Hazardous Substances Results El Morro SAJU_0001.pdf
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- HAZARDOUS MATERIALS DISPOSAL
- Solicitation number
- 140P5421Q0027
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| File | Type | Posted |
|---|---|---|
| ADDENDUM TO SOW_0001.pdf | ||
| Sol_140P5421Q0027_Amd_0001.pdf | ||
| QUESTIONS_0001.pdf | ||
| Access and Parking to El Morro.pdf | ||
| Wage Rate Determination.pdf | ||
| SOW.pdf | ||
| Sol_140P5421Q0027.pdf |
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PO Box 3545 Bayamón, PR 00958 Ph (787)376-9010 Fax (787)995-0005 hpena@zimmetry.com www.zimmetry.com
December 4, 2020
Jan M. Torres Park Curator San Juan National Historic Site 501 Calle Norzagaray San Juan, Puerto Rico
Re: Water Sampling at San Juan Historic Site at El Morro Powder Magazine & Casamata, San Juan, PR
Dear Mr. Torres:
A sampling for chemical substances was performed on 6 November of 2020 at the San Juan National Historic Site El Morro. Two sites were identified were the materials are stored: Powder Magazine in El Morro at Casamata, San Juan Puerto Rico.
The purpose of this sampling was to collect and analyze the chemical substances located at several containers which preserve historic artillery ammunition to determine whether the substances are hazardous for disposal purposes. The parameters measured where RCI (Reactivity, Corrosivity, Ignitability) and TCLP Metals (Toxicity Leachate Procedure) in compliance with local, state and federal regulations and standards, established by EPA and the local agencies for the proper management of hazardous and non-hazardous waste. The sampling and analysis was performed by Sanco Laboratories, Inc. and the results were evaluated by Milagros Caraballo Vargas and Harry Peña Ruiz.
A total of eighteen (18) samples were analyzed by Sanco Laboratories, Inc. in San Juan Puerto Rico.
Thirteen (13) samples of the containers resulted above the allowed levels and shall be disposed as hazardous material in compliance with the RCRA. Attached find the analytical results and chain of custody.
Sampling Materials:
1. Clear PVC Bailer
2. Sample bottle
3. Bucket
4. Gloves
5. Sharpie
6. Book
7. Chain Custody
8. Ice
9. Collection container
10. Fridge
ZIMMETRY ENVIRONMENTAL MANAGEMENT CORP.
San Juan Historic Site Water Sampling
El Morro Powder Magazine & Casamata San Juan, PR
Procedure:
All storage containers were labeled with a unique identification number, starting from 001 to 018. In each container two types of extraction and sampling were carried out. The first was to identify RCI and the second was to identify TCLP Metals. Each sampling bottle was previously identified with date, time, sampling location and description of the type of sample to be carried out in the same way as its chain of custody. 1.0 L of the chemical substance contained in the containers and a solid sample of a partition wood from one of the containers were collected in each sampling bottle.
Twelve (12) samples were collected at the Powder Magazine storage and six (6) at the Casamata storage. Seventeen (17) samples were collected and a Clear PVC Bailer was used for the extraction of the chemical substance, where the previously identified sampling bottles were completely filled, and quickly capped after each collection. Fifteen (15) containers were identified that contained liner and three (3) that did not. The containers that did not contain liner were of the following samples:
001, 003 and 016.
Results:
The following samples results are above the regulatory limits and are considered as a hazardous waste.
Thirteen (13) samples resulted above of the levels allowed. Seven (7) samples were positive for RCI (SJHS-002, SJHS-004, SJHS-010, SJHS-014, SJHS-015, SJHS-017 and SJHS-018), presenting Corrosivity parameters (EPA HW No. D002).
Eight (8) samples resulted positive for TCLP Metals. The samples: SJHS-001, SJHS-003, SJHS-004, SJHS-008, SJHS-014 and SJHS-016 resulted with levels of Chromium above the regulatory limit (EPA HW No. D007) and samples: SJHS-005 and SJHS-006 resulted with Lead levels above the regulatory limit (EPA HW No. D008).
El Morro Powder Magazine & Casamata San Juan, PR
Table 1‐1: Summary of Components Positive of TCLP & RCI
Log Number Sample Type of Analysis
Positive Toxic Substance Limit Result
Quantities
201109K001 SJHS‐001 TCLP Metals Chromium 5.0 mg/l 10.0 180 gal.
201109K002 SJHS‐002 RCI Corrosivity 2‐12.5 Std. Units 12.9 194.5 gal.
201109K003 SJHS‐003 TCLP Metals Chromium 5.0 mg/l 8.40 165 gal.
201109K004 SJHS‐004
RCI Corrosivity 2‐12.5 Std. Units 12.6
180 gal.
TCLP Metals Chromium 5.0 mg/l 9.80
201109K005 SJHS‐005 TCLP Metals Lead 5.0 mg/l 13.40 201 gal.
