W9123721Q0019.pdf

SEE ADDENDUM

(No Collect Calls)

W9123721Q0019 09-Nov-2020

b. TELEPHONE NUMBER

304.399.5337

8. OFFER DUE DATE/LOCAL TIME

11:00 AM 09 Dec 2020

5. SOLICITATION NUMBER 6. SOLICITATION ISSUE DATE

AUTHORIZED FOR LOCAL REPRODUCTION

PREVIOUS EDITION IS NOT USABLE

STANDARD FORM 1449 (REV. 2/2012)

Prescribed by GSA – FAR (48 CFR) 53.212

(TYPE OR PRINT)

(SIGNATURE OF CONTRACTING OFFICER)

ADDENDA ARE

26. TOTAL AWARD AMOUNT (For Gov t. Use Only )

23.

CODE 10. THIS ACQUISITION IS

SUCH ADDRESS IN OFFER

17b. CHECK IF REMITTANCE IS DIFFERENT AND PUT

BELOW IS CHECKED

TELEPHONE NO.

W912379. ISSUED BY

18b. SUBMIT INVOICES TO ADDRESS SHOWN IN BLOCK 18a. UNLESS BLOCK

7. FOR SOLICITATION

INFORMATION CALL:

a. NAME

CYNTHIA A OXLEY

2. CONTRACT NO. 3. AWARD/EFFECTIVE DATE 4. ORDER NUMBER

(TYPE OR PRINT)

30b. NAME AND TITLE OF SIGNER 30c. DATE SIGNED 31b. NAME OF CONTRACTING OFFICER

30a. SIGNATURE OF OFFEROR/CONTRACTOR 31a.UNITED STATES OF AMERICA

0 27a. SOLICITATION INCORPORATES BY REFERENCE FAR 52.212-1. 52.212-4. FAR 52.212-3. 52.212-5 ARE ATTACHED.

25. ACCOUNTING AND APPROPRIATION DATA

1. REQUISITION NUMBER

20.

ADDITIONAL SHEETS SUBJECT TO THE TERMS AND CONDITIONS SPECIFIED.

OFFEROR TO COMPLETE BLOCKS 12, 17, 23, 24, AND 30

SOLICITATION/CONTRACT/ORDER FOR COMMERCIAL ITEMS

W81F8E00591055

ARE NOT ATTACHED

27b. CONTRACT/PURCHASE ORDER INCORPORATES BY REFERENCE FAR 52.212-4. FAR 52.212-5 IS ATTACHED. ADDENDA ARE ARE NOT ATTACHED

(BLOCK 5), INCLUDING ANY ADDITIONS OR CHANGES WHICH ARE

SET FORTH HEREIN, IS ACCEPTED AS TO ITEMS:

. YOUR OFFER ON SOLICITATION

28. CONTRACTOR IS REQUIRED TO SIGN THIS DOCUMENT AND RETURN

% FOR:SET ASIDE:UNRESTRICTED ORX

SMALL BUSINESS

17a.CONTRACTOR/ CODE FACILITY

OFFEROR CODE

USACE, CONTRACTING DIVISION

CYNTHIA OXLEY, 502 8TH STREET

HUNTINGTON WV 25701

18a. PAYMENT WILL BE MADE BY CODE

RATED ORDER UNDER

DPAS (15 CFR 700)

13a. THIS CONTRACT IS A

13b. RATING

CODE15. DELIVER TO CODE 16. ADMINISTERED BY

SEE SCHEDULE

12. DISCOUNT TERMS11. DELIVERY FOR FOB DESTINA-

TION UNLESS BLOCK IS

MARKED

SEE SCHEDULE

14. METHOD OF SOLICITATION

RFQ IFB RFPX

304-399-5281FAX:

TEL: 304-399-5337 SERVICE-DISABLED

VETERAN-OWNED

SMALL BUSINESS

8(A)

HUBZONE SMALL

BUSINESS

SIZE STANDARD:

$16,500,000

NAICS:

541380

X

OFFER DATED

29. AWARD OF CONTRACT: REF.

DELIVER ALL ITEMS SET FORTH OR OTHERWISE IDENTIFIED ABOVE AND ON ANY

COPIES TO ISSUING OFFICE. CONTRACTOR AGREES TO FURNISH AND

EMAIL:

TEL:

31c. DATE SIGNED

SEE SCHEDULE

SCHEDULE OF SUPPLIES/ SERVICESITEM NO. QUANTITY UNIT UNIT PRICE AMOUNT

24.22.21.19.

WOMEN-OWNED SMALL BUSINESS (WOSB)

ELIGIBLE UNDER THE WOMEN-OWNED

SMALL BUSINESS PROGRAM

EDWOSB

32g. E-MAIL OF AUTHORIZED GOVERNMENT REPRESENTATIVE

SOLICITATION/CONTRACT/ORDER FOR COMMERCIAL ITEMS

(CONTINUED)

PAGE 2 OF66

ACCEPTED, AND CONFORMS TO THE CONTRACT, EXCEPT AS NOTED: ______________________________________________________

32a. QUANTITY IN COLUMN 21 HAS BEEN

RECEIVED INSPECTED

32b. SIGNATURE OF AUTHORIZED GOVERNMENT

REPRESENTATIVE

32c. DATE 32d. PRINTED NAME AND TITLE OF AUTHORIZED GOVERNMENT

REPRESENTATIVE

32e. MAILING ADDRESS OF AUTHORIZED GOVERNMENT REPRESENTATIVE 32f . TELEPHONE NUMBER OF AUTHORIZED GOVERNMENT REPRESENTATIVE

37. CHECK NUMBER

FINALPARTIALCOMPLETE

36. PAYMENT35. AMOUNT VERIFIED

CORRECT FOR

34. VOUCHER NUMBER

FINAL

33. SHIP NUMBER

PARTIAL

38. S/R ACCOUNT NUMBER 39. S/R VOUCHER NUMBER 40. PAID BY

41a. I CERTIFY THIS ACCOUNT IS CORRECT AND PROPER FOR PAYMENT

41b. SIGNATURE AND TITLE OF CERTIFYING OFFICER 41c. DATE

42a. RECEIVED BY (Print)

42b. RECEIVED AT (Location)

42c. DATE REC'D (YY/MM/DD) 42d. TOTAL CONTAINERS

STANDARD FORM 1449 (REV. 2/2012) BACK

Prescribed by GSA – FAR (48 CFR) 53.212

AUTHORIZED FOR LOCAL REPRODUCTION

PREVIOUS EDITION IS NOT USABLE

SEE SCHEDULE

20.

