Amendment_1_Attachment_JF_Carr_Turbine_Oil_Test_Results_Rpt_2208087_Final_v1_0001.pdf

August 11, 2022

Bureau of Reclamation Gary W. Deines

Dear Gary W. Deines:

RE: CARR Turbine Oil Order No.: 2208087

FAX:

TEL: (530) 247-8552

16349 Shasta Dam Blvd Shasta Lake, CA 96019

Specialty Analytical 9011 SE Jannsen Rd

Clackamas, OR 97015

TEL: (503) 607-1331

Website: www.specialtyanalytical.com

Marty French

There were no problems with the analysis and all data for associated QC met EPA or laboratory specifications, except where noted in the Case Narrative, or as qualified with flags. Results apply only to the samples analyzed. Without approval of the laboratory, the reproduction of this report is only permitted in its entirety.

If you have any questions regarding these tests, please feel free to call.

Sincerely, Lab Director

Project: CARR Turbine Oil CLIENT: Bureau of Reclamation

8/11/2022

2208087 Date Reported:

WO#:Specialty Analytical

Analyses Result Qual Units Date AnalyzedDFRL

Lab ID: 2208087-001 Matrix: OIL Client Sample ID GB#1 Unit #2 Collection Date: 8/8/2022 9:45:00 AM

PCB'S IN OIL SW 8082A Analyst: TBSW3580A Aroclor 1016 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1221 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1232 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1242 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1248 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1254 8/10/2022 1:43:00 PM0.500 mg/Kg 10.734 Aroclor 1260 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1262 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Aroclor 1268 8/10/2022 1:43:00 PM0.500 mg/Kg 1ND Surr: Decachlorobiphenyl MI 8/10/2022 1:43:00 PM76.3 - 151 %Rec 1119

Analyses Result Qual Units Date AnalyzedDFRL

Lab ID: 2208087-002 Matrix: OIL Client Sample ID GB#2 Unit #2 Collection Date: 8/8/2022 9:45:00 AM

PCB'S IN OIL SW 8082A Analyst: TBSW3580A Aroclor 1016 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1221 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1232 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1242 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1248 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1254 8/10/2022 2:06:00 PM0.500 mg/Kg 10.716 Aroclor 1260 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1262 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Aroclor 1268 8/10/2022 2:06:00 PM0.500 mg/Kg 1ND Surr: Decachlorobiphenyl SMI 8/10/2022 2:06:00 PM76.3 - 151 %Rec 158.2

8/11/2022

2208087 Date Reported:

WO#:Specialty Analytical

Analyses Result Qual Units Date AnalyzedDFRL

Lab ID: 2208087-003 Matrix: OIL Client Sample ID GB#1 Unit #1 Collection Date: 8/8/2022 9:48:00 AM

PCB'S IN OIL SW 8082A Analyst: TBSW3580A Aroclor 1016 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1221 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1232 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1242 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1248 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1254 8/10/2022 2:30:00 PM0.500 mg/Kg 10.710 Aroclor 1260 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1262 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Aroclor 1268 8/10/2022 2:30:00 PM0.500 mg/Kg 1ND Surr: Decachlorobiphenyl SMI 8/10/2022 2:30:00 PM76.3 - 151 %Rec 159.5

Analyses Result Qual Units Date AnalyzedDFRL

Lab ID: 2208087-004 Matrix: OIL Client Sample ID GB#2 Unit #1 Collection Date: 8/8/2022 9:48:00 AM

PCB'S IN OIL SW 8082A Analyst: TBSW3580A Aroclor 1016 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1221 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1232 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1242 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1248 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1254 8/10/2022 2:53:00 PM0.500 mg/Kg 10.718 Aroclor 1260 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1262 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Aroclor 1268 8/10/2022 2:53:00 PM0.500 mg/Kg 1ND Surr: Decachlorobiphenyl SMI 8/10/2022 2:53:00 PM76.3 - 151 %Rec 158.8

8/11/2022

2208087 Date Reported:

WO#:Specialty Analytical

Analyses Result Qual Units Date AnalyzedDFRL

Lab ID: 2208087-005 Matrix: OIL Client Sample ID Blank Collection Date: 8/8/2022 11:00:00 AM

PCB'S IN OIL SW 8082A Analyst: TBSW3580A Aroclor 1016 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1221 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1232 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1242 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1248 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1254 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1260 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1262 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Aroclor 1268 8/10/2022 3:17:00 PM0.500 mg/Kg 1ND Surr: Decachlorobiphenyl SMI 8/10/2022 3:17:00 PM76.3 - 151 %Rec 156.5

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Sample Receipt Checklist Specialty Analytical 9011 SE Jannsen Rd

Clackamas, Oregon 97015

Website: www.specialtyanalytical.com

TEL: 503-607-1331 FAX: 503-607-1336

Client Name BUREAU_OF_REC Work Order Number 2208087

Date and Time Receive 8/10/2022 10:57:30 AM Received by: Julie ClayRcptNo: 1

Completed by Reviewed by:

Carrier name: FedEx

Custody seals intact on sample bottles? Yes No Not Present

Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Not Present

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No Was an attempt made to cool the samples? Yes No NA

Yes No No VialsWater - Were bubbles absent in VOC vials?

