DO22_Newark_Bay_Final_Report_Tables_5_10_2017.pdf

Data Report

Delivery Order #0022:

Newark Bay Upland

CONTRACT NO. W912DS-12-D-0011

Prepared by Battelle 141 Longwater Drive Suite 202 Norwell, MA 02061

Prepared for US Army Corps of Engineers, NY District 26 Federal Plaza Rm 1937 New York, NY 10278

May 2017

Newark Bay Upland 2017 Composite A

Newark Bay Upland 2017 - Composite A - Sediment Volatiles

Volatiles Action Level Action Level

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 ug/kg ug/L Comp A Q A Comp A Q A Comp A Q

Chloromethane (Methyl Chloride) 4000 30 12 U 13 U 5 U Bromomethane 25000 10 12 U 13 U 5 U Vinyl chloride 700 5 12 U 13 U 5 U Chloroethane 220000 NA 12 U F1 13 U 5 U Methylene chloride (Dichloromethane) 34000 3 5.3 J B 7.4 J B 5.4 B Acetone 70000000 700 35 J 260 26 Carbon disulfide 7800000 NA 12 U 13 U 5 U 1,1-Dichloroethene 11000 2 12 U 13 U 5 U 1,1-Dichloroethane 8000 50 12 U F1 13 U 5 U 1,2-Dichloroethene (total) 10 24 U F1 25 U 10 U Chloroform 600 6 12 U F1 13 U 5 U 1,2-Dichloroethane 900 NA 12 U 13 U 5 U 2-Butanone (MEK) 3100000 300 12 U 55 5 U 1,1,1-Trichloroethane 290000 30 12 U F1 13 U 5 U Carbon tetrachloride 600 2 12 U F1 13 U 5 U Bromodichloromethane 1000 1 12 U F1 13 U 5 U 1,2-Dichloropropane 2000 1 12 U F1 13 U 5 U cis-1,3-Dichloropropene NA NA 12 U F1 13 U 5 U Trichloroethene 7000 1 12 U F1 13 U 5 U Dibromochloromethane 3000 10 12 U 13 U 5 U 1,1,2-Trichloroethane 2000 3 12 U 13 U 5 U Benzene 2000 1 12 U F1 13 U 5 U trans-1,3-dichloropropene NA NA 12 U 13 U 5 U Bromoform 81000 4 12 U 13 U 5 U 4-Methyl-2-pentanone (MIBK) NA 400 12 U 13 U 5 U 2-Hexanone NA NA 12 U 13 U 5 U Tetrachloroethene 2000 1 12 U 13 U 5 U 1,1,2,2-Tetrachloroethane 1000 NA 12 U 13 U 5 U Toluene 6300000 1000 12 U F1 13 U 5 U Chlorobenzene 510000 50 12 U 13 U 5 U Ethyl benzene 7800000 700 12 U 13 U 5 U Styrene 90000 100 12 U 13 U 5 U Xylenes(Total) 12000000 1000 24 U 25 U 10 U Acrolein 500 240 U F1 250 U 100 U Acrylonitrile 900 120 U 130 U 50 U 1,2-Dibromo-3-chloropropane 80 12 U 13 U 5 U 1,2-Dibromoethane 8 12 U 13 U 5 U Dichlorodifluoromethane 490000 12 U 13 U 5 U * 1,2-Dichloroethene (cis) 230000 12 U F1 13 U 5 U 1,2-Dichloroethene (trans) 300000 12 U F1 13 U 5 U Methyl acetate 78000000 60 U 63 U 25 U * Methyl tert-butyl ether (MTBE) 110000 12 U 13 U 5 U * Tertiary butyl alcohol (TBA) 1400000 120 U 130 U 50 U Trichlorofluoromethane 23000000 12 U F1 13 U 5 U Combined 1,3-dichloropropenes (SUM) cis 2000 0.2 1,4-dioxane 2400 U 2500 U 9.6 U n-propylbenzene 12 U F1 13 U 5 U sec-butylbenzene 12 U 13 U 5 U tert-butylbenzene 12 U 13 U 5 U 1,2,4-trimethylbenzene 12 U F1 13 U 5 U 1,3,5-trimethylbenzene 12 U 13 U 5 U

Newark Bay Upland 2017 - Composite A - Sediment Semivolatiles

Semivolatiles Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 ug/kg ug/kg mg/L mg/L Comp A Q A Comp A Q A Comp A Q

Phenol 18000000 660 4 0.01 1200 U 410 U 0.0096 U bis(2-Chloroethyl)ether 400 660 0.01 0.01 240 U 84 U 0.0019 U 2-Chlorophenol 310000 660 0.005 0.01 1200 U 410 U 0.0096 U 1,3-Dichlorobenzene 5300000 660 0.6 0.01 1200 U 410 U 0.0096 U 1,4-Dichlorobenzene 5000 660 0.075 0.01 1200 U 410 U 0.0096 U 1,2-Dichlorobenzene 5300000 660 0.6 0.01 1200 U 410 U 0.0096 U 2-Methylphenol (o-cresol) 310000 660 NA 0.01 1200 U 410 U 0.0096 U 1-Chloropropane-2,2'-oxybis/ bis(2-chloroisop 23000 660 0.3 0.01 240 U 84 U 0.0019 U 4-Methylphenol (p-cresol) (co-elutes with 3-met 31000 660 NA 0.01 1200 U 410 U 0.0096 U N-Nitroso-Di-N-Propylamine 200 660 0.02 0.01 240 U 84 U 0.0019 U Hexachloroethane 35000 660 0.01 0.01 1200 U 410 U 0.0096 U Nitrobenzene 31000 660 0.01 0.01 2400 U 840 U 0.019 U Isophorone 510000 660 0.1 0.01 1200 U 410 U 0.0096 U 2-Nitrophenol NA 660 NA 0.01 1200 U 410 U 0.0096 U 2,4-Dimethylphenol 1200000 660 0.1 0.01 1200 U 410 U 0.0096 U bis(2-Chloroethoxy)methane NA 660 NA 0.01 1200 U 410 U 0.0096 U 2,4-Dichlorophenol 180000 660 0.02 0.01 240 U 84 U 0.0019 U 1,2,4-Trichlorobenzene 73000 660 0.009 0.01 1200 U 410 U 0.0096 U Naphthalene 6000 660 0.3 0.01 58 J 84 U 0.0019 U 4-Chloroaniline NA 1300 NA 0.02 1200 U 410 U 0.0096 U Hexachloro-1,3-butadiene 6000 660 NA 0.01 240 U 84 U 0.0019 U 4-Chloro-3-methylphenol NA 1300 NA 0.02 1200 U 410 U 0.0096 U 2-Methylnaphthalene 230000 660 NA 0.01 45 J 84 U 0.0019 U Hexachlorocyclopentadiene 45000 660 0.05 0.01 1200 U 410 U 0.0096 U 2,4,6-Trichlorophenol 19000 660 0.02 0.01 1200 U 410 U 0.0096 U 2,4,5-Trichlorophenol 6100000 660 0.7 0.01 1200 U 410 U 0.0096 U 2-Chloronaphthalene NA 660 NA 0.01 240 U 84 U 0.0019 U 2-Nitroaniline 39000 3300 NA 0.05 6100 U 2100 U 0.048 U Dimethylphthalate NA 660 NA 0.01 1200 U 410 U 0.0096 U Acenaphthylene 300000000 660 NA 0.01 120 J 28 J 0.0019 U 2,6-Dinitrotoluene 700 660 0.01 0.01 1200 U 410 U 0.0096 U 3-Nitroaniline NA 3300 NA 0.05 6100 U 2100 U 0.048 U

Newark Bay Upland 2017 - Composite B - Sediment Semivolatiles, con't.

Semivolatiles, continued Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 ug/kg ug/kg mg/L mg/L Comp A Q A Comp A Q A Comp A Q

Acenaphthene 3400000 660 0.4 0.01 43 J 84 U 0.0019 U 2,4-Dinitrophenol 120000 3300 0.04 0.05 6100 U 2100 U 0.048 U 4-Nitrophenol NA 3300 NA 0.05 6100 U 2100 U 0.048 U Dibenzofuran NA 660 NA 0.01 1200 U 410 U 0.0096 U 2,4-Dinitrotoluene 700 660 0.01 0.01 1200 U 410 U 0.0096 U Diethylphthalate 49000000 660 5 0.01 1200 U 64 J 0.0096 U 4-Chlorophenyl-phenylether NA 660 NA 0.01 1200 U 410 U 0.0096 U Fluorene 2300000 660 0.3 0.01 240 U 84 U 0.0019 U 4-Nitroaniline NA 660 NA 0.02 6100 U 2100 U 0.048 U 4,6-Dinitro-2-methylphenol 6000 3300 NA 0.05 6100 U 2100 U 0.048 U N-Nitrosodiphenylamine 99000 660 0.02 0.01 1200 U 410 U 0.0096 U 4-Bromophenyl-phenylether NA 660 NA 0.01 1200 U 410 U 0.0096 U Hexachlorobenzene 300 660 0.01 0.01 240 U 84 U 0.0019 U Pentachlorophenol 3000 3300 0.001 0.05 1200 U 410 U 0.0096 U Phenanthrene 300000000 6600 NA 0.01 170 J 30 J 0.0019 U Anthracene 17000000 6600 2 0.01 160 J 25 J 0.0019 U Carbazole 24000 330 NA 0.01 50 J 84 U 0.0019 U Di-n-butylphthalate 6100000 330 0.9 0.01 1200 U 410 U 0.0096 U Fluoranthene 2300000 660 0.3 0.01 390 81 J 0.0019 U Pyrene 1700000 660 0.2 0.01 350 73 J 0.0019 U Butylbenzylphthalate 1200000 660 0.1 0.01 1200 U 410 U 0.0096 U 3,3'-Dichlorobenzidine 1000 1300 0.06 0.02 1200 U 410 U 0.0096 U Benzo(a)anthracene 600 660 NA 0.01 260 56 J 0.0019 U Chrysene 62000 660 NA 0.01 300 67 J 0.0019 U bis(2-Ethylhexyl)phthalate 35000 660 0.03 0.01 460 J 840 U 0.019 U DI-n-octylphthalate 2400000 660 0.1 0.01 1200 U 410 U 0.0096 U Benzo(b)fluoranthene 600 660 NA 0.01 340 71 J 0.0019 U Benzo(k)fluoranthene 6000 660 NA 0.01 91 J 35 J 0.0019 U Benzo(a)pyrene 200 660 NA 0.01 270 73 J 0.0019 U Indeno(1,2,3-cd)pyrene 600 660 NA 0.01 170 J 47 J 0.0019 U Dibenzo(a,h)anthracene 200 660 NA 0.01 240 U 84 U 0.0019 U Benzo(ghi)perylene 30000000 660 NA 0.01 260 53 J 0.0019 U Pyridine NA 1200 U 410 U 0.0096 U Acetophenone 2000 1200 U 410 U 0.019 U Atrazine 210000 1200 U 410 U 0.019 U Benzaldehyde 6100000 1200 U 410 U 0.019 U Benzidine 700 24000 U 8400 U 0.19 U 1,1'-Biphenyl 3100000 1200 U 410 U 0.0096 U Caprolactam 31000000 6100 U 2100 U 0.048 U 1,2-Diphenylhydrazine 700 1200 U 410 U 0.0096 U N-Nitrosodimethylamine 700 1200 U 410 U 0.0096 U Total Cresol

