Exhibit_E_Sample_21-R-1000.pdf

20PH-2874

Fuel Oil Reclaimed

FROM TO

NAVSUP FLEET LOGISTICS CENTER JOINT BASE PEARL HARBOR HICKAM YON 336

FUEL LABORATORY, CODE 704

300 NECHES ST. BLDG 1685

PEARL HARBOR, HI 96860

LAB SAMPLE NUMBER SAMPLE DESCRIPTION

DATE SAMPLED DATE RECEIVED DATE TESTS COMPLETED

10/8/2020 9:00 AM 12/8/2020

PRODUCT CODE TEST TYPE SAMPLE VOLUME

FOR FULL QUART

REPRESENTATIVE VOLUME REPORT CREATED BY SAMPLE TAKEN BY

240,554 GALLON PB

MIN MAX USE RESULT UNIT

REPORT C&B

REPORT PASS

REPORT *

38 60.0 °C

1000 <200 ppm

25 40 41.0

2.0 <0.10 %vol

NEUTRAL NEUTRAL

50 18 %

2.0 0.03 %wt

2.0 15.0 1.947 cSt

30 90 * SU

0.15 0.002 %wt

0.5 0.025 %wt

-6.7 -27.0 °C

100 ** mg/L

10 ** mg/L

5 ** mg/L

2 ** mg/L

MIL-PRF-24951 REF (B): USE LIMIT

PRODUCT AS REPRESENTED BY SAMPLE MEET:

SPEC. LIMITS OF REF (A)? USE LIMITS OF REF (B)? NO

REMARKS:

TESTED BY VERIFIED BY

CC/BG/MT

**Additional testing performed by Hawaii Analytical Laboratory and completed on 12/02/20, see attached report for test results.

NOT SUITABLE FOR USE

NO

*Test not performed.

10/8/2020

3:56 PM

REF (A):

FTM 1151.1

TEST METHOD

D4176

FISCPINST 5090.9A

FISCPINST 5090.9A

D93

SW846 9077 (METHOD C)

D4052

D1796

FTM 5101.7

D5453

D5949

ANALYSIS OF

EXPLOSIVENESS

SULFUR

VISCOSITY @40°C

VISCOSITY @50°C

EPA, TOTAL HALOGENS

GRAVITY, API @60°F

WATER & SEDIMENT

NEUTRALITY

TEST

APPEARANCE

DETERGENCY, FUEL SAMPLE

20PH-2874

8:30 AM

YON 336, COMPOSITE OF TANKS (1, 2, 3, 4), ALL LEVEL, AFTER RECEIPT FROM B1

IT

REVERSE DETERGENCY, WATER SAMPLE

FLASH POINT, PMCC

D473 SEDIMENT BY EXTRACTION

POUR POINT

ASH, SULFATED

D445

D2161 (D88)

D874

SW846 6010B CADMIUM (Cd)

SW846 6010B LEAD (Pb)

SW846 6010B CHROMIUM (Cr)

SW846 6010B ARSENIC (As)

Hawaii Analytical Laboratory 3615 Harding Avenue, Suite 308, Honolulu, Hawaii, 96816

Tel: (808) 735-0422 – Fax: (808) 735-0047

AIHA Accredited Laboratory NVLAP Lab code 200655-0 - ISO/IEC 17025:2005 Accredited Laboratory

Controlled Document ID M-100: HAL Letterhead Template Rev: 20140701

December 2, 2020

Benjamin Fergurgur

NAVSUP FLC JBPHH

300 Neches Building 1685 Honolulu, HI 96818

Project Name: Fuel Oil Reclaim Determination Date collected: 10/8/2020 and 11/20/2020 Date received: 11/20/2020

HAL #: 202010137

Dear Mr. Fergurgur, Enclosed are the analytical results for the samples received by our laboratory on November 20, 2020.

The samples on the chain of custody were received in good condition unless otherwise noted.

The oil samples submitted for lead, cadmium, chromium and arsenic analyses were subcontracted Eurofins Calscience Laboratory in Garden Grove, CA. Its report is enclosed in its entirety.

Results in this report are based on the sampling data provided by the client and refer only to the samples as they were received at the laboratory. Unless otherwise requested, all samples will be discarded 14 days from the date of this report.

Quality assurance data is collected to accompany all analyses and to ensure that results generated meet Hawaii Analytical Laboratory’s quality standards. This data is available upon request.

Please contact us at 808.735.0422 if you have questions.

Thank you for using Hawaii Analytical Laboratory and have a great day!