SCHEDULE OF SUPPLIES/ SERVICES

21.

QUANTITY UNIT

22. 23.

UNIT PRICE

24.

AMOUNT

19.

ITEM NO.

INSTRUCTIONS TO OFFERORS

This Request for Quote (RFQ) is for an Indefinite Delivery, Indefinite Quantity (IDIQ) Contract to provide all management, labor, supplies, materials and equipment necessary to perform Water Quality Analysis Services for the US Army Corps of Engineers, Huntington, District. All work shall be performed in strict compliance with the attached Performance Work Statement (PWS) and all other terms, clauses and conditions incorporated herein. The base period for this contract will be from on Date of Award through 30 September 2021.

Note: This solicitation contains an option clause to extend the awarded contract for up to four (4) additional one-year option periods. The one-year option periods are as follows:

Option Period 1: 1 October 2021 through 30 September 2022 Option Period 2: 1 October 2022 through 30 September 2023 Option Period 3: 1 October 2023 through 30 September 2024 Option Period 4: 1 October 2024 through 30 September 2025

Simplified acquisition procedures for commercial services are being used in this procurement in accordance with FAR 13.500(c)(2).

One award will be made from this RFQ. The Government intends to evaluate quotes and award a contract without discussions with offerors (See 52.212-1(g)).

This procurement is an unrestricted procurement, under NAICS code 541380 ($16.5 million average annual receipts for the previous three years).

The Method of Payment under this contract will be Electronic Funds Transfer (EFT) to a commercial bank account specified by the Contractor.

There is no bonding requirement for this procurement action.

Quotes will not be accepted for quantities less than the quantities specified in the price breakout schedule.

Failure to submit a unit price for all items listed (base period and option periods) will be considered as a material deviation from the requirements of the Request for Quote (RFQ) and the quote will be rejected.

IMPORTANT NOTICE: Effective September 26, 2018 and in accordance with FAR Clause 52.204-7, “an Offeror is required to be registered in SAM when submitting an offer or quotation, and shall continue to be registered until time of award, during performance, and through final payment of any contract, basic agreement, basic ordering agreement, or blanket purchasing agreement resulting from this solicitation.” Vendors are highly encouraged to check their registration status and plan accordingly prior to submitting an offer. Vendors can check whether an account is active by performing a query by their CAGE or Unique Entity Identifier (known as DUNS). Vendors are highly encouraged to begin registering as soon as possible in order to be considered for contract awards. Remember, there is no cost to use SAM. To find out additional information about the changes of the SAM registration process, contractors should visit the Frequently Asked Questions (FAQ) link located at the top of the SAM homepage (https://beta.sam.gov).

Submit Offers to: cynthia.a.oxley@usace.army.mil

Quotes are due on the date and time identified on page 1 (box 8) of this solicitation. Electronic and fax submittals will not be accepted.

For contractual/technical questions, please contract Cynthia Oxley at 304-399-5337 or by email at cynthia.a.oxley@usace.army.mil

Evaluation—Commercial Items, IAW FAR 52.212-2:

(a) The Government will award a contract resulting from this solicitation to the responsible offeror whose offer conforms to the solicitation and will be most advantageous to the Government, price and other factors considered.

Factors A and B are of equal importance. The remaining factors (C, D and E) are listed in descending order of importance with Factors A and B being significantly more important than factors C, D and E.

Notwithstanding any other provisions of these specifications concerning the method of award, the best value trade-off process will be used in this acquisition with award made, as a whole, to the offeror whose quote conforms to the solicitation and has been evaluated as most advantageous to the Government with appropriate consideration given to the evaluation factors: Technical Capability, Management and Administration, Past Performance and Price. Offerors will be cautioned that the award may not necessarily be made to the lowest price offered.

All non-priced factors, when combined, are more important than price. Thus, price is not expected to be the controlling factor in the selection of the Contractor for this solicitation. However, as the evaluated merit of competing technical offers becomes more equal, total price and other price factors will become more important in the selection. Total price and other price factors could become the deciding factor for selection, depending upon whether the most acceptable technical offer is determined to be worth the cost differential, if any.

The evaluation approach for all technical factors is as follows: The offer will be evaluated to determine the extent to which each requirement has been addressed in accordance with the terms and conditions listed in this solicitation.

A. Technical Capability

This factor evaluates the offeror’s proposed capability to perform specific tasks that may be required for the basic contract period and all option years. Marginal levels of overall demonstrated ability to perform these tasks could indicate either a lack of ability to perform or lack of understanding concerning mission requirements and may result in the entire proposal receiving an unfavorable rating and/or being eliminated from the competitive range. The evaluation will focus on the following:

• Document the ability to perform at least fifty percent of analyses in-house. At a minimum, the following tests shall be completed in-house: water analyses - ICP metals, ICP-MS metals, mercury, nitrate/nitrite, ammonia, nitrogen, phosphorus, organic carbon, solids, sulfate, chloride, hot peroxide acidity, total alkalinity, bicarbonate, pH, hardness, specific conductance, sediment analyses - metals and % solids, and animal tissue analyses - % lipids and % moisture.

• Demonstrate the ability to analyze samples by APHA, ASTM, and EPA approved methods and knowledge of the correct container types, preservatives and holding times associated with these methods.

Document the methods that will be used for each analysis. In the event that any method not approved by EPA must be used, prior approval from the Contracting Official is required.

