EGLE_ENVReport_2019-11-26.pdf

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FWS MI MONITOR POTENTIAL VAPOR INTRUSION
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This document contains an environmental laboratory report from the Michigan Department of Environment, Great Lakes, and Energy regarding testing of air samples from the Detroit International Wildlife Refuge in Warren, Michigan. The report details analyses of volatile organic compounds in eight air samples taken from different locations at the refuge using EPA Method TO-15. Detected compounds included benzene, toluene, ethylbenzene, xylenes, and naphthalene. Sample results are reported in micrograms per cubic meter and include qualifiers noting any unidentified peaks, semi-volatile nature of some compounds, and instances where results were below reporting limits. The report provides analytical methods, quality control batch numbers, detection limits, and surrogate recoveries for the tested samples.

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P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

EGLE-RRD-SE MICHIGAN

RE: DETROIT INTERNATIONAL WILDLIFE REFUGE

Warren, MI 48092

27700 Donald Court

Laura Badalamenti

This is the official environmental laboratory report for testing conducted by the Michigan Department of

Environment, Great Lakes, and Energy. Analyses performed by the laboratory were conducted using methods published by the U.S. Environmental Protection Agency, Standard Methods for the Examination of

Water and Wastewater, ASTM, or other published or approved reference methods.

26 November 2019 Work Order: 1911081

Kirby Shane

Laboratory Director

Lab Work Order # 1911081

Page 1 of 20Page 1 of 20

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

EGLE-RRD-SE MICHIGAN

27700 Donald Court

Laura Badalamenti

DETROIT INTERNATIONAL WILDLIFE REFUGE

Warren MI, 48092

Site Code: 82000009 11/26/2019

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1911081-01 Air 11/06/2019Tubing Blank 11/04/2019

1911081-02 Air 11/06/2019Ambient Blank 11/04/2019

1911081-03 Air 11/06/2019VP1-4.5 11/06/2019

1911081-04 Air 11/06/2019VP4-5 11/06/2019

1911081-05 Air 11/06/2019VP6-6.25 11/06/2019

1911081-06 Air 11/06/2019VP7-2.75 11/06/2019

1911081-07 Air 11/06/2019VP8-3 11/06/2019

1911081-08 Air 11/06/2019VP9-3.25 11/06/2019

Notes and Definitions

Y11 Unidentified peaks present in sample.

X1 Method TO-15 is used for the analysis of volatile organic compounds in air. Naphthalene and 2-Methylnaphthalene are semi volatile compounds and results should be considered estimated.

T Reported value is less than the reporting limit (RL). Result is estimated.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detected at or above the reporting limit (RL).ND

Not ApplicableNA

Page 2 of 20Page 2 of 20

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-01

RLCAS #

Client ID: Tubing Blank

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 11/15/19ND B9K1518

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 11/15/19ND B9K1518

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 11/15/19ND B9K1518

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 11/15/19ND B9K1518

3.7 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 11/15/19ND B9K1518

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 11/15/19ND B9K1518

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 11/15/19ND B9K1518

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 11/15/19ND B9K1518

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 11/15/19ND B9K1518

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 11/15/19ND B9K1518

29 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 11/15/19ND B9K1518

4.1 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/15/19ND B9K1518

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 11/15/19ND B9K1518

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 11/15/19ND B9K1518

0.97 ug/m3 1 TO-15Benzene71-43-2 11/15/191.2 B9K1518

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 11/15/19ND B9K1518

3.1 ug/m3 1 TO-15Bromoform75-25-2 11/15/19ND B9K1518

1.2 ug/m3 1 TO-15Bromomethane74-83-9 11/15/19ND B9K1518

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 11/15/19ND B9K1518

0.80 ug/m3 1 TO-15Chloroethane75-00-3 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15Chloroform67-66-3 11/15/19ND B9K1518

0.63 ug/m3 1 TO-15Chloromethane74-87-3 11/15/190.98 B9K1518

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 11/15/19ND B9K1518

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 11/15/19ND B9K1518

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 11/15/191.3 B9K1518

3.6 ug/m3 1 TO-15Hexane110-54-3 11/15/19ND B9K1518

Lab Work Order # 1911081

Page 3 of 20Page 3 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-01

RLCAS #

Client ID: Tubing Blank

QC Batch

Organics-Volatiles

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 11/15/193.7 B9K1518

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 11/15/19ND B9K1518

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 11/15/19ND B9K1518

26 X1ug/m3 1 TO-15Naphthalene91-20-3 11/15/19ND B9K1518

5.5 ug/m3 1 TO-15n-Butylbenzene104-51-8 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15o-Xylene95-47-6 11/15/192.4 B9K1518

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15Styrene100-42-5 11/15/19ND B9K1518

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 11/15/19ND B9K1518

1.1 ug/m3 1 TO-15Toluene108-88-3 11/15/195.3 B9K1518

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 11/15/19ND B9K1518

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 11/15/19ND B9K1518

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 11/15/19ND B9K1518

0.77 ug/m3 1 TO-15Vinyl chloride75-01-4 11/15/19ND B9K1518

70-130110 %Surrogate: Bromofluorobenzene TO-1511/15/19 B9K1518

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/19ND B9K1915

Lab Work Order # 1911081

Page 4 of 20Page 4 of 20 rmcginn Highlight rmcginn Underline rmcginn Underline rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-02