Newark Bay Upland 2017 - Composite A - Pesticides/Aroclors

Pesticides/Aroclors Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 ug/kg ug/kg mg/L mg/L Comp A Q A Comp A Q A Comp A Q alpha-BHC 100 1.9 0.00002 0.00005 2 U 2.1 U 0.000052 U beta-BHC 400 3.3 0.0002 0.00005 2 U 2.1 U 0.000052 U delta-BHC NA 1.7 NA 0.00005 2 U 2.1 U 0.000052 U gamma-BHC (Lindane) 400 2 0.0002 0.00005 2 U 2.1 U 0.000052 U Heptachlor 100 2.1 0.0004 0.00005 2 U 2.1 U 0.000052 U Aldrin 40 2 0.00004 0.00005 2 U 2.1 U 0.000052 U Heptachlor epoxide 70 2.1 0.0002 0.00005 1.4 J p 0.9 J p 0.000052 U Endosulfan I NA 2.1 0.0004 0.00005 2 U 2.1 U 0.000052 U Dieldrin 40 3.3 0.00003 0.0001 0.65 J p 2.1 U 0.000052 U 4,4'-DDE 2000 4.2 0.0001 0.0001 9.1 4 p 0.000052 U Endrin 23000 3.6 0.002 0.0001 3.5 p 2.1 U 0.000052 U Endosulfan II NA 3.3 0.0004 0.0001 2 U 2.1 U 0.000052 U 4,4'-DDD 3000 4.2 0.0001 0.0001 4 p 2.3 p 0.000052 U Endosulfan sulfate 470000 3.6 0.0004 0.0001 2 U 2.1 U 0.000052 U

4,4'-DDT 2000 3.6 0.0001 0.0001 2 U 2.1 U 0.000052 U

Methoxychlor 390000 17 0.04 0.001 2 U 2.1 U 0.000052 U Endrin ketone NA 3.3 NA 0.0001 2 U 2.1 U 0.000052 U Endrin aldehyde NA 3.3 NA 0.0001 2 U 2.1 U 0.000052 U alpha-Chlordane 200 1.7 NA 0.00005 1.7 J 2.1 U 0.000052 U gamma-Chlordane 200 1.7 0.0005 0.00005 2 U 2.1 U 0.000052 U Toxaphene 600 170 0.003 0.005 79 U 83 U 0.0042 U Aroclor-1016 NA 33 NA 0.001 20 U 21 U 0.00042 U Aroclor-1221 NA 67 NA 0.002 20 U 21 U 0.00042 U Aroclor-1232 NA 33 NA 0.001 20 U 21 U 0.00042 U Aroclor-1242 NA 33 NA 0.001 20 U 21 U 0.00042 U Aroclor-1248 NA 33 NA 0.001 20 U 21 U 0.00042 U Aroclor-1254 NA 33 NA 0.001 93 57 0.00042 U Aroclor-1260 NA 33 NA 0.001 44 35 0.00042 U Total Aroclor(SUM) 200 NA 0.005 NA 0 Mirex 2 U 2.1 U 0.000052 U

Newark Bay Upland 2017 - Composite A - Herbicides

Herbicides Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 Comp A Q A Comp A Q A Comp A Q

2,4,5-TP (Silvex) NA NA NA NA 48 U 50 U 0.94 U

2,4-D NA NA NA NA 190 U 200 U 3.8 U

Newark Bay Upland 2017 - Composite A - Metals

Metals Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: mg/kg)

Amended Sediment

(Units: mg/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170123 20170147 20170147 mg/kg mg/kg mg/L mg/L Comp A Q A Comp A Q A Comp A Q

Aluminum 78000 40 0.2 0.2 11000 16000 1.7 Antimony 31 12 0.02 0.06 0.64 J F1 1.3 U 0.01 U Arsenic 19 2 0.008 0.01 11 12 0.01 U Barium 16000 40 2 0.2 56 80 0.037 J Beryllium 16 1 0.02 0.005 0.69 0.83 0.004 U Cadmium 78 1 0.004 0.005 0.43 J 0.43 J 0.005 U Calcium NA 1000 NA 5 7600 F1 72000 180 Chromium NA 2 0.1 0.01 52 58 0.0051 Hexavalent Chromium 120000 0.96 U F1 0.99 U 0.0064 U F1 Trivalent Chromium 20 52 58 0.01 U Cobalt 1,600 10 NA 0.05 9.8 12 0.0031 J Copper 590 5 1 0.025 63 69 0.075 Iron NA 20 0.3 1 25000 26000 0.1 U Lead 400 0.6 0.01 0.003 76 75 0.01 U Magnesium NA 1000 NA 5 7800 9700 5 U Manganese 5900 3 0.05 0.015 640 690 0.015 U Mercury 23 0.1 0.002 0.0002 0.86 F2 0.95 0.0002 U Nickel 1,600 8 0.1 0.04 39 42 0.024 J Potassium NA 1000 NA 5 2600 3900 34 Selenium 390 1 0.05 0.015 1.2 U 1.3 0.01 U Silver 390 2 NA 0.01 1 0.97 0.005 U Sodium NA 1000 50 5 9800 F1 9800 190 Thallium 5 2 0.01 0.01 2.4 U 2.5 U 0.02 U Vanadium 78 10 NA 0.05 31 36 0.0087 J Zinc 23,000 4 5 0.02 150 220 0.02 U Cyanide, total 1,600 0.5 0.2 0.01 2.1 0.42 J 0.0017 J B %Solids NA NA NA NA 41.1 39.9

Newark Bay Upland 2017 - Composite A - Dioxin/Furan

Dioxin/Furan Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ng/kg)

Amended Sediment

(Units: ng/kg)

SPLP

(Units: pg/L) ASI ID # Soil Leachate 20170123 20170147 20170147 ng/kg pg/L Comp A Q A Comp A Q A Comp A Q

2,3,7,8-TCDD NA NA NA NA 4.50 7.86 9.6 U

1,2,3,7,8-PeCDD NA NA NA NA 0.083 U 0.138 U 48 U 1,2,3,4,7,8-HxCDD NA NA NA NA 0.708 1.77 48 U 1,2,3,6,7,8-HxCDD NA NA NA NA 4.06 7.92 0.42 J B 1,2,3,7,8,9-HxCDD NA NA NA NA 3.50 5.77 0.53 J q B 1,2,3,4,6,7,8-HpCDD NA NA NA NA 68.0 137 0.66 J q B

OCDD NA NA NA NA 627 1370 3.8 J B

2,3,7,8-TCDF NA NA NA NA 5.50 # 10.4 # 9.6 U

1,2,3,7,8-PeCDF NA NA NA NA 0.083 U 0.177 U 48 U 2,3,4,7,8-PeCDF NA NA NA NA 2.94 4.59 0.49 J q B 1,2,3,4,7,8-HxCDF NA NA NA NA 9.62 12.1 48 U 1,2,3,6,7,8-HxCDF NA NA NA NA 2.44 0.158 U 48 U 2,3,4,6,7,8-HxCDF NA NA NA NA 1.73 3.39 48 U 1,2,3,7,8,9-HxCDF NA NA NA NA 0.083 U 0.197 U 48 U 1,2,3,4,6,7,8-HpCDF NA NA NA NA 41.8 71.4 0.65 J q B 1,2,3,4,7,8,9-HpCDF NA NA NA NA 1.89 0.118 U 0.73 J q B

OCDF NA NA NA NA 72.5 96.5 2.1 J B

Newark Bay Upland 2017 - Composite A - Dioxin/Furan -TEQ Converted values

Dioxin/Furan TEF

Unamended Sediment

(Units: ppt)

Amended Sediment

(Units: ppt)

SPLP

(Units: pg/L)

ASI ID # 20170123 20170147 20170147

Comp A Q A Comp A Q A Comp A Q

2,3,7,8-TCDD 1 4.50 7.86 9.60 U

1,2,3,7,8-PeCDD 1 0.08 U 0.14 U 48.00 U 1,2,3,4,7,8-HxCDD 0.1 0.07 0.18 4.80 U 1,2,3,6,7,8-HxCDD 0.1 0.41 0.79 0.04 J B 1,2,3,7,8,9-HxCDD 0.1 0.35 0.58 0.05 J q B 1,2,3,4,6,7,8-HpCDD 0.01 0.68 1.37 0.01 J q B

