EGLE_ENVReport_2020-10-07.pdf

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FWS MI MONITOR POTENTIAL VAPOR INTRUSION
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This environmental laboratory report details testing conducted by the Michigan Department of Environment, Great Lakes, and Energy on air samples from the Detroit International Wildlife Refuge in Warren, Michigan under solicitation number 140FS224Q0007 for the Fish and Wildlife Service. Analyses identified volatile organic compounds including benzene, toluene, xylenes, and chloroform present in some samples. Methane was also detected in two samples at high concentrations. The report provides results for each air sample tested and identifies compounds analyzed for but not detected.

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

EGLE-RRD-SE MICHIGAN

RE: DETROIT INTERNATIONAL WILDLIFE REFUGE

Warren, MI 48092

27700 Donald Court

Laura Badalamenti

This is the official environmental laboratory report for testing conducted by the Michigan Department of

Environment, Great Lakes, and Energy. Analyses performed by the laboratory were conducted using methods published by the U.S. Environmental Protection Agency, Standard Methods for the Examination of

Water and Wastewater, ASTM, or other published or approved reference methods.

07 October 2020 Work Order: 2008209

Kirby Shane

Laboratory Director

Lab Work Order # 2008209

Page 1 of 19Page 1 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

EGLE-RRD-SE MICHIGAN

27700 Donald Court

Laura Badalamenti

DETROIT INTERNATIONAL WILDLIFE REFUGE

Warren MI, 48092

Site Code: 82000009 10/07/2020

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

2008209-01 Air 08/21/2020VP1-4.5 08/20/2020

2008209-02 Air 08/21/2020VP4-5 08/20/2020

2008209-05 Air 08/21/2020VP7-2.75 08/20/2020

2008209-06 Air 08/21/2020VP8-3 08/20/2020

2008209-07 Air 08/21/2020VP9-3.25 08/20/2020

2008209-08 Air 08/21/202019VPSS-1 08/20/2020

2008209-09 Air 08/21/202019VPSS-2 08/20/2020

2008209-10 Air 08/21/202019VPSS-3 08/20/2020

Notes and Definitions

Y21 Reporting Limits (RL) raised due to matrix interference.

Y11 Unidentified peaks present in sample.

X1 Method TO-15 is used for the analysis of volatile organic compounds in air. Naphthalene and 2-Methylnaphthalene are semi volatile compounds and results should be considered estimated.

T Reported value is less than the reporting limit (RL). Result is estimated.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detected at or above the reporting limit (RL).ND

Not ApplicableNA

Case Narrative

Samples 2008209-03 and -04 were received under vacuum. No analysis is possible.

Page 2 of 19Page 2 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-01

RLCAS #

Client ID: VP1-4.5

QC Batch

Organics-Volatiles See note Y11

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/20ND B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 Tug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/201.3 B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/206.6 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/201.7 B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/2046 B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/205.7 B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/20ND B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/200.78 B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 09/18/2038 B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/203.0 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/208.4 B0I2109

Page 3 of 19Page 3 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-01

RLCAS #

Client ID: VP1-4.5

QC Batch

Organics-Volatiles See note Y11

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/20160 B0I2109

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2030 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/201.9 B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/207.6 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/20ND B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/2031 B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2042 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/201.8 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/204.1 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130102 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/2023 B0I1418

Page 4 of 19Page 4 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-02

RLCAS #

Client ID: VP4-5

QC Batch

Organics-Volatiles See note Y11

17 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 09/18/20ND B0I2109

21 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

17 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

75 ug/m3 10 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

18 ug/m3 10 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

15 ug/m3 10 TO-151,2,3-Trimethylbenzene526-73-8 09/18/20ND B0I2109

38 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 09/18/20ND B0I2109

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 09/18/20ND B0I2109

6.7 ug/m3 10 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 09/18/20840 B0I2109

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

300 X1ug/m3 10 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

42 ug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

17 ug/m3 10 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

11 ug/m3 10 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

9.7 ug/m3 10 TO-15Benzene71-43-2 09/18/2047 B0I2109

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

31 ug/m3 10 TO-15Bromoform75-25-2 09/18/20ND B0I2109

12 ug/m3 10 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

14 ug/m3 10 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

8.0 ug/m3 10 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

15 ug/m3 10 TO-15Chloroform67-66-3 09/18/20ND B0I2109

6.3 A05ug/m3 10 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/2030 B0I2109

14 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

10 ug/m3 10 TO-15Cyclohexane110-82-7 09/18/20160 B0I2109

26 ug/m3 10 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 09/18/20ND B0I2109

