Exhibit_E2.PDF

16PH-0765

Fuel Oil Reclaimed

FROM TO:

NAVSUP FLEET LOGISTICS CENTER JOINT BASE PEARL HARBOR HICKAM YON-336

FUEL LABORATORY (CODE 704)

1942 GAFFNEY STREET STE 100

PEARL HARBOR, HI 96860-4549

LAB SAMPLE NO. SOURCE OF SAMPLE (Truck, Tank, Aircraft, etc.)

DATE SAMPLED DATE LOGGED IN DATE TESTS COMPLETE

3/17/2016 10:46 AM 3/22/2016

PRODUCT CODE TEST TYPE SAMPLE VOLUME

FOR FOR-FULL 4 QUART

REPRESENTATIVE VOLUME REPORT CREATED BY SAMPLE TAKEN BY

243,689 GALLON RK

MARKING LIMITS OF REF (A) & (B) RESULTS METHOD NO

D4176

FISCPINST 5090.9A

FISCPINST 5090.9A

D93

SW846 9077 (METHOD C)

D4052

D1796

FTM 5101.7

D5705

FTM 1151.1

D5453

D445

D2161(D88)

D874

D473

D5949

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 8082

MIL-PRF-24951 REF (B): USE LIMIT

PRODUCT AS REPRESENTED BY SAMPLE MEET:

SPEC. LIMITS OF REF (A)? YES USE LIMITS OF REF (B)? YES

REMARKS:

MT

TESTED BY VERIFIED BY

<0.41*

3.279

34.9

0.000

0.013

-33.0

*PCB and Metal testing performed by Test America and completed on 03/28/2016, see attached report for test results.

ARSENIC, mg/L (As) 5 MAX

2.0 MAX

ON SPEC

<0.250*

2 MAX

<0.1

NEUTRAL

<0.5

0.01

50 MAX

GRAVITY, API @60°F

WATER & SEDIMENT, %VOL 2.0 MAX

<10 MAXHYDROGEN SULFIDES, ppm

EXPLOSIVENESS, %

25 - 40

RH/ML

C&B

EPA, TOTAL HALOGENS, ppm

3/17/2016

APPEARANCE REPORT

PASS

2001000 MAX

31.8

POUR POINT, @°C

<0.41*

0.19*

ANALYSIS OF

16PH-0765

10:20 AM

YON 336, COMPOSITE OF TANKS (1, 2, 3, 4), ALL LEVEL, PRIOR TO SALE, QUALITY

CHECK

NEUTRALITY

DETERGENCY (OIL)

REVERSE DETERGENCY (WATER)

FLASH POINT, PMCC, @°C

PASS

PASS

38 MIN

NEUTRAL

**Test not performed.

REF (A):

CADMIUM, mg/L (Cd)

PCB, ppm

<0.10*

100 MAX

10 MAX

6:13 AM

SULFUR, %WT 2.0 MAX

0.15 MAX

0.50 MAX

-6.7 MAX

2.0-15.0VISCOSITY, @40°C, cSt

30 - 90

LEAD, mg/L (Pb)

CHROMIUM, mg/L (Cr)

VISCOSITY, @50°C, SU

ASH, SULFATED, %WT

SEDIMENT BY EXTRACTION, %WT

ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Honolulu 4429 Malaai St. #104 Honolulu, HI 96818 Tel: (808)486-5227

TestAmerica Job ID: 370-372-1 Client Project/Site: YON 336

For:

NAVSUP Fleet Logistics Cntr Pearl Harbor 1942 Gaffney St Suite 100 Fuel Dept Code 702 Pearl Harbor, Hawaii 96860

Attn: Marissa Tanaka

Authorized for release by:

3/28/2016 1:33:44 PM

Pat Abe, Senior Project Manager (808)486-5227 pat.abe@testamericainc.com

Designee for

Craig Pilialoha, Project Manager I (808)486-5227 craig.pilialoha@testamericainc.com