• Document efforts to be aware of and adapt to evolving industry standards such as changes in methods, instrumentation, or procedures.

• Provide standard operating procedures (SOP) for laboratory procedures for sample login, sample tracking, and throughput, and for analytical procedures.

• Document the plan to monitor and ensure high quality work when subcontractors are utilized.

• Demonstrate an understanding of the concept of complex relational databases. Provide examples of any electronic data deliverable (EDD) formats that can be used in the delivery of test results. Include any types of EDDs used for any previous DoD or other contracts.

• Demonstrate knowledge of and ability to follow procedures specific to DoD sample preparation and analysis, such as those found in the Inland Testing Manual.

• Demonstrate knowledge of current industry standards in test methods and instrumentation.

• Demonstrate knowledge of relationships between parameters in water quality testing and phenomena occurring in water environments. Demonstrate familiarity with water quality characteristics or conditions and how they may be related to different lab analyses. Explain how this understanding relates to lab processes.

• Demonstrate the ability to accurately associate sample identification information with test results, as each sample progresses through the laboratory.

• Demonstrate the ability to provide laboratory bench sheets, either in hard copy, on a compact disk or as an electronic mail attachment.

B. Management and Administration

As part of their quote, the contractor should furnish a plan that will insure that the proper level of effort is directed toward each aspect of the services required; that the offeror has at his or her disposal the organization and personnel required by the specification of the contract; and assure that all work will be performed as specified. The considerations listed below are not sub-factors and will not receive individual ratings:

Personnel and Organization - This factor evaluates the offerors proposed organizational structure and personnel provided for overall management of the work associated with this contract. The evaluation will focus on the following:

• Person(s) provided who will be the on-site Contractor Representative(s).

• Technical trades personnel to be utilized to perform the work with focus on their education, background, experiences, licenses, certificates, or other information evidencing their qualifications.

• Organizational placement of personnel and whether such individuals are current on the offeror’s payroll or have been personally committed for employment on this contract.

• Proposed subcontractors and their role in the contract.

• Personnel management policies regarding standards of conduct and disciplinary practices.

• Strike Contingency Plan.

• Administrative procedures to assure availability of key management personnel to be contacted as the need arises.

Quality Control - This consideration assesses the offeror’s ability to provide a Quality Control Program to insure total compliance with the contract requirements and a high quality product for the Government. The consideration will focus on the following:

• Inspection system covering all the tasks identified under factor 1.

• Method of identifying deficiencies in the quality of work performed before the level of performance is unacceptable.

• Filing system of all inspections conducted by the Contractor and the corrective action taken.

• Method insuring that employees have full knowledge of assignments and that appropriate technical expertise is utilized with each work assignment.

Capacity/Equipment– This consideration assesses the offeror’s ability to perform work associated with this contract safely and in compliance and have adequate staff and instrumentation to complete approximately $300,000 in contract work in a satisfactory and efficient manner.

The evaluation will focus on the following information:

• Document whether any work will be subcontracted, because of either capacity limitations or inability to perform certain tests in-house.

• Document contingencies in the event of instrument failure or sample quantity exceeding lab capacity. Demonstrate ability to manage sample throughput especially during periods of increased quantities of samples. This includes attention to storage and login of samples, assignment of lab identification numbers, and adequate tracking of sample progress from analyst to analyst to avoid sample mix-ups. Document facility specifications and show that laboratory has adequate designated areas for specific functions.

• Provide a statement describing the organization’s preventative and breakdown maintenance program and submit a complete detailed plan of operation in the event of equipment failure.

Location of Firm in the General Geographical Area – This consideration assesses the offeror’s ability in providing the required services within the geographical boundaries of the contract. The proposal should provide the location of the home office and all branch offices and define which offices will be involved in the performance of this contract.

Provide a narrative for each office identified describing their proposed role and type of support provided (i.e. personnel, equipment, and material). Include in your narrative the location(s) from which the majority of personnel and equipment would be provided for work proposed under this contract. This consideration will focus on the following:

• Location of these offices and their proximity to the Huntington District Office for coordination of work.

• The impact of these locations as it relates to the ability and cost of mobilizing/demobilizing personnel and equipment.

C. Past Performance

Information on performance on recent and/or relevant performance within the past five years including names and phone numbers of references and type of work performed. Also, provide this information on any proposed subcontractors. Absent any recent and relevant past performance history or when the performance record is so sparse that no meaningful confidence assessment rating can be reasonably assigned, the offeror will be assigned an “unknown confidence rating” and their quote will not be evaluated either favorably or unfavorably on past performance. The Government may use data provided by the offeror and data obtained from other sources, includingcontractor performance assessment reporting system (CPARS) and data in Government files or and their current and past performance under Federal, State or Local government or commercial contracts for same or similar services. Past Performance will be evaluated for relevancy of similar service/support, complexity, dollar value, contract type and degree of subcontracting/teaming (very relevant, relevant, somewhat relevant, not relevant) and confidence (substantial, satisfactory, limited or no confidence). An unknown confidence rating will be given if the offeror’s performance record is so sparse that no meaningful confidence assessment rating can be reasonably assigned.

NOTE: The Past Performance Questionnaire (Attachment A) included in the solicitation is provided for the offeror or its team members to submit to the client for each project the offeror includes in its quote for Past Performance. Ensure correct phone numbers and email addresses are provided for the client point of contact. If different from the client point of contact, also include the name and phone number of the Contracting Officer. Completed Past Performance Questionnaires should be submitted with your quote. If the offeror is unable to obtain a completed PPQ from a client for a project(s) before quote closing date, the offeror should complete and submit with the quote the first page of the PPQ (Attachment A), which will provide contract and client information for the respective project(s). Offerors should follow-up with clients/references to ensure timely submittal of questionnaires.

If the client requests, questionnaires may be submitted directly to the Government ' s point of contact, Cindy Oxley via email at cynthia.a.oxley@usace.army.mil prior to quote closing date or other date listed in the quote instructions. Offerors shall not incorporate by reference into their quote PPQs previously submitted for other RFQs.

