WRA-3073EXHIBITD.pdf

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Attached to
Removal of Hazardous Waste and Oil/Water Separator Maintenance Deer Island Treatment Plant
Solicitation number
S119219-vCurrent
Issued by
Suffolk County, Woburn City, Massachusetts

About this file

This document is an Exhibit D that details the removal of hazardous waste streams from the Deer Island Treatment Plant (DITP). The exhibit lists various test codes, accumulation streams, and process streams associated with the analysis and disposal of aqueous, flammable, chlorinated, and combined waste samples. The document outlines the specific testing procedures, sample preparation methods, and analytical techniques used to characterize and manage the DITP's hazardous waste streams.

The exhibit provides a comprehensive overview of the various waste stream sources, their chemical compositions, and the appropriate handling and disposal protocols. This information is essential for ensuring compliance with environmental regulations and maintaining the safe operation of the DITP's waste management processes.

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Removal of Hazardous Waste DITP Waste Stream Sources Exhibit D

Sat. # Tests/Testcode Accumulation Stream Process Stream 316C-A1-1-0 BOD Aqueous Acidic Demand 1 316C-A6-1-0 COD Vials Aqueous Acidic Demand 1 316A-B1-1-0 TKN (spare) Aqueous Acidic Distillation & Digestion 1 421-B5-1-0 PHC Aqueous Acidic Extraction 1 421-E1-1-0 HAA Aqueous Acidic- CONTAINS MTBE * HAA Extraction 1 326-A1-1-0 Cr6-AQUVV Aqueous Acidic Hex Chrome Analysis 1 331-F1-1-0 ICP, GFA,HG Aqueous Acidic Metals Analysis 1 327-B1-1-0 ICP, GFA,HG Aqueous Acidic Metals Digestion 1 421-C6-1-0 PESAQ608 Aqueous Acidic PCB cleanups 1

316A-G1-1-0 Phenol, Nitrate/ite, Phos, TP/TN, TDN/TDP Aqueous Acidic Skalar-Colorimetry 1

316A-E1-1-0 Phenol, NO3, NO2, Phos, TN/TP (spare) Aqueous Acidic Skalar-Colorimetry 1

316A-F1-1-0 Phenol, NO3, NO2, Phos, TN/TP, TDN/TDP Aqueous Acidic Skalar-Colorimetry 1

325-B1-1-0 SLF-AQTCO Aqueous Acidic Sulfide Titration 1 437-D2-1-0 Microtox Aqueous Acidic Toxicity analysis 1 421-C6-2-0 FORMAQHLC Non-chlorinated aqueous LC1050 2 447-A1-2-0 VOA-AQ624 Non-chlorinated aqueous Spent samples 2 138-A4-3-0 Disposal Aqueous Basic Disposal 3 316A-B1-3-0 TKN Aqueous Basic Distillation & Digestion 3 316B-A1-3-0 Cl-, SO4 Aqueous Basic Ion chromatography 3 316A-G2-3-0 CN Aqueous Basic Skalar-Colorimetry 3 316A-F1-3-0 NH3 Aqueous Basic Skalar-Colorimetry 3 316A-G1-3-0 NH3 Aqueous Basic Skalar-Colorimetry 3

316A-E1-3-0 Phenol, NO3, NO2, Phos, TN/TP, TDN/TDP (spare) Aqueous Basic Skalar-Colorimetry 3

327-A1-3-0 Ag--AQFAA Aqueous Basic Special Silver Analysis 3 326-A2-3-0 SLF-AQUVV Aqueous Basic Sulfide Colorimetric 3 437-D1-4-0 Chlorophyll Flammable Solvents Extraction (filter grinding) 4 421-B4-4-0 * FOG-AQSPE Aqueous Flammable HEM Analysis 4 316B-A1-4-0 MeOH Flammable Solvents Ion chromatography 4 447-A1-4-0 VOA-AQ625 Flammable Solvents MeOH rinse 4 421-B4-4-0 MBAS Flammable Solvents Separatory Funnels 4 421-D4-4-0 PESAQ608 Flammable Solvents Solvent Exchange 4 448-A1-4-0 ABN/PAH Flammable Solvents Waste Pump Oil 4 421-B5-5-0 PHC Chlorinated Solvents Extraction 5 421-D1-5-0 PES/ABN Chlorinated Solvents Extraction/TVAP 5 421-B3-5-0 MBAS Chlorinated Solvents Separatory Funnels 5

Removal of Hazardous Waste DITP Waste Stream Sources Exhibit D

Sat. # Tests/Testcode Accumulation Stream Process Stream 421-D3-6-0 PES, ABN, FORM Chlorinated acidic aqueous Separatory Funnel 6 421-D3-6-1 PES, ABN, FORM Chlorinated acidic aqueous Separatory Funnel 6 421-B3-6-0 MBAS Chlorinated acidic aqueous Separatory Funnels 6 327-B1-7-0 HG Stannous Chloride Mercury Analysis 7 421-A4-8A-0 PHC Combined GC Injection Vials Extraction 8A 420-A1-8A-0 PES Combined GC Injection vials GC Analysis 8A 448-A1-8A-0 ABN/PAH Combined GC Injection vials GC Autosampler 8A

325-A1-8B-0 Particulate N+C, CHN Combined General Solids CHN Analyzer Thermal Conductivity 8B 421-B3-8B-0 PHC Combined General Solids Extraction 8B 421-A4-8B-0 PHC, FOG Combined General Solids Extraction 8B 421-D2-8B-0 PES/ABN/HAA Combined General Solids Extraction/TVAP 8B 421-A4-8B-0 ** FOG-AQSPE Solid Waste HEM Analysis 8B

Definition of Abbreviations:

BOD Biochemical Oxygen Demand CN cyanide COD Chemical Oxygen Demand NH3 ammonia TKN Total Kjeldahl Nitrogen Ag--AQFAA silver PHC Petroleum Hydrocarbons TVAP turbovap HAA Haloacetic acids Cr6-AQUVV Hexavalent chromium

ICP, GFA,HG

inductively coupled plasma, graphite furnace atomic absorption, mercury

PESAQ608 pesticides Phenol, Nitrate/ite, Phos, TP/TN, TDN/TDP total phosphorus, total nitrogen, total dissolved nitrogen, total dissolved phosphorus

Phenol, NO3, NO2, Phos, TN/TP (spare) nitrate, nitrite SLF-AQTCO sulfide FORMAQHLC formadehyde VOA-AQ624 volatile organic analysis Cl-, SO4 chloride, sulfate FOG-AQSPE fats, oils, and grease MeOH methanol MBAS methylene blue active substances ABN/PAH acid base neutrals, polyaromatic hydrocarbons Particulate N+C, CHN nitrogen + carbon, carbon, hydrogen, nitrogen GC Analysis gas chromatography HEM Analysis hexane extractable material

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