Part 2_Ken's Party Store_DCSpec_Rev02-19_05-30-2019.pdf

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761/18031. SAR Ken's Party Store - UST Removal
Solicitation number
RFQ 171 190000000481 3
Issued by
Clinton County, Michigan

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Summary of Ken's Party Store Demolition Project Documentation

This bidding and contract document package represents a comprehensive demolition and remediation project for Ken's Party Store in Bay City, Michigan, involving the State of Michigan Department of Environmental Quality and PM Environmental, Inc. The project encompasses environmental assessment, hazardous materials surveying, and pre-demolition abatement work for an abandoned garage structure at 1470 North Clare Avenue, Harrison, Michigan. The scope includes identification and quantification of asbestos-containing materials (ACM), lead paint assessment, universal waste removal, and environmental sampling. Specifically, the survey identified 265 linear feet of asbestos-containing interior window glazing (3% chrysotile), 36 linear feet of exterior window caulk (5% chrysotile), and 1,000 square feet of flat roofing materials. Environmental laboratory analyses were conducted by the MDEQ Environmental Laboratory with work orders completed in March 2018, and the Pre-Demolition Hazardous Materials Survey was finalized on August 8, 2018. The survey identified two fluorescent light fixtures, two ballasts potentially containing PCBs, and two high-intensity discharge lighting fixtures requiring proper disposal as universal waste.

The documentation includes detailed laboratory analytical reports for water samples and soil borings at the site, indicating volatile organic compounds, diesel range organics, and oil range organics detected at various depths. Lead paint sampling identified measurable lead concentrations in three of six samples collected. The remediation work must comply with OSHA Construction Industry Standards for Lead (29 CFR 1926.62), EPA asbestos regulations under AHERA (40 CFR Part 763), and Resource Conservation and Recovery Act (RCRA) requirements for hazardous waste disposal. PM Environmental recommended a contingency allowance of fifteen percent for unknown factors and an additional twenty percent for engineering and testing fees in cost projections. All hazardous materials removal must be performed by licensed and certified contractors, with air monitoring and personal protective equipment required for workers exposed to lead-containing surfaces during demolition activities.

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Part 1_Ken's Party Store_DCSpec_Rev02-19_05-30-2019.pdf PDF
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Bidding and Contract Document (2/19) Project Name: Ken’s Party Store File No. 761/18031.SAR

APPENDIX V

LABORATORY ANALYTICAL REPORTS

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-SAGINAW BAY

RE: DEQ/KEN'S PARTY STORE

Bay City, MI 48708

401 Ketchum St., Suite B

Lisa Chadwick

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 05 March 2018 Work Order: 1801138

Price: $3,060.00

Kirby Shane

Laboratory Director

Lab Work Order # 1801138

Page 1 of 39Page 1 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-SAGINAW BAY

401 Ketchum St., Suite B

Lisa Chadwick

DEQ/KEN'S PARTY STORE

Bay City MI, 48708

Site Code: CMI081 03/05/2018

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1801138-01 Water 01/26/2018TMW-1 01/24/2018

1801138-02 Water 01/26/2018TMW-2 01/24/2018

1801138-03 Water 01/26/2018TMW-3 01/24/2018

1801138-04 Water 01/26/2018TMW-4 01/25/2018

1801138-05 Water 01/26/2018TMW-5 01/24/2018

1801138-06 Water 01/26/2018TMW-6 01/24/2018

1801138-07 Water 01/26/2018TMW-7 01/24/2018

1801138-08 Water 01/26/2018TMW-8 01/24/2018

1801138-09 Water 01/26/2018TMW-9 01/24/2018

1801138-10 Water 01/26/2018TMW-10 01/24/2018

1801138-11 Water 01/26/2018TMW-11 01/25/2018

1801138-12 Water 01/26/2018TMW-12 01/25/2018

Notes and Definitions

Y17 Probable petroleum product(s) present.

Y11 Unidentified peaks present in sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

T Reported value is less than the reporting limit (RL). Result is estimated.

