DRAFT Price Schedule for RFI W912DW25RFI191A.pdf

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RFI for Analytical & Data Validation Services for Environmental Sample Analysis
Solicitation number
W912DW-25-RFI-191A
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This document is a draft price schedule for a Request for Information (RFI) for environmental analytical and data validation services. The U.S. Army Corps of Engineers Seattle District anticipates awarding a single Indefinite Delivery Indefinite Quantity (IDIQ) task order contract with a $1,000,000 total capacity over five years (one base year and four option years). The contract will cover chemical analysis and testing services for various environmental matrices including soil, water, sediment, and air, with a focus on laboratories serving Washington, Oregon, Idaho, and Montana.

The extensive price schedule details over 100 specific analytical testing methods across categories such as conventional/wet chemistry, metals, pesticides, petroleum hydrocarbons, SVOCs, VOCs, and waste characterization. Each testing method includes multiple data validation levels (2A, 2B, and 4) and pricing variations based on sample quantity (1-5, 6-20, and 21+ samples). The contract requires Department of Defense Environmental Laboratory Accreditation Program (ELAP) certification, and bidders must be capable of performing or subcontracting a comprehensive range of environmental testing methodologies. The RFI seeks industry input on the draft performance work statement and pricing structure, with responses due by 14:00 PDT on 25 July 2025.

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Line Item Numbering Schema

YG -N-V

Variable Name Valid Values Description Y Contract Year 1 through 5 G Group Number 01 through 12

N Test Description Line Number

1 through 40 (as needed)

V Data Validation Level

2A, 2B, or 4 (as needed)

Unit Price Test Description Matrix Method Line Item 1-5

Samples 6-20 Samples

21+ Samples

Conventional / Wet Chemistry Alkalinity, as CaCO3 water EPA 310.1 / SM 2320B 101-1

Level 2A Data Validation 101-1-2A Level 2B Data Validation 101-1-2B Level 4 Data Validation 101-1-4

Anions, Individual EPA 300.0 / SM 4500 101-2 Level 2A Data Validation 101-2-2A Level 2B Data Validation 101-2-2B Level 4 Data Validation 101-2-4

Anions, Standard Scan (Br, Cl, PO4, F, S04, NO2-N, and NO3-N)

EPA 300.0 101-3

Level 2A Data Validation 101-3-2A Level 2B Data Validation 101-3-2B Level 4 Data Validation 101-3-4

Biochemical Oxygen Demand, 5-Day EPA 405.1 / SM 5210B 101-4 Level 2A Data Validation 101-4-2A Level 2B Data Validation 101-4-2B Level 4 Data Validation 101-4-4

Chemical Oxygen Demand water EPA 410.1-4 /

SM 5220D

101-5

Level 2A Data Validation 101-5-2A Level 2B Data Validation 101-5-2B Level 4 Data Validation 101-5-4

Chlorine, Total Residual water EPA 330.4 / 330.5 101-6 Level 2A Data Validation 101-6-2A Level 2B Data Validation 101-6-2B Level 4 Data Validation 101-6-4

Coliform, Total or Fecal soil or water SM 9221D/E 101-7 Level 2A Data Validation 101-7-2A Level 2B Data Validation 101-7-2B Level 4 Data Validation 101-7-4

Cyanide, Total soil or water EPA 335.2 / 335.4 /

9010 / SM 4500-CN-C

101-8

Level 2A Data Validation 101-8-2A Level 2B Data Validation 101-8-2B Level 4 Data Validation 101-8-4

Cyanide, Amenable to Chlorination soil or water EPA 335.1 / 335.4 / 9010 / 9012 /

SM 4500-CN-G

101-9

Level 2A Data Validation 101-9-2A Level 2B Data Validation 101-9-2B Level 4 Data Validation 101-9-4

Denotes specific contract year for the worksheet tab.

Denotes general analytical groupings, in bold and gray shading.

Each individual test description.

Validation level for that corresponding specific test description.