13 ug/m3 10 TO-15Ethylbenzene100-41-4 09/18/2022 B0I2109

36 ug/m3 10 TO-15Hexane110-54-3 09/18/201200 B0I2109

Page 5 of 19Page 5 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-02

RLCAS #

Client ID: VP4-5

QC Batch

Organics-Volatiles See note Y11

15 ug/m3 10 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 09/18/2069 B0I2109

11 ug/m3 10 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

270 X1ug/m3 10 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

56 ug/m3 10 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

15 ug/m3 10 TO-15n-Propylbenzene103-65-1 09/18/20ND B0I2109

13 ug/m3 10 TO-15o-Xylene95-47-6 09/18/2023 B0I2109

17 ug/m3 10 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

13 ug/m3 10 TO-15Styrene100-42-5 09/18/20ND B0I2109

21 ug/m3 10 TO-15Tetrachloroethylene127-18-4 09/18/2025 B0I2109

11 ug/m3 10 TO-15Toluene108-88-3 09/18/2051 B0I2109

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

14 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

16 ug/m3 10 TO-15Trichloroethylene79-01-6 09/18/2030 B0I2109

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 09/18/20ND B0I2109

7.8 ug/m3 10 TO-15Vinyl chloride75-01-4 09/18/2016 B0I2109

70-130102 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

8000 ppmv 40 8015Methane74-82-8 09/11/20320000 B0I1418

Page 6 of 19Page 6 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-05

RLCAS #

Client ID: VP7-2.75

QC Batch

Organics-Volatiles See note Y21

8.3 ug/m3 5 TO-151,1,1-Trichloroethane71-55-6 09/21/20ND B0I2313

11 ug/m3 5 TO-151,1,2,2-Tetrachloroethane79-34-5 09/21/20ND B0I2313

8.3 ug/m3 5 TO-151,1,2-Trichloroethane79-00-5 09/21/20ND B0I2313

6.2 ug/m3 5 TO-151,1-Dichloroethane75-34-3 09/21/20ND B0I2313

6.1 ug/m3 5 TO-151,1-Dichloroethylene75-35-4 09/21/20ND B0I2313

38 ug/m3 5 TO-151,2,3-Trichlorobenzene87-61-6 09/21/20ND B0I2313

9.2 ug/m3 5 TO-151,2,3-Trichloropropane96-18-4 09/21/20ND B0I2313

7.5 ug/m3 5 TO-151,2,3-Trimethylbenzene526-73-8 09/21/20ND B0I2313

19 ug/m3 5 TO-151,2,4-Trichlorobenzene120-82-1 09/21/20ND B0I2313

7.5 ug/m3 5 TO-151,2,4-Trimethylbenzene95-63-6 09/21/20ND B0I2313

12 ug/m3 5 TO-151,2-Dibromoethane106-93-4 09/21/20ND B0I2313

9.2 ug/m3 5 TO-151,2-Dichlorobenzene95-50-1 09/21/20ND B0I2313

6.2 ug/m3 5 TO-151,2-Dichloroethane107-06-2 09/21/20ND B0I2313

7.1 ug/m3 5 TO-151,2-Dichloropropane78-87-5 09/21/20ND B0I2313

7.5 ug/m3 5 TO-151,3,5-Trimethylbenzene108-67-8 09/21/20ND B0I2313

3.4 ug/m3 5 TO-151,3-Butadiene106-99-0 09/21/20ND B0I2313

9.2 ug/m3 5 TO-151,3-Dichlorobenzene541-73-1 09/21/20ND B0I2313

9.2 ug/m3 5 TO-151,4-Dichlorobenzene106-46-7 09/21/20ND B0I2313

7.1 ug/m3 5 TO-152,2,4-Trimethylpentane540-84-1 09/21/20ND B0I2313

75 ug/m3 5 TO-152-Butanone (MEK)78-93-3 09/21/20ND B0I2313

150 X1ug/m3 5 TO-152-Methylnaphthalene91-57-6 09/21/20ND B0I2313

21 ug/m3 5 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/21/20ND B0I2313

8.6 ug/m3 5 TO-15Acetonitrile75-05-8 09/21/20ND B0I2313

5.5 ug/m3 5 TO-15Acrylonitrile107-13-1 09/21/20ND B0I2313

4.9 ug/m3 5 TO-15Benzene71-43-2 09/21/20ND B0I2313

10 ug/m3 5 TO-15Bromodichloromethane75-27-4 09/21/20ND B0I2313

16 ug/m3 5 TO-15Bromoform75-25-2 09/21/20ND B0I2313

5.9 ug/m3 5 TO-15Bromomethane74-83-9 09/21/20ND B0I2313

9.6 ug/m3 5 TO-15Carbon tetrachloride56-23-5 09/21/20ND B0I2313

7.0 ug/m3 5 TO-15Chlorobenzene108-90-7 09/21/20ND B0I2313

4.0 ug/m3 5 TO-15Chloroethane75-00-3 09/21/20ND B0I2313

7.5 ug/m3 5 TO-15Chloroform67-66-3 09/21/20ND B0I2313

