21 8/10/2016

TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177

TestAmerica Job ID: 490-109934-1 TestAmerica Sample Delivery Group: Mountain Home AFB Client Project/Site: MHAFB MSA Pesticides

For:

CH2M Hill, Inc.

322 E. Front St.

Suite 200 Boise, Idaho 83702

Attn: Mike Wirtz

Authorized for release by:

8/22/2016 5:06:23 PM

Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm

Project/Site: MHAFB MSA Pesticides

TestAmerica Job ID: 490-109934-1 SDG: Mountain Home AFB

TestAmerica Nashville

8/22/2016

Cover Page

Table of Contents

Sample Summary

Case Narrative

Definitions

Client Sample Results

QC Sample Results

QC Association

Chronicle

Method Summary

Certification Summary

Chain of Custody

Receipt Checklists

TestAmerica Job ID: 490-109934-1Client: CH2M Hill, Inc.

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-109934-1 2999 Solid 08/16/16 08:45 08/17/16 09:00

490-109934-2 3007 Solid 08/16/16 08:55 08/17/16 09:00

490-109934-3 3010 Solid 08/16/16 09:15 08/17/16 09:00

TestAmerica Nashville

Page 3 of 18 8/22/2016

Client: CH2M Hill, Inc. TestAmerica Job ID: 490-109934-1 Project/Site: MHAFB MSA Pesticides SDG: Mountain Home AFB

Job ID: 490-109934-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative 490-109934-1

Comments

No additional comments.

Receipt

The samples were received on 8/17/2016 9:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 5.7º C.

GC Semi VOA Method(s) 8081A:

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TestAmerica Nashville Page 4 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Nashville

Page 5 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Lab Sample ID: 490-109934-1Client Sample ID: 2999 Matrix: SolidDate Collected: 08/16/16 08:45

Date Received: 08/17/16 09:00

Method: 8081A - Organochlorine Pesticides (GC)

RL MDL

4,4'-DDD ND 0.00166 0.000420 mg/Kg 08/18/16 11:01 08/19/16 12:19 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.00166 0.000488 mg/Kg 08/18/16 11:01 08/19/16 12:19 14,4'-DDE ND

0.00166 0.000830 mg/Kg 08/18/16 11:01 08/19/16 12:19 14,4'-DDT ND

0.00166 0.000303 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Aldrin ND

0.00166 0.000195 mg/Kg 08/18/16 11:01 08/19/16 12:19 1alpha-BHC ND

0.00166 0.000439 mg/Kg 08/18/16 11:01 08/19/16 12:19 1beta-BHC ND

0.00166 0.000420 mg/Kg 08/18/16 11:01 08/19/16 12:19 1alpha-Chlordane ND

0.0488 0.0354 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Chlordane (technical) ND

0.00166 0.000976 mg/Kg 08/18/16 11:01 08/19/16 12:19 1delta-BHC ND

0.00166 0.000390 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Dieldrin ND

0.00166 0.000459 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endosulfan I ND

0.00166 0.000537 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endosulfan II ND

0.00166 0.000488 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endosulfan sulfate ND

0.00166 0.000420 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endrin ND

0.00166 0.000498 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endrin aldehyde ND

0.00166 0.000576 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Endrin ketone ND

0.00166 0.000381 mg/Kg 08/18/16 11:01 08/19/16 12:19 1gamma-BHC (Lindane) ND

0.00166 0.000771 mg/Kg 08/18/16 11:01 08/19/16 12:19 1gamma-Chlordane ND

0.00166 0.000410 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Heptachlor ND

0.00166 0.000634 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Heptachlor epoxide ND

0.00322 0.000478 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Methoxychlor ND

0.0651 0.0412 mg/Kg 08/18/16 11:01 08/19/16 12:19 1Toxaphene ND

DCB Decachlorobiphenyl (Surr) 72 25 - 150 08/18/16 11:01 08/19/16 12:19 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Tetrachloro-m-xylene 78 08/18/16 11:01 08/19/16 12:19 121 - 145