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 1 of 12

DRAFT

Cyanide, Free water ASTM D4282 101-10 Level 2A Data Validation 101-10-2A Level 2B Data Validation 101-10-2B Level 4 Data Validation 101-10-4

Cyanide, Weak and Dissociable soil or water SM 4500-CN-I 101-11 Level 2A Data Validation 101-11-2A Level 2B Data Validation 101-11-2B Level 4 Data Validation 101-11-4

Dissolved Oxygen, Lab/Probe EPA 106.2 / 360.1 / SM 4500-O C

101-12

Level 2A Data Validation 101-12-2A Level 2B Data Validation 101-12-2B Level 4 Data Validation 101-12-4

Grain size ASTM D6913 / D7928 101-13 Level 2A Data Validation 101-13-2A Level 2B Data Validation 101-13-2B Level 4 Data Validation 101-13-4

Grain size PSEP 1995 101-14 Level 2A Data Validation 101-14-2A Level 2B Data Validation 101-14-2B Level 4 Data Validation 101-14-4

Grain size, 16 fractions Plumb 1981 101-15 Level 2A Data Validation 101-15-2A Level 2B Data Validation 101-15-2B Level 4 Data Validation 101-15-4

Hardness, As CaCO3 EPA 130.2 / 200.8 /

101-16

Level 2A Data Validation 101-16-2A Level 2B Data Validation 101-16-2B Level 4 Data Validation 101-16-4

Hardness, Ca, MG calculation EPA 200.7 / 6010 101-17 Level 2A Data Validation 101-17-2A Level 2B Data Validation 101-17-2B Level 4 Data Validation 101-17-4

Nitrogen, Total Kjeldahl Nitrogen soil or water EPA 351.2 / 351.3 /

351.4 / SM 4500-Norg

101-18

Level 2A Data Validation 101-18-2A Level 2B Data Validation 101-18-2B Level 4 Data Validation 101-18-4

Nitrogen, Ammonia soil or water EPA 350.1-3 101-19 Level 2A Data Validation 101-19-2A

Level 2B Data Validation 101-19-2B Level 4 Data Validation 101-19-4

Oil and Grease, Silica Gel Treated soil or water EPA 1664 101-20 Level 2A Data Validation 101-20-2A

Level 2B Data Validation 101-20-2B Level 4 Data Validation 101-20-4

Organotins, Total PSEP 101-21 Level 2A Data Validation 101-21-2A Level 2B Data Validation 101-21-2B Level 4 Data Validation 101-21-4

Orthophosphate soil or water EPA 365.3 101-22 Level 2A Data Validation 101-22-2A Level 2B Data Validation 101-22-2B Level 4 Data Validation 101-22-4

Perchlorate soil or water EPA 6860 101-23 Level 2A Data Validation 101-23-2A Level 2B Data Validation 101-23-2B Level 4 Data Validation 101-23-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 2 of 12 pH soil or water EPA 150.1 / 9040 /

9045 / SM 4500-H+

101-24

Level 2A Data Validation 101-24-2A Level 2B Data Validation 101-24-2B Level 4 Data Validation 101-24-4

Phenolics, Manual Distillation soil or water EPA 420.1 / 9065 /

SM 5530D

101-25

Level 2A Data Validation 101-25-2A Level 2B Data Validation 101-25-2B Level 4 Data Validation 101-25-4

Phenols & Methylphenols (Cresols), Blank Not Included air EPA TO-8 101-26

Level 2A Data Validation 101-26-2A Level 2B Data Validation 101-26-2B Level 4 Data Validation 101-26-4

Phosphorus, Total water EPA 365.1 101-27 Level 2A Data Validation 101-27-2A Level 2B Data Validation 101-27-2B Level 4 Data Validation 101-27-4

Settleable Solids EPA 160.5 / SM 2540F 101-28 Level 2A Data Validation 101-28-2A Level 2B Data Validation 101-28-2B Level 4 Data Validation 101-28-4

Specific Conductance soil or water EPA 120.1 / 9050 /

SM 2510

101-29

Level 2A Data Validation 101-29-2A Level 2B Data Validation 101-29-2B Level 4 Data Validation 101-29-4

Sulfide, Titrimetric or Colorimetric water EPA 376.1 / 376.2 / SM 4500-S2 D/F

101-30

Level 2A Data Validation 101-30-2A Level 2B Data Validation 101-30-2B Level 4 Data Validation 101-30-4

Sulfide, PSEP Total soil or water PSEP 1995 101-31 Level 2A Data Validation 101-31-2A Level 2B Data Validation 101-31-2B Level 4 Data Validation 101-31-4