1,2,3,4,6,7,8,9-OCDD 0.0003 0.19 0.41 0.00 J B

2,3,7,8-TCDF 0.1 0.55 # 1.04 # 0.96 U

1,2,3,7,8-PeCDF 0.03 0.00 U 0.01 U 1.44 U 2,3,4,7,8-PeCDF 0.3 0.88 1.38 0.15 J q B 1,2,3,4,7,8-HxCDF 0.1 0.96 1.21 4.80 U 1,2,3,6,7,8-HxCDF 0.1 0.24 0.02 U 4.80 U 2,3,4,6,7,8-HxCDF 0.1 0.17 0.34 4.80 U 1,2,3,7,8,9-HxCDF 0.1 0.01 U 0.02 U 4.80 U 1,2,3,4,6,7,8-HpCDF 0.01 0.42 0.71 0.01 J q B 1,2,3,4,7,8,9-HpCDF 0.01 0.02 0.00 U 0.01 J q B

1,2,3,4,6,7,8,9-OCDF 0.0003 0.02 0.03 0.00 J B

TOTAL TEF as 2,3,7,8-TCDD 9.55 16.09 84.26

Newark Bay Upland 2017 Composite B

Newark Bay Upland 2017 - Composite B - Sediment Volatiles

Volatiles Action Level Action Level

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 ug/kg ug/L Comp B Q A Comp B Q A Comp B Q

Chloromethane (Methyl Chloride) 4000 30 12 U 10 U 5 U Bromomethane 25000 10 12 U 10 U 5 U Vinyl chloride 700 5 12 U 10 U 5 U Chloroethane 220000 NA 12 U 10 U 5 U Methylene chloride (Dichloromethane) 34000 3 5.6 J B 5.9 J B 5.1 B Acetone 70000000 700 48 U 200 30 Carbon disulfide 7800000 NA 12 U 10 U 5 U 1,1-Dichloroethene 11000 2 12 U 10 U 5 U 1,1-Dichloroethane 8000 50 12 U 10 U 5 U 1,2-Dichloroethene (total) 10 24 U 21 U 10 U Chloroform 600 6 12 U 10 U 5 U 1,2-Dichloroethane 900 NA 12 U 10 U 5 U 2-Butanone (MEK) 3100000 300 12 U 53 5 U 1,1,1-Trichloroethane 290000 30 12 U 10 U 5 U Carbon tetrachloride 600 2 12 U 10 U 5 U Bromodichloromethane 1000 1 12 U 10 U 5 U 1,2-Dichloropropane 2000 1 12 U 10 U 5 U cis-1,3-Dichloropropene NA NA 12 U 10 U 5 U Trichloroethene 7000 1 12 U 10 U 5 U Dibromochloromethane 3000 10 12 U 10 U 5 U 1,1,2-Trichloroethane 2000 3 12 U 10 U 5 U Benzene 2000 1 12 U 10 U 5 U trans-1,3-dichloropropene NA NA 12 U 10 U 5 U Bromoform 81000 4 12 U 10 U 5 U 4-Methyl-2-pentanone (MIBK) NA 400 12 U 10 U 5 U 2-Hexanone NA NA 12 U 10 U 5 U Tetrachloroethene 2000 1 12 U 10 U 5 U 1,1,2,2-Tetrachloroethane 1000 NA 12 U 10 U 5 U Toluene 6300000 1000 12 U 10 U 5 U Chlorobenzene 510000 50 12 U 10 U 5 U Ethyl benzene 7800000 700 12 U 10 U 5 U Styrene 90000 100 12 U 10 U 5 U Xylenes(Total) 12000000 1000 24 U 21 U 10 U Acrolein 500 240 U 210 U 100 U Acrylonitrile 900 120 U 100 U 50 U 1,2-Dibromo-3-chloropropane 80 12 U 10 U 5 U 1,2-Dibromoethane 8 12 U 10 U 5 U Dichlorodifluoromethane 490000 12 U 10 U 5 U * 1,2-Dichloroethene (cis) 230000 12 U 10 U 5 U 1,2-Dichloroethene (trans) 300000 12 U 10 U 5 U Methyl acetate 78000000 60 U 52 U 25 U * Methyl tert-butyl ether (MTBE) 110000 12 U 10 U 5 U * Tertiary butyl alcohol (TBA) 1400000 120 U 100 U 50 U Trichlorofluoromethane 23000000 12 U 10 U 5 U Combined 1,3-dichloropropenes (SUM) cis 2000 0.2 1,4-dioxane 3200 U 2100 U 9.6 U n-propylbenzene 12 U 10 U 5 U sec-butylbenzene 12 U 10 U 5 U tert-butylbenzene 12 U 10 U 5 U 1,2,4-trimethylbenzene 12 U 10 U 5 U 1,3,5-trimethylbenzene 12 U 10 U 5 U

Newark Bay Upland 2017 - Composite B - Sediment Semivolatiles

Semivolatiles Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 ug/kg ug/kg mg/L mg/L Comp B Q A Comp B Q A Comp B Q

Phenol 18000000 660 4 0.01 1600 U 340 U 0.0096 U bis(2-Chloroethyl)ether 400 660 0.01 0.01 320 U 69 U 0.0019 U 2-Chlorophenol 310000 660 0.005 0.01 1600 U 340 U 0.0096 U 1,3-Dichlorobenzene 5300000 660 0.6 0.01 1600 U 340 U 0.0096 U 1,4-Dichlorobenzene 5000 660 0.075 0.01 1600 U 340 U 0.0096 U 1,2-Dichlorobenzene 5300000 660 0.6 0.01 1600 U 340 U 0.0096 U 2-Methylphenol (o-cresol) 310000 660 NA 0.01 1600 U 340 U 0.0096 U 1-Chloropropane-2,2'-oxybis/ bis(2-chloroisop 23000 660 0.3 0.01 320 U 69 U 0.0019 U 4-Methylphenol (p-cresol) (co-elutes with 3-met 31000 660 NA 0.01 1600 U 340 U 0.0096 U N-Nitroso-Di-N-Propylamine 200 660 0.02 0.01 320 U 69 U 0.0019 U Hexachloroethane 35000 660 0.01 0.01 1600 U 340 U 0.0096 U Nitrobenzene 31000 660 0.01 0.01 3200 U 690 U 0.019 U Isophorone 510000 660 0.1 0.01 1600 U 340 U 0.0096 U 2-Nitrophenol NA 660 NA 0.01 1600 U 340 U 0.0096 U 2,4-Dimethylphenol 1200000 660 0.1 0.01 1600 U 340 U 0.0096 U bis(2-Chloroethoxy)methane NA 660 NA 0.01 1600 U 340 U 0.0096 U 2,4-Dichlorophenol 180000 660 0.02 0.01 320 U 69 U 0.0019 U 1,2,4-Trichlorobenzene 73000 660 0.009 0.01 1600 U 340 U 0.0096 U Naphthalene 6000 660 0.3 0.01 95 J 69 U 0.0019 U 4-Chloroaniline NA 1300 NA 0.02 1600 U 340 U 0.0096 U Hexachloro-1,3-butadiene 6000 660 NA 0.01 320 U 69 U 0.0019 U 4-Chloro-3-methylphenol NA 1300 NA 0.02 1600 U 340 U 0.0096 U 2-Methylnaphthalene 230000 660 NA 0.01 55 J 69 U 0.0019 U Hexachlorocyclopentadiene 45000 660 0.05 0.01 1600 U 340 U 0.0096 U 2,4,6-Trichlorophenol 19000 660 0.02 0.01 1600 U 340 U 0.0096 U 2,4,5-Trichlorophenol 6100000 660 0.7 0.01 1600 U 340 U 0.0096 U 2-Chloronaphthalene NA 660 NA 0.01 320 U 69 U 0.0019 U 2-Nitroaniline 39000 3300 NA 0.05 8100 U 1700 U 0.048 U Dimethylphthalate NA 660 NA 0.01 1600 U 340 U 0.0096 U Acenaphthylene 300000000 660 NA 0.01 180 J 33 J 0.0019 U 2,6-Dinitrotoluene 700 660 0.01 0.01 1600 U 340 U 0.0096 U 3-Nitroaniline NA 3300 NA 0.05 8100 U 1700 U 0.048 U

Newark Bay Upland 2017 - Composite B - Sediment Semivolatiles, con't.

Semivolatiles, continued Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 ug/kg ug/kg mg/L mg/L Comp B Q A Comp B Q A Comp B Q

Acenaphthene 3400000 660 0.4 0.01 320 U 84 U 0.0019 U 2,4-Dinitrophenol 120000 3300 0.04 0.05 8100 U 1700 U 0.048 U 4-Nitrophenol NA 3300 NA 0.05 8100 U 1700 U 0.048 U Dibenzofuran NA 660 NA 0.01 1600 U 340 U 0.0096 U 2,4-Dinitrotoluene 700 660 0.01 0.01 1600 U 340 U 0.0096 U Diethylphthalate 49000000 660 5 0.01 1600 U 340 U 0.0096 U 4-Chlorophenyl-phenylether NA 660 NA 0.01 1600 U 340 U 0.0096 U Fluorene 2300000 660 0.3 0.01 83 J 69 U 0.0019 U 4-Nitroaniline NA 660 NA 0.02 8100 U 1700 U 0.048 U 4,6-Dinitro-2-methylphenol 6000 3300 NA 0.05 8100 U 1700 U 0.048 U N-Nitrosodiphenylamine 99000 660 0.02 0.01 1600 U 340 U 0.0096 U 4-Bromophenyl-phenylether NA 660 NA 0.01 1600 U 340 U 0.0096 U Hexachlorobenzene 300 660 0.01 0.01 320 U 69 U 0.0019 U Pentachlorophenol 3000 3300 0.001 0.05 1600 U 340 U 0.0096 U Phenanthrene 300000000 6600 NA 0.01 230 J 36 J 0.0019 U Anthracene 17000000 6600 2 0.01 230 J 28 J 0.0019 U Carbazole 24000 330 NA 0.01 59 J 69 U 0.0019 U Di-n-butylphthalate 6100000 330 0.9 0.01 1600 U 340 U 0.0096 U Fluoranthene 2300000 660 0.3 0.01 610 89 0.0019 U Pyrene 1700000 660 0.2 0.01 570 79 0.0019 U Butylbenzylphthalate 1200000 660 0.1 0.01 1600 U 340 U 0.0096 U 3,3'-Dichlorobenzidine 1000 1300 0.06 0.02 1600 U 340 U 0.0096 U Benzo(a)anthracene 600 660 NA 0.01 430 61 J 0.0019 U Chrysene 62000 660 NA 0.01 460 72 0.0019 U bis(2-Ethylhexyl)phthalate 35000 660 0.03 0.01 750 J 170 J 0.019 U DI-n-octylphthalate 2400000 660 0.1 0.01 1600 U 340 U 0.0096 U Benzo(b)fluoranthene 600 660 NA 0.01 460 63 J 0.0019 U Benzo(k)fluoranthene 6000 660 NA 0.01 290 J 46 J 0.0019 U Benzo(a)pyrene 200 660 NA 0.01 500 75 0.0019 U Indeno(1,2,3-cd)pyrene 600 660 NA 0.01 310 J 53 J 0.0019 U Dibenzo(a,h)anthracene 200 660 NA 0.01 140 J 69 U 0.0019 U Benzo(ghi)perylene 30000000 660 NA 0.01 380 61 J 0.0019 U Pyridine NA 1600 U 340 U 0.0096 U Acetophenone 2000 1600 U 340 U 0.019 U Atrazine 210000 1600 U 340 U 0.019 U Benzaldehyde 6100000 1600 U 340 U 0.019 U Benzidine 700 32000 U 6900 U 0.19 U 1,1'-Biphenyl 3100000 1600 U 340 U 0.0096 U Caprolactam 31000000 8100 U 1700 U 0.048 U 1,2-Diphenylhydrazine 700 1600 U 340 U 0.0096 U N-Nitrosodimethylamine 700 1600 U 340 U 0.0096 U