RLCAS #

Client ID: Ambient Blank

QC Batch

Organics-Volatiles

1.7 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 11/15/19ND B9K1518

2.1 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 11/15/19ND B9K1518

1.7 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 11/15/19ND B9K1518

7.5 ug/m3 1 TO-151,2,3-Trichlorobenzene87-61-6 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,2,3-Trichloropropane96-18-4 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,2,3-Trimethylbenzene526-73-8 11/15/19ND B9K1518

3.7 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 11/15/19ND B9K1518

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 11/15/19ND B9K1518

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 11/15/19ND B9K1518

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 11/15/19ND B9K1518

1.5 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 11/15/19ND B9K1518

0.67 ug/m3 1 TO-151,3-Butadiene106-99-0 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 11/15/19ND B9K1518

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 11/15/19ND B9K1518

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 11/15/19ND B9K1518

15 ug/m3 1 TO-152-Butanone (MEK)78-93-3 11/15/19ND B9K1518

29 X1ug/m3 1 TO-152-Methylnaphthalene91-57-6 11/15/19ND B9K1518

4.1 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/15/19ND B9K1518

1.7 ug/m3 1 TO-15Acetonitrile75-05-8 11/15/19ND B9K1518

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 11/15/19ND B9K1518

0.97 ug/m3 1 TO-15Benzene71-43-2 11/15/19ND B9K1518

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 11/15/19ND B9K1518

3.1 ug/m3 1 TO-15Bromoform75-25-2 11/15/19ND B9K1518

1.2 ug/m3 1 TO-15Bromomethane74-83-9 11/15/19ND B9K1518

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 11/15/19ND B9K1518

0.80 ug/m3 1 TO-15Chloroethane75-00-3 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15Chloroform67-66-3 11/15/19ND B9K1518

0.63 ug/m3 1 TO-15Chloromethane74-87-3 11/15/191.2 B9K1518

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 11/15/19ND B9K1518

1.0 ug/m3 1 TO-15Cyclohexane110-82-7 11/15/19ND B9K1518

2.6 ug/m3 1 TO-15Dibromochloromethane124-48-1 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 11/15/192.3 B9K1518

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 11/15/19ND B9K1518

3.6 ug/m3 1 TO-15Hexane110-54-3 11/15/19ND B9K1518

Lab Work Order # 1911081

Page 5 of 20Page 5 of 20 rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-02

RLCAS #

Client ID: Ambient Blank

QC Batch

Organics-Volatiles

1.5 ug/m3 1 TO-15Isopropylbenzene98-82-8 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 11/15/19ND B9K1518

1.1 ug/m3 1 TO-15Methylene chloride75-09-2 11/15/19ND B9K1518

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 11/15/19ND B9K1518

26 X1ug/m3 1 TO-15Naphthalene91-20-3 11/15/19ND B9K1518

5.5 ug/m3 1 TO-15n-Butylbenzene104-51-8 11/15/19ND B9K1518

1.5 ug/m3 1 TO-15n-Propylbenzene103-65-1 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15o-Xylene95-47-6 11/15/19ND B9K1518

