Exhibit_E_Sample_23-R-1000 Results.pdf

22PH-2250

Fuel Oil Reclaimed

FROM TO

NAVSUP FLEET LOGISTICS CENTER JOINT BASE PEARL HARBOR HICKAM YON 335

FUEL LABORATORY, CODE 704

300 NECHES ST. BLDG 1685

PEARL HARBOR, HI 96860

LAB SAMPLE NUMBER SAMPLE DESCRIPTION

DATE SAMPLED DATE RECEIVED DATE TESTS COMPLETED

8/26/2022 1:26 PM 9/7/2022

PRODUCT CODE TEST TYPE SAMPLE VOLUME

FOR FULL QUART

REPRESENTATIVE VOLUME REPORT CREATED BY SAMPLE TAKEN BY

248,525 GALLON LE

MIN MAX USE RESULT UNIT

REPORT C&B

REPORT PASS

REPORT *

38 67.0 °C

1000 400 ppm

25 40 38.3

2.0 <0.1 %vol

NEUTRAL NEUTRAL

50 13 %

2.0 0.10 %wt

2.0 15.0 2.858 cSt

30 90 33.9 SU

0.15 0.002 %wt

0.5 0.010 %wt

-6.7 -9.0 °C

100 ** mg/L

10 ** mg/L

5 ** mg/L

2 ** mg/L

MIL-PRF-24951 REF (B): USE LIMIT

PRODUCT AS REPRESENTED BY SAMPLE MEET:

SPEC. LIMITS OF REF (A)? USE LIMITS OF REF (B)? YES

REMARKS:

TESTED BY VERIFIED BY

CC/BF

SW846 6010B CADMIUM (Cd)

SW846 6010B LEAD (Pb)

SW846 6010B CHROMIUM (Cr)

SW846 6010B ARSENIC (As)

REVERSE DETERGENCY, WATER SAMPLE

FLASH POINT, PMCC

D473 SEDIMENT BY EXTRACTION

POUR POINT

ASH, SULFATED

D445

D2161 (D88)

D874

ANALYSIS OF

EXPLOSIVENESS

SULFUR

VISCOSITY @40°C

VISCOSITY @50°C

EPA, TOTAL HALOGENS

GRAVITY, API @60°F

WATER & SEDIMENT

NEUTRALITY

TEST

APPEARANCE

DETERGENCY, FUEL SAMPLE

22PH-2250

12:45 PM

SIERRA PIER 23 STATION 13, YON 335, COMPOSITE OF TANKS (1, 2, 3, 4), ALL LEVEL, AFTER

RECEIPT FROM B1, PRIOR TO SALE, QUALITY CHECK

PB/IT

8/26/2022

10:23 AM

REF (A):

FTM 1151.1

TEST METHOD

D4176

FISCPINST 5090.9A

FISCPINST 5090.9A

D93

SW846 9077 (METHOD C)

D4052

D1796

FTM 5101.7

D5453

D5949

**Additional testing performed by Hawaii Analytical Laboratory and completed on 09/01/22, see attached report for test results.

ON SPEC

YES

*Test not performed.

Hawaii Analytical Laboratory 3615 Harding Avenue, Suite 308, Honolulu, Hawaii, 96816

Tel: (808) 735-0422 – Fax: (808) 735-0047

AIHA Accredited Laboratory NVLAP Lab code 200655-0 - ISO/IEC 17025:2005 Accredited Laboratory

Controlled Document ID M-100: HAL Letterhead Template Rev: 20140701

September 2, 2022

Benjamin Fegurgur

NAVSUP FLC JBPHH

300 Neches Street BLDG 1685 Honolulu, HI 96826

Project Name: Fuel Oil Reclaim Prior to Sale Date collected: 8/26/2022 Date received: 8/30/2022

HAL #: 202208385

Dear Mr. Fegurgur, Enclosed are the analytical results for the sample received by our laboratory on August 30, 2022. The sample on the chain of custody was received in good condition unless otherwise noted.

The oil sample submitted for lead, cadmium, chromium and arsenic analyses was subcontracted Eurofins Environment Testing America in Tustin, CA. Its report is enclosed in its entirety.