However, this does not preclude the Government from utilizing previously submitted PPQ information in the past performance evaluation.

D. (Small Business Participation Plan)

All Offerors (both large and small businesses) are required to complete a Small Business Participation Plan. Offerors shall propose the level of participation of small businesses (as a small business prime and/or small business subcontractors) in the performance of the acquisition relative to the objectives/goals set forth in the evaluation of this area.

(a) Check the applicable size and categories for the PRIME offeror only—Check all applicable boxes:

( ) Large Prime Or ( ) Small Business Prime; also categorized as (if applicable):

( ) Woman-Owned Small Business (WOSB) ( ) Historically Underutilized Business Zone Small Business (HUBZ) ( ) Small Disadvantaged Small Business (SDB) ( ) Service-Disabled Veteran-Owned Small Business (SDVOSB)

(b) Submit the total combined percentage of work to be performed by both large and small businesses (include the percentage of work to be performed both by Prime and Subcontractors):

Example: If Prime proposes a price of $1,000,000 (including all options), and small business(es) will provide $250,000 in services/supplies as a prime or subcontractor, the % planned for small businesses is 25% and 75% for large business, equaling 100%.

Total Percentage planned for Large Business(es) _______% = $__________ Total Percentage planned for Small Business(es) _______% = $__________ (When combined, Large and Small Business totals must Equal 100%)

(c) Please indicate the total percentage of participation to be performed by each type of subcategory small business. The percentage of work performed by Small Businesses that qualify in multiple small business categories may be counted in each category.

Example: Company A (a WOSB and a SDVOSB) will perform 2%. Company B (a HUBZ and a WOSB) will perform 3%. Results equate to: WOSB 5%; SDVOSB 2%; HUBZone 3%.

Woman-Owned Small Business ______%

HUBZone Small Business ______% Small Disadvantaged Small Business ______% Service-Disabled Veteran-Owned Small Business ______%

(d) List principle supplies/services to be performed by Small Businesses:

Example: If a Small Business qualifies also as a WOSB and a SDVOSB, and you can add them to each category below in which they qualify.

Name of Company Identify Type of Service/Supply Woman-Owned Small Business:

HUBZone Small Business Small Disadvantaged Business:

Service-Disabled Veteran-Owned Small Business:

(e) Describe the extent of commitment to use small businesses (for example, what types of commitments if any are in place for this specific acquisition either—small business prime, written contract, verbal, enforceable, non-enforceable, joint venturing, mentor-protégé, etc.)

(f) ________________________________________________________________

Additional Important Note for Large Business ONLY:

A Small Business Subcontracting Plan is Required (FAR 52.219-9).

Separate from Small Business Participation Plan, large business offerors must also submit a subcontracting plan meeting the requirements of FAR 52.219-9 and DFARS 252.219-7003 (or DFARS 252.219-7004 if the offeror has a comprehensive subcontracting plan.) Large businesses must submit acceptable subcontracting plans to be eligible for award. Subcontracting Plans shall reflect and be consistent with the commitments offered in the Small Business Participation Plan.

E. Cost/Price: Cost/Price will be evaluated for the purpose of determining the reasonableness and completeness of prices offered. Total price and price factors may become the deciding factor for selection, depending upon whether the most acceptable technical quote is determined to be worth the cost differential, if any.

(a) Options. The Government will evaluate offers for award purposes by adding the total price for all options to the total price for the basic requirement. The Government may determine that an offer is unacceptable if the option prices are significantly unbalanced.

Evaluation of options shall not obligate the Government to exercise the option(s).

(b) FAR 52.217-8, Option to Extend Services is included in this solicitation and any resultant contract. The rates to be used during the continued performance of any services will be the rates in effect at the time of the extension.

BASE PERIOD-DATE OF AWARD TO 30 SEP 2021

GENERAL WATER CHEMISTRY ANALYSES

CLIN Description (MDL) Medium Unit

Preferred

Analysis

Method(s)

EST.

QTY U/P TOTAL

0001 Solids: Dissolved, Suspended, and Total (2) Water mg/L USGS or

Standard

Methods 2540

0002 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Water mg/L Lachat or EPA 330

0003 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Water mg/L EPA 300 series or Standard

Methods 2320

0004 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (1), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1

Water ug/L EPA 200 series 350

0005 Hardness, by calculation or titration (5) Water mg/L Standard

Methods 2340

0006 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3)

Water ug/L EPA 200 series 1

0007 Metals by ICP or ICP-MS: Ca (0.04), Mg

(0.4), Na (0.4), K (0.4)

Water mg/L EPA 200 series 1

0008 Analysis of one metal by ICP to lowest practical detection limit

0009 Analysis of one metal by GFAA or ICP-MS to lowest practical detection limit

0010 Silicon (0.25) Water mg/L EPA 200 series 1

0011 Mercury (0.2) Water ug/L EPA 245.1 1

0012 Mercury, low level (<1) Water ng/L EPA 1631 1

0013 Acidity, Total (phenolphthalein) (5) Water mg/L Standard

Methods 2310

0014 Acidity, Methyl Orange (5) Water mg/L Standard

0015 Acidity, Hot Peroxide (5) Water mg/L Standard

0016 Alkalinity, total (5) Water mg/L Standard

0017 Alkalinity, Phenolphthalein (5) Water mg/L Standard

0018 Biological/Biochemical Oxygen Demand

(BOD), 5-Day, to lowest practical detection limit

Water mg/L 1

0019 Carbonaceous Biological/Biochemical

Oxygen Demand (CBOD), to lowest

0020 Chemical Oxygen Demand (COD), to lowest

0021 Bromide (0.25) Water mg/L EPA 300 series 60

0022 Fluoride (0.3) Water mg/L EPA 300 series 1

0023 Iodide (0.3) Water mg/L EPA 300 series 1

0024 Total organic carbon, to lowest practical detection limit

0025 Total inorganic carbon, to lowest practical

0026 Nitrate Nitrogen (0.01) Water mg/L Lachat or EPA 1

0027 Nitrite Nitrogen (0.1) Water mg/L Lachat or EPA 1

0028 Total Kjeldahl Nitrogen (0.1) Water mg/L Lachat or EPA 1

0029 Organic Nitrogen, to lowest practical

0030 Orthophosphorus (0.005) Water mg/L EPA 300 series 1

SEDIMENT, ELUTRIATE, AND ORGANIC ANALYSES (Elutriate costs must include elutriate preparation)

CLIN Description (MDL) Medium Unit

Preferred

Analysis

Method(s)

EST.

