A21_Technical_Exhibit_2B(Sample_preservation_and_holding_times).docx

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W91QVN19R0147
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Technical Exhibit 2B

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Technical Exhibit 2B

Sample preservation and holding times

Parameter
Unit
Container
Preservative
Holding

time Accreditation

Number of Container(s)
GROUP
Type
Size
MS/MSD or MD
Total
n-Hexane extract, mineral oil
mg/L
PE/Glass
1L
HCl, pH <2
28 days
WQMA
─
x 2
3
A
n-Hexane extract, animal/vegetable oil
mg/L
PE/Glass
1L
HCl, pH <2
28 days
WQMA
─
x 2
3
B
Phenol
mg/L
Glass
1L
Copper sulfate,

Phosphoric acid

28 days
WQMA
pH<2, 4℃
x 2
3
C
Cyanide
mg/L
PE/Glass
1L
NaOH,

12 pellets

14 days
WQMA
pH>12, 4℃
x 1
2
D
Metals, Recoverable
Chromium
mg/L
PE
125mL
HNO3, pH <2
180 days

WQMA

pH<2, 4℃
x 1
2
E

Zinc

Copper

Cadmium

Arsenic

Lead

Mercury

28 days
WQMA
Metals, Dissolved
Soluble iron
mg/L
PE
125mL
pH <2
180 days

WQMA

MUST filter (0.45㎛) after collecting

x 1
2
F

Soluble manganese

Organic phosphorous
mg/L
Amber Glass
1 L
pH5~8, with NaOH, H2SO4
ext 7 days

anl14days

WQMA
4℃
x 2
3
G
Hexavalent Chromium
mg/L
PE
1L
None
24 hours
WQMA
4℃
x 1
2

H

Total suspended solids
mg/L
PE/Glass
None
7 days
WQMA
Fluoride
mg/L
PE
None
28 days
WQMA
PCB
mg/L
Amber Glass
1L
None
ext 7 days

anl14days

WQMA
4℃
x 2
3
I
Coliform bacteria
numbers

/mL

sterilized PE
1L
None
24hr
WQMA
<4℃
x 1
2
J
Total nitrogen
mg/L
PE/Glass
1L
H2SO4
28 days
WQMA
pH<2, 4℃
X 2
3
K
Total phosphorus
mg/L

WQMA

Parameter
Unit
Container
Preservative
Holding

time Accreditation

Number of Container(s)
GROUP
VOCs
Trichloroethylene
mg/L
Amber Glass
40 mL
HCl, pH <2
14 days
WQMA
4℃
x 2

L L

Tetrachloroethylene
mg/L
Alkyl benzene sulfonate (ABS)
mg/L
PE/Glass
500mL
None
48 hr
WQMA
4℃
x 2
3
M
pH
pH Unit
NA
NA
None
ASAP
WQMA
4℃
NA
NA
N
BOD
mg/L
PE
1L
None
48 hr
WQMA
NA
1
Duplicate
mg/L
NA
NA
None
ASAP
WQMA
4℃
NA
NA
O
BLANK
℃
PE/Glass
1L
None
48 hr
WQMA
4℃
x 1
2
P

NOTES:

1. WQMA: Water Quality Measurement Agent, registered in GyeongGi-Do

2. NELAP : National Environmental Laboratory Accreditation Program

3. KSTM: Korea Standard Test Method

4. pH and temperature will be measured on site.

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