KR Reporting limit(s) raised due to low sample volume submitted.

A11 Result is estimated due to high initial verification standard criteria failure.

A09 Result is estimated due to high recovery of batch quality control.

A07 Result(s) and reporting limit(s) are estimated due to poor precision.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

A01 Result(s) and reporting limit(s) are estimated due to low surrogate recovery.

100 Sample is a matrix spike. Result is not available due to matrix interference.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Page 2 of 39Page 2 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 3 of 39Page 3 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11596.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115107 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115102 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 4 of 39Page 4 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Semivolatiles

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

1.0 ug/L 1 8270Naphthalene91-20-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11545.0 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11538.0 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11579.2 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 5 of 39Page 5 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Volatiles

10 ug/L 10 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

10 ug/L 10 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

50 ug/L 10 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trimethylbenzene526-73-8 01/31/1878 B8A3102

50 ug/L 10 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

10 ug/L 10 82601,2,4-Trimethylbenzene95-63-6 01/31/18380 B8A3102

10 ug/L 10 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

10 ug/L 10 82601,3,5-Trimethylbenzene108-67-8 01/31/18120 B8A3102

10 ug/L 10 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

10 ug/L 10 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

50 ug/L 10 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

50 ug/L 10 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

50 Xug/L 10 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

200 ug/L 10 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

50 ug/L 10 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

50 ug/L 10 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

10 ug/L 10 8260Benzene71-43-2 01/31/18ND B8A3102

10 ug/L 10 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

10 ug/L 10 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

10 ug/L 10 8260Bromoform75-25-2 01/31/18ND B8A3102

50 ug/L 10 8260Bromomethane74-83-9 01/31/18ND B8A3102

10 ug/L 10 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

10 ug/L 10 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

10 ug/L 10 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

50 ug/L 10 8260Chloroethane75-00-3 01/31/18ND B8A3102

10 ug/L 10 8260Chloroform67-66-3 01/31/18ND B8A3102

50 ug/L 10 8260Chloromethane74-87-3 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

50 ug/L 10 8260Cyclohexane110-82-7 01/31/18ND B8A3102

10 ug/L 10 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

10 ug/L 10 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 6 of 39Page 6 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Volatiles

50 ug/L 10 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

50 ug/L 10 8260Diethyl ether60-29-7 01/31/18ND B8A3102

50 ug/L 10 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

10 ug/L 10 8260Ethylbenzene100-41-4 01/31/1835 B8A3102

50 ug/L 10 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

50 ug/L 10 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

10 ug/L 10 8260Hexane110-54-3 01/31/1828 B8A3102

10 ug/L 10 8260Isopropylbenzene98-82-8 01/31/1816 B8A3102

20 ug/L 10 8260m & p - Xylene1330-20-7 01/31/1838 B8A3102

50 ug/L 10 8260Methylene chloride75-09-2 01/31/18ND B8A3102

10 ug/L 10 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

50 Xug/L 10 8260Naphthalene91-20-3 01/31/18ND B8A3102

10 ug/L 10 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

10 ug/L 10 8260n-Propylbenzene103-65-1 01/31/1872 B8A3102

10 ug/L 10 8260o-Xylene95-47-6 01/31/1817 B8A3102

10 ug/L 10 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

10 ug/L 10 8260Styrene100-42-5 01/31/18ND B8A3102

10 ug/L 10 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

500 ug/L 10 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

50 ug/L 10 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

10 ug/L 10 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

50 ug/L 10 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

10 ug/L 10 8260Toluene108-88-3 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

10 ug/L 10 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11597.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115106 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115102 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 7 of 39Page 7 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Semivolatiles See note Y17

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/185.7 B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

1.0 ug/L 1 8270Naphthalene91-20-3 02/09/187.4 B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11551.8 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11540.6 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11567.1 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 8 of 39Page 8 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Volatiles

10 ug/L 10 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

10 ug/L 10 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

50 ug/L 10 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trimethylbenzene526-73-8 01/31/18530 B8A3102