QTY LINE ITEM TOTAL

0031 Granulometric Particle-Size Determination, by Sieve Analyses

Sediment % finer

ASTM D-422 10

0032 Granulometric Particle-Size Determinations, by Sieve and Hydrometer Analyses

Sediment % finer

ASTM D-422 4

0033 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Water ug/L EPA 8000 series

0034 Total Oil and Grease, to lowest practical

Water mg/L EPA 1664 4

0035 Total phenolics, to lowest practical detection

Water mg/L EPA 420.1 4

0036 Metals by ICP or ICP-MS: Al (20), Fe (5), (5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Water ug/L EPA 200 series 4

0037 Chloride (0.5) Water mg/L Lachat or EPA 4

0038 Hardness, by titration or calculation (5) Water mg/L Standard

0039 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Water mg/L Lachat or EPA 4

0040 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on current EPA

Priority Pollutant Lists; Herbicides found on current EPA 8151 method list, all to lowest practical detection levels

Elutriate ug/L EPA 8000

0041 Total Oil and Grease, to lowest practical

Elutriate mg/L EPA 1664 4

0042 Total phenolics, to lowest practical detection

Elutriate mg/L EPA 420.1 4

0043 Metals by ICP or ICP-MS: Al (20), Fe (5), (5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Elutriate ug/L EPA 200 series 4

0044 Chloride (0.5) Elutriate mg/L Lachat or EPA 4

0045 Hardness, by titration or calculation (5) Elutriate mg/L Standard

0046 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Elutriate mg/L Lachat or EPA 4

0047 Volatile Compounds (VOCs) by GC/MS on current EPA Priority Pollutant List, to lowest practical detection limits

Sediment ug/L EPA 8000

0048 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Water ug/L EPA 8270 1

0049 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Water ug/L EPA 8151 1

0050 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Water ug/L EPA 8082 1

0051 Pesticides on current EPA Priority Pollutant

Water ug/L EPA 8081 1

0052 Atrazine, to lowest practical detection limit Water ug/L 1

0053 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Water ug/L 1

0054 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Water ug/L 1

0055 Surfactants by MBAS assay, to lowest practical detection limits

Water ug/L MBAS assay 1

0056 Cyanide, to lowest practical detection limits Water mg/L 1

0057 Polynuclear Aromatic Hydrocarbons (PAHs) lowest practical detection limit

Elutriate ug/L EPA 8270 1

0058 Herbicides found on current EPA 8151 limits

Elutriate ug/L EPA 8151 1

0059 Aroclor-specific polychlorinated biphenyls

Elutriate ug/L EPA 8082 1

0060 Pesticides on current EPA Priority Pollutant

Elutriate ug/L EPA 8081 1

0061 Atrazine, to lowest practical detection limit Elutriate ug/L 1

0062 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Elutriate ug/L 1

0063 Total Petroleum Hydrocarbons (TPH), diesel to lowest practical detection limits

Elutriate ug/L 1

0064 Surfactants by MBAS assay, to lowest

Elutriate ug/L MBAS assay 1

0065 Cyanide, to lowest practical detection limits Elutriate mg/L 1

0066 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Sediment ug/k g

EPA 8000

0067 Total Oil and Grease, to lowest practical

Sediment mg/k g

EPA 1664 1

0068 Total phenolics, to lowest practical detection

Sediment mg/k

EPA 420.1 1

0069 Metals by ICP or ICP-MS: Al (20), Fe (5), (5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Sediment ug/k

EPA 200 series 1

0070 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Sediment mg/k

Lachat or EPA 1

0071 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Sediment mg/k g

EPA 300 series or Standard

0072 Polynuclear Aromatic Hydrocarbons (PAHs) lowest practical detection limit

Sediment ug/k

EPA 8270 1

0073 Herbicides found on current EPA 8151 limits

Sediment ug/k

EPA 8151 1

0074 Aroclor-specific polychlorinated biphenyls list, to lowest practical detection limits

Sediment ug/k

EPA 8082 1

0075 Pesticides on current EPA Priority Pollutant

Sediment ug/k

EPA 8081 1

0076 Atrazine, to lowest practical detection limit Sediment ug/k

0077 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Sediment ug/k

0078 Total Petroleum Hydrocarbons (TPH), diesel to lowest practical detection limits

Sediment ug/k

0079 Surfactants by MBAS assay, to lowest

Sediment ug/k

MBAS assay 1

0080 Cyanide, to lowest practical detection limits Sediment mg/kg 1

0081 Analysis of one metal by ICP to lowest

Sediment ug/k

0082 Analysis of one metal by GFAA or ICP-MS to lowest practical detection limit

Sediment ug/k

0083 Total organic carbon, to lowest practical

Sediment mg/kg 1

0084 Total inorganic carbon, to lowest practical

Sediment mg/kg 1

CHLOROPHYLL AND ALGAE ANALYSES

CLIN Description (MDL) Medium Unit

Preferred

Analysis

Method(s)

EST.