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm http://www.testamericainc.com mailto:pat.abe@testamericainc.com mailto:craig.pilialoha@testamericainc.com

Table of Contents

Client: NAVSUP Fleet Logistics Cntr Pearl Harbor Project/Site: YON 336

TestAmerica Job ID: 370-372-1

TestAmerica Honolulu

3/28/2016

Cover Page

Table of Contents

Sample Summary

Case Narrative

Client Sample Results

Method Summary

Chronicle

QC Sample Results

QC Association

Definitions

Certification Summary

Chain of Custody

Receipt Checklists

Sample Summary TestAmerica Job ID: 370-372-1Client: NAVSUP Fleet Logistics Cntr Pearl Harbor

Project/Site: YON 336

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

370-372-1 16PH-0765 Waste 03/18/16 08:00 03/18/16 10:37

TestAmerica Honolulu

Page 3 of 18 3/28/2016

Case Narrative Client: NAVSUP Fleet Logistics Cntr Pearl Harbor TestAmerica Job ID: 370-372-1 Project/Site: YON 336

Job ID: 370-372-1

Laboratory: TestAmerica Honolulu

Narrative

Job Narrative 370-372-1

Comments

No additional comments.

Receipt

The sample was received on 3/18/2016 10:37 AM; the sample arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 12.0º C.

GC Semi VOA Method(s) 8082: The following sample required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: 16PH-0765 (370-372-1).

Method(s) 8082: The following samples required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: (LCS 720-199304/2-A), (MB 720-199304/1-A), (720-71088-A-1-A) and (720-71088-A-1-C DU).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Organic Prep

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TestAmerica Honolulu Page 4 of 18 3/28/2016

Client Sample Results

Project/Site: YON 336

Lab Sample ID: 370-372-1Client Sample ID: 16PH-0765 Matrix: WasteDate Collected: 03/18/16 08:00

Date Received: 03/18/16 10:37

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

RL MDL

PCB-1016 ND 250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1221 ND

250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1232 ND

250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1242 ND

250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1248 ND

250 41 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1254 ND

250 61 ug/Kg 03/24/16 18:01 03/25/16 01:15 1PCB-1260 ND

DCB Decachlorobiphenyl 82 30 - 148 03/24/16 18:01 03/25/16 01:15 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Tetrachloro-m-xylene 100 03/24/16 18:01 03/25/16 01:15 142 - 147

Method: 6010B - Metals (ICP)

RL MDL

Arsenic 0.19 J 0.81 0.069 mg/Kg 03/22/16 14:42 03/24/16 20:57 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.41 0.058 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Barium ND

0.10 0.010 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Cadmium ND

0.41 0.043 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Chromium ND

0.41 0.085 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Lead ND

0.81 0.12 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Selenium 0.28 J B

0.20 0.041 mg/Kg 03/22/16 14:42 03/23/16 19:26 1Silver ND

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.0057 J B 0.0086 0.0021 mg/Kg 03/24/16 13:57 03/24/16 20:43 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Honolulu

Page 5 of 18 3/28/2016

Method Summary

Project/Site: YON 336

Method Method Description LaboratoryProtocol

SW8468082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL PLS

SW8466010B Metals (ICP) TAL PLS

SW8467471A Mercury (CVAA) TAL PLS

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919

TestAmerica Honolulu

Page 6 of 18 3/28/2016

Lab Chronicle

Project/Site: YON 336

Client Sample ID: 16PH-0765 Lab Sample ID: 370-372-1 Matrix: WasteDate Collected: 03/18/16 08:00

Date Received: 03/18/16 10:37

Prep 3580A 03/24/16 18:01 BSY199304 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 1 199271 03/25/16 01:15 DCH TAL PLSTotal/NA