Adjusted? Checked by

Any No and/or NA (not applicable) response must be detailed in the comments section be

Are matrices correctly identified on Chain of custody? Yes No

Custody Seals present? Yes No

Sample Tags Present? Yes No Sample Tags Listed on COC? Yes No

Completed Date: 8/10/2022 10:58:59 AM Reviewed Date: 8/11/2022 11:18:53 AM

Is it clear what analyses were requested? Yes No

Were correct preservatives used and noted? Yes No NA

Were container lables complete (ID, Pres, Date)? Yes No

All samples received at a temp. of > 0° C to 6.0° C? Yes No NA Response when temperature is outside of range:

Preservative added to bottles:

Approved by client.

Sample Temp. taken and recorded upon receipt? Yes No ºC22.3To

Yes No NAWater - Was there Chlorine Present?

Yes No NAWater - pH acceptable upon receipt?

Are Samples considered acceptable? Yes No

Traffic Report or Packing Lists present? Yes No Air Bill Sticker Not PresentAirbill or Sticker?

Airbill No:

Tag Numbers:

Intact Broken LeakingSample Condition?

Case Number: SDG: SAS:

Sample Receipt Checklist Specialty Analytical 9011 SE Jannsen Rd

Clackamas, Oregon 97015

Website: www.specialtyanalytical.com

TEL: 503-607-1331 FAX: 503-607-1336

Client Contacted? Yes No NA Person Contacted:

Contact Mode: Phone: Fax: Email: In Person:

Client Instructions:

Date Contacted: Contacted By:

Regarding:

Comments:

CorrectiveAction:

8/11/2022

Definition Only 2208087

Date:

WO#:

Definitions:

Specialty Analytical 9011 SE Jannsen Rd

Clackamas, Oregon 97015

Website: www.specialtyanalytical.com

TEL: 503-607-1331 FAX: 503-607-1336

KEY TO FLAGS

A: This sample contains a Gasoline Range Organic not identified as a specific hydrocarbon product. The result was qualified against gasoline calibration standards.

A1: This sample contains a Diesel Range Organic not identified as a specific hydrocarbon product.

The result was qualified against diesel calibration standards.

A2: This sample contains a Lube Oil Range Organic not identified as a specific hydrocarbon product. The result was qualified against lube oil calibration standards.

A3: The results was determined to be Non-Detect based on hydrocarbon pattern recognition. The product was carry-over from another hydrocarbon type.

A4: The product appears to be aged or degraded.

B: The blank exhibited a positive result greater than the reporting limit for this compound.

CN: See Case Narrative.

E: Result exceeds the calibration range for this compound. The result should be considered an estimate.

F: The positive result for this hydrocarbon is due to single component contamination. The product does not match any hydrocarbon in the fuels library.

FS: Follow-up testing is suggested.

G: Result may be biased high due to biogenic interferences. Clean up is recommended.

H: Sample was analyzed outside recommended holding time.

HT: � At client’s request, samples was analyzed outside of recommended holding time.

HP: Sample was analyzed outside recommended holding time due to VOA having pH >2.

J: The results for this analyte is between the MDL and the PQL and should be considered an

2208087

Date:

WO#:

Definitions:

Specialty Analytical 9011 SE Jannsen Rd

Clackamas, Oregon 97015

Website: www.specialtyanalytical.com

TEL: 503-607-1331 FAX: 503-607-1336

estimated concentration.

K: Diesel result is biased high due to amount of Oil contained in the sample.

L: Diesel result is biased high due to amount of Gasoline contained in the sample.

M: Oil result is biased high due to amount of Diesel contained in the sample.

N : Gasoline result is biased high due to amount of Diesel contained in the sample.

MC: Sample concentration is greater than 4x the spiked value, the spiked value is considered insignificant.

MI : Result is outside control limits due to matrix interference.

NH: Sample matrix is non-homogeneous

MSA: Value determined by Method of Standard Addition.

O: Laboratory Control Standard (LCS) exceeded laboratory control limits but meets CCV criteria.

Data meets EPA requirements.

Q: Detection levels elevated due to sample matrix.

R: RPD control limits were exceeded

RF : Duplicate failed due to result being at or near the method-reporting limit.

RP: Matrix spike values exceed established QC limits; post digestion spike is in control.

S: Recovery is outside control limits.

SC: CCV or LCS exceeded high recovery control limits, but associated samples are non-detect. Data meets EPA requirements.

SL: LCS exceeded recovery control limits, but associated MS/MSD passing. Data meets EPA requirements.

2208087

Date:

WO#:

Definitions:

Specialty Analytical 9011 SE Jannsen Rd

Clackamas, Oregon 97015

Website: www.specialtyanalytical.com

TEL: 503-607-1331 FAX: 503-607-1336

TA: Sample treated with ascorbic acid for the removal of thiocyanates.