Lab Report 91021.pdf

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DEMO BUILDING 91021 Federal contract opportunity
Solicitation number
FA441725XXXXX
Issued by
Department of the Air Force Special Operations Command

About this file

This document is a Certificate of Analysis from Advanced Environmental Laboratories for hazardous waste testing of water samples collected from Hurlburt Field on June 23, 2022. The laboratory conducted analytical testing using multiple EPA-approved methods (SW-846 series) on two water samples (labeled 29-22 and 30-22), examining metals (including arsenic, barium, cadmium, chromium, lead, selenium, silver, and mercury) and volatile organic compounds.

The analytical results indicate that all tested metals and volatile compounds were either undetected or detected below quantifiable limits. The laboratory's quality control measures, including method blanks, lab control samples, and matrix spike tests, were within acceptable ranges. The report was prepared for Oneida Total Integrated Enterprises in San Antonio, TX, with a final date of July 7, 2022, and is accredited by NELAC (National Environmental Laboratory Accreditation Conference) under certification number E82574.

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Text version

Craig Myers

Sincerely, CMyers@aellab.com

July 07, 2022

Breanne Whipple Oneida Total Integrated Enterprises 9607 McAllister Freeway Suite 310 San Antonio, TX 78216

RE: Workorder: J2208465 Hurlburt Field Hazardous Waste

Dear Breanne Whipple:

Enclosed are the analytical results for sample(s) received by the laboratory on Tuesday June 28, 2022. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. The analytical results for the samples contained in this report were submitted for analysis as outlined by the Chain of Custody and results pertain only to these samples.

If you have any questions concerning this report, please feel free to contact me.

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574 www.aellab.com www.chemware.com

Sample Summary

Lab ID Sample ID Matrix Method Date Collected Date Received Analytes Reported Basis

J2208465001 29-22 WA SW-846 6010 06/23/2022 09:30 06/28/2022 07:00 7 NA

J2208465001 29-22 WA SW-846 7470A 06/23/2022 09:30 06/28/2022 07:00 1 NA

J2208465001 29-22 WA SW-846 8260B 06/23/2022 09:30 06/28/2022 07:00 11 NA

J2208465002 30-22 WA SW-846 6010 06/23/2022 09:30 06/28/2022 07:00 7 NA

J2208465002 30-22 WA SW-846 7470A 06/23/2022 09:30 06/28/2022 07:00 1 NA

J2208465002 30-22 WA SW-846 8260B 06/23/2022 09:30 06/28/2022 07:00 11 NA

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

Parameter Qualifiers U The compound was analyzed for but not detected.

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

Analytical Results Qualifiers

Lab Qualifiers J DOH Certification #E82574 (FL NELAC) AEL-Jacksonville

J DOD-ELAP Certification #L21-470 (ISO/IEC 17025:2017) AEL-Jacksonville

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

Analytical Results J2208465001Lab ID:

Sample ID: 29-22 Date Collected: 06/23/2022 09:30 Date Received: 06/28/2022 07:00

Matrix: Water

Parameter Results Units PQL MDL DF Prepared Analyzed Lab

METALS, TCLP (SW-846 3010A/SW-846 6010)

Arsenic 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:49 J

Barium 0.27 mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:49 J

Cadmium 0.0050 U mg/L 0.020 0.0050 1 06/30/2022 08:18 07/01/2022 21:49 J

Chromium 0.050 U mg/L 0.20 0.050 1 06/30/2022 08:18 07/01/2022 21:49 J

Lead 0.030 U mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:49 J

Selenium 0.40 U mg/L 1.6 0.40 1 06/30/2022 08:18 07/01/2022 21:49 J

Silver 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:49 J

METALS, TCLP (SW-846 7470A)

Mercury 0.000055 U mg/L 0.0005

0.0000 55 1 06/30/2022 09:26 06/30/2022 14:10 J

VOLATILES, TCLP (SW-846 5030B/SW-846 8260B)

1,1-Dichloroethylene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J

1,2-Dichloroethane 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

1,4-Dichlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J

2-Butanone (MEK) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Benzene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Carbon Tetrachloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Chlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J

Chloroform 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J

Tetrachloroethylene (PCE) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Trichloroethene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Vinyl Chloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab

1,2-Dichloroethane-d4 (S) mg/L 0.50 0.55 110 70 - 128 J

Toluene-d8 (S) mg/L 0.50 0.51 102 77 - 119 J

Bromofluorobenzene (S) mg/L 0.50 0.54 108 86 - 123 J

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

J2208465002Lab ID:

Sample ID: 30-22 Date Collected: 06/23/2022 09:30 Date Received: 06/28/2022 07:00

Matrix: Water

Parameter Results Units PQL MDL DF Prepared Analyzed Lab

METALS, TCLP (SW-846 3010A/SW-846 6010)

Arsenic 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:53 J

Barium 1.2 mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:53 J

Cadmium 0.0050 U mg/L 0.020 0.0050 1 06/30/2022 08:18 07/01/2022 21:53 J

Chromium 0.050 U mg/L 0.20 0.050 1 06/30/2022 08:18 07/01/2022 21:53 J

Lead 0.030 U mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:53 J

Selenium 0.40 U mg/L 1.6 0.40 1 06/30/2022 08:18 07/01/2022 21:53 J

Silver 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:53 J

METALS, TCLP (SW-846 7470A)

Mercury 0.000055 U mg/L 0.0005

0.0000 55 1 06/30/2022 09:26 06/30/2022 14:15 J

VOLATILES, TCLP (SW-846 5030B/SW-846 8260B)

1,1-Dichloroethylene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J

1,2-Dichloroethane 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

1,4-Dichlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J

2-Butanone (MEK) 0.013 mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Benzene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Carbon Tetrachloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Chlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J

Chloroform 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J

Tetrachloroethylene (PCE) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Trichloroethene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Vinyl Chloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab

1,2-Dichloroethane-d4 (S) mg/L 0.50 0.56 112 70 - 128 J

Toluene-d8 (S) mg/L 0.50 0.52 103 77 - 119 J

Bromofluorobenzene (S) mg/L 0.50 0.54 108 86 - 123 J

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Batch: CVAj/1557 Preparation Method: SW-846 7470A Associated Lab IDs: J2208465001, J2208465002

Analysis Method: SW-846 7470A

Parameter Results Units PQL MDL Lab Mercury 0.000011 U mg/L 0.00010 0.000011 J

Method Blank(4372128)

Lab Control Sample (4372129)

Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab Mercury mg/L 0.0020 0 92 80 - 120 J

Matrix Spike (4372130); Matrix Spike Duplicate (4372131); Parent Lab Sample (J2208349001)

Parameter Units Spiked Amount

Spike Result

Spike Recovery

Control Limits

Dup Result

Dup Recovery RPD

RPD

Limit Lab

Mercury mg/L 0.0020 0 95 80 - 120 0 96 1 20 J

QC Results

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Batch: ICPj/2013 Preparation Method: SW-846 3010A Associated Lab IDs: J2208465001, J2208465002

Analysis Method: SW-846 6010

Parameter Results Units PQL MDL Lab Arsenic 0.0080 U mg/L 0.032 0.0080 J

Barium 0.0030 U mg/L 0.012 0.0030 J

Cadmium 0.00050 U mg/L 0.0020 0.00050 J

Chromium 0.0050 U mg/L 0.020 0.0050 J

Lead 0.0030 U mg/L 0.012 0.0030 J

Selenium 0.040 U mg/L 0.16 0.040 J

Silver 0.0080 U mg/L 0.032 0.0080 J

Method Blank(4371471)

Lab Control Sample (4371472)

Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab Arsenic mg/L 0.16 .15 91 80 - 120 J

Barium mg/L 0.06 .05 90 80 - 120 J

Cadmium mg/L 0.01 .01 91 80 - 120 J

Chromium mg/L 0.10 .09 89 80 - 120 J

Lead mg/L 0.06 .06 91 80 - 120 J

Selenium mg/L 0.80 .71 89 80 - 120 J

Silver mg/L 0.16 .14 86 80 - 120 J

Matrix Spike (4371473); Matrix Spike Duplicate (4371474); Parent Lab Sample (J2208349001)

Parameter Units Spiked Amount

Spike Result

Spike Recovery

Control Limits

Dup Result

Dup Recovery RPD

RPD

Limit Lab

Arsenic mg/L 0.16 .19 117 75 - 125 .14 91 25 20 J

Barium mg/L 0.06 .07 51 75 - 125 .06 26 23 20 J

Cadmium mg/L 0.01 .01 119 75 - 125 .01 96 21 20 J

Chromium mg/L 0.10 .11 114 75 - 125 .09 90 24 20 J

Lead mg/L 0.06 .07 117 75 - 125 .06 92 24 20 J

Selenium mg/L 0.80 .94 117 75 - 125 .74 92 24 20 J

Silver mg/L 0.16 .25 156 75 - 125 .29 182 15 20 J

QC Result Comments Matrix Spike - 4371473 - Barium

J4|Estimated Result

QC Results

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Result Comments Matrix Spike - 4371473 - Silver

