B08 W50S80-20-Q-0002_EMO Sampling_QA-27Dec19_USEPA Testing Methods.pdf

Inorganic Non-Metals

Number Method Title

120.1 Conductance (Specific Conductance, μmhos, 25 °C) by Conductivity Meter

130.1 Hardness, Total (mg/L as CaCO3) (Colorimetric, Automated EDTA) by Spectrophotometer

150.2 pH, Continuous Monitoring (Electrometric) by pH Meter

160.4 Residue, Volatile (Gravimetric, Ignition at 550 °C) by Muffle Furnace

180.1 Turbidity by Nephelometry. Revision 2.0

300.0 Inorganic Anions by Ion Chromatography. Revision 2.1

300.1 Inorganic Anions in Drinking Water by Ion Chromatography. Revision 1.0

310.2 Alkalinity, Colorimetric, Automated Methyl Orange

335.4 Total Cyanide by Semi-Automated Colorimetry. Revision 1.0

350.1 Ammonia Nitrogen by Semi-Automated Colorimetry. Revision 2.0

351.1 Total Kjeldahl Nitrogen (Colorimetric, Automated Phenate) by Autoanalyzer

351.2 Total Kjeldahl Nitrogen by Semi-Automated Colorimetry. Revision 2.0

352.1 Nitrogen, Nitrate (Colorimetric, Brucine) by Spectrophotometer

353.2 Nitrate-Nitrite by Automated Colorimetry. Revision 2.0

365.1 Phosphorus by Semi-Automated Colorimetry. Revision 2.0

365.3 Phosphorus, All Forms, Colorimetric, Ascorbic Acid, Two Reagent

365.4 Phosphorus, Total, Colorimetric, Automated, Block Digester, Automated Analyzer II

375.2 Sulfate by Automated Colorimetry. Revision 2.0

410.3 Chemical Oxygen Demand (Titrimetric, High Level for Saline Waters) by Titration

410.4 Chemical Oxygen Demand by Semi-Automated Colorimetry. Revision 2.0

1627 Kinetic Test Method for the Prediction of Mine Drainage Quality

OIA-1677-09 Available Cyanide by Ligand Exchange and Flow Injection Analysis (FIA)

• Regulatory history

Metals

200.2 Sample Preparation Procedure for Spectrochemical Determination of Total Recoverable Elements. Revision 2.8

200.5 Trace Elements in Drinking Water by Axially Viewed Inductively Coupled Plasma-Atomic Emission Spectrometry. Revision 4.2

200.7 Metals and Trace Elements in Water and Wastes by Inductively Coupled Plasma-Atomic Emission Spectrometry. Revision 4.4

200.8 Trace Elements in Water and Wastes by Inductively Coupled Plasma-Mass Spectrometry. Revision 5.4

200.9 Trace Elements by Stabilized Temperature Graphite Furnace Atomic Absorption Spectrometry. Revision 2.2

206.5 Arsenic, Sample Digestion Prior to Total Arsenic Analysis by Silver Diethyldithiocarbamate or Hydride Procedures

218.6 Dissolved Hexavalent Chromium in Drinking Water, Groundwater, and Industrial Wastewater by Ion Chromatography. Revision 3.3

• Regulatory history

231.2 Gold, Atomic Absorption, Furnace Technique

235.2 Iridium, Atomic Absorption, Furnace Technique

245.1 Mercury in Water by Cold Vapor Atomic Absorption Spectrometry. Revision 3.0

245.2 Mercury, Cold Vapor Technique, Automated

245.7 Mercury in Water by Cold Vapor Atomic Fluorescence Spectrometry. Revision 2.0

252.2 Osmium, Atomic Absorption, Furnace Technique

253.2 Palladium, Atomic Absorption, Furnace Technique

255.2 Platinum, Atomic Absorption, Furnace Technique

265.2 Rhodium, Atomic Absorption, Furnace Technique

267.2 Ruthenium, Atomic Absorption, Furnace Technique

279.2 Thallium, Atomic Absorption, Furnace Technique

283.2 Titanium, Atomic Absorption, Furnace Technique

289.2 Zinc, Atomic Absorption, Furnace Technique

1631E Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry. Revision E

Organics

420.1 Phenolics, Total Recoverable, Spectrophotometric, Manual 4-AAP With Distillation

420.4 Total Recoverable Phenolics by Semi-Automated Colorimetry. Revision 1.0

525.1 Organic Compounds in Drinking Water by Liquids-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry. Revision 2.2

525.2 Organic Compounds in Drinking Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry. Revision 2.0

601 Purgeable Halocarbons

602 Purgeable Aromatics

603 Acrolein and Acrylonitrile

604 Phenols

605 Benzidines

606 Phthalate Ester

607 Nitrosamines

608.1 Organochlorine Pesticides in Municipal and Industrial Wastewater

608.2 Certain Organochlorine Pesticides in Municipal and Industrial Wastewater

608.3 Organochlorine Pesticides and PCBs by GC/HSD (replaces Method 608)

609 Nitroaromatics and Isophorone

610 Polynuclear Aromatic Hydrocarbons

611 Haloethers

612 Chlorinated Hydrocarbons

613 2,3,7,8-Tetrachloro Dibenzo-p-Dioxin

614 Organophosphorus Pesticides in Municipal and Industrial Wastewater

614.1 Organophosphorus Pesticides in Municipal and Industrial Wastewater

615 Chlorinated Herbicides in Municipal and Industrial Wastewater

617 Organohalide Pesticides and PCBs in Municipal and Industrial Wastewater

619 Triazine Pesticides in Municipal and Industrial Wastewater

622 Organophosphorus Pesticides in Municipal and Industrial Wastewater

622.1 Thiophosphate Pesticides in Municipal and Industrial Wastewater

624.1 Purgeables by GC/MS (replaces Method 624)

625.1 Base/Neutrals and Acids by GC/MS (replaces Method 625)

• Validation of SPE Products & Associated Procedures with Method 625.1

632 Carbamate and Urea Pesticides in Municipal and Industrial Wastewater

1613B Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS. Revision B

• Regulatory History

1624B Volatile Organic Compounds by Isotope Dilution GC/MS

1625B Semivolatile Organic Compounds by Isotope Dilution GC/MS

1664A n-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated n-Hexane Extractable Material (SGT-HEM;

Non-polar Material) by Extraction and Gravimetry. Revision A

• Regulatory history

1664B n-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated n-Hexane Extractable Material (SGT-HEM;

Non-polar Material) by Extraction and Gravimetry. Revision B