3.2 ug/m3 5 TO-15Chloromethane74-87-3 09/21/20ND B0I2313

6.1 ug/m3 5 TO-15cis-1,2-Dichloroethylene156-59-2 09/21/20ND B0I2313

6.9 ug/m3 5 TO-15cis-1,3-Dichloropropylene10061-01-5 09/21/20ND B0I2313

5.3 ug/m3 5 TO-15Cyclohexane110-82-7 09/21/20ND B0I2313

13 ug/m3 5 TO-15Dibromochloromethane124-48-1 09/21/20ND B0I2313

7.6 ug/m3 5 TO-15Dichlorodifluoromethane75-71-8 09/21/20ND B0I2313

6.6 ug/m3 5 TO-15Ethylbenzene100-41-4 09/21/20ND B0I2313

18 ug/m3 5 TO-15Hexane110-54-3 09/21/20ND B0I2313

Page 7 of 19Page 7 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-05

RLCAS #

Client ID: VP7-2.75

QC Batch

Organics-Volatiles See note Y21

7.5 ug/m3 5 TO-15Isopropylbenzene98-82-8 09/21/20ND B0I2313

6.6 ug/m3 5 TO-15m & p - Xylene1330-20-7 09/21/2011 B0I2313

5.3 ug/m3 5 TO-15Methylene chloride75-09-2 09/21/20ND B0I2313

9.2 ug/m3 5 TO-15Methyltertiarybutylether1634-04-4 09/21/20ND B0I2313

130 X1ug/m3 5 TO-15Naphthalene91-20-3 09/21/20ND B0I2313

28 ug/m3 5 TO-15n-Butylbenzene104-51-8 09/21/20ND B0I2313

7.5 ug/m3 5 TO-15n-Propylbenzene103-65-1 09/21/20ND B0I2313

6.6 ug/m3 5 TO-15o-Xylene95-47-6 09/21/20ND B0I2313

8.4 ug/m3 5 TO-15sec-Butylbenzene135-98-8 09/21/20ND B0I2313

6.5 ug/m3 5 TO-15Styrene100-42-5 09/21/20ND B0I2313

10 ug/m3 5 TO-15Tetrachloroethylene127-18-4 09/21/20ND B0I2313

5.8 ug/m3 5 TO-15Toluene108-88-3 09/21/2014 B0I2313

6.1 ug/m3 5 TO-15trans-1,2-Dichloroethylene156-60-5 09/21/20ND B0I2313

6.9 ug/m3 5 TO-15trans-1,3-Dichloropropylene10061-02-6 09/21/20ND B0I2313

8.2 ug/m3 5 TO-15Trichloroethylene79-01-6 09/21/208.8 B0I2313

8.6 ug/m3 5 TO-15Trichlorofluoromethane75-69-4 09/21/20ND B0I2313

3.9 ug/m3 5 TO-15Vinyl chloride75-01-4 09/21/20ND B0I2313

70-13088.3 %Surrogate: Bromofluorobenzene TO-1509/21/20 B0I2313

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 8 of 19Page 8 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-06

RLCAS #

Client ID: VP8-3

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/203.0 B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 Tug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/201.3 B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/205.7 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 Tug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/201.4 B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/202.5 B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/20ND B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/203.2 B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/201.2 B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 Tug/m3 1 TO-15Cyclohexane110-82-7 09/18/200.92 B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/202.1 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/204.9 B0I2109

Page 9 of 19Page 9 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-06

RLCAS #

Client ID: VP8-3

QC Batch

Organics-Volatiles

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2020 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/201.7 B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/205.7 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/20ND B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/2041 B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2021 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/2018 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/203.0 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130102 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 10 of 19Page 10 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-07