Newark Bay Upland 2017 - Composite B - Pesticides/Aroclors

Pesticides/Aroclors Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 ug/kg ug/kg mg/L mg/L Comp B Q A Comp B Q A Comp B Q alpha-BHC 100 1.9 0.00002 0.00005 2 U 1.7 U 0.000052 U beta-BHC 400 3.3 0.0002 0.00005 2 U 1.7 U 0.000052 U delta-BHC NA 1.7 NA 0.00005 2 U 1.7 U 0.000052 U gamma-BHC (Lindane) 400 2 0.0002 0.00005 2 U 1.7 U 0.000052 U Heptachlor 100 2.1 0.0004 0.00005 2 U 1.7 U 0.000052 U Aldrin 40 2 0.00004 0.00005 2 U 1.7 U 0.000052 U Heptachlor epoxide 70 2.1 0.0002 0.00005 1.4 J p 0.8 J p 0.000052 U Endosulfan I NA 2.1 0.0004 0.00005 2 U 1.7 U 0.000052 U Dieldrin 40 3.3 0.00003 0.0001 0.98 J p 0.44 J p 0.000052 U 4,4'-DDE 2000 4.2 0.0001 0.0001 8.4 p 6.5 0.000052 U Endrin 23000 3.6 0.002 0.0001 2 U 1.7 U 0.000052 U Endosulfan II NA 3.3 0.0004 0.0001 2 U 1.7 U 0.000052 U 4,4'-DDD 3000 4.2 0.0001 0.0001 4.4 p 2.3 p 0.000052 U Endosulfan sulfate 470000 3.6 0.0004 0.0001 2 U 1.7 U 0.000052 U

4,4'-DDT 2000 3.6 0.0001 0.0001 2 U 1.7 U 0.000052 U

Methoxychlor 390000 17 0.04 0.001 2 U 1.7 U 0.000052 U Endrin ketone NA 3.3 NA 0.0001 2 U 1.7 U 0.000052 U Endrin aldehyde NA 3.3 NA 0.0001 2 U 1.7 U 0.000052 U alpha-Chlordane 200 1.7 NA 0.00005 1.9 J 1.3 J 0.000052 U gamma-Chlordane 200 1.7 0.0005 0.00005 2 U 1.7 U 0.000052 U Toxaphene 600 170 0.003 0.005 80 U 68 U 0.0042 U Aroclor-1016 NA 33 NA 0.001 20 U 17 U 0.00042 U Aroclor-1221 NA 67 NA 0.002 20 U 17 U 0.00042 U Aroclor-1232 NA 33 NA 0.001 20 U 17 U 0.00042 U Aroclor-1242 NA 33 NA 0.001 20 U 17 U 0.00042 U Aroclor-1248 NA 33 NA 0.001 20 U 17 U 0.00042 U Aroclor-1254 NA 33 NA 0.001 160 51 0.00042 U Aroclor-1260 NA 33 NA 0.001 100 30 0.00042 U Total Aroclor(SUM) 200 NA 0.005 NA 0 Mirex 2 U 1.7 U 0.000052 U

Newark Bay Upland 2017 - Composite B - Herbicides

Herbicides Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 Comp B Q A Comp B Q A Comp B Q

2,4,5-TP (Silvex) NA NA NA NA 48 U 41 U 0.94 U

2,4-D NA NA NA NA 190 U 170 U 3.8 U

Newark Bay Upland 2017 - Composite B - Metals

Sediment

(Units: mg/kg)

Amended Sediment

(Units: mg/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170124 20170148 20170148 mg/kg mg/kg mg/L mg/L Comp B Q A Comp B Q A Comp B Q

Aluminum 78000 40 0.2 0.2 12000 13000 1.5 Antimony 31 12 0.02 0.06 0.62 J 0.98 U 0.01 U Arsenic 19 2 0.008 0.01 11 10 0.01 U Barium 16000 40 2 0.2 67 73 0.034 J Beryllium 16 1 0.02 0.005 0.75 0.69 0.004 U Cadmium 78 1 0.004 0.005 0.51 J 0.38 J 0.005 U Calcium NA 1000 NA 5 7400 58000 190 Chromium NA 2 0.1 0.01 59 52 0.0055 Hexavalent Chromium 120000 0.94 U 0.82 U 0.0064 U Trivalent Chromium 20 59 52 0.01 U Cobalt 1,600 10 NA 0.05 11 9.6 0.003 J Copper 590 5 1 0.025 71 60 0.11 Iron NA 20 0.3 1 27000 22000 0.1 U Lead 400 0.6 0.01 0.003 84 65 0.01 U Magnesium NA 1000 NA 5 8100 7900 5 U Manganese 5900 3 0.05 0.015 610 530 0.015 U Mercury 23 0.1 0.002 0.0002 1 0.82 0.0002 U Nickel 1,600 8 0.1 0.04 40 35 0.024 J Potassium NA 1000 NA 5 2800 3300 34 Selenium 390 1 0.05 0.015 1.1 U 1.1 0.0048 J Silver 390 2 NA 0.01 1 0.84 0.005 U Sodium NA 1000 50 5 9400 7700 190 Thallium 5 2 0.01 0.01 2.3 U 2 U 0.02 U Vanadium 78 10 NA 0.05 32 28 0.0082 J Zinc 23,000 4 5 0.02 160 190 0.02 U Cyanide, total 1,600 0.5 0.2 0.01 1.1 0.27 J 0.003 J %Solids NA NA NA NA 41.5 48.2

Newark Bay Upland 2017 - Composite B - Dioxin/Furan

Dioxin/Furan Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ng/kg)

Amended Sediment

(Units: ng/kg)

SPLP

(Units: pg/L) ASI ID # Soil Leachate 20170124 20170148 20170148 ng/kg pg/L Comp B Q A Comp B Q A Comp B Q

2,3,7,8-TCDD NA NA NA NA 11.0 14.2 9.6 U

1,2,3,7,8-PeCDD NA NA NA NA 0.0932 U 0.676 U 48 U 1,2,3,4,7,8-HxCDD NA NA NA NA 1.26 1.09 U 48 U 1,2,3,6,7,8-HxCDD NA NA NA NA 4.47 16.6 0.25 J q B 1,2,3,7,8,9-HxCDD NA NA NA NA 4.33 0.995 U 48 U 1,2,3,4,6,7,8-HpCDD NA NA NA NA 97.9 236 48 U OCDD NA NA NA NA 927 1320 2 J q B

2,3,7,8-TCDF NA NA NA NA 7.78 # 8.93 # 9.6 U

1,2,3,7,8-PeCDF NA NA NA NA 0.116 U 0.469 U 48 U 2,3,4,7,8-PeCDF NA NA NA NA 4.78 0.619 U 48 U 1,2,3,4,7,8-HxCDF NA NA NA NA 16.7 14.6 0.24 J q B 1,2,3,6,7,8-HxCDF NA NA NA NA 3.75 0.338 U 48 U 2,3,4,6,7,8-HxCDF NA NA NA NA 2.77 0.413 U 0.24 J q 1,2,3,7,8,9-HxCDF NA NA NA NA 0.116 U 2.18 48 U 1,2,3,4,6,7,8-HpCDF NA NA NA NA 64.0 73.7 0.33 J B 1,2,3,4,7,8,9-HpCDF NA NA NA NA 3.31 3.68 0.35 J B OCDF NA NA NA NA 113 98.2 1.5 J q B

Newark Bay Upland 2017 - Composite B - Dioxin/Furan -TEQ Converted values

Dioxin/Furan TEF

Unamended Sediment

(Units: ppt)

Amended Sediment

(Units: ppt)

SPLP

(Units: pg/L)

ASI ID # 20170124 20170148 20170148

Comp B Q A Comp B Q A Comp B Q

2,3,7,8-TCDD 1 10.97 14.15 9.60 U

1,2,3,7,8-PeCDD 1 0.09 U 0.68 U 48.00 U 1,2,3,4,7,8-HxCDD 0.1 0.13 0.11 U 4.80 U 1,2,3,6,7,8-HxCDD 0.1 0.45 1.66 0.03 J q B 1,2,3,7,8,9-HxCDD 0.1 0.43 0.10 U 4.80 U 1,2,3,4,6,7,8-HpCDD 0.01 0.98 2.36 0.48 U 1,2,3,4,6,7,8,9-OCDD 0.0003 0.28 0.40 0.00 J q B

