Rpt_1712662_Chichiltah_N_N_IOC_Cn_Na_F_0002.pdf

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CHICHILTAH BS LANDFILL CLEAN CLOSURE
Solicitation number
140A0922Q0049
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This document contains an analytical report from Hall Environmental Analysis Laboratory regarding water quality testing of two wells, Well 646 and Well 647, located at the Chichiltah BS Landfill in New Mexico. The report provides results of tests conducted on samples from the two wells for compounds including nitrites, nitrates, metals, and anions. Testing was performed using EPA methods 200.7, 200.8, 245.1 and 300.0. The report also includes quality control sample results. Accompanying the analytical report is a related federal contract opportunity notice for clean closure of the Chichiltah BS Landfill located in New Mexico. The solicitation is identified as number 140A0922Q0049 and is issued by the Department of the Interior Bureau of Indian Affairs Navajo Region.

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January 17, 2018

Division of Env. Cultural & Safety Mgmt.

Genevieve Henry

Dear Genevieve Henry:

RE: Chichiltah BS 093534005 OrderNo.: 1712662

FAX (505) 863-8369

TEL: (505) 863-8330

PO Box 1060 Room 130 Gallup, NM 87305

Hall Environmental Analysis Laboratory 4901 Hawkins NE

Albuquerque, NM 87109

Website: www.hallenvironmental.com

TEL: 505-345-3975 FAX: 505-345-4107

Hall Environmental Analysis Laboratory received 2 sample(s) on 12/12/2017 for the analyses presented in the following report.

Andy Freeman

These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. In order to properly interpret your results, it is imperative that you review this report in its entirety.

See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag.

When necessary, data qualifiers are provided on both the sample analysis report and the QC summary report, both sections should be reviewed. All samples are reported, as received, unless otherwise indicated. Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH and residual chlorine are qualified as being analyzed outside of the recommended holding time.

Please don't hesitate to contact HEAL for any additional information or clarifications.

ADHS Cert #AZ0682 -- NMED-DWB Cert #NM9425 -- NMED-Micro Cert #NM0190

Sincerely, Laboratory Manager 4901 Hawkins NE Albuquerque, NM 87109 http://www.hallenvironmental.com http://www.hallenvironmental.com

Location:

Matrix: Aqueous

Collection Date: 12/11/2017 11:00:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-001A

Client Sample ID: Well 646

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 300.0: ANIONS Analyst: MRA SDWIS Date Analyzed

Nitrogen, Nitrite (As N) 12/12/2017 8:03:40 PM0.10 mg/L 11.0ND1041 Nitrogen, Nitrate (As N) 12/12/2017 8:03:40 PM0.10 mg/L 110ND1037

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range PQL Practical Quanitative Limit RL Reporting Detection Limit

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Collection Date: 12/11/2017 11:00:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-001B

Client Sample ID: Well 646

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 200.7: METALS Analyst: pmf SDWIS Date Analyzed

Barium 1/2/2018 8:17:49 PM0.0020 mg/L 12.00.291010 Beryllium 1/2/2018 8:17:49 PM0.0020 mg/L 10.0040ND1075 Cadmium 1/2/2018 8:17:49 PM0.0020 mg/L 10.0050ND1015 Chromium 1/2/2018 8:17:49 PM0.0060 mg/L 10.10ND1020 Sodium 1/2/2018 8:17:49 PM1.0 mg/L 1241052

EPA 200.8: METALS Analyst: JLF SDWIS Date Analyzed

Antimony 1/5/2018 2:47:49 PM0.0010 mg/L 10.0060ND1074 Arsenic 1/5/2018 2:47:49 PM0.0010 mg/L 10.0100.00191005 Selenium 1/12/2018 5:03:39 PM0.0050 mg/L 50.050ND1045 Thallium 12/28/2017 8:05:34 PM0.00050 mg/L 10.0020ND1085

EPA METHOD 245.1: MERCURY Analyst: MED SDWIS Date Analyzed

Mercury 1/5/2018 11:51:30 AM0.00020 mg/L 10.0020ND1035

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Collection Date: 12/11/2017 11:00:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-001C

