Lab Report 91021.pdf
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- DEMO BUILDING 91021 Federal contract opportunity
- Solicitation number
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About this file
This document is a Certificate of Analysis from Advanced Environmental Laboratories for hazardous waste testing of water samples collected from Hurlburt Field on June 23, 2022. The laboratory conducted analytical testing using multiple EPA-approved methods (SW-846 series) on two water samples (labeled 29-22 and 30-22), examining metals (including arsenic, barium, cadmium, chromium, lead, selenium, silver, and mercury) and volatile organic compounds.
The analytical results indicate that all tested metals and volatile compounds were either undetected or detected below quantifiable limits. The laboratory's quality control measures, including method blanks, lab control samples, and matrix spike tests, were within acceptable ranges. The report was prepared for Oneida Total Integrated Enterprises in San Antonio, TX, with a final date of July 7, 2022, and is accredited by NELAC (National Environmental Laboratory Accreditation Conference) under certification number E82574.
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| PWS - CP1142169 Demo Facility 91021 (19 Feb 25).pdf | ||
| Drawings Bldg-91021.pdf |
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Text version
Craig Myers
Sincerely, CMyers@aellab.com
July 07, 2022
Breanne Whipple Oneida Total Integrated Enterprises 9607 McAllister Freeway Suite 310 San Antonio, TX 78216
RE: Workorder: J2208465 Hurlburt Field Hazardous Waste
Dear Breanne Whipple:
Enclosed are the analytical results for sample(s) received by the laboratory on Tuesday June 28, 2022. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. The analytical results for the samples contained in this report were submitted for analysis as outlined by the Chain of Custody and results pertain only to these samples.
If you have any questions concerning this report, please feel free to contact me.
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574 www.aellab.com www.chemware.com
Sample Summary
Lab ID Sample ID Matrix Method Date Collected Date Received Analytes Reported Basis
J2208465001 29-22 WA SW-846 6010 06/23/2022 09:30 06/28/2022 07:00 7 NA
J2208465001 29-22 WA SW-846 7470A 06/23/2022 09:30 06/28/2022 07:00 1 NA
J2208465001 29-22 WA SW-846 8260B 06/23/2022 09:30 06/28/2022 07:00 11 NA
J2208465002 30-22 WA SW-846 6010 06/23/2022 09:30 06/28/2022 07:00 7 NA
J2208465002 30-22 WA SW-846 7470A 06/23/2022 09:30 06/28/2022 07:00 1 NA
J2208465002 30-22 WA SW-846 8260B 06/23/2022 09:30 06/28/2022 07:00 11 NA
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
Parameter Qualifiers U The compound was analyzed for but not detected.
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
Analytical Results Qualifiers
Lab Qualifiers J DOH Certification #E82574 (FL NELAC) AEL-Jacksonville
J DOD-ELAP Certification #L21-470 (ISO/IEC 17025:2017) AEL-Jacksonville
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
Analytical Results J2208465001Lab ID:
Sample ID: 29-22 Date Collected: 06/23/2022 09:30 Date Received: 06/28/2022 07:00
Matrix: Water
Parameter Results Units PQL MDL DF Prepared Analyzed Lab
METALS, TCLP (SW-846 3010A/SW-846 6010)
Arsenic 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:49 J
Barium 0.27 mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:49 J
Cadmium 0.0050 U mg/L 0.020 0.0050 1 06/30/2022 08:18 07/01/2022 21:49 J
Chromium 0.050 U mg/L 0.20 0.050 1 06/30/2022 08:18 07/01/2022 21:49 J
Lead 0.030 U mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:49 J
Selenium 0.40 U mg/L 1.6 0.40 1 06/30/2022 08:18 07/01/2022 21:49 J
Silver 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:49 J
METALS, TCLP (SW-846 7470A)
Mercury 0.000055 U mg/L 0.0005
0.0000 55 1 06/30/2022 09:26 06/30/2022 14:10 J
VOLATILES, TCLP (SW-846 5030B/SW-846 8260B)
1,1-Dichloroethylene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J
1,2-Dichloroethane 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
1,4-Dichlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J