1.7 ug/m3 1 TO-15sec-Butylbenzene135-98-8 11/15/19ND B9K1518

1.3 ug/m3 1 TO-15Styrene100-42-5 11/15/19ND B9K1518

2.1 ug/m3 1 TO-15Tetrachloroethylene127-18-4 11/15/19ND B9K1518

1.1 ug/m3 1 TO-15Toluene108-88-3 11/15/19ND B9K1518

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 11/15/19ND B9K1518

1.4 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 11/15/19ND B9K1518

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 11/15/19ND B9K1518

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 11/15/19ND B9K1518

0.77 ug/m3 1 TO-15Vinyl chloride75-01-4 11/15/19ND B9K1518

70-130109 %Surrogate: Bromofluorobenzene TO-1511/15/19 B9K1518

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/19ND B9K1915

Page 6 of 20Page 6 of 20

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-03

RLCAS #

Client ID: VP1-4.5

QC Batch

Organics-Volatiles See note Y11

42 ug/m3 25 TO-151,1,1-Trichloroethane71-55-6 11/13/19ND B9K1418

52 ug/m3 25 TO-151,1,2,2-Tetrachloroethane79-34-5 11/13/19ND B9K1418

42 ug/m3 25 TO-151,1,2-Trichloroethane79-00-5 11/13/19ND B9K1418

31 ug/m3 25 TO-151,1-Dichloroethane75-34-3 11/13/19ND B9K1418

30 ug/m3 25 TO-151,1-Dichloroethylene75-35-4 11/13/19ND B9K1418

190 ug/m3 25 TO-151,2,3-Trichlorobenzene87-61-6 11/13/19ND B9K1418

46 ug/m3 25 TO-151,2,3-Trichloropropane96-18-4 11/13/19ND B9K1418

37 ug/m3 25 TO-151,2,3-Trimethylbenzene526-73-8 11/13/19ND B9K1418

94 ug/m3 25 TO-151,2,4-Trichlorobenzene120-82-1 11/13/19ND B9K1418

37 ug/m3 25 TO-151,2,4-Trimethylbenzene95-63-6 11/13/19ND B9K1418

58 ug/m3 25 TO-151,2-Dibromoethane106-93-4 11/13/19ND B9K1418

46 ug/m3 25 TO-151,2-Dichlorobenzene95-50-1 11/13/19ND B9K1418

31 ug/m3 25 TO-151,2-Dichloroethane107-06-2 11/13/19ND B9K1418

35 ug/m3 25 TO-151,2-Dichloropropane78-87-5 11/13/19ND B9K1418

37 ug/m3 25 TO-151,3,5-Trimethylbenzene108-67-8 11/13/19ND B9K1418

17 ug/m3 25 TO-151,3-Butadiene106-99-0 11/13/19ND B9K1418

46 ug/m3 25 TO-151,3-Dichlorobenzene541-73-1 11/13/19ND B9K1418

46 ug/m3 25 TO-151,4-Dichlorobenzene106-46-7 11/13/19ND B9K1418

36 ug/m3 25 TO-152,2,4-Trimethylpentane540-84-1 11/13/192600 B9K1418

370 ug/m3 25 TO-152-Butanone (MEK)78-93-3 11/13/19ND B9K1418

740 X1ug/m3 25 TO-152-Methylnaphthalene91-57-6 11/13/19ND B9K1418

100 ug/m3 25 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/13/19ND B9K1418

