DCSpec (Part 5).pdf

BOREHOLE

AND

WELL LOG

Site

Address

BORING/WELL:

Sagasser & Associates, Inc.

699 S. Wisconsin Ave

Gaylord, MI 49735

(989) 732-5800

(989) 732-5825 (fax) info@sagasser-associates.com www.sagasser-associates.com

County:

Township:

Town: : Range: Sec. #:

Location

Date:

Driller:

Logged by

Drill Method:

Total Depth:

Well Const.

Annulus seal

Lithology

Lithologic Description

Depth bgl

Sample Field Results PID and visual/olfactory Type ID asphalt coarse gravel, medium to fine SAND, dusky brown/ black

3 ppm saturated, medium to fine SAND, orange moderate yellowish brown wood medium to fine SAND, moderate yellowish

Soil TB-5-6.5’

1010, 10.5 g, 40 ppm brown peat, soupy, dusky brown

GW TB-5 6.6 ppm, 1017 medium to fine SAND, moderate yellowish brown w/ fine gravel

4 ppm

End of boring at 10 ft

Elev. Datum: North American Vertical Datum of 1988 (NAVD88) Lat: 44°17'53.80197''

Grd. Elev: 1144.32’ (348.787 m) T.O.C.: n/a Long: -84°39'07.99940''

SWL: ~ 2 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: 417195.149 (m)

Screen Type: 1-inch, 010-slot, PVC Easting: 607353.076 (m)

Annulus sealed by: Backfilled with bentonite. Sheet # 1 of 1

TB – 5

Surplus Inc. (846-2B)

777 W. Houghton Lake Drive, Prudenville

September 13, 2019

Alluvial Earth

Scot Egleston

Probe – Direct Push

10’

Roscommon County

Denton

15 22-N 3-W

See Site Map

CS

CS

B mailto:info@sagasser-associates.com http://www.sagasser-associates.com/

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID gravel & SAND, dark yellowish brown light brown 5yr 5/6, medium to fine SAND

7 ppm medium to fine SAND, moderate yellowish brown

Soil

PNA’s 3- 4’ saturated

Soil

TB-6-4’

TB-Dup

1530, 10.9 g

10.1 g wood, peat

SILT w/ some clay, dusky brown medium to fine SAND w/ some coarse gravel

45 ppm

GW TB-6 11.6 ppm w/ some fine gravel

Oil-Soil (+)

7.2 ppm

End of Boring

Elev. Datum: North American Vertical Datum of 1988 (NAVD88) Lat: 44°17'53.89866''

Grd. Elev: 1144.55’ (348.858 m) T.O.C.: n/a Long: -84°39'08.16367''

SWL: ~ 3 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: 417198.071 (m)

Screen Type: 1-inch, 010-slot, PVC Easting: 607349.387 (m)

TB – 6

Scot Egleston

Probe – Direct Push

See Site Map

CS

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID concrete

1.9 ppm orange moderate yellowish brown, saturated

Soil TB-7-3.5’

1042, 10.5 g, saturated peat, moderate brown 5yr 3/4

SILT, dusky yellowish brown

733 ppm medium to fine SAND w/ fine gravel

15 ppm

Oil-Soil (-) no gravel

GW TB-7 10.2ppm

CLAY

12 ppm fine SAND, pale yellowish brown

Elev. Datum: North American Vertical Datum of 1988 (NAVD88) Lat: 44°17'53.93794''

Grd. Elev: 1144.50’ (348.844 m) T.O.C.: n/a Long: -84°39'08.40213''

SWL: ~ 3 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: 417199.196 (m)

Screen Type: 1-inch, 010-slot, PVC Easting: 607344.085 (m)

TB – 7

Scot Egleston

Probe – Direct Push

See Site Map

CS

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID concrete medium to fine SAND, dark yellowish brown

1 ppm gravel, saturated medium to fine SAND, dark yellowish orange brown

Soil TB-8-4’

1053, 10.3 g, saturated, 1 ppm w/ silt wood peat

SILT, black

1 ppm

LOAM, dusky brown

GW TB-8 1055, 1.7 ppm medium to fine SAND w/ fine to coarse gravel medium light grey w/ fine gravel no gravel

1.6 ppm pale yellowish brown

Elev. Datum: North American Vertical Datum of 1988 (NAVD88) Lat: 44°17'53.93430''

Grd. Elev: 1144.72’ (348.910 m) T.O.C.: n/a Long: -84°39'08.92691''

SWL: ~ 2 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: 417198.892 (m)

Screen Type: 1-inch, 010-slot, PVC Easting: 607332.459 (m)

TB – 8

Scot Egleston

Probe – Direct Push

See Site Map

CS

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID topsoil / sandy banded medium to fine SAND

<1 ppm

4 Soil TB-9-4.5’

1126, 10.3 g, saturated saturated pale yellowish brown medium to fine SAND, pale yellowish brown w/ occasional medium gravel

GW TB-9 1127, 2ppm

Elev. Datum: North American Vertical Datum of 1988 (NAVD88) Lat: n/a

Grd. Elev: n/a T.O.C.: n/a Long: n/a

SWL: ~ 4 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: n/a

Screen Type: 1-inch, 010-slot, PVC Easting: n/a

TB – 9

Scot Egleston

Probe – Direct Push

See Site Map

CS

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID topsoil light yellowish orange

Soil TB-10-4’

1138, 10.9 g, saturated, <1 ppm pale yellowish brown, saturated

GW TB-10 1.2 ppm, 1139

1.3 ppm w/ fine gravel, more fine SAND

1.3 ppm no gravel, more fine SAND

SWL: ~ 4 ft Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: n/a

TB – 10

Scot Egleston

Probe – Direct Push

See Site Map

CS

Logged by

Annulus bgl

Sample Field Results PID and visual/olfactory Type ID concrete medium to fine SAND, light brown 5yr 5/6

1.8 ppm saturated

Oil-Soil (-)

GW TB-11 3 ppm dark yellowish brown

Soil

TB-11-

4.5’ (sat)

1130, 10.8 g, 67 ppm

End of boring at 5 ft

SWL: ~2’ Well Depth: n/a Datum: Michigan GeoRef

Casing Type: 1-inch PVC Northing: n/a

TB – 11

Scot Egleston

Probe – Direct Push

5’

See Site Map

CS B

Patterns:

Sand, grey

Sand, brown

Soil collapse

Soil Cuttings

Silt, grey

Silt, brown

Bentonite

Loam, grey

Clay, grey

Clay, brown cement

Loam, brown

Bedrock, limestone

Bedrock, sandstone

Asphalt, peat, shale

Silty Sand

C

SC

C

Sagasser & Associates, Inc. Triage Summary Report – Surplus Inc. (Denton Twp.)