RLCAS #

Client ID: VP9-3.25

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/202.0 B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/20ND B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/205.4 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 Tug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/201.3 B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/20ND B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/20ND B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/20ND B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 09/18/20ND B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/202.2 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/207.7 B0I2109

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/20ND B0I2109

Page 11 of 19Page 11 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-07

RLCAS #

Client ID: VP9-3.25

QC Batch

Organics-Volatiles

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2030 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/201.8 B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/207.2 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/20ND B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/2031 B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2029 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/202.0 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/204.5 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130102 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 12 of 19Page 12 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-08

RLCAS #

Client ID: 19VPSS-1

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/20ND B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/20ND B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/203.6 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/20ND B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/20ND B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/20ND B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/20ND B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 09/18/20ND B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/202.2 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/202.6 B0I2109

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/20ND B0I2109

Page 13 of 19Page 13 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-08

RLCAS #

Client ID: 19VPSS-1

QC Batch

Organics-Volatiles

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2010 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/203.1 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/20ND B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/207.0 B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2016 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/206.4 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/203.1 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130101 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 14 of 19Page 14 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-09

RLCAS #

Client ID: 19VPSS-2

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/20ND B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/20ND B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/205.1 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/20ND B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/20ND B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/20ND B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/20ND B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 09/18/20ND B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/202.1 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/204.1 B0I2109

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/20ND B0I2109

Page 15 of 19Page 15 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-09

RLCAS #

Client ID: 19VPSS-2

QC Batch

Organics-Volatiles

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2016 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/204.6 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/20ND B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/202.9 B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2024 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/201.6 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/204.0 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130101 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 16 of 19Page 16 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-10

RLCAS #

Client ID: 19VPSS-3

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/18/20ND B0I2109

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/18/20ND B0I2109

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/18/20ND B0I2109

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 09/18/20ND B0I2109

3.8 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/18/205.0 B0I2109

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/18/20ND B0I2109

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/18/20ND B0I2109

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/18/20ND B0I2109

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/18/20ND B0I2109

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/18/20ND B0I2109

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/18/205.9 B0I2109

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/18/20ND B0I2109

30 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 09/18/20ND B0I2109

4.2 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/18/20ND B0I2109

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/18/20ND B0I2109

0.97 ug/m3 1 TO-15Benzene71-43-2 09/18/205.1 B0I2109

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/18/20ND B0I2109

3.1 ug/m3 1 TO-15Bromoform75-25-2 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15Bromomethane74-83-9 09/18/20ND B0I2109

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/18/20ND B0I2109

0.80 ug/m3 1 TO-15Chloroethane75-00-3 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Chloroform67-66-3 09/18/208.6 B0I2109

0.63 A05ug/m3 1 TO-15Chloromethane74-87-3 09/18/20ND B0I2109

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/18/20ND B0I2109

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 09/18/205.0 B0I2109

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/18/202.1 B0I2109

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/18/2050 B0I2109

3.6 ug/m3 1 TO-15Hexane110-54-3 09/18/2043 B0I2109

Page 17 of 19Page 17 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 2008209-10

RLCAS #

Client ID: 19VPSS-3

QC Batch

Organics-Volatiles

1.5 Tug/m3 1 TO-15Isopropylbenzene98-82-8 09/18/201.3 B0I2109

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/18/2015 B0I2109

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 09/18/20ND B0I2109

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/18/20ND B0I2109

27 X1ug/m3 1 TO-15Naphthalene91-20-3 09/18/20ND B0I2109

5.6 ug/m3 1 TO-15n-Butylbenzene104-51-8 09/18/20ND B0I2109

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 09/18/201.5 B0I2109

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/18/204.9 B0I2109

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 09/18/20ND B0I2109

1.3 ug/m3 1 TO-15Styrene100-42-5 09/18/206.7 B0I2109

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/18/20ND B0I2109

1.1 ug/m3 1 TO-15Toluene108-88-3 09/18/2029 B0I2109

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/18/20ND B0I2109

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/18/20ND B0I2109

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/18/202.5 B0I2109

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/18/202.7 B0I2109

0.78 ug/m3 1 TO-15Vinyl chloride75-01-4 09/18/20ND B0I2109

70-130101 %Surrogate: Bromofluorobenzene TO-1509/18/20 B0I2109

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 09/11/20ND B0I1418

20 ppmv 1 8015Ethylene74-85-1 09/11/20ND B0I1418

20 ppmv 1 8015Methane74-82-8 09/11/20ND B0I1418

Page 18 of 19Page 18 of 19

File details come from the government source that posted it. Updated .