TestAmerica Nashville

Page 6 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Lab Sample ID: 490-109934-2Client Sample ID: 3007 Matrix: SolidDate Collected: 08/16/16 08:55

Date Received: 08/17/16 09:00

Method: 8081A - Organochlorine Pesticides (GC)

RL MDL

4,4'-DDD ND 0.00335 0.000846 mg/Kg 08/18/16 11:01 08/19/16 12:31 2

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.00335 0.000984 mg/Kg 08/18/16 11:01 08/19/16 12:31 24,4'-DDE ND

0.00335 0.00167 mg/Kg 08/18/16 11:01 08/19/16 12:31 24,4'-DDT ND

0.00335 0.000610 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Aldrin ND

0.00335 0.000394 mg/Kg 08/18/16 11:01 08/19/16 12:31 2alpha-BHC ND

0.00335 0.000886 mg/Kg 08/18/16 11:01 08/19/16 12:31 2beta-BHC ND

0.00335 0.000846 mg/Kg 08/18/16 11:01 08/19/16 12:31 2alpha-Chlordane ND

0.0984 0.0714 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Chlordane (technical) ND

0.00335 0.00197 mg/Kg 08/18/16 11:01 08/19/16 12:31 2delta-BHC ND

0.00335 0.000787 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Dieldrin ND

0.00335 0.000925 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endosulfan I ND

0.00335 0.00108 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endosulfan II ND

0.00335 0.000984 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endosulfan sulfate ND

0.00335 0.000846 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endrin ND

0.00335 0.00100 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endrin aldehyde ND

0.00335 0.00116 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Endrin ketone ND

0.00335 0.000767 mg/Kg 08/18/16 11:01 08/19/16 12:31 2gamma-BHC (Lindane) ND

0.00335 0.00155 mg/Kg 08/18/16 11:01 08/19/16 12:31 2gamma-Chlordane ND

0.00335 0.000827 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Heptachlor ND

0.00335 0.00128 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Heptachlor epoxide ND

0.00649 0.000964 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Methoxychlor ND

0.131 0.0830 mg/Kg 08/18/16 11:01 08/19/16 12:31 2Toxaphene ND

DCB Decachlorobiphenyl (Surr) 73 25 - 150 08/18/16 11:01 08/19/16 12:31 2

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Tetrachloro-m-xylene 72 08/18/16 11:01 08/19/16 12:31 221 - 145

TestAmerica Nashville

Page 7 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Lab Sample ID: 490-109934-3Client Sample ID: 3010 Matrix: SolidDate Collected: 08/16/16 09:15

Date Received: 08/17/16 09:00

Method: 8081A - Organochlorine Pesticides (GC)

RL MDL

4,4'-DDD ND 0.00169 0.000427 mg/Kg 08/18/16 11:01 08/19/16 12:44 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.00169 0.000497 mg/Kg 08/18/16 11:01 08/19/16 12:44 14,4'-DDE ND

0.00169 0.000845 mg/Kg 08/18/16 11:01 08/19/16 12:44 14,4'-DDT ND

0.00169 0.000308 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Aldrin ND

0.00169 0.000199 mg/Kg 08/18/16 11:01 08/19/16 12:44 1alpha-BHC ND

0.00169 0.000447 mg/Kg 08/18/16 11:01 08/19/16 12:44 1beta-BHC ND

0.00169 0.000427 mg/Kg 08/18/16 11:01 08/19/16 12:44 1alpha-Chlordane ND

0.0497 0.0361 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Chlordane (technical) ND

0.00169 0.000994 mg/Kg 08/18/16 11:01 08/19/16 12:44 1delta-BHC ND

0.00169 0.000398 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Dieldrin ND

0.00169 0.000467 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endosulfan I ND

0.00169 0.000547 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endosulfan II ND

0.00169 0.000497 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endosulfan sulfate ND

0.00169 0.000427 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endrin ND

0.00169 0.000507 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endrin aldehyde ND

0.00169 0.000586 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Endrin ketone ND

0.00169 0.000388 mg/Kg 08/18/16 11:01 08/19/16 12:44 1gamma-BHC (Lindane) ND

0.00169 0.000785 mg/Kg 08/18/16 11:01 08/19/16 12:44 1gamma-Chlordane ND

0.00169 0.000417 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Heptachlor ND

