Requirements and Specifications (1).pdf

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Requirements / Specifications: Sample Holder for Thermo Fisher (S)TEM 1 Version 1.0 (2019) Double-click on for further assistance.

Use this document to detail specifications/requirements for an item and/or ancillary services.

TITLE: Sample Holder for Thermo Fisher (S)TEM Requesting Lab/Division/Group: PML/Applied Physics Division/ Quantitative Nanostructure Characterization Group

General Statement of Need The heating/biasing (S)TEM sample holder is needed for in operando studies of a wide variety of electrical and optical devices.

Items and/or Ancillary Services

Item 1: Heating-Biasing Holder for Thermo Fisher (S)TEM Quantity: one Specifications: 1.Temperature range of operation: ambient to 900 °C (higher is better). 2.Temperature accuracy: 95 % (higher is better). 3.Image stability at 900 °C: 1 nm/min (lower is better). 4.Controllable heating and cooling rates: up to 100 °C/ms. 5.In-situ temperature measurement or individually calibrated MEMS heating device. 6.Bias voltage range: 0 to 40 V (higher is better). 7.Current range: 2 pA to 100 mA. 8.Simultaneous application of temperature and field: up to 40 V at 900 °C. 9.Electrodes to perform 4-point probe electrical measurements simultaneously with sample heating. 10.Software for temporally recording electrical and temperature control and measurement. 11.α-tilt range: ± 30 ° (higher is better). 12.β-tilt range: ± 15 ° (higher is better). 13.Friction-free tilting in both alpha and beta directions to prevent electrical contacts on the chip from scraping against the probes. 14.EDS Compatible: 70 % line of sight at 0 ° tilt. 15.MEMS chips specimen holders must be compatible with FIB sample and contact preparation. 16.MEMs chips specimen holders must have minimal electrical leakage (lower is better). 17.MEMS chips specimen holders available with sample support films that are stable at the maximum specified temperature: holey carbon, silicon nitride, and through-hole (no film).

18.Compatibility with Thermo Fisher Spectra and Talos S/TEM instruments and software. 19.Compliance with the TEM manufacturer’s certification for X-ray safety, mechanical tolerance and vacuum safety.

20.Scientific viability of the holder demonstrated through record of publications based on using the tool.

21.A dedicated service team for fast, reliable contact. 22.Instant access to searchable PDF manuals, troubleshooting guides, application notes, real time tracking and updates on all service requests, and online ordering of MEMS devices.

Separately Priced Options and Services:

Item 2: 1. Software that allows off-line analysis of images and their metadata (so processing does not have to be done on the TEM). 2.Software that actively corrects sample drift by analyzing the live data and utilizing either/both physical means (stage and beam) and digital means for the correction.

3.Software that synchronously records in-situ heating and electrical parameters and TEM parameters (such as spot size, dwell time, exposure time, etc.) directly into the metadata of each image. 4.Software that will recommend the optimal temperature ramp rate to achieve maximum resolution for a desired field of view.

Quantity: one Specifications: [Enter quantity here.]

[List any other item(s) or service requirements here using the same format above.]

Requirements / Specifications: Sample Holder for Thermo Fisher (S)TEM 2

Service Requirements / Item Specifications

Section Requirements/Specifications Planning Considerations ☒ N/A

☐ List any visits required to allow potential vendors to see site specific constraints.

[Explain requirement here] ☐ US citizen required on-site (foreign nationals require preregistration 30 days prior) ☐ Vendor rep on-site more than three days ☐ Other considerations: [List other considerations to ensure an accurate quote]

Shipping & Delivery ☐ N/A

[Enter shipping and delivery information by item here.] Shipping criteria:

☐ Partial delivery acceptable ☐ Direct delivery to building required [Explain need for requirement here] Building has: ☐ Loading dock ☐ Containerization preference: [Choose container] Other requirements: [List any other requirements here] Delivery date criteria:

☒ Delivery of goods, installation, and training shall be completed no later than: 2 months ARO ☐ Deliver no earlier than: [Insert date here] ☐ Other: [List other shipping, delivery, or specil requirements]

Electronic Media ☐ N/A

[Enter electronic media requirements by item here.] ☒ Software ☒ Electronic manuals ☐ License Key ☐ Other: [List any other Electronic Media requirements here] [Enter email address for software delivery here]

Installation ☐ N/A

[Enter installation requirements by item here.] ☒ Vendor technician on site ☐ Rigging ☐ Uncrating / Unpackaging ☐ Removal of packaging material ☐ Equipment set up ☐ Start-up services ☐ Turn key installation ☐ Other [Enter details here.] Note: When installation is required, TPOC or COR shall be the coordination point.

Facility / Utility Considerations ☒ N/A

[List site specific utility considerations by item here.] ☐ OFPM Work Order Number(s) [List any Work Order Number(s) here] ☐ Power available Voltage: [Enter voltage here] (V) Max Current: [Enter max current draw here] (A)

Requirements / Specifications: Sample Holder for Thermo Fisher (S)TEM 3

Phase: [Choose phase] Frequency: [Typically 60Hz] (Hz) NEMA Plug Type: [Enter plug type here] (i.e.: NEMA L5-20P) Environment: [Choose environment] Other power consideration: [List any other power considerations here] ☐ Utility connections: [List relevant available utilities, pressure(s), and flowrate(s)] ☐ Other considerations: [List other considerations to ensure an accurate quote]

Warranty ☐ N/A

[Choose warranty type here.] [If you require an Extended Manufacturer Warranty, describe the warranty requirements per item here.] What is included?

☐ Labor ☐ Parts ☐ Travel ☐ Cost and liability for returns ☐ Other: [Enter other requirements here] ☒ Warranty length: one year Period Length:[Ex. month, 6 month, year etc.]

Training ☐ N/A

[Training requirements (who, when, what, where) here. If on-site, is travel necessary?] ☒ On-site ☐ Off-site location: [Enter location(s) here] ☒ Number of trainees: three Scope of training:

☒ Operations ☒ Maintenance ☒ Troubleshooting ☒ Safety ☐ Other: [Enter other scope requirements here] ☐ Training materials to be provided: [Describe requirement here] ☐ Other: [Enter other training requirements here] Note: When training is required, TPOC or COR shall be the coordination point.

Inspection and Acceptance ☐ N/A

[Enter inspection requirements per item here] ☒ Planned government acceptance testing (7 business days) ☐ Gov’t acceptance expected to take longer than 7 business days: [Duration] ☐ Inspection and acceptance plan: [Explain here] ☐ Other: [Enter other requirements here]

Maintenance ☒ N/A

[Describe your maintenance requirements per item here] Period Length: [Ex. month, 6 month, year etc.] What is included?

☐ Labor ☐ Spare parts ☐ Consumables ☐ Travel ☐ Cost and liability for returns ☐ Software updates ☐ Manuals ☐ Service plan length: [Enter service plan length here]

Requirements / Specifications: Sample Holder for Thermo Fisher (S)TEM 4

☐ Other: [Enter other requirements here] ☐ Requirements: [Enter requirements here] (i.e.: onsite within 72 hours, etc.)

☐ Option Period 1 ☐ Option Period 2 ☐ Option Period 3 ☐ Option Period 4

Government Furnished Material / Equipment ☒ N/A

[List any government furnished material/equipment per item here] ☐ Samples for testing ☐ Government equipment which will leave gov't site (TPOC must coordinate with division property custodian) Serial Number: [Enter Serial Number here] Description: [Enter description here] NIST property number: [Enter NIST property number here] ☐ Other: [Enter other details here]

Travel ☒ N/A

[Describe any travel requirements per item here] ☐ Explain: [Explain here] ☐ Other: [Enter other requirements here] Vendor: To the maximum extent possible, include as part of appropriate sections above (maintenance, repair, etc.). Otherwise, it will be a separate line item, reimbursable per the Federal Travel Regulation.

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