Project #41305-00846-2B 777 W. Houghton Lake Drive, Prudenville, Roscommon County, MI

Attachment D - Laboratory Reports and COC Sheets

Work Order:

Report Date:

Client:

Attention:

Project Name:

Project Number:

1909164-01 1909164-02 1909164-03 1909164-04 1909164-05 1909164-06 1909164-07 1909164-08 1909164-09 1909164-10 1909164-11 1909164-12 1909164-13

TB-1-16'' TB-2-5'(SAT) TB-3-3'(SAT) TB-4-3'(SAT) TB-5-6.5'(SAT) TB-6-4'(SAT) TB-7-3.5'(SAT) TB-8-4'(SAT) TB-9-4.5'(SAT) TB-10-4'(SAT) TB-11-4.5(SAT) TB-Duplicate Field Blank

9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019

9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019

Analyte Units Method

1,1,1,2-Tetrachloroethane ug/kg dry 8260 100 1,500 ID 6,200 480,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,1,1-Trichloroethane ug/kg dry 8260 50 4,000 1,800 250,000 500,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,1,2,2-Tetrachloroethane ug/kg dry 8260 50 170 1,600 4,300 53,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,1,2-Trichloroethane ug/kg dry 8260 50 100 6,600 4,600 180,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,1-Dichloroethane ug/kg dry 8260 50 18,000 15,000 230,000 27,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,1-Dichloroethylene ug/kg dry 8260 50 140 2,600 62 200,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2,3-Trichlorobenzene ug/kg dry 8260 NA NA NA NA NA <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

1,2,3-Trichloropropane ug/kg dry 8260 100 840 NA 4,000 1,300,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2,3-Trimethylbenzene ug/kg dry 8260 NA NA NA NA NA <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2,4-Trichlorobenzene ug/kg dry 8260 250 4,200 5,900 9,600,000 990,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

1,2,4-Trimethylbenzene ug/kg dry 8260 100 2,100 570 4,300,000 32,000,000 <63 <94 <110 <77 180 <610 <67 <71 <68 <76 <100 <620 <50

1,2-Dibromoethane ug/kg dry 8260 20 20 110 670 92 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2-Dichlorobenzene ug/kg dry 8260 100 14,000 280 11,000,000 19,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2-Dichloroethane ug/kg dry 8260 50 100 7,200 2,100 91,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,2-Dichloropropane ug/kg dry 8260 50 100 4,600 4,000 140,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,3,5-Trimethylbenzene ug/kg dry 8260 100 1,800 1,100 2,600,000 32,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,3-Dichlorobenzene ug/kg dry 8260 100 170 680 26,000 200,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

1,4-Dichlorobenzene ug/kg dry 8260 100 1,700 360 19,000 400,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

2,2,4-Trimethylpentane ug/kg dry 8260 2,500 ID NA 110,000 ID <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

2-Butanone (MEK) ug/kg dry 8260 750 260,000 44,000 54,000,000 120,000,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

2-Methylnaphthalene ug/kg dry 8260 330 57,000 4,200 2,700,000 8,100,000 <310 <470 <550 <380 650 <3000 <330 <360 <340 <380 <510 <3100 <250

2-Propanone (acetone) ug/kg dry 8260 1,000 15,000 34,000 290,000,000 23,000,000 <1300 <1900 <2200 <1500 <2000 <12000 <1300 <1400 <1400 <1500 <2000 <12000 <1000

4-Methyl-2-pentanone (MIBK) ug/kg dry 8260 2,500 36,000 ID 37,000,000 56,000,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Acrylonitrile ug/kg dry 8260 100 100 100 6,600 16,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Benzene ug/kg dry 8260 50 100 4,000 1,600 180,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Bromochloromethane ug/kg dry 8260 NA NA NA NA NA <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Bromodichloromethane ug/kg dry 8260 100 1,600 ID 1,200 110,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Bromoform ug/kg dry 8260 100 1,600 ID 150,000 820,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Bromomethane ug/kg dry 8260 200 200 700 860 320,000 <250 <370 <440 <310 <400 <2400 <270 <280 <270 <300 <410 <2500 <200

Carbon disulfide ug/kg dry 8260 250 16,000 ID 76,000 7,200,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Carbon tetrachloride ug/kg dry 8260 50 100 900 190 96,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Chlorobenzene ug/kg dry 8260 50 2,000 500 120,000 4,300,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Chloroethane ug/kg dry 8260 250 8,600 22,000 2,900,000 2,600,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Chloroform ug/kg dry 8260 50 1,600 7,000 7,200 1,200,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Chloromethane ug/kg dry 8260 250 5,200 ID 2,300 1,600,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250 cis-1,2-Dichloroethylene ug/kg dry 8260 50 1,400 12,000 22,000 2,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 cis-1,3-Dichloropropylene ug/kg dry 8260 NA NA NA NA NA <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Cyclohexane ug/kg dry 8260 NA NA NA NA NA <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Dibromochloromethane ug/kg dry 8260 100 1,600 ID 3,900 110,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Dibromomethane ug/kg dry 8260 250 1,600 NA ID 2,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Dichlorodifluoromethane ug/kg dry 8260 250 95,000 ID 900,000 52,000,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Diethyl ether ug/kg dry 8260 200 200 ID 28,000,000 110,000,000 <250 <370 <440 <310 <400 <2400 <270 <280 <270 <300 <410 <2500 <200

Diisopropyl Ether ug/kg dry 8260 250 600 ID 670,000 920,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Ethylbenzene ug/kg dry 8260 50 1,500 360 87,000 22,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Ethyltertiarybutylether ug/kg dry 8260 250 980 ID 540,000 ID <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Hexachloroethane ug/kg dry 8260 300 430 1,800 40,000 230,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Hexane ug/kg dry 8260 NA 180,000 NA 510,000 92,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Isopropylbenzene ug/kg dry 8260 250 91,000 3,200 400,000 25,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 m & p - Xylene ug/kg dry 8260 NA NA NA NA NA <130 <190 <220 <150 <200 <1200 <130 <140 <140 <150 <200 <1200 <100

Methylene chloride ug/kg dry 8260 100 100 30,000 45,000 1,300,000 <130 <190 <220 <150 <200 <1200 <130 <140 <140 <150 <200 <1200 <100