201109K007 SJHS‐007 TCLP Metals Lead 5.0 mg/l 7.20 216 gal.
201109K008 SJHS‐008 TCLP Metals Chromium 5.0 mg/l 5.3 165 gal.
201109K001
SJHS‐010 RCI Corrosivity 2‐12.5 Std. Units 12.7 180 gal.
201109K014 SJHS‐014
RCI Corrosivity 2‐12.5 Std. Units 12.8
187 gal.
TCLP Metals Chromium 5.0 mg/l 11.3
201109K015 SJHS‐015 RCI Corrosivity 2‐12.5 Std. Units 12.7 209 gal.
201109K016
(S‐Solid) SJHS‐016 TCLP Metals Chromium 5.0 mg/l 6.9 1.4 sqt.
201109K001
SJHS‐017 RCI Corrosivity 2‐12.5 Std. Units 12.80 247 gal.
201109K001
SJHS‐018 RCI Corrosivity 2‐12.5 Std. Units 12.80 224 gal.
El Morro Powder Magazine & Casamata San Juan, PR
APPENDIX A: CHAIN OF CUSTODY AND LABORATORY
RESULTS
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine
El Morro Powder Magazine Site Reference
El Morro Powder Magazine Site Reference
El Morro Powder Magazine Site Reference
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-001
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-001
El Morro Powder Magazine Sampling SJHS-001
El Morro Powder Magazine Sampling SJHS-001
Sampling SJHS-002
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-002
El Morro Powder Magazine Sampling SJHS-003
El Morro Powder Magazine Sampling SJHS-003
Sampling SJHS-003
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-004
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-004
El Morro Powder Magazine Sampling SJHS-004
El Morro Powder Magazine Sampling SJHS-004
Sampling SJHS-005
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-006
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-007
El Morro Powder Magazine Sampling SJHS-007
El Morro Powder Magazine Sampling SJHS-007
Sampling SJHS-007
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-008
El Morro Powder Magazine Sampling SJHS-008
El Morro Powder Magazine Sampling SJHS-008
Sampling SJHS-008
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-009
El Morro Powder Magazine Sampling SJHS-009
El Morro Powder Magazine Sampling SJHS-009
Sampling SJHS-009
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-010
Sampling SJHS-010
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-010
El Morro Powder Magazine Sampling SJHS-010
El Morro Powder Magazine Sampling SJHS-011
Sampling SJHS-011
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-011
El Morro Powder Magazine Sampling SJHS-011
El Morro Powder Magazine Sampling SJHS-011
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-012
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Powder Magazine Sampling SJHS-12
El Morro Powder Magazine Sampling SJHS-012
El Morro Powder Magazine Sampling SJHS-012
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Casamata
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Site Reference
El Morro Casamata Site Reference
El Morro Casamata Sampling SJHS-013
Sampling SJHS-013
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-013
El Morro Casamata Sampling SJHS-013
El Morro Casamata Sampling SJHS-013
Sampling SJHS-014
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-014
El Morro Casamata Sampling SJHS-014
El Morro Casamata Sampling SJHS-014
Sampling SJHS-014
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-014
El Morro Casamata Sampling SJHS-015
El Morro Casamata Sampling SJHS-015
Sampling SJHS-015
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-015
El Morro Casamata Sampling SJHS-015
El Morro Casamata Sampling SJHS-015
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
Sampling SJHS-016
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-016
El Morro Casamata Sampling SJHS-016
El Morro Casamata Sampling SJHS-016
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-016
El Morro Casamata Sampling SJHS-016
El Morro Casamata Sampling SJHS-017
Sampling SJHS-017
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-018
El Morro Casamata Sampling SJHS-018
El Morro Casamata Sampling SJHS-018
Sampling SJHS-018
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-018
El Morro Casamata Sampling SJHS-018
El Morro Casamata Sampling SJHS-018
Sampling SJHS-018
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
El Morro Casamata Sampling SJHS-018
Sampling Materials
Sampling Materials
Sampling Transport
El Morro Powder Magazine & Casamata San Juan, PR
Photographic documentation is for reference purposes and doesn't necessarily include all the surfaces with lead based paint and/or components containing lead
APPENDIX B: PROJECT PHOTOGRAPHS
Sampling Transport
El Morro Powder Magazine & Casamata San Juan, PR
APPENDIX C: LOCATION OF POSITIVE MATERIALS
| morro process Letter Report.pdf |
| 201109K011 ZIMMETRY Historic Site El Morro 11 09 2020.pdf |
| 201109K016 ZIMMETRY Historic Site El Morro 11 09 2020.pdf |
| 201109K001 ZIMMETRY Historic Site El Morro 11 09 2020.pdf |
| Appendix B Photo 1.pdf |
| Appendix B Photo 2.pdf |
| El Morro Powder Magazine Layout1 (1).pdf |
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