Actlab_Assay.xlsx

XLSX spreadsheet 32 KB Posted Dec 20, 2018

Attached to: Request for Information Samarium, Europium, and Gadolinium (SEG) Concentrate Separation
Solicitation number: SP8000-RFI-2SEG
Issued by: Defense Logistics Agency Strategic Materials

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Assay for SEG Concentrate Separation

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RFI-2-SEG_Concentrate_Separation_12202018.pdf	PDF	Dec 20, 2018

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Results

Report Number: A18-13902
Report Date: 25/10/2018
Analyte Symbol	Ga	Cl	Mass	F	Total S	Pb	Ta2O5	Nb2O5	ZrO2	Si	SiO2	Al	Al2O3	Mn	MnO	Mg	MgO	Ca	CaO	Na	Na2O	K	K2O	P	P2O5	Sc	Sc2O3	Ti	TiO2	V	V2O5	Cr	Cr2O3	Fe	Fe2O3(T)	Ga	Ga2O3	Pb	PbO	U	U3O8	Th	ThO2	Y	La	La2O3	Ce	CeO2	Pr
Unit Symbol	ppm	%	g	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	ppm	ppm	%	%	ppm	ppm	ppm	ppm	%	%	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm
Detection Limit	5	0.01		0.01	0.01	0.01		0.003	0.003	0.005	0.01	0.006	0.01	0.0008	0.001	0.006	0.01	0.008	0.01	0.008	0.01	0.009	0.01	0.01	0.01	1	2	0.01	0.001	5	9	20	30	0.007	0.01	1	1	5	5	0.1	0.1	0.1	0.1	2	0.1	0.1	0.1	0.1	0.05
Analysis Method	PPXRF	INAA	INAA	FUS-ISE	CS	FUS-Na2O2	FUS-XRF	FUS-XRF	FUS-XRF	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-MS	FUS-MS	FUS-ICP	FUS-ICP	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-ICP	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS
SEG001	< 5	0.15	1.06	< 0.01	< 0.01	0.05		< 0.003	< 0.003	0.01	0.02	0.578	1.09	0.005	0.007	0.025	0.04	0.135	0.19	0.008	0.01	0.022	0.03	< 0.01	< 0.01	< 1	< 2	0.02	0.026	176	314	< 20	< 30	0.024	0.03	2	2	44	47	< 0.1	< 0.1	2.6	2.9	15010	195	229	299	367.6	61.7