Methyltertiarybutylether ug/kg dry 8260 250 800 140,000 9,900,000 1,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Naphthalene ug/kg dry 8260 330 35,000 730 250,000 16,000,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250 n-Butylbenzene ug/kg dry 8260 50 1,600 ID ID 2,500,000 <63 <94 <110 <77 250 <610 <67 <71 <68 <76 <100 <620 <50 n-Propylbenzene ug/kg dry 8260 100 1,600 ID ID 2,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 o-Xylene ug/kg dry 8260 NA NA NA NA NA <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 sec-Butylbenzene ug/kg dry 8260 50 1,600 ID ID 2,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Styrene ug/kg dry 8260 50 2,700 2,100 250,000 400,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 tert-Butylbenzene ug/kg dry 8260 50 1,600 ID ID 2,500,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 tertiary Butyl Alcohol ug/kg dry 8260 2,500 78,000 NA 310,000,000 120,000,000 <3100 <4700 <5500 <3800 <5000 <30000 <3300 <3600 <3400 <3800 <5100 <31000 <2500 tertiaryAmylmethylether ug/kg dry 8260 250 3,900 NA 58,000 29,000,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Tetrachloroethylene ug/kg dry 8260 50 100 1,200 11,000 200,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Tetrahydrofuran ug/kg dry 8260 1,000 1,900 220,000 1,300,000 2,900,000 <310 <470 <550 <380 <500 <3000 <330 <360 <340 <380 <510 <3100 <250

Toluene ug/kg dry 8260 100 16,000 5,400 330,000 50,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 trans-1,2-Dichloroethylene ug/kg dry 8260 50 2,000 30,000 23,000 3,800,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50 trans-1,3-Dichloropropylene ug/kg dry 8260 NA NA NA NA NA <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Trichloroethylene ug/kg dry 8260 50 100 4,000 1,000 110,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Trichlorofluoromethane ug/kg dry 8260 100 52,000 NA 2,800,000 79,000,000 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

Vinyl chloride ug/kg dry 8260 40 40 260 270 3,800 <63 <94 <110 <77 <100 <610 <67 <71 <68 <76 <100 <620 <50

% Total Solids % 2540 B NA NA NA NA NA 87.3 78.5 75.0 83.8 78.5 79.5 84.3 82.4 84.8 84.9 72.2 79.2 100

SWET19-GLD-SURPLUS INC.(DENTON TWP)

Michigan Department of Environmental Quality Analytical Testing Report

1909164

10/9/2019 13:13

MDEQ-RRD-CADILLAC

Nick Swiger

T400/7826

Sample Number

Sample ID

Sample Depth

Date Collected Target Detection

Limit (TDL)

Drinking Water

Protection

Criteria (DWPC)

Groundwater

Surface Water

Protection

Criteria (GSIPC)

Soil

Volatilization to

Indoor Air

Inhalation

Criteria (SVIIC)

Letters in criteria columns refer to Footnotes of the Criteria/RBSLs tables.

Direct Contact

Criteria (DCC)

Organics-Volatiles

Grey indicates contaminant was detected.

Yellow indicates contaminant exceeds DWPC.

Blue indicates contaminant exceeds GSIPC.

Green indicates contaminant exceeds both DWPC and GSIPC.

Date Received

Orange indicates contaminant exceeds one or more criteria; SVIIC and/or DCC.

“ID” means insufficient data to develop criterion.

“NA” means a criterion or value is not available or, in the case of background, not applicable.

“NLL” means hazardous substance is not likely to leach under most soil conditions.

“NLV” means hazardous substance is not likely to volatilize under most conditions.

Work Order:

Report Date:

Client:

Attention:

Project Name:

Project Number:

1909164-01 1909164-02 1909164-03 1909164-04 1909164-05 1909164-06 1909164-07 1909164-08 1909164-09 1909164-10 1909164-11

TB-1-16'' TB-2-5'(SAT) TB-3-3'(SAT) TB-4-3'(SAT) TB-5-6.5'(SAT) TB-6-4'(SAT) TB-7-3.5'(SAT) TB-8-4'(SAT) TB-9-4.5'(SAT) TB-10-4'(SAT) TB-11-4.5(SAT)

9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019 9/13/2019

9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019 9/17/2019

Analyte Units Method

2-Methylnaphthalene ug/kg dry 8270 330 57,000 4,200 2,700,000 8,100,000 <290 <320 <330 <300 <320 570 <300 <300 <290 <290 <350

Acenaphthene ug/kg dry 8270 330 300,000 8,700 190,000,000 41,000,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Acenaphthylene ug/kg dry 8270 330 5,900 ID 1,600,000 1,600,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Anthracene ug/kg dry 8270 330 41,000 ID 1,000,000,000 230,000,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Benz[a]anthracene ug/kg dry 8270 330 NLL NLL NLV 20,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Benzo[a]pyrene ug/kg dry 8270 330 NLL NLL NLV 2,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Benzo[b]fluoranthene ug/kg dry 8270 330 NLL NLL ID 20,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Benzo[g,h,i]perylene ug/kg dry 8270 330 NLL NLL NLV 2,500,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Benzo[k]fluoranthene ug/kg dry 8270 330 NLL NLL NLV 200,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Chrysene ug/kg dry 8270 330 NLL NLL ID 2,000,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Dibenz[a,h]anthracene ug/kg dry 8270 330 NLL NLL NLV 2,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Fluoranthene ug/kg dry 8270 330 730,000 5,500 1,000,000,000 46,000,000 <110 180 <130 <120 <130 <130 130 <120 <120 <120 <140

Fluorene ug/kg dry 8270 330 390,000 5,300 580,000,000 27,000,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Indeno(1,2,3-c,d)pyrene ug/kg dry 8270 330 NLL NLL NLV 20,000 <230 <250 <270 <240 <250 <250 <240 <240 <240 <240 <280

Naphthalene ug/kg dry 8270 330 35,000 730 250,000 16,000,000 <110 <130 <130 <120 <130 280 <120 <120 <120 <120 <140

Phenanthrene ug/kg dry 8270 330 56,000 2,100 2,800,000 1,600,000 <110 <130 <130 <120 <130 <130 <120 <120 <120 <120 <140

Pyrene ug/kg dry 8270 330 480,000 ID 1,000,000,000 29,000,000 <110 160 <130 <120 <130 <130 <120 <120 <120 <120 <140

SWET19-GLD-SURPLUS INC.(DENTON TWP)

Michigan Department of Environmental Quality Analytical Testing Report

1909164

10/9/2019 13:13

MDEQ-RRD-CADILLAC

Nick Swiger

T400/7826

Sample Number

Sample ID

Sample Depth

Date Collected Target

Detection Limit

(TDL)

Drinking Water

Protection

Criteria (DWPC)

Groundwater

Surface Water

Protection

Criteria (GSIPC)

Soil

Volatilization to

Indoor Air

Inhalation

Criteria (SVIIC)

Letters in criteria columns refer to Footnotes of the Criteria/RBSLs tables.