TOC soil or water EPA 9060 101-32 Level 2A Data Validation 101-32-2A Level 2B Data Validation 101-32-2B Level 4 Data Validation 101-32-4

Hexane Extractable Material, Silica Treated water EPA 1664 101-33

Level 2A Data Validation 101-33-2A Level 2B Data Validation 101-33-2B Level 4 Data Validation 101-33-4

Total Phosphorus Colorimetric soil or water EPA 365.1 101-34 Level 2A Data Validation 101-34-2A Level 2B Data Validation 101-34-2B Level 4 Data Validation 101-34-4

Total Solids EPA 160.3 / 160.4 / SM 2540B

101-35

Level 2A Data Validation 101-35-2A Level 2B Data Validation 101-35-2B Level 4 Data Validation 101-35-4

Total Dissolved Solids water EPA 160.1 / SM 2540C 101-36 Level 2A Data Validation 101-36-2A Level 2B Data Validation 101-36-2B Level 4 Data Validation 101-36-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 3 of 12

Total Suspended Solids water EPA 160.2 /

SM 2540D

101-37

Level 2A Data Validation 101-37-2A Level 2B Data Validation 101-37-2B Level 4 Data Validation 101-37-4

Total Volatile Solids EPA 160.4 / SM 2540E 101-38 Level 2A Data Validation 101-38-2A Level 2B Data Validation 101-38-2B Level 4 Data Validation 101-38-4

Total Volatile Suspended Solids EPA 160.4 / SM 2540E 101-39 Level 2A Data Validation 101-39-2A Level 2B Data Validation 101-39-2B Level 4 Data Validation 101-39-4

Turbidity EPA 180.1 / SM 2130B 101-40 Level 2A Data Validation 101-40-2A Level 2B Data Validation 101-40-2B Level 4 Data Validation 101-40-4

Metals Metals, Including Digestion EPA 200.7 / 200.8 /

6010 / 6020 102-1

Level 2A Data Validation 102-1-2A Level 2B Data Validation 102-1-2B Level 4 Data Validation 102-1-4

Metals, Including Digestion But No Other Preparation tissue EPA 200.8 / 6020 102-2

Level 2A Data Validation 102-2-2A Level 2B Data Validation 102-2-2B Level 4 Data Validation 102-2-4

Priority Pollutant Metals ICP/MS: Sb, As, Be, Cd, Cr, Cu, Pb, Ni, Se, Ag, Tl, Zn CVAA: Hg soil or water EPA 6020

EPA 7470 / 7471

102-3

Level 2A Data Validation 102-3-2A Level 2B Data Validation 102-3-2B Level 4 Data Validation 102-3-4

California Administrative Manual 17 Metals, CA Title 22 ICP: Ba, Be, Cr, Co, Cu, Ni, Ag, V, Zn ICP/ MS: Sb, As, Cd, Pb, Mo, SE, Tl CVAA: Hg

EPA 200.7 / 6010

EPA 200.8 / 6020

EPA 245.1 / 7470

102-4

Level 2A Data Validation 102-4-2A Level 2B Data Validation 102-4-2B Level 4 Data Validation 102-4-4

Superfund Contract Laboratory Program Target Analyte List Metals ICP: Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, K, Ag, Na, V, Zn ICP/: Sb, As, Cd, Pb, Tl CVAA: Hg

EPA 6010

EPA 6020

EPA 7470 / 7471

102-5

Level 2A Data Validation 102-5-2A Level 2B Data Validation 102-5-2B Level 4 Data Validation 102-5-4

RCRA Total Metals ICP: As, Ba, Cd, Cr, Pb, Ag, Se CVAA: Hg

EPA 6010

EPA 7470 / 7471

102-6

Level 2A Data Validation 102-6-2A Level 2B Data Validation 102-6-2B Level 4 Data Validation 102-6-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 4 of 12

RCRA Model Toxics Control Act Limits ICP: As, Ba, Cd, Cr, Pb, Ag, Se CVAA: Hg soil or water EPA 6010

EPA 7470 / 7471

102-7

Level 2A Data Validation 102-7-2A Level 2B Data Validation 102-7-2B Level 4 Data Validation 102-7-4