0.00169 0.000646 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Heptachlor epoxide ND

0.00328 0.000487 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Methoxychlor ND

0.0663 0.0419 mg/Kg 08/18/16 11:01 08/19/16 12:44 1Toxaphene ND

DCB Decachlorobiphenyl (Surr) 64 25 - 150 08/18/16 11:01 08/19/16 12:44 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Tetrachloro-m-xylene 69 08/18/16 11:01 08/19/16 12:44 121 - 145

TestAmerica Nashville

Page 8 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Method: 8081A - Organochlorine Pesticides (GC)

Client Sample ID: Method BlankLab Sample ID: MB 490-363741/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 364047 Prep Batch: 363741

RL MDL

4,4'-DDD ND 0.00170 0.000430 mg/Kg 08/18/16 11:01 08/19/16 11:41 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.0005000.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 14,4'-DDE

ND 0.0008500.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 14,4'-DDT

ND 0.0003100.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Aldrin

ND 0.0002000.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1alpha-BHC

ND 0.0004500.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1beta-BHC

ND 0.0004300.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1alpha-Chlordane

ND 0.03630.0500 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Chlordane (technical)

ND 0.001000.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1delta-BHC

ND 0.0004000.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Dieldrin

ND 0.0004700.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endosulfan I

ND 0.0005500.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endosulfan II

ND 0.0005000.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endosulfan sulfate

ND 0.0004300.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endrin

ND 0.0005100.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endrin aldehyde

ND 0.0005900.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Endrin ketone

ND 0.0003900.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1gamma-BHC (Lindane)

ND 0.0007900.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1gamma-Chlordane

ND 0.0004200.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Heptachlor

ND 0.0006500.00170 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Heptachlor epoxide

ND 0.0004900.00330 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Methoxychlor

ND 0.04220.0667 mg/Kg 08/18/16 11:01 08/19/16 11:41 1Toxaphene

DCB Decachlorobiphenyl (Surr) 78 25 - 150 08/19/16 11:41 1

MB MB

Surrogate

08/18/16 11:01

Dil FacPrepared AnalyzedQualifier Limits%Recovery

83 08/18/16 11:01 08/19/16 11:41 1Tetrachloro-m-xylene 21 - 145

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-363741/16-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 364047 Prep Batch: 363741

4,4'-DDD 0.0166 0.01332 mg/Kg 80 52 - 142

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

4,4'-DDE 0.0166 0.01368 mg/Kg 83 46 - 138

4,4'-DDT 0.0166 0.01438 mg/Kg 87 25 - 150

Aldrin 0.0166 0.01373 mg/Kg 83 49 - 127 alpha-BHC 0.0166 0.01338 mg/Kg 81 49 - 127 beta-BHC 0.0166 0.01392 mg/Kg 84 44 - 130 alpha-Chlordane 0.0166 0.01428 mg/Kg 86 51 - 133 delta-BHC 0.0166 0.01358 mg/Kg 82 48 - 129

Dieldrin 0.0166 0.01334 mg/Kg 81 48 - 128

Endosulfan I 0.0166 0.01382 mg/Kg 83 51 - 124

Endosulfan II 0.0166 0.01382 mg/Kg 83 51 - 132

Endosulfan sulfate 0.0166 0.01321 mg/Kg 80 49 - 129

Endrin 0.0166 0.01426 mg/Kg 86 46 - 130

Endrin aldehyde 0.0166 0.01315 mg/Kg 79 46 - 130

Endrin ketone 0.0166 0.01256 mg/Kg 76 43 - 138 gamma-BHC (Lindane) 0.0166 0.01329 mg/Kg 80 47 - 130

TestAmerica Nashville

Page 9 of 18 8/22/2016

SDG: Mountain Home AFBProject/Site: MHAFB MSA Pesticides

Method: 8081A - Organochlorine Pesticides (GC) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-363741/16-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 364047 Prep Batch: 363741 gamma-Chlordane…