50 ug/L 10 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

10 ug/L 10 82601,2,4-Trimethylbenzene95-63-6 01/31/181600 B8A3102

10 ug/L 10 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

10 ug/L 10 82601,3,5-Trimethylbenzene108-67-8 01/31/18480 B8A3102

10 ug/L 10 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

10 ug/L 10 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

50 ug/L 10 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

50 ug/L 10 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

50 Xug/L 10 82602-Methylnaphthalene91-57-6 01/31/1862 B8A3102

200 ug/L 10 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

50 ug/L 10 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

50 ug/L 10 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

10 ug/L 10 8260Benzene71-43-2 01/31/18ND B8A3102

10 ug/L 10 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

10 ug/L 10 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

10 ug/L 10 8260Bromoform75-25-2 01/31/18ND B8A3102

50 ug/L 10 8260Bromomethane74-83-9 01/31/18ND B8A3102

10 ug/L 10 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

10 ug/L 10 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

10 ug/L 10 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

50 ug/L 10 8260Chloroethane75-00-3 01/31/18ND B8A3102

10 ug/L 10 8260Chloroform67-66-3 01/31/18ND B8A3102

50 ug/L 10 8260Chloromethane74-87-3 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

50 ug/L 10 8260Cyclohexane110-82-7 01/31/18210 B8A3102

10 ug/L 10 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

10 ug/L 10 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 9 of 39Page 9 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Volatiles

50 ug/L 10 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

50 ug/L 10 8260Diethyl ether60-29-7 01/31/18ND B8A3102

50 ug/L 10 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

10 ug/L 10 8260Ethylbenzene100-41-4 01/31/181700 B8A3102

50 ug/L 10 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

50 ug/L 10 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

10 ug/L 10 8260Hexane110-54-3 01/31/18200 B8A3102

10 ug/L 10 8260Isopropylbenzene98-82-8 01/31/1889 B8A3102

200 ug/L 100 8260m & p - Xylene1330-20-7 02/01/187900 B8A3102

50 ug/L 10 8260Methylene chloride75-09-2 01/31/18ND B8A3102

10 ug/L 10 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

50 Xug/L 10 8260Naphthalene91-20-3 01/31/18380 B8A3102

10 ug/L 10 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

10 ug/L 10 8260n-Propylbenzene103-65-1 01/31/18230 B8A3102

10 ug/L 10 8260o-Xylene95-47-6 01/31/181800 B8A3102

10 Tug/L 10 8260sec-Butylbenzene135-98-8 01/31/189.9 B8A3102

10 ug/L 10 8260Styrene100-42-5 01/31/18ND B8A3102

10 ug/L 10 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

500 ug/L 10 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

50 ug/L 10 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

10 ug/L 10 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

50 ug/L 10 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

10 ug/L 10 8260Toluene108-88-3 01/31/18310 B8A3102

10 ug/L 10 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

10 ug/L 10 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11594.1 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115103 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-11599.0 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 10 of 39Page 10 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Semivolatiles See note Y17

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/1853 B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

10 ug/L 10 8270Naphthalene91-20-3 02/16/18270 B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11563.3 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11548.3 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11573.1 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 11 of 39Page 11 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 12 of 39Page 12 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11598.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115106 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115101 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 13 of 39Page 13 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Semivolatiles

5.3 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.1 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.1 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11534.2 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11535.3 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11574.7 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 14 of 39Page 14 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 15 of 39Page 15 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11597.7 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115108 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115103 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 16 of 39Page 16 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Semivolatiles

5.5 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.1 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.2 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.2 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.1 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11558.5 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11559.9 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11573.8 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 17 of 39Page 17 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 02/02/18ND B8B0202

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 02/02/18ND B8B0202

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 02/02/1817 B8B0202

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 02/02/18110 B8B0202

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 02/02/1857 B8B0202

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 02/02/18ND B8B0202

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 02/02/18200 B8B0202

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 02/02/18ND B8B0202

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 02/02/1813 B8B0202

20 ug/L 1 82602-Propanone (acetone)67-64-1 02/02/18ND B8B0202

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 02/02/18ND B8B0202

5.0 ug/L 1 8260Acrylonitrile107-13-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Benzene71-43-2 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromochloromethane74-97-5 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromodichloromethane75-27-4 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromoform75-25-2 02/02/18ND B8B0202