Prep 3050B 199142 03/22/16 14:42 JNG TAL PLSTotal/NA

Analysis 6010B 1 199259 03/23/16 19:26 SLK TAL PLSTotal/NA

Prep 3050B 199142 03/22/16 14:42 JNG TAL PLSTotal/NA

Analysis 6010B 1 199341 03/24/16 20:57 ASB TAL PLSTotal/NA

Prep 7471A 199299 03/24/16 13:57 MJD TAL PLSTotal/NA

Analysis 7471A 1 199335 03/24/16 20:43 SLK TAL PLSTotal/NA

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919

TestAmerica Honolulu

Page 7 of 18 3/28/2016

QC Sample Results

Project/Site: YON 336

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

Client Sample ID: Method BlankLab Sample ID: MB 720-199304/1-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199272 Prep Batch: 199304

RL MDL

PCB-1016 ND 250 42 ug/Kg 03/24/16 15:48 03/24/16 21:05 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 42250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1221

ND 42250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1232

ND 42250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1242

ND 42250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1248

ND 42250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1254

ND 63250 ug/Kg 03/24/16 15:48 03/24/16 21:05 1PCB-1260

DCB Decachlorobiphenyl 96 30 - 148 03/24/16 21:05 1

MB MB

Surrogate

03/24/16 15:48

Dil FacPrepared AnalyzedQualifier Limits%Recovery

102 03/24/16 15:48 03/24/16 21:05 1Tetrachloro-m-xylene 42 - 147

Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-199304/2-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199272 Prep Batch: 199304

PCB-1016 4000 4020 ug/Kg 100 85 - 153

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

PCB-1260 4000 3900 ug/Kg 98 82 - 151

DCB Decachlorobiphenyl 30 - 148

Surrogate

LCS LCS

Qualifier Limits%Recovery

103Tetrachloro-m-xylene 42 - 147

Client Sample ID: DuplicateLab Sample ID: 720-71088-A-1-C DU Matrix: Waste Prep Type: Total/NA Analysis Batch: 199272 Prep Batch: 199304

PCB-1016 ND ND ug/Kg NC 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

PCB-1221 ND ND ug/Kg NC 20

PCB-1232 ND ND ug/Kg NC 20

PCB-1242 ND ND ug/Kg NC 20

PCB-1248 ND ND ug/Kg NC 20

PCB-1254 ND ND ug/Kg NC 20

PCB-1260 ND ND ug/Kg NC 20

DCB Decachlorobiphenyl 30 - 148

Surrogate

DU DU

Qualifier Limits%Recovery

97Tetrachloro-m-xylene 42 - 147

TestAmerica Honolulu

Page 8 of 18 3/28/2016

Project/Site: YON 336

Method: 6010B - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 720-199142/1-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199243 Prep Batch: 199142

RL MDL

Arsenic ND 1.0 0.085 mg/Kg 03/22/16 14:42 03/23/16 15:48 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.0729 J 0.0710.50 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Barium

ND 0.0120.13 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Cadmium

ND 0.0530.50 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Chromium

ND 0.110.50 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Lead

0.264 J 0.151.0 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Selenium

ND 0.0510.25 mg/Kg 03/22/16 14:42 03/23/16 15:48 1Silver

Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-199142/2-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199243 Prep Batch: 199142

Arsenic 50.0 44.8 mg/Kg 90 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Barium 50.0 44.4 mg/Kg 89 80 - 120

Cadmium 50.0 48.3 mg/Kg 97 80 - 120

Chromium 50.0 46.5 mg/Kg 93 80 - 120

Lead 50.0 46.8 mg/Kg 94 80 - 120

Selenium 50.0 48.0 mg/Kg 96 80 - 120

Silver 25.0 23.8 mg/Kg 95 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 720-199142/3-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199243 Prep Batch: 199142

Arsenic 45.5 39.5 mg/Kg 87 69 - 119

Analyte

LCSSRM LCSSRM

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Barium 579 452 mg/Kg 78 61 - 117

Cadmium 201 185 mg/Kg 92 67 - 118

Chromium 106 90.9 mg/Kg 86 67 - 121

Lead 302 268 mg/Kg 89 62 - 113

Selenium 133 127 mg/Kg 96 63 - 126

Silver 33.5 30.1 mg/Kg 90 51 - 130

Client Sample ID: Matrix SpikeLab Sample ID: 720-70949-A-1-C MS Matrix: Waste Prep Type: Total/NA Analysis Batch: 199243 Prep Batch: 199142