43 ug/m3 25 TO-15Acetonitrile75-05-8 11/13/19ND B9K1418

28 ug/m3 25 TO-15Acrylonitrile107-13-1 11/13/19ND B9K1418

24 ug/m3 25 TO-15Benzene71-43-2 11/13/191200 B9K1418

51 ug/m3 25 TO-15Bromodichloromethane75-27-4 11/13/19ND B9K1418

79 ug/m3 25 TO-15Bromoform75-25-2 11/13/19ND B9K1418

30 ug/m3 25 TO-15Bromomethane74-83-9 11/13/19ND B9K1418

48 ug/m3 25 TO-15Carbon tetrachloride56-23-5 11/13/19ND B9K1418

35 ug/m3 25 TO-15Chlorobenzene108-90-7 11/13/19ND B9K1418

20 ug/m3 25 TO-15Chloroethane75-00-3 11/13/19ND B9K1418

37 ug/m3 25 TO-15Chloroform67-66-3 11/13/19ND B9K1418

16 ug/m3 25 TO-15Chloromethane74-87-3 11/13/19ND B9K1418

30 ug/m3 25 TO-15cis-1,2-Dichloroethylene156-59-2 11/13/19ND B9K1418

35 ug/m3 25 TO-15cis-1,3-Dichloropropylene10061-01-5 11/13/19ND B9K1418

26 ug/m3 25 TO-15Cyclohexane110-82-7 11/13/19660 B9K1418

65 ug/m3 25 TO-15Dibromochloromethane124-48-1 11/13/19ND B9K1418

38 ug/m3 25 TO-15Dichlorodifluoromethane75-71-8 11/13/19ND B9K1418

33 ug/m3 25 TO-15Ethylbenzene100-41-4 11/13/19170 B9K1418

89 ug/m3 25 TO-15Hexane110-54-3 11/13/195400 B9K1418

Lab Work Order # 1911081

Page 7 of 20Page 7 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-03

RLCAS #

Client ID: VP1-4.5

QC Batch

Organics-Volatiles See note Y11

37 ug/m3 25 TO-15Isopropylbenzene98-82-8 11/13/19ND B9K1418

33 ug/m3 25 TO-15m & p - Xylene1330-20-7 11/13/19460 B9K1418

26 ug/m3 25 TO-15Methylene chloride75-09-2 11/13/19ND B9K1418

46 ug/m3 25 TO-15Methyltertiarybutylether1634-04-4 11/13/19ND B9K1418

670 X1ug/m3 25 TO-15Naphthalene91-20-3 11/13/19ND B9K1418

140 ug/m3 25 TO-15n-Butylbenzene104-51-8 11/13/19ND B9K1418

37 ug/m3 25 TO-15n-Propylbenzene103-65-1 11/13/19ND B9K1418

33 ug/m3 25 TO-15o-Xylene95-47-6 11/13/19140 B9K1418

42 ug/m3 25 TO-15sec-Butylbenzene135-98-8 11/13/19ND B9K1418

32 ug/m3 25 TO-15Styrene100-42-5 11/13/19ND B9K1418

52 ug/m3 25 TO-15Tetrachloroethylene127-18-4 11/13/19130 B9K1418

29 ug/m3 25 TO-15Toluene108-88-3 11/13/193100 B9K1418

30 ug/m3 25 TO-15trans-1,2-Dichloroethylene156-60-5 11/13/19ND B9K1418

35 ug/m3 25 TO-15trans-1,3-Dichloropropylene10061-02-6 11/13/19ND B9K1418

41 ug/m3 25 TO-15Trichloroethylene79-01-6 11/13/19ND B9K1418

43 ug/m3 25 TO-15Trichlorofluoromethane75-69-4 11/13/19ND B9K1418

19 ug/m3 25 TO-15Vinyl chloride75-01-4 11/13/19ND B9K1418

70-13081.6 %Surrogate: Bromofluorobenzene TO-1511/13/19 B9K1418

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/1937 B9K1915

Lab Work Order # 1911081

Page 8 of 20Page 8 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-04

RLCAS #

Client ID: VP4-5

QC Batch

Organics-Volatiles See note Y11

42 ug/m3 25 TO-151,1,1-Trichloroethane71-55-6 11/13/19ND B9K1806

52 ug/m3 25 TO-151,1,2,2-Tetrachloroethane79-34-5 11/13/19ND B9K1806

42 ug/m3 25 TO-151,1,2-Trichloroethane79-00-5 11/13/19ND B9K1806

31 ug/m3 25 TO-151,1-Dichloroethane75-34-3 11/13/19ND B9K1806

30 ug/m3 25 TO-151,1-Dichloroethylene75-35-4 11/13/19ND B9K1806

190 ug/m3 25 TO-151,2,3-Trichlorobenzene87-61-6 11/13/19ND B9K1806

46 ug/m3 25 TO-151,2,3-Trichloropropane96-18-4 11/13/19ND B9K1806

37 ug/m3 25 TO-151,2,3-Trimethylbenzene526-73-8 11/13/19ND B9K1806

94 ug/m3 25 TO-151,2,4-Trichlorobenzene120-82-1 11/13/19ND B9K1806

37 ug/m3 25 TO-151,2,4-Trimethylbenzene95-63-6 11/13/19ND B9K1806

58 ug/m3 25 TO-151,2-Dibromoethane106-93-4 11/13/19ND B9K1806

46 ug/m3 25 TO-151,2-Dichlorobenzene95-50-1 11/13/19ND B9K1806

31 ug/m3 25 TO-151,2-Dichloroethane107-06-2 11/13/19ND B9K1806

35 ug/m3 25 TO-151,2-Dichloropropane78-87-5 11/13/19ND B9K1806

37 ug/m3 25 TO-151,3,5-Trimethylbenzene108-67-8 11/13/19ND B9K1806

17 ug/m3 25 TO-151,3-Butadiene106-99-0 11/13/19ND B9K1806

46 ug/m3 25 TO-151,3-Dichlorobenzene541-73-1 11/13/19ND B9K1806

46 ug/m3 25 TO-151,4-Dichlorobenzene106-46-7 11/13/19ND B9K1806

36 ug/m3 25 TO-152,2,4-Trimethylpentane540-84-1 11/13/192800 B9K1806

370 ug/m3 25 TO-152-Butanone (MEK)78-93-3 11/13/19ND B9K1806

740 X1ug/m3 25 TO-152-Methylnaphthalene91-57-6 11/13/19ND B9K1806

100 ug/m3 25 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/13/19ND B9K1806