Anne Antin Quality Manager Hawaii Analytical Laboratory 3615 Harding Ave. Ste. 308 Honolulu, HI 96816 Phone: (808) 735-0422 E-mail: aantin@analyzehawaii.com

ANALYTICAL REPORT

Eurofins Calscience LLC 7440 Lincoln Way Garden Grove, CA 92841 Tel: (714)895-5494

Laboratory Job ID: 570-44638-1 Client Project/Site: 202010137 Fuel Oil Reclaim Determination

For:

Hawaii Analytical Laboratory 3615 Harding Ave Suite 308 Honolulu, Hawaii 96816

Attn: Anne Antin

Authorized for release by:

12/2/2020 3:21:01 PM

Terri Chang, Project Manager I (714)895-5494 Terri.Chang@eurofinset.com

The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/services-we-offer/ask-the-expert http://www.eurofinsus.com/Env mailto:Terri.Chang@eurofinset.com

Table of Contents

Client: Hawaii Analytical Laboratory Project/Site: 202010137 Fuel Oil Reclaim Determination

Laboratory Job ID: 570-44638-1

Eurofins Calscience LLC

12/2/2020

Cover Page

Table of Contents

Definitions/Glossary

Case Narrative

Detection Summary

Client Sample Results

QC Sample Results

QC Association Summary

Lab Chronicle

Certification Summary

Method Summary

Sample Summary

Chain of Custody

Receipt Checklists

Definitions/Glossary Job ID: 570-44638-1Client: Hawaii Analytical Laboratory

Project/Site: 202010137 Fuel Oil Reclaim Determination

Qualifiers

Metals Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CFU Colony Forming Unit

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MCL EPA recommended "Maximum Contaminant Level"

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

MPN Most Probable Number

MQL Method Quantitation Limit

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

NEG Negative / Absent

POS Positive / Present

PQL Practical Quantitation Limit

PRES Presumptive

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TNTC Too Numerous To Count

Eurofins Calscience LLC

Page 3 of 14 12/2/2020

Case Narrative Client: Hawaii Analytical Laboratory Job ID: 570-44638-1 Project/Site: 202010137 Fuel Oil Reclaim Determination

Job ID: 570-44638-1

Laboratory: Eurofins Calscience LLC

Narrative

Job Narrative 570-44638-1

Comments

No additional comments.

Receipt

The samples were received on 11/24/2020 10:30 AM; the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 23.9º C.

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Eurofins Calscience LLC Page 4 of 14 12/2/2020

Detection Summary

Project/Site: 202010137 Fuel Oil Reclaim Determination

Client Sample ID: 20PH-2874 Lab Sample ID: 570-44638-1

No Detections.

Client Sample ID: 20PH-3316 Lab Sample ID: 570-44638-2

Arsenic

RL

1.49 mg/Kg

MDL

0.513

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1J0.568 6010B

Cadmium 0.990 mg/Kg0.267 Total/NA17.30 6010B

Chromium 0.495 mg/Kg0.281 Total/NA15.25 6010B

Eurofins Calscience LLC

This Detection Summary does not include radiochemical test results.

Page 5 of 14 12/2/2020

Client Sample Results

Project/Site: 202010137 Fuel Oil Reclaim Determination

Method: 6010B - Metals (ICP)

Lab Sample ID: 570-44638-1Client Sample ID: 20PH-2874 Matrix: WasteDate Collected: 10/08/20 00:00

Date Received: 11/24/20 10:30

RL MDL

Arsenic ND 1.50 0.518 mg/Kg 12/01/20 15:00 12/02/20 10:33 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.00 0.270 mg/Kg 12/01/20 15:00 12/02/20 10:33 1Cadmium ND

0.500 0.284 mg/Kg 12/01/20 15:00 12/02/20 10:33 1Chromium ND

1.00 0.264 mg/Kg 12/01/20 15:00 12/02/20 10:33 1Lead ND

Lab Sample ID: 570-44638-2Client Sample ID: 20PH-3316 Matrix: WasteDate Collected: 11/20/20 00:00

Date Received: 11/24/20 10:30

RL MDL

Arsenic 0.568 J 1.49 0.513 mg/Kg 12/01/20 15:00 12/02/20 10:35 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.990 0.267 mg/Kg 12/01/20 15:00 12/02/20 10:35 1Cadmium 7.30

0.495 0.281 mg/Kg 12/01/20 15:00 12/02/20 10:35 1Chromium 5.25

0.990 0.261 mg/Kg 12/01/20 15:00 12/02/20 10:35 1Lead ND

Eurofins Calscience LLC

Page 6 of 14 12/2/2020

QC Sample Results

Project/Site: 202010137 Fuel Oil Reclaim Determination

Method: 6010B - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 570-113163/1-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 113386 Prep Batch: 113163

RL MDL

Arsenic ND 1.46 0.503 mg/Kg 12/01/20 15:00 12/02/20 10:26 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.2620.971 mg/Kg 12/01/20 15:00 12/02/20 10:26 1Cadmium

