IRPOD_NSN_1H_6810_01-386-5562_X2.pdf

04/02/2015

ITEM NAMENATIONAL STOCK NUMBER

DRAWING PREPARER/MANUFACTURER

REVISION

MANUFACTURER'S PART NO./DRAWING NO. RSP

ACTIVITY

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1.0 SCOPE

THIS DOCUMENT PROVIDES THE REQUIREMENTS FOR THE PROCUREMENT OF ONE-QUART BOTTLES

OF AQUEOUS AMMONIUM HYDROXIDE CONTAINING ZINC OXIDE THAT IS ISOTOPICALLY DEPLETED

IN ZINC-64.

2.0 LIST OF APPLICABLE DOCUMENTS

IF A SUPPLIER QUOTES TO A LATER REVISION OF THE DRAWING (OR CATALOG ITEM) THAN

SPECIFIED BELOW, SUBMITTAL OF QUOTE SHALL INCLUDE TWO (2) COPIES OF THE REVISED

DOCUMENT AND AN EVALUATION OF THE INTERCHANGEABILITY. THE FOLLOWING DOCUMENTS AND

CHANGE DATA ARE APPLICABLE TO THE EXTENT SPECIFIED IN THIS IRPOD, THE DRAWINGS, OR

OTHER DOCUMENTS INVOKED BY THIS IRPOD. CONTRACTING AGENCY APPROVAL IS REQUIRED TO

USE EARLIER SPECIFICATION VERSIONS THAN THOSE LISTED HEREIN, EXCEPT AS IDENTIFIED

BELOW. IF NO DOCUMENT VERSION IS LISTED, THEN ANY VERSION OF THE DOCUMENT MAY BE

USED.

RAW MATERIAL REQUIRED HEREIN MAY HAVE BEEN PROCESSED OR TESTED (FOR EXAMPLE, HEAT

TREATED OR ULTRASONICALLY TESTED) AS REQUIRED BY THE RAW MATERIAL SPECIFICATION

PRIOR TO RECEIPT OF THIS ORDER USING PREVIOUS VERSIONS OF PROCESSING OR TESTING

SPECIFICATIONS. THIS PROCESSING AND TESTING NEED NOT BE REPEATED IF:

1.IT COMPLIED WITH THE APPLICABLE REQUIREMENTS OF THE

PROCESSING/TESTING SPECIFICATION VERSIONS IN EFFECT AT THE TIME OF

THE ACTUAL PROCESSING OR TESTING AND

2.ALL REQUIREMENTS OF THE RAW MATERIAL SPECIFICATION VERSION LISTED

HEREIN HAVE BEEN SATISFIED.

SECTION 6.0 IDENTIFIES SPECIAL REQUIREMENTS FOR SUBMITTAL OF THE PROCEDURES USED

FOR COMPLETED PROCESSING AND TESTING. ALL PROCESSING AND TESTING PERFORMED AFTER

RECEIPT OF THIS ORDER SHALL CONFORM TO THE PROCESSING/TESTING SPECIFICATION

VERSIONS LISTED HEREIN.

DOCUMENT NUMBER VERSION TITLE

FEDERAL SPECIFICATIONS

PPP-C-2020 A, NOTICE 1 CHEMICALS, LIQUID, DRY, AND PASTE, PACKAGING

OF

PPP-C-186 C, NOTICE 1 CONTAINERS, PACKAGING AND PACKING FOR DRUGS,

CHEMICALS, AND PHARMACEUTICALS

FEDERAL STANDARDS

FED-STD-313 D, NOTICE 1 MATERIAL SAFETY DATA, TRANSPORTATION SAFETY

DATA AND DISPOSAL DATA FOR HAZARDOUS

MATERIAL FURNISHED TO GOVERNMENT ACTIVITIES

MILITARY STANDARDS

DRAWING PREPARER/MANUFACTURER

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MIL-STD-129 P MARKING FOR SHIPMENT AND STORAGE (PART 1 OF

4 PARTS)

OTHERS

TITLE 29 OCCUPATIONAL SAFETY AND HEALTH

ADMINISTRATION REQUIREMENTS

CODE OF FEDERAL REGULATIONS

CHAPTER XVII

TITLE 49 DEPARTMENT OF TRANSPORTATION CODE OF FEDERAL

REGULATIONS HAZARDOUS MATERIAL REGULATIONS

PARTS 100 - 199

AMERICAN CHEMICAL 8TH EDITION REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