43 ug/m3 25 TO-15Acetonitrile75-05-8 11/13/19ND B9K1806

28 ug/m3 25 TO-15Acrylonitrile107-13-1 11/13/19ND B9K1806

24 ug/m3 25 TO-15Benzene71-43-2 11/13/191400 B9K1806

51 ug/m3 25 TO-15Bromodichloromethane75-27-4 11/13/19ND B9K1806

79 ug/m3 25 TO-15Bromoform75-25-2 11/13/19ND B9K1806

30 ug/m3 25 TO-15Bromomethane74-83-9 11/13/19ND B9K1806

48 ug/m3 25 TO-15Carbon tetrachloride56-23-5 11/13/19ND B9K1806

35 ug/m3 25 TO-15Chlorobenzene108-90-7 11/13/19ND B9K1806

20 ug/m3 25 TO-15Chloroethane75-00-3 11/13/19ND B9K1806

37 ug/m3 25 TO-15Chloroform67-66-3 11/13/19ND B9K1806

16 ug/m3 25 TO-15Chloromethane74-87-3 11/13/19ND B9K1806

30 ug/m3 25 TO-15cis-1,2-Dichloroethylene156-59-2 11/13/19ND B9K1806

35 ug/m3 25 TO-15cis-1,3-Dichloropropylene10061-01-5 11/13/19ND B9K1806

26 ug/m3 25 TO-15Cyclohexane110-82-7 11/13/19640 B9K1806

65 ug/m3 25 TO-15Dibromochloromethane124-48-1 11/13/19ND B9K1806

38 ug/m3 25 TO-15Dichlorodifluoromethane75-71-8 11/13/19ND B9K1806

33 ug/m3 25 TO-15Ethylbenzene100-41-4 11/13/19190 B9K1806

89 ug/m3 25 TO-15Hexane110-54-3 11/13/195300 B9K1806

Lab Work Order # 1911081

Page 9 of 20Page 9 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-04

RLCAS #

Client ID: VP4-5

QC Batch

Organics-Volatiles See note Y11

37 ug/m3 25 TO-15Isopropylbenzene98-82-8 11/13/19ND B9K1806

33 ug/m3 25 TO-15m & p - Xylene1330-20-7 11/13/19540 B9K1806

26 ug/m3 25 TO-15Methylene chloride75-09-2 11/13/19ND B9K1806

46 ug/m3 25 TO-15Methyltertiarybutylether1634-04-4 11/13/19ND B9K1806

660 X1ug/m3 25 TO-15Naphthalene91-20-3 11/13/19ND B9K1806

140 ug/m3 25 TO-15n-Butylbenzene104-51-8 11/13/19ND B9K1806

37 ug/m3 25 TO-15n-Propylbenzene103-65-1 11/13/19ND B9K1806

33 ug/m3 25 TO-15o-Xylene95-47-6 11/13/19150 B9K1806

42 ug/m3 25 TO-15sec-Butylbenzene135-98-8 11/13/19ND B9K1806

32 ug/m3 25 TO-15Styrene100-42-5 11/13/19ND B9K1806

52 ug/m3 25 TO-15Tetrachloroethylene127-18-4 11/13/19210 B9K1806

29 ug/m3 25 TO-15Toluene108-88-3 11/13/193600 B9K1806

30 ug/m3 25 TO-15trans-1,2-Dichloroethylene156-60-5 11/13/19ND B9K1806

35 ug/m3 25 TO-15trans-1,3-Dichloropropylene10061-02-6 11/13/19ND B9K1806

41 ug/m3 25 TO-15Trichloroethylene79-01-6 11/13/19ND B9K1806

43 ug/m3 25 TO-15Trichlorofluoromethane75-69-4 11/13/19ND B9K1806

19 ug/m3 25 TO-15Vinyl chloride75-01-4 11/13/19ND B9K1806

70-13080.1 %Surrogate: Bromofluorobenzene TO-1511/13/19 B9K1806

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/191900 B9K1915

Lab Work Order # 1911081

Page 10 of 20Page 10 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-05

RLCAS #

Client ID: VP6-6.25

QC Batch

Organics-Volatiles See note Y11

42 ug/m3 25 TO-151,1,1-Trichloroethane71-55-6 11/13/19ND B9K1418

52 ug/m3 25 TO-151,1,2,2-Tetrachloroethane79-34-5 11/13/19ND B9K1418

42 ug/m3 25 TO-151,1,2-Trichloroethane79-00-5 11/13/19ND B9K1418

31 ug/m3 25 TO-151,1-Dichloroethane75-34-3 11/13/19ND B9K1418

30 ug/m3 25 TO-151,1-Dichloroethylene75-35-4 11/13/19ND B9K1418

190 ug/m3 25 TO-151,2,3-Trichlorobenzene87-61-6 11/13/19ND B9K1418

46 ug/m3 25 TO-151,2,3-Trichloropropane96-18-4 11/13/19ND B9K1418

37 ug/m3 25 TO-151,2,3-Trimethylbenzene526-73-8 11/13/19ND B9K1418

94 ug/m3 25 TO-151,2,4-Trichlorobenzene120-82-1 11/13/19ND B9K1418

37 ug/m3 25 TO-151,2,4-Trimethylbenzene95-63-6 11/13/19ND B9K1418

58 ug/m3 25 TO-151,2-Dibromoethane106-93-4 11/13/19ND B9K1418

46 ug/m3 25 TO-151,2-Dichlorobenzene95-50-1 11/13/19ND B9K1418

31 ug/m3 25 TO-151,2-Dichloroethane107-06-2 11/13/19ND B9K1418

35 ug/m3 25 TO-151,2-Dichloropropane78-87-5 11/13/19ND B9K1418

37 ug/m3 25 TO-151,3,5-Trimethylbenzene108-67-8 11/13/19ND B9K1418

17 ug/m3 25 TO-151,3-Butadiene106-99-0 11/13/19ND B9K1418

46 ug/m3 25 TO-151,3-Dichlorobenzene541-73-1 11/13/19ND B9K1418

46 ug/m3 25 TO-151,4-Dichlorobenzene106-46-7 11/13/19ND B9K1418

36 ug/m3 25 TO-152,2,4-Trimethylpentane540-84-1 11/13/192000 B9K1418

370 ug/m3 25 TO-152-Butanone (MEK)78-93-3 11/13/19ND B9K1418

740 X1ug/m3 25 TO-152-Methylnaphthalene91-57-6 11/13/19ND B9K1418

100 ug/m3 25 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/13/19ND B9K1418