Client Sample ID: Well 646

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 300.0: ANIONS Analyst: MRA SDWIS Date Analyzed

Fluoride 12/15/2017 1:53:33 AM0.10 mg/L 14.00.111025

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Collection Date: 12/11/2017 11:15:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-002A

Client Sample ID: Well 647

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 300.0: ANIONS Analyst: MRA SDWIS Date Analyzed

Nitrogen, Nitrite (As N) 12/12/2017 8:28:31 PM0.10 mg/L 11.0ND1041 Nitrogen, Nitrate (As N) 12/12/2017 8:28:31 PM0.10 mg/L 110ND1037

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Collection Date: 12/11/2017 11:15:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-002B

Client Sample ID: Well 647

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 200.7: METALS Analyst: pmf SDWIS Date Analyzed

Barium 1/2/2018 8:25:46 PM0.0020 mg/L 12.00.391010 Beryllium 1/2/2018 8:25:46 PM0.0020 mg/L 10.0040ND1075 Cadmium 1/2/2018 8:25:46 PM0.0020 mg/L 10.0050ND1015 Chromium 1/2/2018 8:25:46 PM0.0060 mg/L 10.10ND1020 Sodium 1/2/2018 8:25:46 PM1.0 mg/L 1401052

EPA 200.8: METALS Analyst: JLF SDWIS Date Analyzed

Antimony 1/5/2018 2:54:22 PM0.0010 mg/L 10.0060ND1074 Arsenic 1/5/2018 3:00:56 PM0.0050 mg/L 50.010ND1005 Selenium 1/12/2018 5:08:33 PM0.010 mg/L 100.050ND1045 Thallium 12/28/2017 8:12:08 PM0.00050 mg/L 10.0020ND1085

EPA METHOD 245.1: MERCURY Analyst: MED SDWIS Date Analyzed

Mercury 1/5/2018 11:53:31 AM0.00020 mg/L 10.0020ND1035

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Collection Date: 12/11/2017 11:15:00 AMFacility: CHICHILT

Analyses Result Qual Units

CLIENT: Division of Env. Cultural & Safety

Lab ID: 1712662-002C

Client Sample ID: Well 647

1/17/2018

Analytical Report 1712662

Date Reported:

Lab Order:

Received Date: 12/12/2017 12:55:00 PM Compliance Safe:

RL MCL DF

Hall Environmental Analysis Laboratory, Inc.

EPA METHOD 300.0: ANIONS Analyst: MRA SDWIS Date Analyzed

Fluoride 12/15/2017 2:18:21 AM0.10 mg/L 14.00.121025

Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

Project: Chichiltah BS 093534005 Client: Division of Env. Cultural & Safety Mgmt.

17-Jan-18

QC SUMMARY REPORT 1712662WO#:

Hall Environmental Analysis Laboratory, Inc.

Sample ID MB-B

Batch ID: B48123

Analysis Date: 1/2/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 48123

SeqNo: 1544026

MBLKSampType: TestCode: EPA Method 200.7: Metals

Barium 0.0020ND Beryllium 0.0020ND Cadmium 0.0020ND Chromium 0.0060ND Sodium 1.0ND

Sample ID LCS-B

Batch ID: B48123

Analysis Date: 1/2/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 48123

SeqNo: 1544030

LCSSampType: TestCode: EPA Method 200.7: Metals

Barium 0.5000 97.4 85 1150.0020 00.49 Beryllium 0.5000 104 85 1150.0020 00.52 Cadmium 0.5000 99.1 85 1150.0020 00.50 Chromium 0.5000 101 85 1150.0060 00.51 Sodium 50.00 101 85 1151.0 050

Qualifiers:

* Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

17-Jan-18

QC SUMMARY REPORT 1712662WO#:

Hall Environmental Analysis Laboratory, Inc.