5.0 ug/L 1 8260Bromomethane74-83-9 02/02/18ND B8B0202

1.0 ug/L 1 8260Carbon disulfide75-15-0 02/02/18ND B8B0202

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 02/02/18ND B8B0202

1.0 ug/L 1 8260Chlorobenzene108-90-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Chloroethane75-00-3 02/02/18ND B8B0202

1.0 ug/L 1 8260Chloroform67-66-3 02/02/18ND B8B0202

5.0 ug/L 1 8260Chloromethane74-87-3 02/02/18ND B8B0202

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 02/02/18ND B8B0202

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 02/02/18ND B8B0202

5.0 ug/L 1 8260Cyclohexane110-82-7 02/02/18ND B8B0202

1.0 ug/L 1 8260Dibromochloromethane124-48-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Dibromomethane74-95-3 02/02/18ND B8B0202

Page 18 of 39Page 18 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Volatiles See note Y11

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 02/02/18ND B8B0202

5.0 ug/L 1 8260Diethyl ether60-29-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 02/02/18ND B8B0202

1.0 ug/L 1 8260Ethylbenzene100-41-4 02/02/182.3 B8B0202

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 02/02/18ND B8B0202

5.0 ug/L 1 8260Hexachloroethane67-72-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Hexane110-54-3 02/02/1864 B8B0202

1.0 ug/L 1 8260Isopropylbenzene98-82-8 02/02/185.7 B8B0202

2.0 ug/L 1 8260m & p - Xylene1330-20-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Methylene chloride75-09-2 02/02/18ND B8B0202

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 02/02/18ND B8B0202

5.0 Xug/L 1 8260Naphthalene91-20-3 02/02/18ND B8B0202

1.0 ug/L 1 8260n-Butylbenzene104-51-8 02/02/18ND B8B0202

1.0 ug/L 1 8260n-Propylbenzene103-65-1 02/02/1831 B8B0202

1.0 ug/L 1 8260o-Xylene95-47-6 02/02/18ND B8B0202

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 02/02/1813 B8B0202

1.0 ug/L 1 8260Styrene100-42-5 02/02/18ND B8B0202

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 02/02/18ND B8B0202

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 02/02/18ND B8B0202

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 02/02/18ND B8B0202

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 02/02/18ND B8B0202

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 02/02/18ND B8B0202

1.0 ug/L 1 8260Toluene108-88-3 02/02/18ND B8B0202

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 02/02/18ND B8B0202

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 02/02/18ND B8B0202

1.0 ug/L 1 8260Trichloroethylene79-01-6 02/02/18ND B8B0202

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 02/02/18ND B8B0202

1.0 ug/L 1 8260Vinyl chloride75-01-4 02/02/18ND B8B0202

85-115102 %Surrogate: Bromofluorobenzene 826002/02/18 B8B0202

82.7-115104 %Surrogate: Dibromofluoromethane 826002/02/18 B8B0202

85-115102 %Surrogate: Toluene-d8 826002/02/18 B8B0202

Page 19 of 39Page 19 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Semivolatiles See note Y17

5.0 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/188.0 B8A3108

1.0 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.0 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.0 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.0 ug/L 1 8270Naphthalene91-20-3 02/23/182.1 B8A3108

1.0 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11564.3 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11566.0 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11569.5 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 20 of 39Page 20 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 21 of 39Page 21 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11595.5 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115107 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115100 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 22 of 39Page 22 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Semivolatiles

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.0 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11548.8 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11549.7 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11572.2 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 23 of 39Page 23 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-08

RLCAS #

Client ID: TMW-8

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 24 of 39Page 24 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-08

RLCAS #

Client ID: TMW-8

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND…

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