43 ug/m3 25 TO-15Acetonitrile75-05-8 11/13/19ND B9K1418

28 ug/m3 25 TO-15Acrylonitrile107-13-1 11/13/19ND B9K1418

24 ug/m3 25 TO-15Benzene71-43-2 11/13/191000 B9K1418

51 ug/m3 25 TO-15Bromodichloromethane75-27-4 11/13/19ND B9K1418

79 ug/m3 25 TO-15Bromoform75-25-2 11/13/19ND B9K1418

30 ug/m3 25 TO-15Bromomethane74-83-9 11/13/19ND B9K1418

48 ug/m3 25 TO-15Carbon tetrachloride56-23-5 11/13/19ND B9K1418

35 ug/m3 25 TO-15Chlorobenzene108-90-7 11/13/19ND B9K1418

20 ug/m3 25 TO-15Chloroethane75-00-3 11/13/19ND B9K1418

37 ug/m3 25 TO-15Chloroform67-66-3 11/13/19ND B9K1418

16 ug/m3 25 TO-15Chloromethane74-87-3 11/13/19ND B9K1418

30 ug/m3 25 TO-15cis-1,2-Dichloroethylene156-59-2 11/13/19ND B9K1418

35 ug/m3 25 TO-15cis-1,3-Dichloropropylene10061-01-5 11/13/19ND B9K1418

26 ug/m3 25 TO-15Cyclohexane110-82-7 11/13/19370 B9K1418

65 ug/m3 25 TO-15Dibromochloromethane124-48-1 11/13/19ND B9K1418

38 ug/m3 25 TO-15Dichlorodifluoromethane75-71-8 11/13/19ND B9K1418

33 ug/m3 25 TO-15Ethylbenzene100-41-4 11/13/1991 B9K1418

89 ug/m3 25 TO-15Hexane110-54-3 11/13/193100 B9K1418

Lab Work Order # 1911081

Page 11 of 20Page 11 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-05

RLCAS #

Client ID: VP6-6.25

QC Batch

Organics-Volatiles See note Y11

37 ug/m3 25 TO-15Isopropylbenzene98-82-8 11/13/19ND B9K1418

33 ug/m3 25 TO-15m & p - Xylene1330-20-7 11/13/19250 B9K1418

26 ug/m3 25 TO-15Methylene chloride75-09-2 11/13/19ND B9K1418

46 ug/m3 25 TO-15Methyltertiarybutylether1634-04-4 11/13/19ND B9K1418

670 X1ug/m3 25 TO-15Naphthalene91-20-3 11/13/19ND B9K1418

140 ug/m3 25 TO-15n-Butylbenzene104-51-8 11/13/19ND B9K1418

37 ug/m3 25 TO-15n-Propylbenzene103-65-1 11/13/19ND B9K1418

33 ug/m3 25 TO-15o-Xylene95-47-6 11/13/1979 B9K1418

42 ug/m3 25 TO-15sec-Butylbenzene135-98-8 11/13/19ND B9K1418

32 ug/m3 25 TO-15Styrene100-42-5 11/13/19ND B9K1418

52 ug/m3 25 TO-15Tetrachloroethylene127-18-4 11/13/19160 B9K1418

29 ug/m3 25 TO-15Toluene108-88-3 11/13/192100 B9K1418

30 ug/m3 25 TO-15trans-1,2-Dichloroethylene156-60-5 11/13/19ND B9K1418

35 ug/m3 25 TO-15trans-1,3-Dichloropropylene10061-02-6 11/13/19ND B9K1418

41 ug/m3 25 TO-15Trichloroethylene79-01-6 11/13/19ND B9K1418

43 ug/m3 25 TO-15Trichlorofluoromethane75-69-4 11/13/19ND B9K1418

19 ug/m3 25 TO-15Vinyl chloride75-01-4 11/13/19ND B9K1418

70-13087.3 %Surrogate: Bromofluorobenzene TO-1511/13/19 B9K1418

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/194300 B9K1915

Lab Work Order # 1911081

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TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-06

RLCAS #

Client ID: VP7-2.75

QC Batch

Organics-Volatiles See note Y11

17 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 11/14/19ND B9K2008

21 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 11/14/19ND B9K2008

17 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 11/14/19ND B9K2008

75 ug/m3 10 TO-151,2,3-Trichlorobenzene87-61-6 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2,3-Trichloropropane96-18-4 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,3-Trimethylbenzene526-73-8 11/14/19ND B9K2008

37 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 11/14/1927 B9K2008

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 11/14/19ND B9K2008

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 11/14/19ND B9K2008

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 11/14/19ND B9K2008

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 11/14/19ND B9K2008

6.7 ug/m3 10 TO-151,3-Butadiene106-99-0 11/14/19ND B9K2008

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 11/14/19ND B9K2008

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 11/14/19ND B9K2008

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 11/14/19530 B9K2008

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 11/14/19ND B9K2008

290 A05, X1ug/m3 10 TO-152-Methylnaphthalene91-57-6 11/14/19ND B9K2008

41 Tug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/14/1938 B9K2008

17 ug/m3 10 TO-15Acetonitrile75-05-8 11/14/19ND B9K2008

11 ug/m3 10 TO-15Acrylonitrile107-13-1 11/14/19ND B9K2008

9.7 ug/m3 10 TO-15Benzene71-43-2 11/14/19480 B9K2008

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 11/14/19ND B9K2008

31 ug/m3 10 TO-15Bromoform75-25-2 11/14/19ND B9K2008

12 ug/m3 10 TO-15Bromomethane74-83-9 11/14/19ND B9K2008

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15Chlorobenzene108-90-7 11/14/1922 B9K2008

8.0 ug/m3 10 TO-15Chloroethane75-00-3 11/14/19ND B9K2008

15 ug/m3 10 TO-15Chloroform67-66-3 11/14/19ND B9K2008

6.3 ug/m3 10 TO-15Chloromethane74-87-3 11/14/19ND B9K2008

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 11/14/19ND B9K2008

14 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 11/14/19ND B9K2008

10 ug/m3 10 TO-15Cyclohexane110-82-7 11/14/19110 B9K2008

26 ug/m3 10 TO-15Dibromochloromethane124-48-1 11/14/19ND B9K2008

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Ethylbenzene100-41-4 11/14/1999 B9K2008