Direct Contact

Criteria (DCC)

Organics-Semivolatiles

Grey indicates contaminant was detected.

Yellow indicates contaminant exceeds DWPC.

Blue indicates contaminant exceeds GSIPC.

Green indicates contaminant exceeds both DWPC and GSIPC.

Date Received

Orange indicates contaminant exceeds one or more criteria; SVIIC and/or DCC.

“ID” means insufficient data to develop criterion.

“NA” means a criterion or value is not available or, in the case of background, not applicable.

“NLL” means hazardous substance is not likely to leach under most soil conditions.

“NLV” means hazardous substance is not likely to volatilize under most conditions.

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-CADILLAC

RE: SWET19-GLD-SURPLUS INC.(DENTON TWP)

Cadillac, MI 49601-2158

120 W. Chapin Street

Nick Swiger

This is the official environmental laboratory report for testing conducted by the Michigan Department of

Environment, Great Lakes, and Energy. Analyses performed by the laboratory were conducted using methods published by the U.S. Environmental Protection Agency, Standard Methods for the Examination of

Water and Wastewater, ASTM, or other published or approved reference methods.

09 October 2019 Work Order: 1909164

Price: $3,731.50

Kirby Shane

Laboratory Director

Lab Work Order # 1909164

Page 1 of 42Page 1 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-CADILLAC

120 W. Chapin Street

Nick Swiger

SWET19-GLD-SURPLUS INC.(DENTON TWP)

Cadillac MI, 49601-2158

Site Code: T400/7826 10/09/2019

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1909164-01 Soil/Sediment 09/17/2019TB-1-16'' 09/13/2019

1909164-02 Soil/Sediment 09/17/2019TB-2-5'(SAT) 09/13/2019

1909164-03 Soil/Sediment 09/17/2019TB-3-3'(SAT) 09/13/2019

1909164-04 Soil/Sediment 09/17/2019TB-4-3'(SAT) 09/13/2019

1909164-05 Soil/Sediment 09/17/2019TB-5-6.5'(SAT) 09/13/2019

1909164-06 Soil/Sediment 09/17/2019TB-6-4'(SAT) 09/13/2019

1909164-07 Soil/Sediment 09/17/2019TB-7-3.5'(SAT) 09/13/2019

1909164-08 Soil/Sediment 09/17/2019TB-8-4'(SAT) 09/13/2019

1909164-09 Soil/Sediment 09/17/2019TB-9-4.5'(SAT) 09/13/2019

1909164-10 Soil/Sediment 09/17/2019TB-10-4'(SAT) 09/13/2019

1909164-11 Soil/Sediment 09/17/2019TB-11-4.5(SAT) 09/13/2019

1909164-12 Soil/Sediment 09/17/2019TB-Duplicate 09/13/2019

1909164-13 Soil/Sediment 09/17/2019Field Blank 09/13/2019

Notes and Definitions

Y20 Reporting Limits (RL) raised due to matrix.

Y17 Probable petroleum product(s) present.

Y11 Unidentified peaks present in sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

A09 Result is estimated due to high recovery of batch quality control.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detected at or above the reporting limit (RL).ND dry Sample results reported on a dry weight basis

Not ApplicableNA

Page 2 of 42Page 2 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-01

RLCAS #

Client ID: TB-1-16''

QC Batch

Organics-Volatiles

63 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 09/18/19ND B9I1811

63 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 09/18/19ND B9I1811

63 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 09/18/19ND B9I1811

63 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 09/18/19ND B9I1811

63 ug/kg dry 50 82601,1-Dichloroethane75-34-3 09/18/19ND B9I1811

63 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 09/18/19ND B9I1811

310 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 09/18/19ND B9I1811

310 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2-Dibromoethane106-93-4 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2-Dichloroethane107-06-2 09/18/19ND B9I1811

63 ug/kg dry 50 82601,2-Dichloropropane78-87-5 09/18/19ND B9I1811

63 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 09/18/19ND B9I1811

63 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 09/18/19ND B9I1811

63 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 09/18/19ND B9I1811

310 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 09/18/19ND B9I1811

310 ug/kg dry 50 82602-Butanone (MEK)78-93-3 09/18/19ND B9I1811

310 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 09/18/19ND B9I1811

1300 ug/kg dry 50 82602-Propanone (acetone)67-64-1 09/18/19ND B9I1811

310 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 09/18/19ND B9I1811

310 ug/kg dry 50 8260Acrylonitrile107-13-1 09/18/19ND B9I1811

63 ug/kg dry 50 8260Benzene71-43-2 09/18/19ND B9I1811

63 ug/kg dry 50 8260Bromochloromethane74-97-5 09/18/19ND B9I1811

63 ug/kg dry 50 8260Bromodichloromethane75-27-4 09/18/19ND B9I1811

63 ug/kg dry 50 8260Bromoform75-25-2 09/18/19ND B9I1811

250 ug/kg dry 50 8260Bromomethane74-83-9 09/18/19ND B9I1811

63 ug/kg dry 50 8260Carbon disulfide75-15-0 09/18/19ND B9I1811

63 ug/kg dry 50 8260Carbon tetrachloride56-23-5 09/18/19ND B9I1811

63 ug/kg dry 50 8260Chlorobenzene108-90-7 09/18/19ND B9I1811

310 ug/kg dry 50 8260Chloroethane75-00-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260Chloroform67-66-3 09/18/19ND B9I1811

310 ug/kg dry 50 8260Chloromethane74-87-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 09/18/19ND B9I1811

63 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 09/18/19ND B9I1811

310 ug/kg dry 50 8260Cyclohexane110-82-7 09/18/19ND B9I1811

63 ug/kg dry 50 8260Dibromochloromethane124-48-1 09/18/19ND B9I1811

63 ug/kg dry 50 8260Dibromomethane74-95-3 09/18/19ND B9I1811

Page 3 of 42Page 3 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-01

RLCAS #

Client ID: TB-1-16''

QC Batch

Organics-Volatiles

310 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 09/18/19ND B9I1811

250 ug/kg dry 50 8260Diethyl ether60-29-7 09/18/19ND B9I1811

310 ug/kg dry 50 8260Diisopropyl Ether108-20-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260Ethylbenzene100-41-4 09/18/19ND B9I1811