Chromium, Hexavalent water EPA 7196 / SM 3500-Cr D

102-8

Level 2A Data Validation 102-8-2A Level 2B Data Validation 102-8-2B Level 4 Data Validation 102-8-4

Chromium, Hexavalent soil EPA 3060 / 7196 102-9 Level 2A Data Validation 102-9-2A Level 2B Data Validation 102-9-2B Level 4 Data Validation 102-9-4

Chromium, Hexavalent water EPA 218.6 / 7199 102-10 Level 2A Data Validation 102-10-2A Level 2B Data Validation 102-10-2B Level 4 Data Validation 102-10-4

Lead air NIOSH 7082 102-11 Level 2A Data Validation 102-11-2A Level 2B Data Validation 102-11-2B Level 4 Data Validation 102-11-4

Mercury EPA 245.1 / 245.2 / 7470 / 7471

102-12

Level 2A Data Validation 102-12-2A Level 2B Data Validation 102-12-2B Level 4 Data Validation 102-12-4

Mercury, Cold Vapor with 20 ng/L LOD water EPA 1631 / 7470 102-13 Level 2A Data Validation 102-13-2A Level 2B Data Validation 102-13-2B Level 4 Data Validation 102-13-4

Mercury, Low Level soil or water EPA 1631 / 7470 / 7471 102-14

Level 2A Data Validation 102-14-2A Level 2B Data Validation 102-14-2B Level 4 Data Validation 102-14-4

Perfluorinated Compounds Per- and Polyfluorinated Alkyl Substances (drinking water) drinking water EPA 537.1 103-1

Level 2A Data Validation 103-1-2A Level 2B Data Validation 103-1-2B Level 4 Data Validation 103-1-4

Per- and Polyfluorinated Alkyl Substances (drinking water) drinking water EPA 533 103-2

Level 2A Data Validation 103-2-2A Level 2B Data Validation 103-2-2B Level 4 Data Validation 103-2-4

Per- and Polyfluorinated Alkyl Substances soil or water EPA 1633 103-3

Level 2A Data Validation 103-3-2A Level 2B Data Validation 103-3-2B Level 4 Data Validation 103-3-4

Pesticides, Herbicides, and PCBs, Including Permanganate and Sulfur Cleanup In Analysis Organochlorine Pesticides EPA 608 / 8081 104-1

Level 2A Data Validation 104-1-2A Level 2B Data Validation 104-1-2B Level 4 Data Validation 104-1-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 5 of 12

Organochlorine Pesticides, Low-Level or National Oceanic and Atmospheric Administration Status and Trends

EPA 8081 104-2

Level 2A Data Validation 104-2-2A Level 2B Data Validation 104-2-2B Level 4 Data Validation 104-2-4

Organochlorine Pesticides Low-Level, Including Gel Permeation Chromatography with 1.0-2.0 µg/kg wet weight LOQ (10.0 µg/kg wet weight LOQ for methoxychlor) tissue EPA 8081 104-3

Level 2A Data Validation 104-3-2A Level 2B Data Validation 104-3-2B Level 4 Data Validation 104-3-4

Organophosphorus Pesticides EPA 8141 / 8270 SIM 104-4 Level 2A Data Validation 104-4-2A Level 2B Data Validation 104-4-2B Level 4 Data Validation 104-4-4

Pesticides EPA 1699 104-5 Level 2A Data Validation 104-5-2A Level 2B Data Validation 104-5-2B Level 4 Data Validation 104-5-4

Herbicides EPA 8041 / 8151 104-6 Level 2A Data Validation 104-6-2A Level 2B Data Validation 104-6-2B Level 4 Data Validation 104-6-4

PCB, With Cleanup solid, oil, water, or wipes

EPA 608 / 8082 104-7

Level 2A Data Validation 104-7-2A Level 2B Data Validation 104-7-2B Level 4 Data Validation 104-7-4

PCBs, Ultra Low-Level soil or water EPA 608 / 8082 104-8 Level 2A Data Validation 104-8-2A Level 2B Data Validation 104-8-2B Level 4 Data Validation 104-8-4

PCBs Ultra Low-Level, Including Gel Permeation Chromatography with 4.0 µg/kg LOQ tissue EPA 608 / 8082 104-9