36 ug/m3 10 TO-15Hexane110-54-3 11/14/19570 B9K2008

Lab Work Order # 1911081

Page 13 of 20Page 13 of 20 rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-06

RLCAS #

Client ID: VP7-2.75

QC Batch

Organics-Volatiles See note Y11

15 ug/m3 10 TO-15Isopropylbenzene98-82-8 11/14/1918 B9K2008

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 11/14/19250 B9K2008

11 ug/m3 10 TO-15Methylene chloride75-09-2 11/14/19ND B9K2008

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 11/14/19ND B9K2008

260 X1ug/m3 10 TO-15Naphthalene91-20-3 11/14/19ND B9K2008

55 ug/m3 10 TO-15n-Butylbenzene104-51-8 11/14/19ND B9K2008

15 ug/m3 10 TO-15n-Propylbenzene103-65-1 11/14/1915 B9K2008

13 ug/m3 10 TO-15o-Xylene95-47-6 11/14/1987 B9K2008

17 ug/m3 10 TO-15sec-Butylbenzene135-98-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Styrene100-42-5 11/14/19ND B9K2008

21 ug/m3 10 TO-15Tetrachloroethylene127-18-4 11/14/1976 B9K2008

11 ug/m3 10 TO-15Toluene108-88-3 11/14/191600 B9K2008

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 11/14/19ND B9K2008

16 ug/m3 10 TO-15Trichloroethylene79-01-6 11/14/19ND B9K2008

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 11/14/19ND B9K2008

7.7 ug/m3 10 TO-15Vinyl chloride75-01-4 11/14/19ND B9K2008

70-13089.9 %Surrogate: Bromofluorobenzene TO-1511/14/19 B9K2008

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/19ND B9K1915

Lab Work Order # 1911081

Page 14 of 20Page 14 of 20 rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-07

RLCAS #

Client ID: VP8-3

QC Batch

Organics-Volatiles See note Y11

17 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 11/14/19ND B9K2008

21 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 11/14/19ND B9K2008

17 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 11/14/19ND B9K2008

75 ug/m3 10 TO-151,2,3-Trichlorobenzene87-61-6 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2,3-Trichloropropane96-18-4 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,3-Trimethylbenzene526-73-8 11/14/19ND B9K2008

37 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 11/14/1922 B9K2008

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 11/14/19ND B9K2008

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 11/14/19ND B9K2008

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 11/14/19ND B9K2008

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 11/14/19ND B9K2008

6.7 ug/m3 10 TO-151,3-Butadiene106-99-0 11/14/19ND B9K2008

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 11/14/19ND B9K2008

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 11/14/19ND B9K2008

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 11/14/191100 B9K2008

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 11/14/19ND B9K2008

290 A05, X1ug/m3 10 TO-152-Methylnaphthalene91-57-6 11/14/19ND B9K2008

41 ug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/14/19ND B9K2008

17 ug/m3 10 TO-15Acetonitrile75-05-8 11/14/19ND B9K2008

11 ug/m3 10 TO-15Acrylonitrile107-13-1 11/14/19ND B9K2008

9.7 ug/m3 10 TO-15Benzene71-43-2 11/14/19860 B9K2008

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 11/14/19ND B9K2008

31 ug/m3 10 TO-15Bromoform75-25-2 11/14/19ND B9K2008

12 ug/m3 10 TO-15Bromomethane74-83-9 11/14/19ND B9K2008

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15Chlorobenzene108-90-7 11/14/19ND B9K2008

8.0 ug/m3 10 TO-15Chloroethane75-00-3 11/14/19ND B9K2008

15 ug/m3 10 TO-15Chloroform67-66-3 11/14/19ND B9K2008

6.3 ug/m3 10 TO-15Chloromethane74-87-3 11/14/19ND B9K2008

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 11/14/19ND B9K2008

14 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 11/14/19ND B9K2008

10 ug/m3 10 TO-15Cyclohexane110-82-7 11/14/19290 B9K2008

26 ug/m3 10 TO-15Dibromochloromethane124-48-1 11/14/19ND B9K2008

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Ethylbenzene100-41-4 11/14/19210 B9K2008

36 ug/m3 10 TO-15Hexane110-54-3 11/14/191700 B9K2008

Lab Work Order # 1911081

Page 15 of 20Page 15 of 20 rmcginn Highlight rmcginn Highlight

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-07

RLCAS #

Client ID: VP8-3

QC Batch

Organics-Volatiles See note Y11

15 ug/m3 10 TO-15Isopropylbenzene98-82-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 11/14/19570 B9K2008

11 ug/m3 10 TO-15Methylene chloride75-09-2 11/14/19ND B9K2008

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 11/14/19ND B9K2008

260 X1ug/m3 10 TO-15Naphthalene91-20-3 11/14/19ND B9K2008

55 ug/m3 10 TO-15n-Butylbenzene104-51-8 11/14/19ND B9K2008

15 ug/m3 10 TO-15n-Propylbenzene103-65-1 11/14/1915 B9K2008

13 ug/m3 10 TO-15o-Xylene95-47-6 11/14/19170 B9K2008

17 ug/m3 10 TO-15sec-Butylbenzene135-98-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Styrene100-42-5 11/14/19ND B9K2008