Results in this report are based on the sampling data provided by the client and refer only to the samples as they were received at the laboratory. Unless otherwise requested, all samples will be discarded 14 days from the date of this report.

Quality assurance data is collected to accompany all analyses and to ensure that results generated meet Hawaii Analytical Laboratory’s quality standards. This data is available upon request.

Please contact us at 808.735.0422 if you have questions.

Thank you for using Hawaii Analytical Laboratory and have a great day!

Anne Antin Quality Manager Hawaii Analytical Laboratory 3615 Harding Ave. Ste. 308 Honolulu, HI 96816 Phone: (808) 735-0422 E-mail: aantin@analyzehawaii.com

ANALYTICAL REPORT

Eurofins Calscience 2841 Dow Avenue, Suite 100 Tustin, CA 92780 Tel: (714)895-5494

Laboratory Job ID: 570-108147-1 Client Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

For:

Hawaii Analytical Laboratory 3615 Harding Ave Suite 308 Honolulu, Hawaii 96816

Attn: Anne Antin

Authorized for release by:

9/2/2022 4:00:48 PM

Terri Chang, Project Manager I (657)210-6295 Terri.Chang@et.eurofinsus.com

The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://eol.et.eurofinsus.com/myEOL/ https://www.eurofinsus.com/environment-testing/ask-the-expert/ http://www.eurofinsus.com/Env mailto:Terri.Chang@et.eurofinsus.com

Table of Contents

Client: Hawaii Analytical Laboratory Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Laboratory Job ID: 570-108147-1

Eurofins Calscience

9/2/2022

Cover Page

Table of Contents

Definitions/Glossary

Case Narrative

Detection Summary

Client Sample Results

QC Sample Results

QC Association Summary

Lab Chronicle

Certification Summary

Method Summary

Sample Summary

Chain of Custody

Receipt Checklists

Definitions/Glossary Job ID: 570-108147-1Client: Hawaii Analytical Laboratory

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CFU Colony Forming Unit

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MCL EPA recommended "Maximum Contaminant Level"

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

MPN Most Probable Number

MQL Method Quantitation Limit

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

NEG Negative / Absent

POS Positive / Present

PQL Practical Quantitation Limit

PRES Presumptive

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TNTC Too Numerous To Count

Eurofins Calscience

Page 3 of 14 9/2/2022

Case Narrative Client: Hawaii Analytical Laboratory Job ID: 570-108147-1 Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Job ID: 570-108147-1

Laboratory: Eurofins Calscience

Narrative

Job Narrative 570-108147-1

Comments

No additional comments.

Receipt

The sample was received on 8/31/2022 9:50 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 25.0º C.

Receipt Exceptions Relinquished time was not listed the Chain-of-Custody (COC).

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Eurofins Calscience Page 4 of 14 9/2/2022

Detection Summary

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Client Sample ID: 22PH-2250 Lab Sample ID: 570-108147-1

No Detections.

Eurofins Calscience

This Detection Summary does not include radiochemical test results.

Page 5 of 14 9/2/2022

Client Sample Results

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Method: 6010B - Metals (ICP)

Lab Sample ID: 570-108147-1Client Sample ID: 22PH-2250 Matrix: WasteDate Collected: 08/26/22 12:45

Date Received: 08/31/22 09:50

RL MDL

Arsenic ND 3.00 1.39 mg/Kg 09/01/22 07:00 09/01/22 21:17 5

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.500 0.0830 mg/Kg 09/01/22 07:00 09/01/22 21:17 5Cadmium ND

1.00 0.186 mg/Kg 09/01/22 07:00 09/01/22 21:17 5Chromium ND

2.00 0.409 mg/Kg 09/01/22 07:00 09/01/22 21:17 5Lead ND

Eurofins Calscience

Page 6 of 14 9/2/2022

QC Sample Results

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Method: 6010B - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 570-260957/1-A ^5 Matrix: Waste Prep Type: Total/NA Analysis Batch: 261326 Prep Batch: 260957

RL MDL

Arsenic ND 3.00 1.39 mg/Kg 09/01/22 07:00 09/01/22 20:09 5

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.08300.500 mg/Kg 09/01/22 07:00 09/01/22 20:09 5Cadmium