2-Butanone (MEK) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Benzene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Carbon Tetrachloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Chlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J
Chloroform 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 01:32 J
Tetrachloroethylene (PCE) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Trichloroethene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Vinyl Chloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 01:32 J
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab
1,2-Dichloroethane-d4 (S) mg/L 0.50 0.55 110 70 - 128 J
Toluene-d8 (S) mg/L 0.50 0.51 102 77 - 119 J
Bromofluorobenzene (S) mg/L 0.50 0.54 108 86 - 123 J
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
J2208465002Lab ID:
Sample ID: 30-22 Date Collected: 06/23/2022 09:30 Date Received: 06/28/2022 07:00
Matrix: Water
Parameter Results Units PQL MDL DF Prepared Analyzed Lab
METALS, TCLP (SW-846 3010A/SW-846 6010)
Arsenic 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:53 J
Barium 1.2 mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:53 J
Cadmium 0.0050 U mg/L 0.020 0.0050 1 06/30/2022 08:18 07/01/2022 21:53 J
Chromium 0.050 U mg/L 0.20 0.050 1 06/30/2022 08:18 07/01/2022 21:53 J
Lead 0.030 U mg/L 0.12 0.030 1 06/30/2022 08:18 07/01/2022 21:53 J
Selenium 0.40 U mg/L 1.6 0.40 1 06/30/2022 08:18 07/01/2022 21:53 J
Silver 0.080 U mg/L 0.32 0.080 1 06/30/2022 08:18 07/01/2022 21:53 J
METALS, TCLP (SW-846 7470A)
Mercury 0.000055 U mg/L 0.0005
0.0000 55 1 06/30/2022 09:26 06/30/2022 14:15 J
VOLATILES, TCLP (SW-846 5030B/SW-846 8260B)
1,1-Dichloroethylene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J
1,2-Dichloroethane 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
1,4-Dichlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J
2-Butanone (MEK) 0.013 mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Benzene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Carbon Tetrachloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Chlorobenzene 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J
Chloroform 0.0050 U mg/L 0.020 0.0050 10 06/29/2022 23:31 06/30/2022 02:21 J
Tetrachloroethylene (PCE) 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Trichloroethene 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Vinyl Chloride 0.0025 U mg/L 0.010 0.0025 10 06/29/2022 23:31 06/30/2022 02:21 J
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab
1,2-Dichloroethane-d4 (S) mg/L 0.50 0.56 112 70 - 128 J
Toluene-d8 (S) mg/L 0.50 0.52 103 77 - 119 J
Bromofluorobenzene (S) mg/L 0.50 0.54 108 86 - 123 J
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Batch: CVAj/1557 Preparation Method: SW-846 7470A Associated Lab IDs: J2208465001, J2208465002
Analysis Method: SW-846 7470A
Parameter Results Units PQL MDL Lab Mercury 0.000011 U mg/L 0.00010 0.000011 J
Method Blank(4372128)
Lab Control Sample (4372129)
Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab Mercury mg/L 0.0020 0 92 80 - 120 J
Matrix Spike (4372130); Matrix Spike Duplicate (4372131); Parent Lab Sample (J2208349001)
Parameter Units Spiked Amount
Spike Result
Spike Recovery
Control Limits
Dup Result
Dup Recovery RPD
RPD
Limit Lab
Mercury mg/L 0.0020 0 95 80 - 120 0 96 1 20 J
QC Results
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Batch: ICPj/2013 Preparation Method: SW-846 3010A Associated Lab IDs: J2208465001, J2208465002
Analysis Method: SW-846 6010
Parameter Results Units PQL MDL Lab Arsenic 0.0080 U mg/L 0.032 0.0080 J
Barium 0.0030 U mg/L 0.012 0.0030 J
Cadmium 0.00050 U mg/L 0.0020 0.00050 J
Chromium 0.0050 U mg/L 0.020 0.0050 J
Lead 0.0030 U mg/L 0.012 0.0030 J
Selenium 0.040 U mg/L 0.16 0.040 J
Silver 0.0080 U mg/L 0.032 0.0080 J
Method Blank(4371471)
Lab Control Sample (4371472)
Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab Arsenic mg/L 0.16 .15 91 80 - 120 J
Barium mg/L 0.06 .05 90 80 - 120 J
Cadmium mg/L 0.01 .01 91 80 - 120 J
Chromium mg/L 0.10 .09 89 80 - 120 J
Lead mg/L 0.06 .06 91 80 - 120 J
Selenium mg/L 0.80 .71 89 80 - 120 J
Silver mg/L 0.16 .14 86 80 - 120 J
Matrix Spike (4371473); Matrix Spike Duplicate (4371474); Parent Lab Sample (J2208349001)
Parameter Units Spiked Amount
Spike Result
Spike Recovery
Control Limits