Sample ID LCS

Batch ID: A48088

Analysis Date: 12/28/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 48088

SeqNo: 1541519

LCSSampType: TestCode: EPA 200.8: Metals

Thallium 0.01250 96.2 85 1150.00050 00.012

Sample ID MB

Batch ID: A48088

Analysis Date: 12/28/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 48088

SeqNo: 1541521

MBLKSampType: TestCode: EPA 200.8: Metals

Thallium 0.00050ND

Sample ID MB

Batch ID: B48247

Analysis Date: 1/5/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 48247

SeqNo: 1549248

MBLKSampType: TestCode: EPA 200.8: Metals

Antimony 0.0010ND Arsenic 0.0010ND

Sample ID LCS

Batch ID: B48247

Analysis Date: 1/5/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 48247

SeqNo: 1549250

LCSSampType: TestCode: EPA 200.8: Metals

Antimony 0.02500 98.9 85 1150.0010 00.025 Arsenic 0.02500 98.7 85 1150.0010 00.025

Sample ID MB

Batch ID: B48432

Analysis Date: 1/12/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 48432

SeqNo: 1557035

MBLKSampType: TestCode: EPA 200.8: Metals

Selenium 0.0010ND

Sample ID LCS

Batch ID: B48432

Analysis Date: 1/12/2018Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 48432

SeqNo: 1557037

LCSSampType: TestCode: EPA 200.8: Metals

Selenium 0.02500 95.3 85 1150.0010 00.024

Qualifiers:

* Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

17-Jan-18

QC SUMMARY REPORT 1712662WO#:

Hall Environmental Analysis Laboratory, Inc.

Sample ID MB-35848

Batch ID: 35848

Analysis Date: 1/5/2018Prep Date: 1/4/2018

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 48223

SeqNo: 1548379

MBLKSampType: TestCode: EPA Method 245.1: Mercury

Mercury 0.00020ND

Sample ID LCS-35848

Batch ID: 35848

Analysis Date: 1/5/2018Prep Date: 1/4/2018

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 48223

SeqNo: 1548380

LCSSampType: TestCode: EPA Method 245.1: Mercury

Mercury 0.005000 99.8 80 1200.00020 00.0050

Qualifiers:

* Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

17-Jan-18

QC SUMMARY REPORT 1712662WO#:

Hall Environmental Analysis Laboratory, Inc.

Sample ID MB

Batch ID: R47752

Analysis Date: 12/12/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 47752

SeqNo: 1526658 mblkSampType: TestCode: EPA Method 300.0: Anions

Nitrogen, Nitrite (As N) 0.10ND Nitrogen, Nitrate (As N) 0.10ND

Sample ID LCS

Batch ID: R47752

Analysis Date: 12/12/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 47752

SeqNo: 1526659 lcsSampType: TestCode: EPA Method 300.0: Anions

Nitrogen, Nitrite (As N) 1.000 96.7 90 1100.10 00.97 Nitrogen, Nitrate (As N) 2.500 98.5 90 1100.10 02.5

Sample ID MB

Batch ID: A47810

Analysis Date: 12/15/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW RunNo: 47810

SeqNo: 1529397 mblkSampType: TestCode: EPA Method 300.0: Anions

Fluoride 0.10ND

Sample ID LCS

Batch ID: A47810

Analysis Date: 12/15/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: LCSW RunNo: 47810

SeqNo: 1529398 lcsSampType: TestCode: EPA Method 300.0: Anions

Fluoride 0.5000 105 90 1100.10 00.53

Sample ID 1712662-002CMS

Batch ID: A47810

Analysis Date: 12/15/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: Well 647 RunNo: 47810

SeqNo: 1529408 msSampType: TestCode: EPA Method 300.0: Anions

Fluoride 0.5000 98.8 68.4 1120.10 0.12120.62

Sample ID 1712662-002CMSD

Batch ID: A47810

Analysis Date: 12/15/2017Prep Date:

Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: Well 647 RunNo: 47810

SeqNo: 1529409 msdSampType: TestCode: EPA Method 300.0: Anions

Fluoride 0.5000 99.9 68.4 112 200.10 0.1212 0.8490.62

Qualifiers:

* Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank D Sample Diluted Due to Matrix E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit P Sample pH Not In Range

S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of limit as specified

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BaseRpt-Hall-Chem-DW
SubContractor_1712662_DOC011718-002_v1.pdf
HALL - QC_ByTestCodeRpt_Ext
COC_1712662_1712662_v1.pdf

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