QTY U/P TOTAL

0085 Spectrophotometric determination of chlorophyll a (corrected and uncorrected), b, and c, pheophytin, and pheophytin ratio

Chlorophyll Standard

Methods

10200-H

0086 Enumeration and identification of cyanobacteria, to lowest possible taxonomic level, including cell counts, density, and biovolume

Algae 5

0087 Enumeration and identification of cyanobacteria, to lowest possible taxonomic level, including cell counts, density, and biovolume; Toxin analysis of dominant bacteria by enzyme linked immunoassay

(ELISA) and/or liquid chromatography-mass spectrometry (LC/MS)

Algae 5

0088 Qualitative identification of cyanobacteria, to lowest possible taxonomic level

Algae 1

0089 Analysis of a single cyanobacteria toxin by

Enzyme Linked Immunoassay (ELISA)

Algae 1

0090 Analysis of cyanobacteria toxins to include microcystins, cylindrospermopsin, anatoxins and saxitoxins by Enzyme linked immunoassay (ELISA) and/or Liquid

Chromatography-Mass Spectrometry

(LC/MS)

Algae 5

BENTHIC MACROINVERTEBRATE

ANALYSES

Preferred

Analysis

Method(s)

EST.

QTY U/P TOTAL

0091 Sorting, identification, and enumeration of benthic macroinvertebrates to lowest possible taxnomic level with life stage; see scope of work for full instructions

Benthic 25

TOTAL FOR BASE PERIOD

OPTION PERIOD ONE-1 OCT 2021 TO 31 SEP 2022

Preferred Analysis

Method(s)

EST.

QTY U/P TOTAL

1001 Solids: Dissolved, Suspended, and Total (2) Water mg/L USGS or Standard

Methods 2540

1002 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Water mg/L Lachat or EPA 330

1003 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Water mg/L EPA 300 series or

Standard Methods

1004 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (1), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1

Water ug/L EPA 200 series 350

1005 Hardness, by calculation or titration (5) Water mg/L Standard Methods

1006 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3)

Water ug/L EPA 200 series 1

1007 Metals by ICP or ICP-MS: Ca (0.04), Mg

(0.4), Na (0.4), K (0.4)

Water mg/L EPA 200 series 1

1008 Analysis of one metal by ICP to lowest practical detection limit

Water ug/L EPA 200 series 1

1009 Analysis of one metal by GFAA or ICP-MS to lowest practical detection limit

Water ug/L EPA 200 series 1

1010 Silicon (0.25) Water mg/L EPA 200 series 1

1011 Mercury (0.2) Water ug/L EPA 245.1 1

1012 Mercury, low level (<1) Water ng/L EPA 1631 1

1013 Acidity, Total (phenolphthalein) (5) Water mg/L Standard Methods

1014 Acidity, Methyl Orange (5) Water mg/L Standard Methods

1015 Acidity, Hot Peroxide (5) Water mg/L Standard Methods

1016 Alkalinity, total (5) Water mg/L Standard Methods

1017 Alkalinity, Phenolphthalein (5) Water mg/L Standard Methods

1018 Biological/Biochemical Oxygen Demand

(BOD), 5-Day, to lowest practical detection limit

Water mg/L 1

1019 Carbonaceous Biological/Biochemical

Oxygen Demand (CBOD), to lowest practical detection limit

Water mg/L 1

1020 Chemical Oxygen Demand (COD), to lowest practical detection limit

Water mg/L 1

1021 Bromide (0.25) Water mg/L EPA 300 series 60

1022 Fluoride (0.3) Water mg/L EPA 300 series 1

1023 Iodide (0.3) Water mg/L EPA 300 series 1

1024 Total organic carbon, to lowest practical detection limit

Water mg/L 1

1025 Total inorganic carbon, to lowest practical detection limit

Water mg/L 1

1026 Nitrate Nitrogen (0.01) Water mg/L Lachat or EPA 1

1027 Nitrite Nitrogen (0.1) Water mg/L Lachat or EPA 1

1028 Total Kjeldahl Nitrogen (0.1) Water mg/L Lachat or EPA 1

1029 Organic Nitrogen, to lowest practical detection limit

Water mg/L 1

1030 Orthophosphorus (0.005) Water mg/L EPA 300 series 1

SEDIMENT, ELUTRIATE, AND ORGANIC ANALYSES (Elutriate costs must include elutriate preparation)

Preferred Analysis

Method(s)

EST.

QTY U/P TOTAL

1031 Granulometric Particle-Size Determination, by Sieve Analyses

Sediment % finer

ASTM D-422 10

1032 Granulometric Particle-Size Determinations, by Sieve and Hydrometer Analyses

Sediment % finer

ASTM D-422 4

1033 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Water ug/L EPA 8000 series 4

1034 Total Oil and Grease, to lowest practical detection limit

Water mg/L EPA 1664 4

1035 Total phenolics, to lowest practical detection limit

Water mg/L EPA 420.1 4

1036 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Water ug/L EPA 200 series 4

1037 Chloride (0.5) Water mg/L Lachat or EPA 4

1038 Hardness, by titration or calculation (5) Water mg/L Standard Methods

1039 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Water mg/L Lachat or EPA 4

1040 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on current EPA

Priority Pollutant Lists; Herbicides found on current EPA 8151 method list, all to lowest practical detection levels

Elutriate ug/L EPA 8000 series 4

1041 Total Oil and Grease, to lowest practical detection limit

Elutriate mg/L EPA 1664 4

1042 Total phenolics, to lowest practical detection

Elutriate mg/L EPA 420.1 4

1043 Metals by ICP or ICP-MS: Al (20), Fe (5), (5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Elutriate ug/L EPA 200 series 4

1044 Chloride (0.5) Elutriate mg/L Lachat or EPA 4

1045 Hardness, by titration or calculation (5) Elutriate mg/L Standard Methods

1046 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Elutriate mg/L Lachat or EPA 4