310 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 09/18/19ND B9I1811

310 ug/kg dry 50 8260Hexachloroethane67-72-1 09/18/19ND B9I1811

63 ug/kg dry 50 8260Hexane110-54-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260Isopropylbenzene98-82-8 09/18/19ND B9I1811

130 ug/kg dry 50 8260m & p - Xylene1330-20-7 09/18/19ND B9I1811

130 ug/kg dry 50 8260Methylene chloride75-09-2 09/18/19ND B9I1811

63 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 09/18/19ND B9I1811

310 Xug/kg dry 50 8260Naphthalene91-20-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260n-Butylbenzene104-51-8 09/18/19ND B9I1811

63 ug/kg dry 50 8260n-Propylbenzene103-65-1 09/18/19ND B9I1811

63 ug/kg dry 50 8260o-Xylene95-47-6 09/18/19ND B9I1811

63 ug/kg dry 50 8260sec-Butylbenzene135-98-8 09/18/19ND B9I1811

63 ug/kg dry 50 8260Styrene100-42-5 09/18/19ND B9I1811

63 ug/kg dry 50 8260tert-Butylbenzene98-06-6 09/18/19ND B9I1811

3100 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 09/18/19ND B9I1811

310 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 09/18/19ND B9I1811

63 ug/kg dry 50 8260Tetrachloroethylene127-18-4 09/18/19ND B9I1811

310 ug/kg dry 50 8260Tetrahydrofuran109-99-9 09/18/19ND B9I1811

63 ug/kg dry 50 8260Toluene108-88-3 09/18/19ND B9I1811

63 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 09/18/19ND B9I1811

63 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 09/18/19ND B9I1811

63 ug/kg dry 50 8260Trichloroethylene79-01-6 09/18/19ND B9I1811

63 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 09/18/19ND B9I1811

63 ug/kg dry 50 8260Vinyl chloride75-01-4 09/18/19ND B9I1811

40.3-194101 %Surrogate: Bromofluorobenzene 826009/18/19 B9I1811

52.1-21799.7 %Surrogate: Dibromofluoromethane 826009/18/19 B9I1811

55.4-196104 %Surrogate: Toluene-d8 826009/18/19 B9I1811

Page 4 of 42Page 4 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-01

RLCAS #

Client ID: TB-1-16''

QC Batch

Organics-Semivolatiles

290 ug/kg dry 1 82702-Methylnaphthalene91-57-6 10/04/19ND B9I1910

110 ug/kg dry 1 8270Acenaphthene83-32-9 10/04/19ND B9I1910

110 ug/kg dry 1 8270Acenaphthylene208-96-8 10/04/19ND B9I1910

110 ug/kg dry 1 8270Anthracene120-12-7 10/04/19ND B9I1910

110 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/04/19ND B9I1910

230 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/04/19ND B9I1910

230 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/04/19ND B9I1910

230 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/04/19ND B9I1910

230 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/04/19ND B9I1910

110 ug/kg dry 1 8270Chrysene218-01-9 10/04/19ND B9I1910

230 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/04/19ND B9I1910

110 ug/kg dry 1 8270Fluoranthene206-44-0 10/04/19ND B9I1910

110 ug/kg dry 1 8270Fluorene86-73-7 10/04/19ND B9I1910

230 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/04/19ND B9I1910

110 ug/kg dry 1 8270Naphthalene91-20-3 10/04/19ND B9I1910

110 ug/kg dry 1 8270Phenanthrene85-01-8 10/04/19ND B9I1910

110 ug/kg dry 1 8270Pyrene129-00-0 10/04/19ND B9I1910

32.9-11584.8 %Surrogate: 2-Fluorobiphenyl 827010/04/19 B9I1910

31.8-11574.4 %Surrogate: Nitrobenzene-d5 827010/04/19 B9I1910

38.5-11599.8 %Surrogate: p-Terphenyl-d14 827010/04/19 B9I1910

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 09/19/1987.3 B9I1821

Page 5 of 42Page 5 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-02

RLCAS #

Client ID: TB-2-5'(SAT)

QC Batch

Organics-Volatiles

94 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 09/18/19ND B9I1811

94 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 09/18/19ND B9I1811

94 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 09/18/19ND B9I1811

94 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 09/18/19ND B9I1811

94 ug/kg dry 50 82601,1-Dichloroethane75-34-3 09/18/19ND B9I1811

94 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 09/18/19ND B9I1811

470 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 09/18/19ND B9I1811

470 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2-Dibromoethane106-93-4 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2-Dichloroethane107-06-2 09/18/19ND B9I1811

94 ug/kg dry 50 82601,2-Dichloropropane78-87-5 09/18/19ND B9I1811

94 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 09/18/19ND B9I1811

94 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 09/18/19ND B9I1811

94 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 09/18/19ND B9I1811

470 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 09/18/19ND B9I1811

470 ug/kg dry 50 82602-Butanone (MEK)78-93-3 09/18/19ND B9I1811

470 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 09/18/19ND B9I1811

1900 ug/kg dry 50 82602-Propanone (acetone)67-64-1 09/18/19ND B9I1811

470 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 09/18/19ND B9I1811

470 ug/kg dry 50 8260Acrylonitrile107-13-1 09/18/19ND B9I1811

94 ug/kg dry 50 8260Benzene71-43-2 09/18/19ND B9I1811

94 ug/kg dry 50 8260Bromochloromethane74-97-5 09/18/19ND B9I1811

94 ug/kg dry 50 8260Bromodichloromethane75-27-4 09/18/19ND B9I1811

94 ug/kg dry 50 8260Bromoform75-25-2 09/18/19ND B9I1811

370 ug/kg dry 50 8260Bromomethane74-83-9 09/18/19ND B9I1811

94 ug/kg dry 50 8260Carbon disulfide75-15-0 09/18/19ND B9I1811

94 ug/kg dry 50 8260Carbon tetrachloride56-23-5 09/18/19ND B9I1811

94 ug/kg dry 50 8260Chlorobenzene108-90-7 09/18/19ND B9I1811

470 ug/kg dry 50 8260Chloroethane75-00-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260Chloroform67-66-3 09/18/19ND B9I1811

470 ug/kg dry 50 8260Chloromethane74-87-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 09/18/19ND B9I1811