2,3,7,8-TCDF 0.1 0.78 # 0.89 # 0.96 U

1,2,3,7,8-PeCDF 0.03 0.00 U 0.01 U 1.44 U 2,3,4,7,8-PeCDF 0.3 1.43 0.19 U 14.40 U 1,2,3,4,7,8-HxCDF 0.1 1.67 1.46 0.02 J q B 1,2,3,6,7,8-HxCDF 0.1 0.38 0.03 U 4.80 U 2,3,4,6,7,8-HxCDF 0.1 0.28 0.04 U 0.02 J q 1,2,3,7,8,9-HxCDF 0.1 0.01 U 0.22 4.80 U 1,2,3,4,6,7,8-HpCDF 0.01 0.64 0.74 0.00 J B 1,2,3,4,7,8,9-HpCDF 0.01 0.03 0.04 0.00 J B 1,2,3,4,6,7,8,9-OCDF 0.0003 0.03 0.03 0.00 J q B TOTAL TEF as 2,3,7,8-TCDD 18.58 23.10 94.16

Newark Bay Upland 2017 Composite C

Newark Bay Upland 2017 - Composite C - Sediment Volatiles

Volatiles Action Level Action Level

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 ug/kg ug/L Comp C Q A Comp C Q A Comp C Q

Chloromethane (Methyl Chloride) 4000 30 12 U 11 U 5 U Bromomethane 25000 10 12 U 11 U 5 U Vinyl chloride 700 5 12 U 11 U 5 U Chloroethane 220000 NA 12 U 11 U 5 U Methylene chloride (Dichloromethane) 34000 3 5.7 J B 6 J B 6.4 B Acetone 70000000 700 48 U 260 30 Carbon disulfide 7800000 NA 12 U 11 U 5 U 1,1-Dichloroethene 11000 2 12 U 11 U 5 U 1,1-Dichloroethane 8000 50 12 U 11 U 5 U 1,2-Dichloroethene (total) 10 24 U 21 U 10 U Chloroform 600 6 12 U 11 U 5 U 1,2-Dichloroethane 900 NA 12 U 11 U 5 U 2-Butanone (MEK) 3100000 300 12 U 85 3.4 J 1,1,1-Trichloroethane 290000 30 12 U 11 U 5 U Carbon tetrachloride 600 2 12 U 11 U 5 U Bromodichloromethane 1000 1 12 U 11 U 5 U 1,2-Dichloropropane 2000 1 12 U 11 U 5 U cis-1,3-Dichloropropene NA NA 12 U 11 U 5 U Trichloroethene 7000 1 12 U 11 U 5 U Dibromochloromethane 3000 10 12 U 11 U 5 U 1,1,2-Trichloroethane 2000 3 12 U 11 U 5 U Benzene 2000 1 12 U 11 U 5 U trans-1,3-dichloropropene NA NA 12 U 11 U 5 U Bromoform 81000 4 12 U 11 U 5 U 4-Methyl-2-pentanone (MIBK) NA 400 12 U 11 U 5 U 2-Hexanone NA NA 12 U 11 U 5 U Tetrachloroethene 2000 1 12 U 11 U 5 U 1,1,2,2-Tetrachloroethane 1000 NA 12 U 11 U 5 U Toluene 6300000 1000 12 U 11 U 5 U Chlorobenzene 510000 50 12 U 11 U 5 U Ethyl benzene 7800000 700 12 U 11 U 5 U Styrene 90000 100 12 U 11 U 5 U Xylenes(Total) 12000000 1000 24 U 21 U 10 U Acrolein 500 240 U 210 U 100 U Acrylonitrile 900 120 U 110 U 50 U 1,2-Dibromo-3-chloropropane 80 12 U 11 U 5 U 1,2-Dibromoethane 8 12 U 11 U 5 U Dichlorodifluoromethane 490000 12 U 11 U 5 U * 1,2-Dichloroethene (cis) 230000 12 U 11 U 5 U 1,2-Dichloroethene (trans) 300000 12 U 11 U 5 U Methyl acetate 78000000 60 U 53 U 25 U * Methyl tert-butyl ether (MTBE) 110000 12 U 11 U 5 U * Tertiary butyl alcohol (TBA) 1400000 120 U 110 U 50 U Trichlorofluoromethane 23000000 12 U 11 U 5 U Combined 1,3-dichloropropenes (SUM) cis 2000 0.2 1,4-dioxane 2400 U 2100 U 1000 U n-propylbenzene 12 U 11 U 5 U sec-butylbenzene 12 U 11 U 5 U tert-butylbenzene 12 U 11 U 5 U 1,2,4-trimethylbenzene 12 U 11 U 5 U 1,3,5-trimethylbenzene 12 U 11 U 5 U

Newark Bay Upland 2017 - Composite C - Sediment Semivolatiles

Semivolatiles Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 ug/kg ug/kg mg/L mg/L Comp C Q A Comp C Q A Comp C Q

Phenol 18000000 660 4 0.01 1200 U 350 U 0.01 U bis(2-Chloroethyl)ether 400 660 0.01 0.01 240 U 70 U 0.002 U 2-Chlorophenol 310000 660 0.005 0.01 1200 U 350 U 0.01 U 1,3-Dichlorobenzene 5300000 660 0.6 0.01 1200 U 350 U 0.01 U 1,4-Dichlorobenzene 5000 660 0.075 0.01 1200 U 350 U 0.01 U 1,2-Dichlorobenzene 5300000 660 0.6 0.01 1200 U 350 U 0.01 U 2-Methylphenol (o-cresol) 310000 660 NA 0.01 1200 U 350 U 0.01 U 1-Chloropropane-2,2'-oxybis/ bis(2-chloroisop 23000 660 0.3 0.01 240 U 70 U 0.002 U 4-Methylphenol (p-cresol) (co-elutes with 3-met 31000 660 NA 0.01 1200 U 350 U 0.01 U N-Nitroso-Di-N-Propylamine 200 660 0.02 0.01 240 U 70 U 0.002 U Hexachloroethane 35000 660 0.01 0.01 1200 U 350 U 0.01 U Nitrobenzene 31000 660 0.01 0.01 2400 U 700 U 0.02 U Isophorone 510000 660 0.1 0.01 1200 U 350 U 0.01 U 2-Nitrophenol NA 660 NA 0.01 1200 U 350 U 0.01 U 2,4-Dimethylphenol 1200000 660 0.1 0.01 1200 U 350 U 0.01 U bis(2-Chloroethoxy)methane NA 660 NA 0.01 1200 U 350 U 0.01 U 2,4-Dichlorophenol 180000 660 0.02 0.01 240 U 70 U 0.002 U 1,2,4-Trichlorobenzene 73000 660 0.009 0.01 1200 U 350 U 0.01 U Naphthalene 6000 660 0.3 0.01 86 J 70 U 0.002 U 4-Chloroaniline NA 1300 NA 0.02 1200 U 350 U 0.01 U Hexachloro-1,3-butadiene 6000 660 NA 0.01 240 U 70 U 0.002 U 4-Chloro-3-methylphenol NA 1300 NA 0.02 1200 U 350 U 0.01 U 2-Methylnaphthalene 230000 660 NA 0.01 48 J 70 U 0.002 U Hexachlorocyclopentadiene 45000 660 0.05 0.01 1200 U 350 U 0.01 U 2,4,6-Trichlorophenol 19000 660 0.02 0.01 1200 U 350 U 0.01 U 2,4,5-Trichlorophenol 6100000 660 0.7 0.01 1200 U 350 U 0.01 U 2-Chloronaphthalene NA 660 NA 0.01 240 U 70 U 0.002 U 2-Nitroaniline 39000 3300 NA 0.05 6100 U 1800 U 0.05 U Dimethylphthalate NA 660 NA 0.01 1200 U 350 U 0.01 U Acenaphthylene 300000000 660 NA 0.01 180 J 33 J 0.002 U 2,6-Dinitrotoluene 700 660 0.01 0.01 1200 U 350 U 0.01 U 3-Nitroaniline NA 3300 NA 0.05 6100 U 1800 U 0.05 U

Newark Bay Upland 2017 - Composite C - Sediment Semivolatiles, con't.

Semivolatiles, continued Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 ug/kg ug/kg mg/L mg/L Comp C Q A Comp C Q A Comp C Q