Level 2A Data Validation 104-9-2A Level 2B Data Validation 104-9-2B Level 4 Data Validation 104-9-4

PCB Congeners, 209 Full List EPA 1668 104-10 Level 2A Data Validation 104-10-2A Level 2B Data Validation 104-10-2B Level 4 Data Validation 104-10-4

PCBs Congeners, Ultra Low-Level 209 Full List tissue EPA 1668 104-11

Level 2A Data Validation 104-11-2A Level 2B Data Validation 104-11-2B Level 4 Data Validation 104-11-4

Pesticides and PCBs, Priority Pollutant List

EPA 625 104-12

Level 2A Data Validation 104-12-2A Level 2B Data Validation 104-12-2B Level 4 Data Validation 104-12-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 6 of 12

Chemical Activated Luciferase Gene Expression, Dioxin and PCB Toxic Equivalency Factors

EPA 4435 104-13

Level 2A Data Validation 104-13-2A Level 2B Data Validation 104-13-2B Level 4 Data Validation 104-13-4

1,4-Dioxane EPA 522 104-14 Level 2A Data Validation 104-14-2A Level 2B Data Validation 104-14-2B Level 4 Data Validation 104-14-4

Petroleum Hydrocarbons Gasoline Range Organics (GRO)/ NWTPH-Gx water AMPH 105-1

Level 2A Data Validation 105-1-2A Level 2B Data Validation 105-1-2B Level 4 Data Validation 105-1-4

GRO/NWTPH-Gx, including 5035 kit soil AMPH 105-2 Level 2A Data Validation 105-2-2A Level 2B Data Validation 105-2-2B Level 4 Data Validation 105-2-4

GRO + Benzene, Toluene, Ethylbenzene, and Xylenes/ NWTPH-Gx Modified water EPA 8021 / AMPH 105-3

Level 2A Data Validation 105-3-2A Level 2B Data Validation 105-3-2B Level 4 Data Validation 105-3-4

GRO + Benzene, Toluene, Ethylbenzene, and Xylenes/NWTPH-Gx Modified, including 5035 kit soil EPA 8021 / AMPH 105-4

Level 2A Data Validation 105-4-2A Level 2B Data Validation 105-4-2B Level 4 Data Validation 105-4-4

Diesel Range Organics/NWTPH-Dx soil or water AMPH 105-5 Level 2A Data Validation 105-5-2A Level 2B Data Validation 105-5-2B Level 4 Data Validation 105-5-4

Total Petroleum Hydrocarbons, GRO EPA 8015 105-6 Level 2A Data Validation 105-6-2A Level 2B Data Validation 105-6-2B Level 4 Data Validation 105-6-4

Total Petroleum Hydrocarbons, Diesel Range Organics

EPA 8015 105-7

Level 2A Data Validation 105-7-2A Level 2B Data Validation 105-7-2B Level 4 Data Validation 105-7-4

Total Petroleum Hydrocarbons, Oil Range Organics

EPA 8015 105-8

Level 2A Data Validation 105-8-2A Level 2B Data Validation 105-8-2B Level 4 Data Validation 105-8-4

Volatile Petroleum Hydrocarbons Fractions

MADEP-VPH-04-1.1 /

Montana Method /

AMPH

105-9

Level 2A Data Validation 105-9-2A Level 2B Data Validation 105-9-2B Level 4 Data Validation 105-9-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 7 of 12

Extractable Petroleum Hydrocarbons Fractions

MADEP-VPH-04-1.1 /

Montana Method /

AMPH

105-10

Level 2A Data Validation 105-10-2A Level 2B Data Validation 105-10-2B Level 4 Data Validation 105-10-4

SVOC

SVOCs, DoD-QSM Std List EPA 525.2 / 8270 106-1

Level 2A Data Validation 106-1-2A Level 2B Data Validation 106-1-2B Level 4 Data Validation 106-1-4

SVOCs, DoD-QSM Std List EPA 8270 SIM 106-2 Level 2A Data Validation 106-2-2A Level 2B Data Validation 106-2-2B Level 4 Data Validation 106-2-4

SVOCs, Puget Sound Dredged Disposal Analysis List

EPA 8270 SIM 106-3

Level 2A Data Validation 106-3-2A Level 2B Data Validation 106-3-2B Level 4 Data Validation 106-3-4