Dup Result
Dup Recovery RPD
RPD
Limit Lab
Arsenic mg/L 0.16 .19 117 75 - 125 .14 91 25 20 J
Barium mg/L 0.06 .07 51 75 - 125 .06 26 23 20 J
Cadmium mg/L 0.01 .01 119 75 - 125 .01 96 21 20 J
Chromium mg/L 0.10 .11 114 75 - 125 .09 90 24 20 J
Lead mg/L 0.06 .07 117 75 - 125 .06 92 24 20 J
Selenium mg/L 0.80 .94 117 75 - 125 .74 92 24 20 J
Silver mg/L 0.16 .25 156 75 - 125 .29 182 15 20 J
QC Result Comments Matrix Spike - 4371473 - Barium
J4|Estimated Result
QC Results
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Result Comments Matrix Spike - 4371473 - Silver
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Arsenic
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Barium
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Cadmium
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Chromium
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Lead
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Selenium
J4|Estimated Result
Matrix Spike Duplicate - 4371474 - Silver
J4|Estimated Result
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Batch: MSVj/4329 Preparation Method: SW-846 5030B Associated Lab IDs: J2208465001, J2208465002
Analysis Method: SW-846 8260B
Parameter Results Units PQL MDL Lab 1,1-Dichloroethylene 0.00050 U mg/L 0.0020 0.00050 J
1,2-Dichloroethane 0.00025 U mg/L 0.0010 0.00025 J
1,4-Dichlorobenzene 0.00050 U mg/L 0.0020 0.00050 J
2-Butanone (MEK) 0.00025 U mg/L 0.0010 0.00025 J
Benzene 0.00025 U mg/L 0.0010 0.00025 J
Carbon Tetrachloride 0.00025 U mg/L 0.0010 0.00025 J
Chlorobenzene 0.00050 U mg/L 0.0020 0.00050 J
Chloroform 0.00050 U mg/L 0.0020 0.00050 J
Tetrachloroethylene (PCE) 0.00025 U mg/L 0.0010 0.00025 J
Trichloroethene 0.00025 U mg/L 0.0010 0.00025 J
Vinyl Chloride 0.00025 U mg/L 0.0010 0.00025 J
Surrogates Parameter Units Spiked Amount Spike Result Spike Recovery Control Limits Lab 1,2-Dichloroethane-d4 (S) ug/L 50 55 109 70 - 128
Bromofluorobenzene (S) ug/L 50 54 109 86 - 123
Toluene-d8 (S) ug/L 50 52 104 77 - 119
Method Blank(4372132)
Lab Control Sample (4372133); Lab Control Sample Duplicate (4372134)
Parameter Units Spiked Amount
Spike Result
Spike Recovery
Control Limits
Dup Result
Dup Recovery RPD
RPD
Limit Lab
1,1-Dichloroethylene mg/L 0.02 .02 104 70 - 130 .02 103 0 20 J
1,2-Dichloroethane mg/L 0.02 .02 111 .02 108 3 J
1,4-Dichlorobenzene mg/L 0.02 .02 102 .02 103 1 J
2-Butanone (MEK) mg/L 0.02 .02 115 .02 120 4 J
Benzene mg/L 0.02 .02 101 70 - 130 .02 102 0 20 J
Carbon Tetrachloride mg/L 0.02 .02 103 .02 104 0 J
Chlorobenzene mg/L 0.02 .02 106 70 - 130 .02 107 1 20 J
Chloroform mg/L 0.02 .02 105 70 - 130 .02 105 1 20 J
Tetrachloroethylene (PCE) mg/L 0.02 .02 99 70 - 130 .02 96 3 20 J
Trichloroethene mg/L 0.02 .02 110 70 - 130 .02 113 3 20 J
Vinyl Chloride mg/L 0.02 .02 83 70 - 130 .02 83 1 20 J
QC Results
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Batch: MSVj/4329 Preparation Method: SW-846 5030B Associated Lab IDs: J2208465001, J2208465002
Analysis Method: SW-846 8260B
Surrogates
Parameter Units Spiked Amount
Spike Result
Spike Recovery
Control Limits
Dup Result
Dup Recovery RPD
RPD
Limit Lab
1,2-Dichloroethane-d4 (S) ug/L 50 53 106 70 - 128 54 108 2
Bromofluorobenzene (S) ug/L 50 51 102 86 - 123 50 100 1
Toluene-d8 (S) ug/L 50 52 105 77 - 119 52 104 1
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
QC Cross Reference Lab ID Sample ID Prep Batch Prep Method CVAj/1557 - SW-846 7470A
J2208465001 29-22 DGMj/3612 SW-846 7470A
J2208465002 30-22 DGMj/3612 SW-846 7470A
ICPj/2013 - SW-846 6010
J2208465001 29-22 DGMj/3609 SW-846 3010A
J2208465002 30-22 DGMj/3609 SW-846 3010A
MSVj/4329 - SW-846 8260B
J2208465001 29-22 MSVj/4328 SW-846 5030B
J2208465002 30-22 MSVj/4328 SW-846 5030B
Advanced Environmental Laboratories, Inc 6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580 Phone: (904) 363-9350
Fax: (904) 363-9354
Workorder:
FINAL
Hurlburt Field Hazardous Waste (J2208465)
Thursday, July 7, 2022 9:18:10 AM Dates and times are displayed using (-04:00)
POWERED BY
v.13.0.0
Certificate of Analysis This report shall not be reproduced, except in full, without the written consent of Advanced Environmental Laboratories, Inc.
NELAP Accredited E82574
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