Acenaphthene 3400000 660 0.4 0.01 52 J 84 U 0.002 U 2,4-Dinitrophenol 120000 3300 0.04 0.05 6100 U 1800 U 0.05 U 4-Nitrophenol NA 3300 NA 0.05 6100 U 1800 U 0.05 U Dibenzofuran NA 660 NA 0.01 1200 U 350 U 0.01 U 2,4-Dinitrotoluene 700 660 0.01 0.01 1200 U 350 U 0.01 U Diethylphthalate 49000000 660 5 0.01 170 J 44 J 0.01 U 4-Chlorophenyl-phenylether NA 660 NA 0.01 1200 U 350 U 0.01 U Fluorene 2300000 660 0.3 0.01 64 J 70 U 0.002 U 4-Nitroaniline NA 660 NA 0.02 6100 U 1800 U 0.05 U 4,6-Dinitro-2-methylphenol 6000 3300 NA 0.05 6100 U 1800 U 0.05 U N-Nitrosodiphenylamine 99000 660 0.02 0.01 1200 U 350 U 0.01 U 4-Bromophenyl-phenylether NA 660 NA 0.01 1200 U 350 U 0.01 U Hexachlorobenzene 300 660 0.01 0.01 240 U 70 U 0.002 U Pentachlorophenol 3000 3300 0.001 0.05 1200 U 350 U 0.01 U Phenanthrene 300000000 6600 NA 0.01 200 J 39 J 0.002 U Anthracene 17000000 6600 2 0.01 190 J 33 J 0.002 U Carbazole 24000 330 NA 0.01 240 U 70 U 0.002 U Di-n-butylphthalate 6100000 330 0.9 0.01 1200 U 350 U 0.01 U Fluoranthene 2300000 660 0.3 0.01 560 110 0.002 U Pyrene 1700000 660 0.2 0.01 490 92 0.002 U Butylbenzylphthalate 1200000 660 0.1 0.01 1200 U 350 U 0.01 U 3,3'-Dichlorobenzidine 1000 1300 0.06 0.02 1200 U 350 U 0.01 U Benzo(a)anthracene 600 660 NA 0.01 380 77 0.002 U Chrysene 62000 660 NA 0.01 420 86 0.002 U bis(2-Ethylhexyl)phthalate 35000 660 0.03 0.01 690 J 88 J 0.02 U DI-n-octylphthalate 2400000 660 0.1 0.01 1200 U 350 U 0.01 U Benzo(b)fluoranthene 600 660 NA 0.01 510 83 0.002 U Benzo(k)fluoranthene 6000 660 NA 0.01 150 J 42 J 0.002 U Benzo(a)pyrene 200 660 NA 0.01 390 86 0.002 U Indeno(1,2,3-cd)pyrene 600 660 NA 0.01 280 55 J 0.002 U Dibenzo(a,h)anthracene 200 660 NA 0.01 130 J 24 J 0.002 U Benzo(ghi)perylene 30000000 660 NA 0.01 330 65 J 0.002 U Pyridine NA 1200 U 350 U 0.01 U Acetophenone 2000 1200 U 350 U 0.02 U Atrazine 210000 1200 U 350 U 0.02 U Benzaldehyde 6100000 1200 U 350 U 0.02 U Benzidine 700 24000 U 7000 U 0.2 U 1,1'-Biphenyl 3100000 1200 U 350 U 0.01 U Caprolactam 31000000 6100 U 1800 U 0.05 U 1,2-Diphenylhydrazine 700 1200 U 350 U 0.01 U N-Nitrosodimethylamine 700 1200 U 350 U 0.01 U

Newark Bay Upland 2017 - Composite C - Pesticides/Aroclors

Pesticides/Aroclors Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 ug/kg ug/kg mg/L mg/L Comp C Q A Comp C Q A Comp C Q alpha-BHC 100 1.9 0.00002 0.00005 2 U 1.7 U 0.000052 U beta-BHC 400 3.3 0.0002 0.00005 2 U 1.7 U 0.000052 U delta-BHC NA 1.7 NA 0.00005 2 U 1.7 U 0.000052 U gamma-BHC (Lindane) 400 2 0.0002 0.00005 2 U 1.7 U 0.000052 U Heptachlor 100 2.1 0.0004 0.00005 2 U 1.7 U 0.000052 U Aldrin 40 2 0.00004 0.00005 2 U 1.7 U 0.000052 U Heptachlor epoxide 70 2.1 0.0002 0.00005 1.3 J p 1.2 J p 0.000052 U Endosulfan I NA 2.1 0.0004 0.00005 2 U 1.7 U 0.000052 U Dieldrin 40 3.3 0.00003 0.0001 0.85 J p 0.54 J p 0.000052 U

4,4'-DDE 2000 4.2 0.0001 0.0001 12 7.4 0.000052 U

Endrin 23000 3.6 0.002 0.0001 2 U 2.5 p 0.000052 U Endosulfan II NA 3.3 0.0004 0.0001 2 U 1.7 U 0.000052 U 4,4'-DDD 3000 4.2 0.0001 0.0001 4.6 p 3 p 0.000052 U Endosulfan sulfate 470000 3.6 0.0004 0.0001 2 U 1.7 U 0.000052 U

4,4'-DDT 2000 3.6 0.0001 0.0001 2 U 1.7 U 0.000052 U

Methoxychlor 390000 17 0.04 0.001 2 U 1.7 U 0.000052 U Endrin ketone NA 3.3 NA 0.0001 2 U 1.7 U 0.000052 U Endrin aldehyde NA 3.3 NA 0.0001 2 U 1.7 U 0.000052 U alpha-Chlordane 200 1.7 NA 0.00005 2 1.4 J 0.000052 U gamma-Chlordane 200 1.7 0.0005 0.00005 2 U 1.7 U 0.000052 U Toxaphene 600 170 0.003 0.005 78 U 69 U 0.0042 U Aroclor-1016 NA 33 NA 0.001 19 U 17 U 0.00042 U Aroclor-1221 NA 67 NA 0.002 19 U 17 U 0.00042 U Aroclor-1232 NA 33 NA 0.001 19 U 17 U 0.00042 U Aroclor-1242 NA 33 NA 0.001 19 U 17 U 0.00042 U Aroclor-1248 NA 33 NA 0.001 19 U 17 U 0.00042 U Aroclor-1254 NA 33 NA 0.001 100 56 0.00042 U Aroclor-1260 NA 33 NA 0.001 63 34 0.00042 U Total Aroclor(SUM) 200 NA 0.005 NA 0 Mirex 2 U 1.7 U 0.000052 U

Newark Bay Upland 2017 - Composite C - Herbicides

Herbicides Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 Comp C Q A Comp C Q A Comp C Q

2,4,5-TP (Silvex) NA NA NA NA 48 U 42 U 0.94 U

Newark Bay Upland 2017 - Composite C - Metals

Sediment

(Units: mg/kg)

Amended Sediment

(Units: mg/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170125 20170149 20170149 mg/kg mg/kg mg/L mg/L Comp C Q A Comp C Q A Comp C Q

Aluminum 78000 40 0.2 0.2 12000 15000 1.3 Antimony 31 12 0.02 0.06 0.49 J 1 U 0.01 U Arsenic 19 2 0.008 0.01 12 9.6 0.01 U Barium 16000 40 2 0.2 73 83 0.056 J Beryllium 16 1 0.02 0.005 0.78 0.78 0.004 U Cadmium 78 1 0.004 0.005 0.51 J 0.41 J 0.005 U Calcium NA 1000 NA 5 8800 94000 240 Chromium NA 2 0.1 0.01 61 52 0.0044 J Hexavalent Chromium 120000 0.96 U 0.85 U 0.0064 U Trivalent Chromium 20 61 52 0.01 U Cobalt 1,600 10 NA 0.05 11 10 0.003 J Copper 590 5 1 0.025 71 56 0.084 Iron NA 20 0.3 1 27000 22000 0.1 U Lead 400 0.6 0.01 0.003 84 61 0.01 U Magnesium NA 1000 NA 5 8300 8900 5 U Manganese 5900 3 0.05 0.015 590 530 0.015 U Mercury 23 0.1 0.002 0.0002 1.3 0.76 0.0002 U Nickel 1,600 8 0.1 0.04 40 33 0.02 J Potassium NA 1000 NA 5 2900 3200 34 Selenium 390 1 0.05 0.015 1.2 U 1.3 0.0051 J Silver 390 2 NA 0.01 1.1 0.77 0.005 U Sodium NA 1000 50 5 9800 7000 190 Thallium 5 2 0.01 0.01 2.5 U 2 U 0.02 U Vanadium 78 10 NA 0.05 33 30 0.05 U Zinc 23,000 4 5 0.02 170 220 0.02 U Cyanide, total 1,600 0.5 0.2 0.01 1.4 0.34 J 0.0019 J %Solids NA NA NA NA 41.4 47.3

Newark Bay Upland 2017 - Composite C - Dioxin/Furan

Dioxin/Furan Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ng/kg)

Amended Sediment

(Units: ng/kg)

SPLP

(Units: pg/L) ASI ID # Soil Leachate 20170125 20170149 20170149 ng/kg pg/L Comp C Q A Comp C Q A Comp C Q

2,3,7,8-TCDD NA NA NA NA 11.6 13.2 9.6 U

1,2,3,7,8-PeCDD NA NA NA NA 0.094 U 0.093 U 48 U 1,2,3,4,7,8-HxCDD NA NA NA NA 0.188 U 0.185 U 48 U 1,2,3,6,7,8-HxCDD NA NA NA NA 5.30 8.57 0.18 J q B 1,2,3,7,8,9-HxCDD NA NA NA NA 4.71 6.361 48 U 1,2,3,4,6,7,8-HpCDD NA NA NA NA 99.4 124 48 U OCDD NA NA NA NA 918 1110 1 J q B

2,3,7,8-TCDF NA NA NA NA 7.61 # 7.53 # 9.6 U

1,2,3,7,8-PeCDF NA NA NA NA 2.61 0.130 U 48 U 2,3,4,7,8-PeCDF NA NA NA NA 5.04 0.167 U 48 U 1,2,3,4,7,8-HxCDF NA NA NA NA 13.7 14.2 48 U 1,2,3,6,7,8-HxCDF NA NA NA NA 3.58 4.15 48 U 2,3,4,6,7,8-HxCDF NA NA NA NA 2.45 2.74 48 U 1,2,3,7,8,9-HxCDF NA NA NA NA 0.141 U 0.408 0.37 J q B 1,2,3,4,6,7,8-HpCDF NA NA NA NA 60.0 59.2 0.27 J B 1,2,3,4,7,8,9-HpCDF NA NA NA NA 2.54 3.06 48 U OCDF NA NA NA NA 98.0 91.3 0.79 J q B

Newark Bay Upland 2017 - Composite C - Dioxin/Furan -TEQ Converted values

Dioxin/Furan TEF

Unamended Sediment

(Units: ppt)

Amended Sediment

(Units: ppt)

SPLP

(Units: pg/L)

ASI ID # 20170125 20170149 20170149

Comp C Q A Comp C Q A Comp C Q

2,3,7,8-TCDD 1 11.58 13.17 9.60 U

1,2,3,7,8-PeCDD 1 0.09 U 0.09 U 48.00 U 1,2,3,4,7,8-HxCDD 0.1 0.02 U 0.02 U 4.80 U 1,2,3,6,7,8-HxCDD 0.1 0.53 0.86 0.02 J q B 1,2,3,7,8,9-HxCDD 0.1 0.47 0.64 4.80 U 1,2,3,4,6,7,8-HpCDD 0.01 0.99 1.24 0.48 U 1,2,3,4,6,7,8,9-OCDD 0.0003 0.28 0.33 0.00 J q B