SVOCs, Priority Pollutant List EPA 625 106-4 Level 2A Data Validation 106-4-2A Level 2B Data Validation 106-4-2B Level 4 Data Validation 106-4-4

SVOCs, Low-Level EPA 8270 SIM 106-5 Level 2A Data Validation 106-5-2A Level 2B Data Validation 106-5-2B Level 4 Data Validation 106-5-4

SVOCs (benzo(a)pyrene, dimethyl nitrosamine, hexachlorobenzene, hexachlorobutadiene)

EPA 8270 106-6

Level 2A Data Validation 106-6-2A Level 2B Data Validation 106-6-2B Level 4 Data Validation 106-6-4

PAH EPA 8270 106-7

Level 2A Data Validation 106-7-2A Level 2B Data Validation 106-7-2B Level 4 Data Validation 106-7-4

PAH air EPA TO-13 106-8 Level 2A Data Validation 106-8-2A Level 2B Data Validation 106-8-2B Level 4 Data Validation 106-8-4

PAH, Low-Level EPA 8270 SIM 106-9 Level 2A Data Validation 106-9-2A Level 2B Data Validation 106-9-2B Level 4 Data Validation 106-9-4

1,4-Dioxane, As SVOC EPA 8270 106-10 Level 2A Data Validation 106-10-2A Level 2B Data Validation 106-10-2B Level 4 Data Validation 106-10-4

Nitramines & Nitroaromatics EPA 8330 106-11 Level 2A Data Validation 106-11-2A Level 2B Data Validation 106-11-2B Level 4 Data Validation 106-11-4

Nitroglycerin & Pentaerythritol Tetranitrate

EPA 8332 106-12

Level 2A Data Validation 106-12-2A Level 2B Data Validation 106-12-2B Level 4 Data Validation 106-12-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 8 of 12

Library Search For Tentatively Identified Compounds

EPA 8270 106-13

Dioxins/Furans EPA 1613 / 8290 106-14 Level 2A Data Validation 106-14-2A Level 2B Data Validation 106-14-2B Level 4 Data Validation 106-14-4

2,3,7,8- tetrachlorodibenzo-p-dioxin/2,3,7,8-tetrachlorodibenzofuran

EPA 1613 / 8290 106-15

Level 2A Data Validation 106-15-2A Level 2B Data Validation 106-15-2B Level 4 Data Validation 106-15-4

Polybromintaed Diphenyl Ethers EPA 1614 106-16 Level 2A Data Validation 106-16-2A Level 2B Data Validation 106-16-2B Level 4 Data Validation 106-16-4

Polybrominated Diphenyl Ethers Congeners (15, 28/33, 46, 47, 66, 57, 99, 100, 119, 153, 154, 155, and 209)

EPA 1614 106-17

Level 2A Data Validation 106-17-2A Level 2B Data Validation 106-17-2B Level 4 Data Validation 106-17-4

PAH, Not Including Prep tissue EPA 8270 106-18 Level 2A Data Validation 106-18-2A Level 2B Data Validation 106-18-2B Level 4 Data Validation 106-18-4

PAH, Including Gel Permeation Chromatography with 5 to 10 ug/kg wet weight LOQ tissue EPA 8270 SIM 106-19

Level 2A Data Validation 106-19-2A Level 2B Data Validation 106-19-2B Level 4 Data Validation 106-19-4

VOC, Including 5035 Kit VOCs, DoD-QSM List EPA 524.2 / 524.3 /

107-1

Level 2A Data Validation 107-1-2A Level 2B Data Validation 107-1-2B Level 4 Data Validation 107-1-4

VOCs, Puget Sound Dredged Disposal Analysis or Safe Drinking Water Act List

EPA 524.2 / 524.3 /

8260 SIM

107-2

Level 2A Data Validation 107-2-2A Level 2B Data Validation 107-2-2B Level 4 Data Validation 107-2-4

VOCs, Priority Pollutant List EPA 624 107-3 Level 2A Data Validation 107-3-2A Level 2B Data Validation 107-3-2B Level 4 Data Validation 107-3-4

VOCs, Thermal Desorption, Blank Not Included air EPA TO-17 107-4

Level 2A Data Validation 107-4-2A Level 2B Data Validation 107-4-2B Level 4 Data Validation 107-4-4