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Report Number: A18-13902
Report Date: 25/10/2018
Analyte Symbol	Ga	Cl	F	Total S	Pb	Ta2O5	Nb2O5	ZrO2	Si	SiO2	Al	Al2O3	Mn	MnO	Mg	MgO	Ca	CaO	Na	Na2O	K	K2O	P	P2O5	Sc	Sc2O3	Ti	TiO2	V	V2O5	Cr	Fe	Fe2O3(T)	Ga	Pb	U	Th	Y	La	Ce	Pr	Nd	Sm	Eu	Gd	Tb	Dy	Ho	Er
Unit Symbol	ppm	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	%	ppm	ppm	%	%	ppm	ppm	ppm	%	%	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm	ppm
Detection Limit	5	0.01	0.01	0.01	0.01	0.003	0.003	0.003	0.005	0.01	0.006	0.01	0.0008	0.001	0.006	0.01	0.008	0.01	0.008	0.01	0.009	0.01	0.01	0.01	1	2	0.01	0.001	5	9	20	0.007	0.01	1	5	0.1	0.1	2	0.1	0.1	0.05	0.1	0.1	0.05	0.1	0.1	0.1	0.1	0.1
Analysis Method	PPXRF	INAA	FUS-ISE	CS	FUS-Na2O2	FUS-XRF	FUS-XRF	FUS-XRF	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-ICP	FUS-MS	FUS-ICP	FUS-ICP	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-ICP	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS	FUS-MS
NIST 694 Meas			3.2
NIST 694 Cert			3.2
DNC-1 Meas									22.15	47.37	9.65	18.22	0.113	0.146	6.09	10.1	8.23	11.52	1.45	1.95	0.192	0.23	0.03	0.06	31		0.29	0.478	147		270	6.95	9.94	14	6			16	3.8			5.4		0.64
DNC-1 Cert									21.99	47.15	9.69	18.34	0.12	0.15	6.06	10.13	8.06	11.49	1.39	1.89	0.19	0.234	0.03	0.07	31		0.29	0.48	148		270	6.94	9.97	15	6.3			18	3.6			5.2		0.59
LKSD-3 Meas																															90					4.7	11.7		50.2	94.5		47.3	8.7	1.6		0.9	5.2
LKSD-3 Cert																															87					4.6	11.4		52	90		44	8	1.5		1	4.9
MAG-1 (Depleted) Meas		3.14
MAG-1 (Depleted) Cert		3.1
TDB-1 Meas																															250						2.5		17.2	40.2		24.2		2.1
TDB-1 Cert																															251						2.7		17	41		23		2.1
BE-N Meas	15
BE-N Cert	17
AC-E Meas	36
AC-E Cert	39
MA-N (Depleted) Meas						0.034	0.03	0.006
MA-N (Depleted) Cert						0.035	0.025	0.003
BaSO4 Meas				14.1
BaSO4 Cert				14
NIST 1632c Meas		0.11
NIST 1632c Cert		0.11
W-2a Meas	16								24.61	52.63	8.14	15.37	0.127	0.164	3.84	6.36	7.9	11.06	1.67	2.25	0.531	0.64	0.05	0.12	35		0.65	1.082	259		90	7.54	10.78	17	8	0.5		20	11	23.8		13	3.3			0.6	3.9	0.8
W-2a Cert	17								24.52	52.4	8.13	15.4	0.13	0.163	3.84	6.37	7.77	10.9	1.59	2.14	0.52	0.626	0.06	0.14	36		0.64	1.06	262		92	7.51	10.7	17	9.3	0.53		24	10	23		13	3.3			0.63	3.6	0.76
SY-4 Meas									23.51	50.29	10.8	20.32	0.083	0.107	0.306	0.51	5.85	8.19	5.08	6.85	1.36	1.64	0.05	0.12	1		0.17	0.286	9			4.3	6.15					116
SY-4 Cert									23.29	49.9	10.95	20.69	0.08	0.108	0.33	0.54	5.75	8.05	5.27	7.1	1.38	1.66	0.06	0.131	1.1		0.17	0.287	8			4.34	6.21					119
CTA-AC-1 Meas																																				4.4	22.7		2140	3300		1150	168	49.4	131	13.5
CTA-AC-1 Cert																																				4.4	21.8		2176	3326		1087	162	46.7	124	13.9
BIR-1a Meas									22.51	48.15	8.38	15.83	0.13	0.168	5.86	9.72	9.67	13.53	1.36	1.83	0.02	0.02	0.01	0.02	44		0.59	0.981	319		370	8.05	11.51		< 5			14	0.6	1.9		2.4		0.57	2.1
BIR-1a Cert									22.33	47.96	8.13	15.5	0.14	0.175	5.84	9.7	9.46	13.3	1.3	1.82	0.02	0.03	0.02	0.021	44		0.58	0.96	310		370	7.87	11.3		3			16	0.63	1.9		2.5		0.55	2
NCS DC86312 Meas																																					25.1		2330	185		1690				35.2	188	35.1	94.4