2,3,7,8-TCDF 0.1 0.76 # 0.75 # 0.96 U

1,2,3,7,8-PeCDF 0.03 0.08 0.00 U 1.44 U 2,3,4,7,8-PeCDF 0.3 1.51 0.05 U 14.40 U 1,2,3,4,7,8-HxCDF 0.1 1.37 1.42 4.80 U 1,2,3,6,7,8-HxCDF 0.1 0.36 0.42 4.80 U 2,3,4,6,7,8-HxCDF 0.1 0.24 0.27 4.80 U 1,2,3,7,8,9-HxCDF 0.1 0.01 U 0.04 0.04 J q B 1,2,3,4,6,7,8-HpCDF 0.01 0.60 0.59 0.00 J B 1,2,3,4,7,8,9-HpCDF 0.01 0.03 0.03 0.48 U 1,2,3,4,6,7,8,9-OCDF 0.0003 0.03 0.03 0.00 J q B TOTAL TEF as 2,3,7,8-TCDD 18.96 19.96 99.42

Newark Bay Upland 2017 Composite D

Newark Bay Upland 2017 - Composite D - Sediment Volatiles

Volatiles Action Level Action Level

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 ug/kg ug/L Comp D Q A Comp D Q A Comp D Q

Chloromethane (Methyl Chloride) 4000 30 11 U 9.9 U 5 U Bromomethane 25000 10 11 U 9.9 U 5 U Vinyl chloride 700 5 11 U 9.9 U 5 U Chloroethane 220000 NA 11 U 9.9 U 5 U Methylene chloride (Dichloromethane) 34000 3 5.1 J B 5.7 J B 3.2 J B Acetone 70000000 700 44 U 160 20 U Carbon disulfide 7800000 NA 11 U 9.9 U 5 U 1,1-Dichloroethene 11000 2 11 U 9.9 U 5 U 1,1-Dichloroethane 8000 50 11 U 9.9 U 5 U 1,2-Dichloroethene (total) 10 22 U 20 U 10 U Chloroform 600 6 11 U 9.9 U 5 U 1,2-Dichloroethane 900 NA 11 U 9.9 U 5 U 2-Butanone (MEK) 3100000 300 11 U 42 3.8 J 1,1,1-Trichloroethane 290000 30 11 U 9.9 U 5 U Carbon tetrachloride 600 2 11 U 9.9 U 5 U Bromodichloromethane 1000 1 11 U 9.9 U 5 U 1,2-Dichloropropane 2000 1 11 U 9.9 U 5 U cis-1,3-Dichloropropene NA NA 11 U 9.9 U 5 U Trichloroethene 7000 1 11 U 9.9 U 5 U Dibromochloromethane 3000 10 11 U 9.9 U 5 U 1,1,2-Trichloroethane 2000 3 11 U 9.9 U 5 U Benzene 2000 1 11 U 9.9 U 5 U trans-1,3-dichloropropene NA NA 11 U 9.9 U 5 U Bromoform 81000 4 11 U 9.9 U 5 U 4-Methyl-2-pentanone (MIBK) NA 400 11 U 9.9 U 5 U 2-Hexanone NA NA 11 U 9.9 U 5 U Tetrachloroethene 2000 1 11 U 9.9 U 5 U 1,1,2,2-Tetrachloroethane 1000 NA 11 U 9.9 U 5 U Toluene 6300000 1000 11 U 9.9 U 5 U Chlorobenzene 510000 50 11 U 9.9 U 5 U Ethyl benzene 7800000 700 11 U 9.9 U 5 U Styrene 90000 100 11 U 9.9 U 5 U Xylenes(Total) 12000000 1000 22 U 20 U 10 U Acrolein 500 220 U 200 U 100 U Acrylonitrile 900 110 U 99 U 50 U 1,2-Dibromo-3-chloropropane 80 11 U 9.9 U 5 U 1,2-Dibromoethane 8 11 U 9.9 U 5 U Dichlorodifluoromethane 490000 11 U 9.9 U 5 U * 1,2-Dichloroethene (cis) 230000 11 U 9.9 U 5 U 1,2-Dichloroethene (trans) 300000 11 U 9.9 U 5 U Methyl acetate 78000000 55 U 50 U 25 U * Methyl tert-butyl ether (MTBE) 110000 11 U 9.9 U 5 U * Tertiary butyl alcohol (TBA) 1400000 110 U 99 U 50 U Trichlorofluoromethane 23000000 11 U 9.9 U 5 U Combined 1,3-dichloropropenes (SUM) cis 2000 0.2 1,4-dioxane 2900 U 2000 U 9.6 U n-propylbenzene 11 U 9.9 U 5 U sec-butylbenzene 11 U 9.9 U 5 U tert-butylbenzene 11 U 9.9 U 5 U 1,2,4-trimethylbenzene 11 U 9.9 U 5 U 1,3,5-trimethylbenzene 11 U 9.9 U 5 U

Newark Bay Upland 2017 - Composite D - Sediment Semivolatiles

Semivolatiles Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 ug/kg ug/kg mg/L mg/L Comp D Q A Comp D Q A Comp D Q

Phenol 18000000 660 4 0.01 1400 U 320 U 0.0096 U bis(2-Chloroethyl)ether 400 660 0.01 0.01 290 U 65 U 0.0019 U 2-Chlorophenol 310000 660 0.005 0.01 1400 U 320 U 0.0096 U 1,3-Dichlorobenzene 5300000 660 0.6 0.01 1400 U 320 U 0.0096 U 1,4-Dichlorobenzene 5000 660 0.075 0.01 1400 U 320 U 0.0096 U 1,2-Dichlorobenzene 5300000 660 0.6 0.01 1400 U 320 U 0.0096 U 2-Methylphenol (o-cresol) 310000 660 NA 0.01 1400 U 320 U 0.0096 U 1-Chloropropane-2,2'-oxybis/ bis(2-chloroisop 23000 660 0.3 0.01 290 U 65 U 0.0019 U 4-Methylphenol (p-cresol) (co-elutes with 3-met 31000 660 NA 0.01 1400 U 320 U 0.0096 U N-Nitroso-Di-N-Propylamine 200 660 0.02 0.01 290 U 65 U 0.0019 U Hexachloroethane 35000 660 0.01 0.01 1400 U 320 U 0.0096 U Nitrobenzene 31000 660 0.01 0.01 2900 U 650 U 0.019 U Isophorone 510000 660 0.1 0.01 1400 U 320 U 0.0096 U 2-Nitrophenol NA 660 NA 0.01 1400 U 320 U 0.0096 U 2,4-Dimethylphenol 1200000 660 0.1 0.01 1400 U 320 U 0.0096 U bis(2-Chloroethoxy)methane NA 660 NA 0.01 1400 U 320 U 0.0096 U 2,4-Dichlorophenol 180000 660 0.02 0.01 290 U 65 U 0.0019 U 1,2,4-Trichlorobenzene 73000 660 0.009 0.01 1400 U 320 U 0.0096 U Naphthalene 6000 660 0.3 0.01 110 J 21 J 0.0019 U 4-Chloroaniline NA 1300 NA 0.02 1400 U 320 U 0.0096 U Hexachloro-1,3-butadiene 6000 660 NA 0.01 290 U 65 U 0.0019 U 4-Chloro-3-methylphenol NA 1300 NA 0.02 1400 U 320 U 0.0096 U 2-Methylnaphthalene 230000 660 NA 0.01 70 J 13 J 0.0019 U Hexachlorocyclopentadiene 45000 660 0.05 0.01 1400 U 320 U 0.0096 U 2,4,6-Trichlorophenol 19000 660 0.02 0.01 1400 U 320 U 0.0096 U 2,4,5-Trichlorophenol 6100000 660 0.7 0.01 1400 U 320 U 0.0096 U 2-Chloronaphthalene NA 660 NA 0.01 290 U 65 U 0.0019 U 2-Nitroaniline 39000 3300 NA 0.05 7300 U 1700 U 0.048 U Dimethylphthalate NA 660 NA 0.01 1400 U 320 U 0.0096 U Acenaphthylene 300000000 660 NA 0.01 200 J 51 J 0.0019 U 2,6-Dinitrotoluene 700 660 0.01 0.01 1400 U 320 U 0.0096 U 3-Nitroaniline NA 3300 NA 0.05 7300 U 1700 U 0.048 U

Newark Bay Upland 2017 - Composite D - Sediment Semivolatiles, con't.

Semivolatiles, continued Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 ug/kg ug/kg mg/L mg/L Comp D Q A Comp D Q A Comp D Q