Arsenic ND 31.4 28.6 mg/Kg 91 75 - 125

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium ND 31.4 27.9 mg/Kg 89 75 - 125

Cadmium ND 31.4 30.5 mg/Kg 97 75 - 125

Chromium ND 31.4 29.3 mg/Kg 93 75 - 125

Lead ND 31.4 29.6 mg/Kg 94 75 - 125

Selenium 0.18 J B 31.4 29.9 mg/Kg 95 75 - 125

Silver ND 15.7 14.9 mg/Kg 95 75 - 125

TestAmerica Honolulu

Page 9 of 18 3/28/2016

Project/Site: YON 336

Method: 6010B - Metals (ICP) (Continued)

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 720-70949-A-1-D MSD Matrix: Waste Prep Type: Total/NA Analysis Batch: 199243 Prep Batch: 199142

Arsenic ND 32.1 28.4 mg/Kg 89 75 - 125 1 20

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium ND 32.1 27.6 mg/Kg 86 75 - 125 1 20

Cadmium ND 32.1 30.4 mg/Kg 95 75 - 125 0 20

Chromium ND 32.1 29.2 mg/Kg 91 75 - 125 1 20

Lead ND 32.1 29.6 mg/Kg 92 75 - 125 0 20

Selenium 0.18 J B 32.1 29.5 mg/Kg 92 75 - 125 1 20

Silver ND 16.0 14.7 mg/Kg 92 75 - 125 1 20

Method: 7471A - Mercury (CVAA)

Client Sample ID: Method BlankLab Sample ID: MB 720-199299/1-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199335 Prep Batch: 199299

RL MDL

Mercury 0.00608 J 0.010 0.0025 mg/Kg 03/24/16 13:57 03/24/16 19:30 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-199299/2-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 199335 Prep Batch: 199299

Mercury 0.833 0.933 mg/Kg 112 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: 16PH-0765Lab Sample ID: 370-372-1 MS Matrix: Waste Prep Type: Total/NA Analysis Batch: 199335 Prep Batch: 199299

Mercury 0.0057 J B 0.714 0.764 mg/Kg 106 75 - 125

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: 16PH-0765Lab Sample ID: 370-372-1 MSD Matrix: Waste Prep Type: Total/NA Analysis Batch: 199335 Prep Batch: 199299

Mercury 0.0057 J B 0.735 0.779 mg/Kg 105 75 - 125 2 20

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

TestAmerica Honolulu

Page 10 of 18 3/28/2016

QC Association Summary

Project/Site: YON 336

GC Semi VOA

Analysis Batch: 199271

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 8082 199304370-372-1 16PH-0765 Total/NA

Analysis Batch: 199272

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 8082 199304720-71088-A-1-C DU Duplicate Total/NA

Waste 8082 199304LCS 720-199304/2-A Lab Control Sample Total/NA

Waste 8082 199304MB 720-199304/1-A Method Blank Total/NA

Prep Batch: 199304

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 3580A370-372-1 16PH-0765 Total/NA

Waste 3580A720-71088-A-1-C DU Duplicate Total/NA

Waste 3580ALCS 720-199304/2-A Lab Control Sample Total/NA

Waste 3580AMB 720-199304/1-A Method Blank Total/NA

Metals

Prep Batch: 199142

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 3050B370-372-1 16PH-0765 Total/NA

Waste 3050B720-70949-A-1-C MS Matrix Spike Total/NA

Waste 3050B720-70949-A-1-D MSD Matrix Spike Duplicate Total/NA

Waste 3050BLCS 720-199142/2-A Lab Control Sample Total/NA

Waste 3050BLCSSRM 720-199142/3-A Lab Control Sample Total/NA

Waste 3050BMB 720-199142/1-A Method Blank Total/NA

Analysis Batch: 199243

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 6010B 199142720-70949-A-1-C MS Matrix Spike Total/NA