1047 Volatile Compounds (VOCs) by GC/MS on current EPA Priority Pollutant List, to lowest practical detection limits

Sediment ug/L EPA 8000 series 4

1048 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Water ug/L EPA 8270 1

1049 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Water ug/L EPA 8151 1

1050 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Water ug/L EPA 8082 1

1051 Pesticides on current EPA Priority Pollutant list, to lowest practical detection limits

Water ug/L EPA 8081 1

1052 Atrazine, to lowest practical detection limit Water ug/L 1

1053 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Water ug/L 1

1054 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Water ug/L 1

1055 Surfactants by MBAS assay, to lowest practical detection limits

Water ug/L MBAS assay 1

1056 Cyanide, to lowest practical detection limits Water mg/L 1

1057 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Elutriate ug/L EPA 8270 1

1058 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Elutriate ug/L EPA 8151 1

1059 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Elutriate ug/L EPA 8082 1

1060 Pesticides on current EPA Priority Pollutant list, to lowest practical detection limits

Elutriate ug/L EPA 8081 1

1061 Atrazine, to lowest practical detection limit Elutriate ug/L 1

1062 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Elutriate ug/L 1

1063 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Elutriate ug/L 1

1064 Surfactants by MBAS assay, to lowest

Elutriate ug/L MBAS assay 1

1065 Cyanide, to lowest practical detection limits Elutriate mg/L 1

1066 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Sediment ug/k g

EPA 8000 series 1

1067 Total Oil and Grease, to lowest practical detection limit

Sediment mg/k g

EPA 1664 1

1068 Total phenolics, to lowest practical detection limit

Sediment mg/k g

EPA 420.1 1

1069 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Sediment ug/k g

EPA 200 series 1

1070 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Sediment mg/k g

Lachat or EPA 1

1071 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Sediment mg/k g

EPA 300 series or

Standard Methods

1072 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Sediment ug/k g

EPA 8270 1

1073 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Sediment ug/k g

EPA 8151 1

1074 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Sediment ug/k g

EPA 8082 1

1075 Pesticides on current EPA Priority Pollutant list, to lowest practical detection limits

Sediment ug/k g

EPA 8081 1

1076 Atrazine, to lowest practical detection limit Sediment ug/k g

1077 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Sediment ug/k g

1078 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Sediment ug/k g

1079 Surfactants by MBAS assay, to lowest practical detection limits

Sediment ug/k g

MBAS assay 1

1080 Cyanide, to lowest practical detection limits Sediment mg/kg 1

1081 Analysis of one metal by ICP to lowest practical detection limit

Sediment ug/k g

EPA 200 series 1

1082 Analysis of one metal by GFAA or ICP-MS to lowest practical detection limit

Sediment ug/k g

EPA 200 series 1

1083 Total organic carbon, to lowest practical detection limit

Sediment mg/kg 1

1084 Total inorganic carbon, to lowest practical detection limit

Sediment mg/kg 1

CHLOROPHYLL AND ALGAE ANALYSES

CLIN Description (MDL) Medium Unit

Preferred Analysis

Method(s)

EST.

QTY U/P TOTAL

1085 Spectrophotometric determination of chlorophyll a (corrected and uncorrected), b, and c, pheophytin, and pheophytin ratio

Chlorophyll Standard Methods

10200-H

1086 Enumeration and identification of cyanobacteria, to lowest possible taxonomic level, including cell counts, density, and biovolume

Algae 5

1087 Enumeration and identification of cyanobacteria, to lowest possible taxonomic level, including cell counts, density, and biovolume; Toxin analysis of dominant bacteria by enzyme linked immunoassay

(ELISA) and/or liquid chromatography-mass spectrometry (LC/MS)

Algae 5

1088 Qualitative identification of cyanobacteria, to lowest possible taxonomic level

Algae 1

1089 Analysis of a single cyanobacteria toxin by

Enzyme Linked Immunoassay (ELISA)

Algae 1

1090 Analysis of cyanobacteria toxins to include microcystins, cylindrospermopsin, anatoxins and saxitoxins by Enzyme linked immunoassay (ELISA) and/or Liquid

Chromatography-Mass Spectrometry

(LC/MS)

Algae 5

Method(s)

EST.

QTY

LINE

ITEM TOTAL

1091 Sorting, identification, and enumeration of benthic macroinvertebrates to lowest possible taxnomic level with life stage; see scope of work for full instructions

Benthic 25

TOTAL FOR OPTION PERIOD

ONE

TOTAL FOR BASE PERIOD AND

OPTION PERIOD ONE

OPTION PERIOD TWO-1 OCT 2022 TO 30 SEP 2023

Preferred Analysis

Method(s)

EST.

QTY U/P TOTAL

2001 Solids: Dissolved, Suspended, and Total (2) Water mg/L USGS or Standard

Methods 2540

2002 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Water mg/L Lachat or EPA 330

2003 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Water mg/L EPA 300 series or

Standard Methods

2004 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (1), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1

Water ug/L EPA 200 series 350

2005 Hardness, by calculation or titration (5) Water mg/L Standard Methods

2006 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3)

Water ug/L EPA 200 series 1

2007 Metals by ICP or ICP-MS: Ca (0.04), Mg

(0.4), Na (0.4), K (0.4)