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Arsenic

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Barium

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Cadmium

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Chromium

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Lead

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Selenium

J4|Estimated Result

Matrix Spike Duplicate - 4371474 - Silver

J4|Estimated Result

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Batch: MSVj/4329 Preparation Method: SW-846 5030B Associated Lab IDs: J2208465001, J2208465002

Analysis Method: SW-846 8260B

Parameter Results Units PQL MDL Lab 1,1-Dichloroethylene 0.00050 U mg/L 0.0020 0.00050 J

1,2-Dichloroethane 0.00025 U mg/L 0.0010 0.00025 J

1,4-Dichlorobenzene 0.00050 U mg/L 0.0020 0.00050 J

2-Butanone (MEK) 0.00025 U mg/L 0.0010 0.00025 J

Benzene 0.00025 U mg/L 0.0010 0.00025 J

Carbon Tetrachloride 0.00025 U mg/L 0.0010 0.00025 J

Chlorobenzene 0.00050 U mg/L 0.0020 0.00050 J

Chloroform 0.00050 U mg/L 0.0020 0.00050 J

Tetrachloroethylene (PCE) 0.00025 U mg/L 0.0010 0.00025 J

Trichloroethene 0.00025 U mg/L 0.0010 0.00025 J

Vinyl Chloride 0.00025 U mg/L 0.0010 0.00025 J

Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab 1,2-Dichloroethane-d4 (S) ug/L 50 55 109 70 - 128

Bromofluorobenzene (S) ug/L 50 54 109 86 - 123

Toluene-d8 (S) ug/L 50 52 104 77 - 119

Method Blank(4372132)

Lab Control Sample (4372133); Lab Control Sample Duplicate (4372134)

Parameter Units Spiked Amount

Spike Result

Spike Recovery

Control Limits

Dup Result

Dup Recovery RPD

RPD

Limit Lab

1,1-Dichloroethylene mg/L 0.02 .02 104 70 - 130 .02 103 0 20 J

1,2-Dichloroethane mg/L 0.02 .02 111 .02 108 3 J

1,4-Dichlorobenzene mg/L 0.02 .02 102 .02 103 1 J

2-Butanone (MEK) mg/L 0.02 .02 115 .02 120 4 J

Benzene mg/L 0.02 .02 101 70 - 130 .02 102 0 20 J

Carbon Tetrachloride mg/L 0.02 .02 103 .02 104 0 J

Chlorobenzene mg/L 0.02 .02 106 70 - 130 .02 107 1 20 J

Chloroform mg/L 0.02 .02 105 70 - 130 .02 105 1 20 J

Tetrachloroethylene (PCE) mg/L 0.02 .02 99 70 - 130 .02 96 3 20 J

Trichloroethene mg/L 0.02 .02 110 70 - 130 .02 113 3 20 J

Vinyl Chloride mg/L 0.02 .02 83 70 - 130 .02 83 1 20 J

QC Results

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Batch: MSVj/4329 Preparation Method: SW-846 5030B Associated Lab IDs: J2208465001, J2208465002

Analysis Method: SW-846 8260B

Surrogates

Parameter Units Spiked Amount

Spike Result

Spike Recovery

Control Limits

Dup Result

Dup Recovery RPD

RPD

Limit Lab

1,2-Dichloroethane-d4 (S) ug/L 50 53 106 70 - 128 54 108 2

Bromofluorobenzene (S) ug/L 50 51 102 86 - 123 50 100 1

Toluene-d8 (S) ug/L 50 52 105 77 - 119 52 104 1

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

QC Cross Reference Lab ID Sample ID Prep Batch Prep Method CVAj/1557 - SW-846 7470A

J2208465001 29-22 DGMj/3612 SW-846 7470A

J2208465002 30-22 DGMj/3612 SW-846 7470A

ICPj/2013 - SW-846 6010

J2208465001 29-22 DGMj/3609 SW-846 3010A

J2208465002 30-22 DGMj/3609 SW-846 3010A

MSVj/4329 - SW-846 8260B

J2208465001 29-22 MSVj/4328 SW-846 5030B

J2208465002 30-22 MSVj/4328 SW-846 5030B

Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216

Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350

Fax: (904) 363-9354

Workorder:

FINAL

Hurlburt Field Hazardous Waste (J2208465)

Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)

POWERED BY

v.13.0.0

Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.

NELAP Accredited E82574

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