94 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 09/18/19ND B9I1811

470 ug/kg dry 50 8260Cyclohexane110-82-7 09/18/19ND B9I1811

94 ug/kg dry 50 8260Dibromochloromethane124-48-1 09/18/19ND B9I1811

94 ug/kg dry 50 8260Dibromomethane74-95-3 09/18/19ND B9I1811

Page 6 of 42Page 6 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-02

RLCAS #

Client ID: TB-2-5'(SAT)

QC Batch

Organics-Volatiles

470 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 09/18/19ND B9I1811

370 ug/kg dry 50 8260Diethyl ether60-29-7 09/18/19ND B9I1811

470 ug/kg dry 50 8260Diisopropyl Ether108-20-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260Ethylbenzene100-41-4 09/18/19ND B9I1811

470 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 09/18/19ND B9I1811

470 ug/kg dry 50 8260Hexachloroethane67-72-1 09/18/19ND B9I1811

94 ug/kg dry 50 8260Hexane110-54-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260Isopropylbenzene98-82-8 09/18/19ND B9I1811

190 ug/kg dry 50 8260m & p - Xylene1330-20-7 09/18/19ND B9I1811

190 ug/kg dry 50 8260Methylene chloride75-09-2 09/18/19ND B9I1811

94 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 09/18/19ND B9I1811

470 Xug/kg dry 50 8260Naphthalene91-20-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260n-Butylbenzene104-51-8 09/18/19ND B9I1811

94 ug/kg dry 50 8260n-Propylbenzene103-65-1 09/18/19ND B9I1811

94 ug/kg dry 50 8260o-Xylene95-47-6 09/18/19ND B9I1811

94 ug/kg dry 50 8260sec-Butylbenzene135-98-8 09/18/19ND B9I1811

94 ug/kg dry 50 8260Styrene100-42-5 09/18/19ND B9I1811

94 ug/kg dry 50 8260tert-Butylbenzene98-06-6 09/18/19ND B9I1811

4700 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 09/18/19ND B9I1811

470 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 09/18/19ND B9I1811

94 ug/kg dry 50 8260Tetrachloroethylene127-18-4 09/18/19ND B9I1811

470 ug/kg dry 50 8260Tetrahydrofuran109-99-9 09/18/19ND B9I1811

94 ug/kg dry 50 8260Toluene108-88-3 09/18/19ND B9I1811

94 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 09/18/19ND B9I1811

94 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 09/18/19ND B9I1811

94 ug/kg dry 50 8260Trichloroethylene79-01-6 09/18/19ND B9I1811

94 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 09/18/19ND B9I1811

94 ug/kg dry 50 8260Vinyl chloride75-01-4 09/18/19ND B9I1811

40.3-194172 %Surrogate: Bromofluorobenzene 826009/18/19 B9I1811

52.1-217181 %Surrogate: Dibromofluoromethane 826009/18/19 B9I1811

55.4-196176 %Surrogate: Toluene-d8 826009/18/19 B9I1811

Page 7 of 42Page 7 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-02

RLCAS #

Client ID: TB-2-5'(SAT)

QC Batch

Organics-Semivolatiles

320 ug/kg dry 1 82702-Methylnaphthalene91-57-6 10/04/19ND B9I1910

130 ug/kg dry 1 8270Acenaphthene83-32-9 10/04/19ND B9I1910

130 ug/kg dry 1 8270Acenaphthylene208-96-8 10/04/19ND B9I1910

130 ug/kg dry 1 8270Anthracene120-12-7 10/04/19ND B9I1910

130 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/04/19ND B9I1910

250 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/04/19ND B9I1910

250 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/04/19ND B9I1910

250 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/04/19ND B9I1910

250 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/04/19ND B9I1910

130 ug/kg dry 1 8270Chrysene218-01-9 10/04/19ND B9I1910

250 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/04/19ND B9I1910

130 ug/kg dry 1 8270Fluoranthene206-44-0 10/04/19180 B9I1910

130 ug/kg dry 1 8270Fluorene86-73-7 10/04/19ND B9I1910

250 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/04/19ND B9I1910

130 ug/kg dry 1 8270Naphthalene91-20-3 10/04/19ND B9I1910

130 ug/kg dry 1 8270Phenanthrene85-01-8 10/04/19ND B9I1910

130 ug/kg dry 1 8270Pyrene129-00-0 10/04/19160 B9I1910

32.9-11587.7 %Surrogate: 2-Fluorobiphenyl 827010/04/19 B9I1910

31.8-11577.0 %Surrogate: Nitrobenzene-d5 827010/04/19 B9I1910

38.5-11599.8 %Surrogate: p-Terphenyl-d14 827010/04/19 B9I1910

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 09/19/1978.5 B9I1821

Page 8 of 42Page 8 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-03

RLCAS #

Client ID: TB-3-3'(SAT)

QC Batch

Organics-Volatiles

110 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 09/19/19ND B9I1812

110 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 09/19/19ND B9I1812

110 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 09/19/19ND B9I1812

110 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 09/19/19ND B9I1812

110 ug/kg dry 50 82601,1-Dichloroethane75-34-3 09/19/19ND B9I1812

110 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 09/19/19ND B9I1812

550 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 09/19/19ND B9I1812

550 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2-Dibromoethane106-93-4 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2-Dichloroethane107-06-2 09/19/19ND B9I1812

110 ug/kg dry 50 82601,2-Dichloropropane78-87-5 09/19/19ND B9I1812

110 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 09/19/19ND B9I1812

110 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 09/19/19ND B9I1812

110 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 09/19/19ND B9I1812

550 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 09/19/19ND B9I1812

550 ug/kg dry 50 82602-Butanone (MEK)78-93-3 09/19/19ND B9I1812

550 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 09/19/19ND B9I1812

2200 ug/kg dry 50 82602-Propanone (acetone)67-64-1 09/19/19ND B9I1812

550 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 09/19/19ND B9I1812

550 ug/kg dry 50 8260Acrylonitrile107-13-1 09/19/19ND B9I1812

110 ug/kg dry 50 8260Benzene71-43-2 09/19/19ND B9I1812

110 ug/kg dry 50 8260Bromochloromethane74-97-5 09/19/19ND B9I1812

110 ug/kg dry 50 8260Bromodichloromethane75-27-4 09/19/19ND B9I1812

110 ug/kg dry 50 8260Bromoform75-25-2 09/19/19ND B9I1812

440 ug/kg dry 50 8260Bromomethane74-83-9 09/19/19ND B9I1812

110 ug/kg dry 50 8260Carbon disulfide75-15-0 09/19/19ND B9I1812

110 ug/kg dry 50 8260Carbon tetrachloride56-23-5 09/19/19ND B9I1812

110 ug/kg dry 50 8260Chlorobenzene108-90-7 09/19/19ND B9I1812

550 ug/kg dry 50 8260Chloroethane75-00-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260Chloroform67-66-3 09/19/19ND B9I1812