Selected Ion Monitoring analyses EPA 8260 SIM 107-5 Level 2A Data Validation 107-5-2A Level 2B Data Validation 107-5-2B Level 4 Data Validation 107-5-4

1,2-Dibromo-3-chloropropane and/or Ethylene Dibromide

EPA 504 / 8011 107-6

Level 2A Data Validation 107-6-2A Level 2B Data Validation 107-6-2B Level 4 Data Validation 107-6-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 9 of 12

Benzene, Toluene, Ethylbenzene, and Xylenes and Methyl tert-Butyl Ether

EPA 8260 107-7

Level 2A Data Validation 107-7-2A Level 2B Data Validation 107-7-2B Level 4 Data Validation 107-7-4

Library Search For Tentatively Identified Compounds

EPA 8260 107-8

F-Listed Solvents EPA 8015 / 8260 / 2070 107-9

Level 2A Data Validation 107-9-2A Level 2B Data Validation 107-9-2B Level 4 Data Validation 107-9-4

Waste Characterization and TCLP, Including Extraction Corrosivity pH EPA 150.1 / 9045 108-1

Level 2A Data Validation 108-1-2A Level 2B Data Validation 108-1-2B Level 4 Data Validation 108-1-4

Ignitability EPA 1010 / 1030 108-2 Level 2A Data Validation 108-2-2A Level 2B Data Validation 108-2-2B Level 4 Data Validation 108-2-4

Paint Filter Liquid Test, Free Liquids EPA 9095 108-3 Level 2A Data Validation 108-3-2A Level 2B Data Validation 108-3-2B Level 4 Data Validation 108-3-4

Filtration - Liquid Samples, Solids <0.5%

EPA 1312 108-4

Level 2A Data Validation 108-4-2A Level 2B Data Validation 108-4-2B Level 4 Data Validation 108-4-4

Zero Headspace Extraction, VOCs Only EPA 1311 / 1312 108-5 Level 2A Data Validation 108-5-2A Level 2B Data Validation 108-5-2B Level 4 Data Validation 108-5-4

TCLP Herbicides EPA 1311 / 8151 108-6 Level 2A Data Validation 108-6-2A Level 2B Data Validation 108-6-2B Level 4 Data Validation 108-6-4

TCLP Pesticides EPA 1311 / 8081 108-7 Level 2A Data Validation 108-7-2A Level 2B Data Validation 108-7-2B Level 4 Data Validation 108-7-4

TCLP RCRA Metals EPA 1311 / 6010 108-8 Level 2A Data Validation 108-8-2A Level 2B Data Validation 108-8-2B Level 4 Data Validation 108-8-4

TCLP Mercury EPA 7740 / 7471 / 245 108-9 Level 2A Data Validation 108-9-2A Level 2B Data Validation 108-9-2B Level 4 Data Validation 108-9-4

TCLP Volatiles EPA 1311 / 8260 108-10 Level 2A Data Validation 108-10-2A Level 2B Data Validation 108-10-2B Level 4 Data Validation 108-10-4

TCLP Semivolatiles EPA 1311 / 8270 108-11 Level 2A Data Validation 108-11-2A Level 2B Data Validation 108-11-2B Level 4 Data Validation 108-11-4

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 10 of 12

Additional Sample Preparation and Cleanup Alumina, Florisil, or Silica Gel Cleanup EPA 3610 / 3611 / 3620

/ 3630 109-1

Sulfur Cleanup EPA 3660 109-2 Sulfuric Acid / Permanganate Cleanup EPA 3665 109-3 Drying Grinding and Sieving EPA 8330 109-4 Shucking, Filleting, Grinding, and Drying tissue PSEP 1995 109-5

Lipids Bligh & Dyer 1959 109-6 Total Solids PSEP 1995 109-7 Microscale Solvent Extraction EPA 3570 109-8 Collection Media and Equipment, Including All Preparation 6-L Summa Canister, Per Week Rental 110-1 1-L Summa Canister, Per Week Rental 110-2 6-L Certified Summa Canister, Per Week Rental 110-3 1-L Certified Summa Canister, Per Week Rental 110-4 1-L Tedlar Bag 110-5 3-L Tedlar Bag 110-6 5-L Tedlar Bag 110-7 10-L Tedlar Bag 110-8

Polyurethane Foam/XAD Cartridge: TO-13A, High Volume 110-9 Polyurethane Foam/XAD Cartridge: TO-13A, Low Volume 110-10

Polyurethane Foam Cartridge: TO-4A, Low or High Volume 110-11 Thermal Desobption Tube 110-12 Flow Controller 110-13 Sample Turnaround Time, Standard = 21 Calendar Days Note: Sample turnaround time cost percentages are applied to the applicable unit linte-item costs listed above.