ND 0.2760.485 mg/Kg 12/01/20 15:00 12/02/20 10:26 1Chromium

ND 0.2560.971 mg/Kg 12/01/20 15:00 12/02/20 10:26 1Lead

Client Sample ID: Lab Control SampleLab Sample ID: LCS 570-113163/2-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 113386 Prep Batch: 113163

Arsenic 50.0 48.06 mg/Kg 96 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Cadmium 50.0 48.36 mg/Kg 97 80 - 120

Chromium 50.0 49.75 mg/Kg 100 80 - 120

Lead 50.0 49.71 mg/Kg 99 80 - 120

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 570-113163/3-A Matrix: Waste Prep Type: Total/NA Analysis Batch: 113386 Prep Batch: 113163

Arsenic 49.5 47.02 mg/Kg 95 80 - 120 2 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Cadmium 49.5 47.98 mg/Kg 97 80 - 120 1 20

Chromium 49.5 49.47 mg/Kg 100 80 - 120 1 20

Lead 49.5 49.15 mg/Kg 99 80 - 120 1 20

Eurofins Calscience LLC

Page 7 of 14 12/2/2020

QC Association Summary

Project/Site: 202010137 Fuel Oil Reclaim Determination

Metals

Prep Batch: 113163

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 3050B570-44638-1 20PH-2874 Total/NA

Waste 3050B570-44638-2 20PH-3316 Total/NA

Waste 3050BMB 570-113163/1-A Method Blank Total/NA

Waste 3050BLCS 570-113163/2-A Lab Control Sample Total/NA

Waste 3050BLCSD 570-113163/3-A Lab Control Sample Dup Total/NA

Analysis Batch: 113386

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Waste 6010B 113163570-44638-1 20PH-2874 Total/NA

Waste 6010B 113163570-44638-2 20PH-3316 Total/NA

Waste 6010B 113163MB 570-113163/1-A Method Blank Total/NA

Waste 6010B 113163LCS 570-113163/2-A Lab Control Sample Total/NA

Waste 6010B 113163LCSD 570-113163/3-A Lab Control Sample Dup Total/NA

Eurofins Calscience LLC

Page 8 of 14 12/2/2020

Lab Chronicle

Project/Site: 202010137 Fuel Oil Reclaim Determination

Client Sample ID: 20PH-2874 Lab Sample ID: 570-44638-1 Matrix: WasteDate Collected: 10/08/20 00:00

Date Received: 11/24/20 10:30

Prep 3050B SP7J12/01/20 15:00 ECL 1113163

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 1.00 g 100 mL

Analysis 6010B 1 113386 12/02/20 10:33 ULPF ECL 1Total/NA

ICP8Instrument ID:

Client Sample ID: 20PH-3316 Lab Sample ID: 570-44638-2 Matrix: WasteDate Collected: 11/20/20 00:00

Date Received: 11/24/20 10:30

Prep 3050B SP7J12/01/20 15:00 ECL 1113163

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 1.01 g 100 mL

Analysis 6010B 1 113386 12/02/20 10:35 ULPF ECL 1Total/NA

ICP8Instrument ID:

Laboratory References:

ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL (714)895-5494

Eurofins Calscience LLC

Page 9 of 14 12/2/2020

Accreditation/Certification Summary

Project/Site: 202010137 Fuel Oil Reclaim Determination

Laboratory: Eurofins Calscience LLC All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.

Authority Program Identification Number Expiration Date

California 10109Los Angeles County Sanitation

Districts

09-30-21

California State 2944 09-30-21

Nevada State CA00111 07-31-21

Oregon NELAP CA300001 01-29-21

USDA US Federal Programs P330-20-00034 02-10-23

Washington State C916-18 10-11-21

Eurofins Calscience LLC

Page 10 of 14 12/2/2020

Method Summary

Project/Site: 202010137 Fuel Oil Reclaim Determination

Method Method Description LaboratoryProtocol

SW8466010B Metals (ICP) ECL 1

SW8463050B Preparation, Metals ECL 1

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL (714)895-5494

Eurofins Calscience LLC

Page 11 of 14 12/2/2020

Sample Summary

Project/Site: 202010137 Fuel Oil Reclaim Determination

Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID

570-44638-1 20PH-2874 Waste 10/08/20 00:00 11/24/20 10:30

570-44638-2 20PH-3316 Waste 11/20/20 00:00 11/24/20 10:30

Eurofins Calscience LLC

Page 12 of 14 12/2/2020

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Login Sample Receipt Checklist

Client: Hawaii Analytical Laboratory Job Number: 570-44638-1

Login Number: 44638

Question Answer Comment

Creator: Soriano, Precy

List Source: Eurofins Calscience

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

FalseCOC is filled out with all pertinent information. Refer to Job Narrative for details.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

Eurofins Calscience Page 14 of 14 12/2/2020