Water mg/L EPA 200 series 1

2008 Analysis of one metal by ICP to lowest practical detection limit

Water ug/L EPA 200 series 1

2009 Analysis of one metal by GFAA or ICP-MS to lowest practical detection limit

Water ug/L EPA 200 series 1

2010 Silicon (0.25) Water mg/L EPA 200 series 1

2011 Mercury (0.2) Water ug/L EPA 245.1 1

2012 Mercury, low level (<1) Water ng/L EPA 1631 1

2013 Acidity, Total (phenolphthalein) (5) Water mg/L Standard Methods

2014 Acidity, Methyl Orange (5) Water mg/L Standard Methods

2015 Acidity, Hot Peroxide (5) Water mg/L Standard Methods

2016 Alkalinity, total (5) Water mg/L Standard Methods

2017 Alkalinity, Phenolphthalein (5) Water mg/L Standard Methods

2018 Biological/Biochemical Oxygen Demand

(BOD), 5-Day, to lowest practical detection limit

Water mg/L 1

2019 Carbonaceous Biological/Biochemical

Oxygen Demand (CBOD), to lowest practical detection limit

Water mg/L 1

2020 Chemical Oxygen Demand (COD), to lowest practical detection limit

Water mg/L 1

2021 Bromide (0.25) Water mg/L EPA 300 series 60

2022 Fluoride (0.3) Water mg/L EPA 300 series 1

2023 Iodide (0.3) Water mg/L EPA 300 series 1

2024 Total organic carbon, to lowest practical

Water mg/L 1

2025 Total inorganic carbon, to lowest practical detection limit

Water mg/L 1

2026 Nitrate Nitrogen (0.01) Water mg/L Lachat or EPA 1

2027 Nitrite Nitrogen (0.1) Water mg/L Lachat or EPA 1

2028 Total Kjeldahl Nitrogen (0.1) Water mg/L Lachat or EPA 1

2029 Organic Nitrogen, to lowest practical detection limit

Water mg/L 1

2030 Orthophosphorus (0.005) Water mg/L EPA 300 series 1

Method(s)

EST.

QTY U/P TOTAL

2031 Granulometric Particle-Size Determination, by Sieve Analyses

Sediment % finer

ASTM D-422 10

2032 Granulometric Particle-Size Determinations, by Sieve and Hydrometer Analyses

Sediment % finer

ASTM D-422 4

2033 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Water ug/L EPA 8000 series 4

2034 Total Oil and Grease, to lowest practical detection limit

Water mg/L EPA 1664 4

2035 Total phenolics, to lowest practical detection limit

Water mg/L EPA 420.1 4

2036 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Water ug/L EPA 200 series 4

2037 Chloride (0.5) Water mg/L Lachat or EPA 4

2038 Hardness, by titration or calculation (5) Water mg/L Standard Methods

2039 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Water mg/L Lachat or EPA 4

2040 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on current EPA

Priority Pollutant Lists; Herbicides found on current EPA 8151 method list, all to lowest practical detection levels

Elutriate ug/L EPA 8000 series 4

2041 Total Oil and Grease, to lowest practical detection limit

Elutriate mg/L EPA 1664 4

2042 Total phenolics, to lowest practical detection limit

Elutriate mg/L EPA 420.1 4

2043 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), 2044 Chloride (0.5) Elutriate mg/L Lachat or EPA 4

2045 Hardness, by titration or calculation (5) Elutriate mg/L Standard Methods

2046 Ammonia (0.02), Nitrate+Nitrite (0.01), Nitrite (0.1)

Elutriate mg/L Lachat or EPA 4

2047 Volatile Compounds (VOCs) by GC/MS on current EPA Priority Pollutant List, to lowest practical detection limits

Sediment ug/L EPA 8000 series 4

2048 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Water ug/L EPA 8270 1

2049 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Water ug/L EPA 8151 1

2050 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Water ug/L EPA 8082 1

2051 Pesticides on current EPA Priority Pollutant list, to lowest practical detection limits

Water ug/L EPA 8081 1

2052 Atrazine, to lowest practical detection limit Water ug/L 1

2053 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Water ug/L 1

2054 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Water ug/L 1

2055 Surfactants by MBAS assay, to lowest practical detection limits

Water ug/L MBAS assay 1

2056 Cyanide, to lowest practical detection limits Water mg/L 1

2057 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Elutriate ug/L EPA 8270 1

2028 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Elutriate ug/L EPA 8151 1

2059 Aroclor-specific polychlorinated biphenyls

(PCBs) on current EPA Priority Pollutant list, to lowest practical detection limits

Elutriate ug/L EPA 8082 1

2060 Pesticides on current EPA Priority Pollutant list, to lowest practical detection limits

Elutriate ug/L EPA 8081 1

2061 Atrazine, to lowest practical detection limit Elutriate ug/L 1

2062 All Congeners of Tetra through Octa

Chlorinated Dioxins and Furans, by High-

Resolution GC/MS

Elutriate ug/L 1

2063 Total Petroleum Hydrocarbons (TPH), diesel range, gasoline range, & oil range organics, to lowest practical detection limits

Elutriate ug/L 1

2064 Surfactants by MBAS assay, to lowest practical detection limits

Elutriate ug/L MBAS assay 1

2065 Cyanide, to lowest practical detection limits Elutriate mg/L 1

2066 VOCs, SVOCs, PAHs, Aroclor-specific

PCBs, and Pesticides on EPA Priority

Pollutant Lists; Herbicides found on current

EPA 8151 method list, all to lowest practical detection levels

Sediment ug/k

EPA 8000 series 1

2067 Total Oil and Grease, to lowest practical

Sediment mg/k g

EPA 1664 1

2068 Total phenolics, to lowest practical detection limit

Sediment mg/k g

EPA 420.1 1

2069 Metals by ICP or ICP-MS: Al (20), Fe (5), Mn (3), As (1), Ca (400), Cd (1), Cr (2), Cu

(5), K (400), Mg (400), Na (400), Ni (5), Pb

(5), Se (1), Zn (3), Ag (5), B (3), Ba (5), Be

(1), Co (5), Sb (10), Sn (10), Sr (1), Ti (10), Tl (5), V (2), Hg by 245.1 (0.2)

Sediment ug/k g

EPA 200 series 1

2070 Nutrients: Nitrate+Nitrite (0.01), Total phosphorus (0.005), Ammonia (0.02), total

Kjeldahl nitrogen (0.10)

Sediment mg/k g

Lachat or EPA 1

2071 Ions: Chloride (0.5), Sulfate (2), Bicarbonate

(5)

Sediment mg/k g

EPA 300 series or

Standard Methods

2072 Polynuclear Aromatic Hydrocarbons (PAHs) on current EPA Priority Pollutant list, to lowest practical detection limit

Sediment ug/k g

EPA 8270 1

2073 Herbicides found on current EPA 8151 method list, to lowest practical detection limits

Sediment ug/k g

EPA 8151 1

2074…