NCS DC86312 Cert																																					23.6		2360	190		1600				34.6	183	36	96.2
ZW-C Meas						0.009		0.009
ZW-C Cert						0.01		0.011
VS-N Meas						0.094	0.104	0.099
VS-N Cert						0.098	0.1	0.095
NCS DC70009 (GBW07241) Meas																																		18			30.3		25.2	63.4	8.1	34.2	12.2		15.1	3.4		4.8	13.4
NCS DC70009 (GBW07241) Cert																																		16.5			28.3		23.7	60.3	7.9	32.9	12.5		14.8	3.3		4.5	13.4
MP-1b Meas					2.05
MP-1b Cert					2.09
MP-1b Meas					2.11
MP-1b Cert					2.09
MP-1b Meas					2.14
MP-1b Cert					2.09
SGR-1b Meas				1.56
SGR-1b Cert				1.53
OREAS 100a (Fusion) Meas																																				136	52.3		270	485	49.5	151		3.91	22.7	3.8		5.2
OREAS 100a (Fusion) Cert																																				135	51.6		260	463	47.1	152		3.71	23.6	3.8		4.81
OREAS 101a (Fusion) Meas																																				425	38.4		825	1400	138	419		8.77		5.6	35.9		20.3
OREAS 101a (Fusion) Cert																																				422	36.6		816	1396	134	403		8.06		5.92	33.3		19.5
OREAS 101b (Fusion) Meas																																				411	35.7		798	1390	126	379	49	8.05		5	31.8	6.3	18.8
OREAS 101b (Fusion) Cert																																				396	37.1		789	1331	127	378	48	7.77		5.37	32.1	6.34	18.7
JR-1 Meas																																		18	20	8.7	28.5		21	49.8	6		6.1	0.3	5.3	1.1	6	1.1	3.9
JR-1 Cert																																		16.1	19.3	8.88	26.7		19.7	47.2	5.58		6.03	0.3	5.06	1.01	5.69	1.11	3.61
NCS DC86318 Meas																																					66.8		2040	419	733	3200	1750	19.3	2270	483	3200	590	1690
NCS DC86318 Cert																																					67		1960	430	740	3430	1720	18.91	2095	470	3220	560	1750
SX18-01 Meas						< 0.003	0.701	0.085
SX18-01 Cert						0.005	0.695	0.093
USZ 25-2006 Meas																																							19400	31000	2790	8530	837	203
USZ 25-2006 Cert																																							19300	29000	2800	8800	900	211
USZ 42-2006 Meas																																			1490		972		22200	30300	2450	6340	508	89
USZ 42-2006 Cert																																			1600		946		21100	27600	2300	6500	539	87.22
CPB-2 Meas					64.7
CPB-2 Cert					63.52
CPB-2 Meas					64.1
CPB-2 Cert					63.52
GS311-4 Meas				0.52
GS311-4 Cert				0.54
GS900-5 Meas				0.35
GS900-5 Cert				0.34
CZN-4 Meas					0.18
CZN-4 Cert					0.1861
CZN-4 Meas					0.18
CZN-4 Cert					0.1861
CZN-4 Meas					0.18
CZN-4 Cert					0.1861
CCU-1e Meas					0.71
CCU-1e Cert					0.703
CCU-1e Meas					0.72
CCU-1e Cert					0.703
CCU-1e Meas					0.71
CCU-1e Cert					0.703
SEG001 Orig	< 5				0.05
SEG001 Dup	< 5				0.06
Method Blank					< 0.01
Method Blank					< 0.01
Method Blank					< 0.01
Method Blank					< 0.01
Method Blank			< 0.01
Method Blank					< 0.01
Method Blank									< 0.005	0.01	< 0.006	< 0.01	0.005	0.007	< 0.006	< 0.01	< 0.008	< 0.01	< 0.008	< 0.01	< 0.009	< 0.01	< 0.01	< 0.01	< 1	< 2	< 0.01	< 0.001	< 5	< 9	< 20	0.007	< 0.01	< 1	< 5	< 0.1	< 0.1	< 2	< 0.1	< 0.1	< 0.05	< 0.1	< 0.1	< 0.05	< 0.1	< 0.1	< 0.1	< 0.1	< 0.1
Method Blank	< 5
Method Blank
Method Blank						< 0.003	< 0.003	< 0.003

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