550 ug/kg dry 50 8260Chloromethane74-87-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 09/19/19ND B9I1812

110 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 09/19/19ND B9I1812

550 ug/kg dry 50 8260Cyclohexane110-82-7 09/19/19ND B9I1812

110 ug/kg dry 50 8260Dibromochloromethane124-48-1 09/19/19ND B9I1812

110 ug/kg dry 50 8260Dibromomethane74-95-3 09/19/19ND B9I1812

Page 9 of 42Page 9 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-03

RLCAS #

Client ID: TB-3-3'(SAT)

QC Batch

Organics-Volatiles

550 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 09/19/19ND B9I1812

440 ug/kg dry 50 8260Diethyl ether60-29-7 09/19/19ND B9I1812

550 ug/kg dry 50 8260Diisopropyl Ether108-20-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260Ethylbenzene100-41-4 09/19/19ND B9I1812

550 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 09/19/19ND B9I1812

550 ug/kg dry 50 8260Hexachloroethane67-72-1 09/19/19ND B9I1812

110 ug/kg dry 50 8260Hexane110-54-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260Isopropylbenzene98-82-8 09/19/19ND B9I1812

220 ug/kg dry 50 8260m & p - Xylene1330-20-7 09/19/19ND B9I1812

220 ug/kg dry 50 8260Methylene chloride75-09-2 09/19/19ND B9I1812

110 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 09/19/19ND B9I1812

550 Xug/kg dry 50 8260Naphthalene91-20-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260n-Butylbenzene104-51-8 09/19/19ND B9I1812

110 ug/kg dry 50 8260n-Propylbenzene103-65-1 09/19/19ND B9I1812

110 ug/kg dry 50 8260o-Xylene95-47-6 09/19/19ND B9I1812

110 ug/kg dry 50 8260sec-Butylbenzene135-98-8 09/19/19ND B9I1812

110 ug/kg dry 50 8260Styrene100-42-5 09/19/19ND B9I1812

110 ug/kg dry 50 8260tert-Butylbenzene98-06-6 09/19/19ND B9I1812

5500 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 09/19/19ND B9I1812

550 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 09/19/19ND B9I1812

110 ug/kg dry 50 8260Tetrachloroethylene127-18-4 09/19/19ND B9I1812

550 ug/kg dry 50 8260Tetrahydrofuran109-99-9 09/19/19ND B9I1812

110 ug/kg dry 50 8260Toluene108-88-3 09/19/19ND B9I1812

110 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 09/19/19ND B9I1812

110 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 09/19/19ND B9I1812

110 ug/kg dry 50 8260Trichloroethylene79-01-6 09/19/19ND B9I1812

110 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 09/19/19ND B9I1812

110 ug/kg dry 50 8260Vinyl chloride75-01-4 09/19/19ND B9I1812

40.3-194184 %Surrogate: Bromofluorobenzene 826009/19/19 B9I1812

52.1-217185 %Surrogate: Dibromofluoromethane 826009/19/19 B9I1812

55.4-196181 %Surrogate: Toluene-d8 826009/19/19 B9I1812

Page 10 of 42Page 10 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-03

RLCAS #

Client ID: TB-3-3'(SAT)

QC Batch

Organics-Semivolatiles

330 ug/kg dry 1 82702-Methylnaphthalene91-57-6 10/04/19ND B9I1910

130 ug/kg dry 1 8270Acenaphthene83-32-9 10/04/19ND B9I1910

130 ug/kg dry 1 8270Acenaphthylene208-96-8 10/04/19ND B9I1910

130 ug/kg dry 1 8270Anthracene120-12-7 10/04/19ND B9I1910

130 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/04/19ND B9I1910

270 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/04/19ND B9I1910

270 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/04/19ND B9I1910

270 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/04/19ND B9I1910

270 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/04/19ND B9I1910

130 ug/kg dry 1 8270Chrysene218-01-9 10/04/19ND B9I1910

270 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/04/19ND B9I1910

130 ug/kg dry 1 8270Fluoranthene206-44-0 10/04/19ND B9I1910

130 ug/kg dry 1 8270Fluorene86-73-7 10/04/19ND B9I1910

270 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/04/19ND B9I1910

130 ug/kg dry 1 8270Naphthalene91-20-3 10/04/19ND B9I1910

130 ug/kg dry 1 8270Phenanthrene85-01-8 10/04/19ND B9I1910

130 ug/kg dry 1 8270Pyrene129-00-0 10/04/19ND B9I1910

32.9-11575.6 %Surrogate: 2-Fluorobiphenyl 827010/04/19 B9I1910

31.8-11568.1 %Surrogate: Nitrobenzene-d5 827010/04/19 B9I1910

38.5-11588.9 %Surrogate: p-Terphenyl-d14 827010/04/19 B9I1910

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 09/19/1975.0 B9I1821

Page 11 of 42Page 11 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-04

RLCAS #

Client ID: TB-4-3'(SAT)

QC Batch

Organics-Volatiles See note Y11

77 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 09/19/19ND B9I1812

77 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 09/19/19ND B9I1812

77 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 09/19/19ND B9I1812

77 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 09/19/19ND B9I1812

77 ug/kg dry 50 82601,1-Dichloroethane75-34-3 09/19/19ND B9I1812

77 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 09/19/19ND B9I1812

380 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 09/19/19ND B9I1812

380 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2-Dibromoethane106-93-4 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2-Dichloroethane107-06-2 09/19/19ND B9I1812

77 ug/kg dry 50 82601,2-Dichloropropane78-87-5 09/19/19ND B9I1812

77 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 09/19/19ND B9I1812

77 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 09/19/19ND B9I1812

77 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 09/19/19ND B9I1812

380 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 09/19/19ND B9I1812

380 ug/kg dry 50 82602-Butanone (MEK)78-93-3 09/19/19ND B9I1812

380 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 09/19/19ND B9I1812

1500 ug/kg dry 50 82602-Propanone (acetone)67-64-1 09/19/19ND B9I1812

380 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 09/19/19ND B9I1812

380 ug/kg dry 50 8260Acrylonitrile107-13-1 09/19/19ND B9I1812

77 ug/kg dry 50 8260Benzene71-43-2 09/19/19ND B9I1812

77 ug/kg dry 50 8260Bromochloromethane74-97-5 09/19/19ND B9I1812

77 ug/kg dry 50 8260Bromodichloromethane75-27-4 09/19/19ND B9I1812

77 ug/kg dry 50 8260Bromoform75-25-2 09/19/19ND B9I1812

310 ug/kg dry 50 8260Bromomethane74-83-9 09/19/19ND B9I1812

77 ug/kg dry 50 8260Carbon disulfide75-15-0 09/19/19ND B9I1812

77 ug/kg dry 50 8260Carbon tetrachloride56-23-5 09/19/19ND B9I1812

77 ug/kg dry 50 8260Chlorobenzene108-90-7 09/19/19ND B9I1812

380 ug/kg dry 50 8260Chloroethane75-00-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260Chloroform67-66-3 09/19/19ND B9I1812