Acenaphthene 3400000 660 0.4 0.01 53 J 84 U 0.0019 U 2,4-Dinitrophenol 120000 3300 0.04 0.05 7300 U 1700 U 0.048 U 4-Nitrophenol NA 3300 NA 0.05 7300 U 1700 U 0.048 U Dibenzofuran NA 660 NA 0.01 1400 U 320 U 0.0096 U 2,4-Dinitrotoluene 700 660 0.01 0.01 1400 U 320 U 0.0096 U Diethylphthalate 49000000 660 5 0.01 1400 U 320 U 0.0096 U 4-Chlorophenyl-phenylether NA 660 NA 0.01 1400 U 320 U 0.0096 U Fluorene 2300000 660 0.3 0.01 93 J 65 U 0.0019 U 4-Nitroaniline NA 660 NA 0.02 7300 U 1700 U 0.048 U 4,6-Dinitro-2-methylphenol 6000 3300 NA 0.05 7300 U 1700 U 0.048 U N-Nitrosodiphenylamine 99000 660 0.02 0.01 1400 U 320 U 0.0096 U 4-Bromophenyl-phenylether NA 660 NA 0.01 1400 U 320 U 0.0096 U Hexachlorobenzene 300 660 0.01 0.01 290 U 65 U 0.0019 U Pentachlorophenol 3000 3300 0.001 0.05 1400 U 320 U 0.0096 U Phenanthrene 300000000 6600 NA 0.01 290 66 0.0019 U Anthracene 17000000 6600 2 0.01 220 J 130 0.0019 U Carbazole 24000 330 NA 0.01 290 U 36 J 0.0019 U Di-n-butylphthalate 6100000 330 0.9 0.01 1400 U 320 U 0.0096 U Fluoranthene 2300000 660 0.3 0.01 680 170 0.0019 U Pyrene 1700000 660 0.2 0.01 590 150 0.0019 U Butylbenzylphthalate 1200000 660 0.1 0.01 1400 U 320 U 0.0096 U 3,3'-Dichlorobenzidine 1000 1300 0.06 0.02 1400 U 320 U 0.0096 U Benzo(a)anthracene 600 660 NA 0.01 410 100 0.0019 U Chrysene 62000 660 NA 0.01 500 120 0.0019 U bis(2-Ethylhexyl)phthalate 35000 660 0.03 0.01 960 J 200 J 0.019 U DI-n-octylphthalate 2400000 660 0.1 0.01 1400 U 320 U 0.0096 U Benzo(b)fluoranthene 600 660 NA 0.01 510 170 0.0019 U Benzo(k)fluoranthene 6000 660 NA 0.01 290 34 J 0.0019 U Benzo(a)pyrene 200 660 NA 0.01 500 120 0.0019 U Indeno(1,2,3-cd)pyrene 600 660 NA 0.01 320 85 0.0019 U Dibenzo(a,h)anthracene 200 660 NA 0.01 290 U 65 U 0.0019 U Benzo(ghi)perylene 30000000 660 NA 0.01 410 110 0.0019 U Pyridine NA 1400 U 320 U 0.0096 U Acetophenone 2000 1400 U 320 U 0.019 U Atrazine 210000 1400 U 320 U 0.019 U Benzaldehyde 6100000 1400 U 320 U 0.0011 J Benzidine 700 29000 U 6500 U 0.19 U 1,1'-Biphenyl 3100000 1400 U 320 U 0.0096 U Caprolactam 31000000 7300 U 1700 U 0.048 U 1,2-Diphenylhydrazine 700 1400 U 320 U 0.0096 U N-Nitrosodimethylamine 700 1400 U 320 U 0.0096 U

Newark Bay Upland 2017 - Composite D - Pesticides/Aroclors

Pesticides/Aroclors Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 ug/kg ug/kg mg/L mg/L Comp D Q A Comp D Q A Comp D Q alpha-BHC 100 1.9 0.00002 0.00005 1.8 U 1.6 U 0.000052 U beta-BHC 400 3.3 0.0002 0.00005 1.8 U 1.6 U 0.000052 U delta-BHC NA 1.7 NA 0.00005 1.8 U 1.6 U 0.000052 U gamma-BHC (Lindane) 400 2 0.0002 0.00005 1.8 U 1.6 U 0.000052 U Heptachlor 100 2.1 0.0004 0.00005 1.8 U 1.6 U 0.000052 U Aldrin 40 2 0.00004 0.00005 1.8 U 1.6 U 0.000052 U Heptachlor epoxide 70 2.1 0.0002 0.00005 1.5 J p 1.1 J p 0.000052 U Endosulfan I NA 2.1 0.0004 0.00005 1.8 U 1.6 U 0.000052 U Dieldrin 40 3.3 0.00003 0.0001 0.96 J p 1.6 U 0.000052 U 4,4'-DDE 2000 4.2 0.0001 0.0001 13 5.9 p 0.000052 U Endrin 23000 3.6 0.002 0.0001 1.8 U 1.6 U 0.000052 U Endosulfan II NA 3.3 0.0004 0.0001 1.8 U 1.6 U 0.000052 U 4,4'-DDD 3000 4.2 0.0001 0.0001 4.7 p 3.3 p 0.000052 U Endosulfan sulfate 470000 3.6 0.0004 0.0001 1.8 U 1.6 U 0.000052 U

4,4'-DDT 2000 3.6 0.0001 0.0001 1.8 U 1.6 U 0.000052 U

Methoxychlor 390000 17 0.04 0.001 1.8 U 1.6 U 0.000052 U Endrin ketone NA 3.3 NA 0.0001 1.8 U 1.6 U 0.000052 U Endrin aldehyde NA 3.3 NA 0.0001 1.8 U 1.6 U 0.000052 U alpha-Chlordane 200 1.7 NA 0.00005 2.2 1.1 J 0.000052 U gamma-Chlordane 200 1.7 0.0005 0.00005 1.8 U 1.6 U 0.000052 U Toxaphene 600 170 0.003 0.005 73 U 65 U 0.0042 U Aroclor-1016 NA 33 NA 0.001 18 U 16 U 0.00042 U Aroclor-1221 NA 67 NA 0.002 18 U 16 U 0.00042 U Aroclor-1232 NA 33 NA 0.001 18 U 16 U 0.00042 U Aroclor-1242 NA 33 NA 0.001 18 U 16 U 0.00042 U Aroclor-1248 NA 33 NA 0.001 18 U 16 U 0.00042 U Aroclor-1254 NA 33 NA 0.001 97 60 0.00042 U Aroclor-1260 NA 33 NA 0.001 52 49 0.00042 U Total Aroclor(SUM) 200 NA 0.005 NA 0 Mirex 1.8 U 1.6 U 0.000052 U

Newark Bay Upland 2017 - Composite D - Herbicides

Herbicides Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ug/kg)

Amended Sediment

(Units: ug/kg)

SPLP

(Units:

ug/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 Comp D Q A Comp D Q A Comp D Q

2,4,5-TP (Silvex) NA NA NA NA 44 U 40 U 0.95 U

2,4-D NA NA NA NA 170 U 160 U 3.8 U

Newark Bay Upland 2017 - Composite D - Metals

Sediment

(Units: mg/kg)

Amended Sediment

(Units: mg/kg)

SPLP

(Units:

mg/L)

ASI ID # Soil Leachate 20170126 20170150 20170150 mg/kg mg/kg mg/L mg/L Comp D Q A Comp D Q A Comp D Q

Aluminum 78000 40 0.2 0.2 13000 11000 1.3 Antimony 31 12 0.02 0.06 0.67 J 0.92 U 0.01 U Arsenic 19 2 0.008 0.01 11 8.2 0.01 U Barium 16000 40 2 0.2 79 63 0.031 J Beryllium 16 1 0.02 0.005 0.81 0.61 0.004 U Cadmium 78 1 0.004 0.005 0.56 0.39 J 0.005 U Calcium NA 1000 NA 5 8300 36000 180 Chromium NA 2 0.1 0.01 62 46 0.0064 Hexavalent Chromium 120000 0.87 U 0.81 U 0.0064 U F1 Trivalent Chromium 20 62 46 0.0064 J Cobalt 1,600 10 NA 0.05 12 8.5 0.0033 J Copper 590 5 1 0.025 70 52 0.14 Iron NA 20 0.3 1 28000 20000 0.1 U Lead 400 0.6 0.01 0.003 79 55 0.01 U Magnesium NA 1000 NA 5 8700 6600 5 U Manganese 5900 3 0.05 0.015 610 460 0.015 U Mercury 23 0.1 0.002 0.0002 1.2 0.91 0.0002 U Nickel 1,600 8 0.1 0.04 51 30 0.03 J Potassium NA 1000 NA 5 2900 2500 33 Selenium 390 1 0.05 0.015 1.1 U 0.56 J 0.0076 J Silver 390 2 NA 0.01 0.94 0.64 0.005 U Sodium NA 1000 50 5 7900 5700 180 Thallium 5 2 0.01 0.01 2.2 U 1.8 U 0.02 U Vanadium 78 10 NA 0.05 33 25 0.0077 J Zinc 23,000 4 5 0.02 160 150 0.02 U Cyanide, total 1,600 0.5 0.2 0.01 0.58 0.38 J 0.01 U %Solids NA NA NA NA 45.7 50.4

Newark Bay Upland 2017 - Composite D - Dioxin/Furan

Dioxin/Furan Action Level NJDEP DL Action Level NJDEP DL

Unamended Sediment

(Units: ng/kg)

Amended Sediment

(Units: ng/kg)

SPLP

(Units: pg/L) ASI ID # Soil Leachate 20170126 20170150 20170150 ng/kg pg/L Comp D Q A Comp D Q A Comp D Q

2,3,7,8-TCDD NA NA NA NA 33.8 30.2 9.6 U

1,2,3,7,8-PeCDD NA NA NA NA 1.15 U 2.02 48 U 1,2,3,4,7,8-HxCDD NA NA NA NA 0.960 U 2.12 48 U 1,2,3,6,7,8-HxCDD NA NA NA NA 1.11 U 8.16 48 U 1,2,3,7,8,9-HxCDD NA NA NA NA 0.980 U 6.47 48 U 1,2,3,4,6,7,8-HpCDD NA NA NA NA 91.4 165 48 U

OCDD NA NA NA NA 946 1680 1.8 J B

2,3,7,8-TCDF NA NA NA NA 7.97 # 10.3 # 9.6 U

1,2,3,7,8-PeCDF NA NA NA NA 0.688 U 4.18 48 U 2,3,4,7,8-PeCDF NA NA NA NA 0.980 U 7.33 0.22 J q B 1,2,3,4,7,8-HxCDF NA NA NA NA 0.626 U 26.4 48 U 1,2,3,6,7,8-HxCDF NA NA NA NA 0.626 U 6.72 48 U 2,3,4,6,7,8-HxCDF NA NA NA NA 0.751 U 3.43 48 U 1,2,3,7,8,9-HxCDF NA NA NA NA 0.814 U 0.401 48 U 1,2,3,4,6,7,8-HpCDF NA NA NA NA 77.9 108 0.3 J q B 1,2,3,4,7,8,9-HpCDF NA NA NA NA 0.960 U 0.095 U 48 U OCDF NA NA NA NA 96.3 167 0.75 J q B

Newark Bay Upland 2017 - Composite D - Dioxin/Furan -TEQ Converted values

Dioxin/Furan TEF

Unamended Sediment

(Units:…