ND 0.1861.00 mg/Kg 09/01/22 07:00 09/01/22 20:09 5Chromium

ND 0.4092.00 mg/Kg 09/01/22 07:00 09/01/22 20:09 5Lead

Client Sample ID: Lab Control SampleLab Sample ID: LCS 570-260957/2-A ^5 Matrix: Waste Prep Type: Total/NA Analysis Batch: 261326 Prep Batch: 260957

Arsenic 50.3 46.21 mg/Kg 92 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec

Limits

Cadmium 50.3 46.70 mg/Kg 93 80 - 120

Chromium 50.3 47.19 mg/Kg 94 80 - 120

Lead 50.3 46.95 mg/Kg 93 80 - 120

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 570-260957/3-A ^5 Matrix: Waste Prep Type: Total/NA Analysis Batch: 261326 Prep Batch: 260957

Arsenic 49.5 45.17 mg/Kg 91 80 - 120 2 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec

Limits LimitRPD

RPD

Cadmium 49.5 46.36 mg/Kg 94 80 - 120 1 20

Chromium 49.5 46.50 mg/Kg 94 80 - 120 1 20

Lead 49.5 46.19 mg/Kg 93 80 - 120 2 20

Eurofins Calscience

Page 7 of 14 9/2/2022

QC Association Summary

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Metals

Prep Batch: 260957

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 3050B570-108147-1 22PH-2250 Total/NA

Waste 3050BMB 570-260957/1-A ^5 Method Blank Total/NA

Waste 3050BLCS 570-260957/2-A ^5 Lab Control Sample Total/NA

Waste 3050BLCSD 570-260957/3-A ^5 Lab Control Sample Dup Total/NA

Analysis Batch: 261326

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 6010B 260957570-108147-1 22PH-2250 Total/NA

Waste 6010B 260957MB 570-260957/1-A ^5 Method Blank Total/NA

Waste 6010B 260957LCS 570-260957/2-A ^5 Lab Control Sample Total/NA

Waste 6010B 260957LCSD 570-260957/3-A ^5 Lab Control Sample Dup Total/NA

Eurofins Calscience

Page 8 of 14 9/2/2022

Lab Chronicle

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Client Sample ID: 22PH-2250 Lab Sample ID: 570-108147-1 Matrix: WasteDate Collected: 08/26/22 12:45

Date Received: 08/31/22 09:50

Prep 3050B CS5Z09/01/22 07:00 EET CAL 4260957

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 2.00 g 50 mL

Analysis 6010B 5 261326 09/01/22 21:17 P1R EET CAL 4Total/NA

ICP11Instrument ID:

Laboratory References:

EET CAL 4 = Eurofins Calscience Tustin, 2841 Dow Avenue, Tustin, CA 92780, TEL (714)895-5494

Eurofins Calscience

Page 9 of 14 9/2/2022

Accreditation/Certification Summary

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Laboratory: Eurofins Calscience The accreditations/certifications listed below are applicable to this report.

Authority Program Identification Number Expiration Date

Oregon NELAP 4175 02-02-23

Eurofins Calscience

Page 10 of 14 9/2/2022

Method Summary

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Method Method Description LaboratoryProtocol

SW8466010B Metals (ICP) EET CAL 4

SW8463050B Preparation, Metals EET CAL 4

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

EET CAL 4 = Eurofins Calscience Tustin, 2841 Dow Avenue, Tustin, CA 92780, TEL (714)895-5494

Eurofins Calscience

Page 11 of 14 9/2/2022

Sample Summary

Project/Site: 202208385 Fuel Oil Reclaim Prior to Sale

Lab Sample ID Client Sample ID Matrix Collected Received

570-108147-1 22PH-2250 Waste 08/26/22 12:45 08/31/22 09:50

Eurofins CalsciencePage 12 of 14 9/2/2022

Page 13 of 14 9/2/2022

Login Sample Receipt Checklist

Client: Hawaii Analytical Laboratory Job Number: 570-108147-1

Login Number: 108147

Question Answer Comment

Creator: Vitente, Precy

List Source: Eurofins Calscience

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

FalseSamples were received on ice. Thermal preservation not required.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

FalseCOC is filled out with all pertinent information. Refer to Job Narrative for details.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

Eurofins Calscience Page 14 of 14 9/2/2022