380 ug/kg dry 50 8260Chloromethane74-87-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 09/19/19ND B9I1812

77 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 09/19/19ND B9I1812

380 ug/kg dry 50 8260Cyclohexane110-82-7 09/19/19ND B9I1812

77 ug/kg dry 50 8260Dibromochloromethane124-48-1 09/19/19ND B9I1812

77 ug/kg dry 50 8260Dibromomethane74-95-3 09/19/19ND B9I1812

Page 12 of 42Page 12 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-04

RLCAS #

Client ID: TB-4-3'(SAT)

QC Batch

Organics-Volatiles See note Y11

380 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 09/19/19ND B9I1812

310 ug/kg dry 50 8260Diethyl ether60-29-7 09/19/19ND B9I1812

380 ug/kg dry 50 8260Diisopropyl Ether108-20-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260Ethylbenzene100-41-4 09/19/19ND B9I1812

380 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 09/19/19ND B9I1812

380 ug/kg dry 50 8260Hexachloroethane67-72-1 09/19/19ND B9I1812

77 ug/kg dry 50 8260Hexane110-54-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260Isopropylbenzene98-82-8 09/19/19ND B9I1812

150 ug/kg dry 50 8260m & p - Xylene1330-20-7 09/19/19ND B9I1812

150 ug/kg dry 50 8260Methylene chloride75-09-2 09/19/19ND B9I1812

77 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 09/19/19ND B9I1812

380 Xug/kg dry 50 8260Naphthalene91-20-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260n-Butylbenzene104-51-8 09/19/19ND B9I1812

77 ug/kg dry 50 8260n-Propylbenzene103-65-1 09/19/19ND B9I1812

77 ug/kg dry 50 8260o-Xylene95-47-6 09/19/19ND B9I1812

77 ug/kg dry 50 8260sec-Butylbenzene135-98-8 09/19/19ND B9I1812

77 ug/kg dry 50 8260Styrene100-42-5 09/19/19ND B9I1812

77 ug/kg dry 50 8260tert-Butylbenzene98-06-6 09/19/19ND B9I1812

3800 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 09/19/19ND B9I1812

380 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 09/19/19ND B9I1812

77 ug/kg dry 50 8260Tetrachloroethylene127-18-4 09/19/19ND B9I1812

380 ug/kg dry 50 8260Tetrahydrofuran109-99-9 09/19/19ND B9I1812

77 ug/kg dry 50 8260Toluene108-88-3 09/19/19ND B9I1812

77 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 09/19/19ND B9I1812

77 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 09/19/19ND B9I1812

77 ug/kg dry 50 8260Trichloroethylene79-01-6 09/19/19ND B9I1812

77 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 09/19/19ND B9I1812

77 ug/kg dry 50 8260Vinyl chloride75-01-4 09/19/19ND B9I1812

40.3-194140 %Surrogate: Bromofluorobenzene 826009/19/19 B9I1812

52.1-217149 %Surrogate: Dibromofluoromethane 826009/19/19 B9I1812

55.4-196141 %Surrogate: Toluene-d8 826009/19/19 B9I1812

Page 13 of 42Page 13 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-04

RLCAS #

Client ID: TB-4-3'(SAT)

QC Batch

Organics-Semivolatiles

300 ug/kg dry 1 82702-Methylnaphthalene91-57-6 10/04/19ND B9I1910

120 ug/kg dry 1 8270Acenaphthene83-32-9 10/04/19ND B9I1910

120 ug/kg dry 1 8270Acenaphthylene208-96-8 10/04/19ND B9I1910

120 ug/kg dry 1 8270Anthracene120-12-7 10/04/19ND B9I1910

120 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/04/19ND B9I1910

240 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/04/19ND B9I1910

240 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/04/19ND B9I1910

240 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/04/19ND B9I1910

240 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/04/19ND B9I1910

120 ug/kg dry 1 8270Chrysene218-01-9 10/04/19ND B9I1910

240 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/04/19ND B9I1910

120 ug/kg dry 1 8270Fluoranthene206-44-0 10/04/19ND B9I1910

120 ug/kg dry 1 8270Fluorene86-73-7 10/04/19ND B9I1910

240 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/04/19ND B9I1910

120 ug/kg dry 1 8270Naphthalene91-20-3 10/04/19ND B9I1910

120 ug/kg dry 1 8270Phenanthrene85-01-8 10/04/19ND B9I1910

120 ug/kg dry 1 8270Pyrene129-00-0 10/04/19ND B9I1910

32.9-11588.3 %Surrogate: 2-Fluorobiphenyl 827010/04/19 B9I1910

31.8-11578.4 %Surrogate: Nitrobenzene-d5 827010/04/19 B9I1910

38.5-115101 %Surrogate: p-Terphenyl-d14 827010/04/19 B9I1910

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 09/19/1983.8 B9I1821

Page 14 of 42Page 14 of 43

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF

ENVIRONMENT, GREAT LAKES, AND ENERGY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1909164-05

RLCAS #

Client ID: TB-5-6.5'(SAT)

QC Batch

Organics-Volatiles See note Y11

100 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 09/19/19ND B9I1812

100 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 09/19/19ND B9I1812

100 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 09/19/19ND B9I1812

100 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 09/19/19ND B9I1812

100 ug/kg dry 50 82601,1-Dichloroethane75-34-3 09/19/19ND B9I1812

100 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 09/19/19ND B9I1812

500 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 09/19/19ND B9I1812

100 ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 09/19/19ND B9I1812

100 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 09/19/19ND B9I1812

500 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 09/19/19ND B9I1812

100 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 09/19/19180 B9I1812

100 ug/kg dry 50 82601,2-Dibromoethane106-93-4 09/19/19ND B9I1812

100 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 09/19/19ND B9I1812

100 ug/kg dry 50 82601,2-Dichloroethane107-06-2 09/19/19ND…