Waste 6010B 199142720-70949-A-1-D MSD Matrix Spike Duplicate Total/NA

Waste 6010B 199142LCS 720-199142/2-A Lab Control Sample Total/NA

Waste 6010B 199142LCSSRM 720-199142/3-A Lab Control Sample Total/NA

Waste 6010B 199142MB 720-199142/1-A Method Blank Total/NA

Analysis Batch: 199259

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 6010B 199142370-372-1 16PH-0765 Total/NA

Prep Batch: 199299

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 7471A370-372-1 16PH-0765 Total/NA

Waste 7471A370-372-1 MS 16PH-0765 Total/NA

Waste 7471A370-372-1 MSD 16PH-0765 Total/NA

Waste 7471ALCS 720-199299/2-A Lab Control Sample Total/NA

Waste 7471AMB 720-199299/1-A Method Blank Total/NA

Analysis Batch: 199335

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 7471A 199299370-372-1 16PH-0765 Total/NA

Waste 7471A 199299370-372-1 MS 16PH-0765 Total/NA

TestAmerica Honolulu

Page 11 of 18 3/28/2016

QC Association Summary

Project/Site: YON 336

Metals (Continued)

Analysis Batch: 199335 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 7471A 199299370-372-1 MSD 16PH-0765 Total/NA

Waste 7471A 199299LCS 720-199299/2-A Lab Control Sample Total/NA

Waste 7471A 199299MB 720-199299/1-A Method Blank Total/NA

Analysis Batch: 199341

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 6010B 199142370-372-1 16PH-0765 Total/NA

TestAmerica Honolulu

Page 12 of 18 3/28/2016

Definitions/Glossary

Project/Site: YON 336

Qualifiers

Metals

Qualifier Description

B Compound was found in the blank and sample.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Honolulu

Page 13 of 18 3/28/2016

Certification Summary

Project/Site: YON 336

Laboratory: TestAmerica Honolulu All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Hawaii N/A9State Program 06-28-10 *

USDA Federal HON-S-206 11-04-16

Laboratory: TestAmerica Irvine All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alaska CA0153110State Program 06-30-16

Arizona State Program 9 AZ0671 10-13-16

California LA Cty Sanitation Districts 9 10256 01-31-17 *

California State Program 9 CA ELAP 2706 06-30-16

Guam State Program 9 Cert. No. 12.002r 01-23-17

Hawaii State Program 9 N/A 01-29-17

Kansas NELAP Secondary AB 7 E-10420 07-31-16

Nevada State Program 9 CA015312007A 07-31-16

New Mexico State Program 6 N/A 01-29-17

Northern Mariana Islands State Program 9 MP0002 01-29-16 *

Oregon NELAP 10 4005 01-29-17

USDA Federal P330-09-00080 07-08-18

Washington State Program 10 900 09-03-16

Laboratory: TestAmerica Pleasanton All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

California 24969State Program 01-31-17

TestAmerica Honolulu

* Certification renewal pending - certification considered valid.

Page 14 of 18 3/28/2016

Page 15 of 18 3/28/2016

Page 16 of 18 3/28/2016

Login Sample Receipt Checklist

Client: NAVSUP Fleet Logistics Cntr Pearl Harbor Job Number: 370-372-1

Login Number: 372

Question Answer Comment

Creator: Pilialoha, Craig O

List Source: TestAmerica Honolulu

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

FalseCooler Temperature is acceptable. Received same day of collection; chilling process has begun.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

TestAmerica Honolulu Page 17 of 18 3/28/2016

Login Sample Receipt Checklist

Client: NAVSUP Fleet Logistics Cntr Pearl Harbor Job Number: 370-372-1

Login Number: 372

Question Answer Comment

Creator: Arauz, Dennis

List Source: TestAmerica Pleasanton

List Creation: 03/21/16 01:39 PMList Number: 2

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

TestAmerica Honolulu Page 18 of 18 3/28/2016