24 Hours 111-1 48 Hours 111-2 72 Hours 111-3

Level 2A Data Validation 111-3-2A Level 2B Data Validation 111-3-2B Level 4 Data Validation 111-3-4

7 Calendar Days 111-4 Level 2A Data Validation 111-4-2A Level 2B Data Validation 111-4-2B Level 4 Data Validation 111-4-4

14 Calendar Days 111-5 Level 2A Data Validation 111-5-2A Level 2B Data Validation 111-5-2B Level 4 Data Validation 111-5-4

21 Calendar Days for Isotope Dilution Methods (Standard = 42 Calendar Days) 111-6 Additional Data Validation Tasks

Hourly Rate Standards Traceability - Level IV/Stage 3 or 4, for each applicable method 112-1 Standards Traceability - Level IV/Stage 3 or 4, for EPA 1633 112-2 Environmental Resources Program Info Management System Project Setup 112-3

112-4

Environmental Resources Program Info Management System Upload 112-5 Populate Each Additional Electronic Data Deliverables 112-6 Naval Installation Restoration Information Solution Upload 112-7 Setup an Electronic Quality Assurance Project Plan 112-8 Data Quality Assessment Report or Quality Control Summary Report 112-9 Alaska Department of Environmental Conservation Checklist 112-10 Laboratory Data Package printing for validation 112-11

Note: Data Validation cost percentages are applied to the project's total cost of data validation.

If the calculated percentage cost is less than the minimum line-item dollar value then the minimum amount is used.

Environmental Resources Program Info Management System Borehole or Well Establishment

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 11 of 12

Abbreviations AMPH Analytical Methods for Petroleum Hydrocarbons CVAA Cold Vapor Atomic Absorption EPA U.S. Environmental Protection Agency GRO Gasoline Range Organics ICP Inductively Coupled Plasma LOQ Limit of Quantitation MS Mass Spectrometry NIOSH National Institute for Occupational Safety and Health PAH Polyaromatic Hydrocarbons PCB Polychlorinated Biphenyl PSEP Puget Sound Estuary Protocols RCRA Resource Conservation and Recovery Act SM Standard Methods SVOC Semivolatile Organic Compounds TCLP Toxicity Characteristic Leaching Procedure TOC Total Organic Carbon USACE U.S. Army Corps of Engineers VOC Volatile Organic Compound

Method References

Plumb, R. J. Jr. (1981) EPA / USACE, "Procedures for Handling and Chemical Analysis of Sediment and Water Samples", Technical Report EPA/CE-81-1: https://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=91018G3V.TXT Massachusetts Department of Environmental Protection, “Method for the Determination of Volatile Petroleum Hydrocarbons”, MADEP-VPH-04-1.1: https://www.mass.gov/doc/massdep-vph-method Montana Department of Environmental Quality, “Montana Risk-Based Corrective Action Guidance for Petroleum Releases”, Appendix C - Montana Method, DEQ-WMRD-RBCA-1: https://deq.mt.gov/cleanupandrec/resources Bligh, E. G. and Dyer, W. J. (1959) Can. J, Biochem, Physiol, 37, 911-917

EPA Methods: https://www.epa.gov/measurements-modeling/collection-methods SM: https://www.standardmethods.org/ Washington Department of Ecology, PSEP, Publication No. 15-09-046:

Washington Department of Ecology, AMPH, Publication No. ECY 97-602:

ASTM International Standards: https://www.astm.org/ NIOSH Manual of Analytical Methods: https://www.cdc.gov/niosh/docs/2003-154/chaps.html

DRAFT Price Schedule for RFI No. W912DW25RFI191A page 12 of 12

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