21 ug/m3 10 TO-15Tetrachloroethylene127-18-4 11/14/19130 B9K2008

11 ug/m3 10 TO-15Toluene108-88-3 11/14/192900 B9K2008

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 11/14/19ND B9K2008

16 ug/m3 10 TO-15Trichloroethylene79-01-6 11/14/19ND B9K2008

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 11/14/19ND B9K2008

7.7 ug/m3 10 TO-15Vinyl chloride75-01-4 11/14/19ND B9K2008

70-13093.1 %Surrogate: Bromofluorobenzene TO-1511/14/19 B9K2008

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/19330 B9K1915

Page 16 of 20Page 16 of 20

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-08

RLCAS #

Client ID: VP9-3.25

QC Batch

Organics-Volatiles See note Y11

17 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 11/14/19ND B9K2008

21 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 11/14/19ND B9K2008

17 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 11/14/19ND B9K2008

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 11/14/19ND B9K2008

75 ug/m3 10 TO-151,2,3-Trichlorobenzene87-61-6 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2,3-Trichloropropane96-18-4 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,3-Trimethylbenzene526-73-8 11/14/19ND B9K2008

37 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 11/14/19ND B9K2008

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 11/14/1921 B9K2008

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 11/14/19ND B9K2008

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 11/14/19ND B9K2008

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 11/14/19ND B9K2008

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 11/14/19ND B9K2008

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 11/14/19ND B9K2008

6.7 ug/m3 10 TO-151,3-Butadiene106-99-0 11/14/19ND B9K2008

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 11/14/19ND B9K2008

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 11/14/19ND B9K2008

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 11/14/191400 B9K2008

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 11/14/19ND B9K2008

290 A05, X1ug/m3 10 TO-152-Methylnaphthalene91-57-6 11/14/19ND B9K2008

41 ug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 11/14/19ND B9K2008

17 ug/m3 10 TO-15Acetonitrile75-05-8 11/14/19ND B9K2008

11 ug/m3 10 TO-15Acrylonitrile107-13-1 11/14/19ND B9K2008

9.7 ug/m3 10 TO-15Benzene71-43-2 11/14/19900 B9K2008

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 11/14/19ND B9K2008

31 ug/m3 10 TO-15Bromoform75-25-2 11/14/19ND B9K2008

12 ug/m3 10 TO-15Bromomethane74-83-9 11/14/19ND B9K2008

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15Chlorobenzene108-90-7 11/14/19ND B9K2008

8.0 ug/m3 10 TO-15Chloroethane75-00-3 11/14/19ND B9K2008

15 ug/m3 10 TO-15Chloroform67-66-3 11/14/19ND B9K2008

6.3 ug/m3 10 TO-15Chloromethane74-87-3 11/14/19ND B9K2008

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 11/14/19ND B9K2008

14 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 11/14/19ND B9K2008

10 ug/m3 10 TO-15Cyclohexane110-82-7 11/14/19260 B9K2008

26 ug/m3 10 TO-15Dibromochloromethane124-48-1 11/14/19ND B9K2008

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Ethylbenzene100-41-4 11/14/19130 B9K2008

36 ug/m3 10 TO-15Hexane110-54-3 11/14/192000 B9K2008

Page 17 of 20Page 17 of 20

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1911081-08

RLCAS #

Client ID: VP9-3.25

QC Batch

Organics-Volatiles See note Y11

15 ug/m3 10 TO-15Isopropylbenzene98-82-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 11/14/19360 B9K2008

11 ug/m3 10 TO-15Methylene chloride75-09-2 11/14/19ND B9K2008

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 11/14/19ND B9K2008

260 X1ug/m3 10 TO-15Naphthalene91-20-3 11/14/19ND B9K2008

55 ug/m3 10 TO-15n-Butylbenzene104-51-8 11/14/19ND B9K2008

15 ug/m3 10 TO-15n-Propylbenzene103-65-1 11/14/19ND B9K2008

13 ug/m3 10 TO-15o-Xylene95-47-6 11/14/19110 B9K2008

17 ug/m3 10 TO-15sec-Butylbenzene135-98-8 11/14/19ND B9K2008

13 ug/m3 10 TO-15Styrene100-42-5 11/14/19ND B9K2008

21 ug/m3 10 TO-15Tetrachloroethylene127-18-4 11/14/19110 B9K2008

11 ug/m3 10 TO-15Toluene108-88-3 11/14/192400 B9K2008

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 11/14/19ND B9K2008

14 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 11/14/19ND B9K2008

16 ug/m3 10 TO-15Trichloroethylene79-01-6 11/14/19ND B9K2008

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 11/14/19ND B9K2008

7.7 ug/m3 10 TO-15Vinyl chloride75-01-4 11/14/19ND B9K2008

70-13094.4 %Surrogate: Bromofluorobenzene TO-1511/14/19 B9K2008

Organics-Methane

20 ppmv 1 8015Ethane74-84-0 11/15/19ND B9K1915

20 ppmv 1 8015Ethylene74-85-1 11/15/19ND B9K1915

20 ppmv 1 8015Methane74-82-8 11/15/19470 B9K1915

Lab Work Order # 1911081

Page 18 of 20Page 18 of 20

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