SOCIETY (ACS) REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

PUBLICATION REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

ASTM D 1293 STANDARD TEST METHODS FOR PH OF WATER

UNIFORM FREIGHT NATIONAL RAILROAD FREIGHT COMMITTEE

CLASSIFICATION RULES NATIONAL RAILROAD FREIGHT COMMITTEE

NATIONAL CLASSIFICA- NATIONAL MOTOR FREIGHT CLASSIFICATION

TION BOARD RULES NATIONAL MOTOR FREIGHT CLASSIFICATION

ASTM E 438-92 STANDARD SPECIFICATION FOR GLASSES IN

LABORATORY APPARATUS

ASTM D 1125 ELECTRICAL CONDUCTIVITY AND RESISTIVITY OF

WATER

3.0 TECHNICAL REQUIREMENTS

3.1 MATERIAL REQUIREMENTS

SPL ZNCOXD/AMHYDROX 8714A12

THE MATERIAL SHALL BE PREPARED FROM 28 TO 30 WEIGHT PERCENT AQUEOUS AMMONIA

CONFORMING TO THE REQUIREMENTS OF THE AMERICAN CHEMICAL SOCIETY (ACS)

SPECIFICATIONS FOR REAGENT CHEMICALS AND PURCHASER-SUPPLIED DEPLETED ZINC OXIDE

(DZO) POWDER. ZINC OXIDE AND THE UNDILUTED AQUEOUS AMMONIA SHALL BE THOROUGHLY

MIXED TO YIELD A HOMOGENEOUS SOLUTION HAVING A ZINC CONCENTRATION OF 4000 TO 5000

PARTS-PER-MILLION (PPM) BY WEIGHT. THE DENSITY OF 28% AQUEOUS AMMONIA IS 0.9 G/ML

AT 20 DEGREES CELIUS.

SHELF LIFE OF THIS ITEM IS SIXTY MONTHS.

THIS ITEM SHALL BE SUPPLIED WITH AT LEAST 85 PERCENT OF ITS

SHELF LIFE REMAINING AT TIME OF SHIPMENT.

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3.2 MANUFACTURING AND PROCESS REQUIREMENTS

SPL ZNCOXD/AMHYDROX 8714A12

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A. MERCURY CONTAMINATION

THIS PRODUCT SHALL NOT CONTAIN AND SHALL NOT BE CONTAMINATED BY

MERCURY OR MERCURY COMPOUNDS. DURING THE MANUFACTURING

PROCESS, TESTS, AND INSPECTIONS, THE PRODUCT SHALL NOT HAVE

COME IN DIRECT CONTACT WITH MERCURY, NOR ANY OF ITS COMPOUNDS,

NOR ANY MERCURY CONTAINING DEVICE EMPLOYING A SINGLE BOUNDARY

OF CONTAINMENT. THE SPECIFIC LIMIT IS THAT THIS ITEM SHALL CONTAIN

LESS THAN OR EQUAL TO 50 PPB MERCURY WHEN TESTED AS SPECIFIED IN

SECTION 4.6 OF THIS IRPOD.

B. FOREIGN MATERIAL EXCLUSION

THE ZINC OXIDE MATERIAL SHALL BE INSPECTED AND CERTIFIED BY

THE GOVERNMENT TO BE FREE OF FOREIGN MATERIAL PER THE BELOW

LISTED REQUIREMENTS PRIOR TO SHIPMENT TO THE VENDOR.

THE SPECIAL ZINC OXIDE/AMMONIUM HYDROXIDE SHALL BE UNIFORM AND

FREE FROM VISIBLE FOREIGN MATERIAL. EXAMPLES OF VISIBLE

FOREIGN MATERIAL INCLUDE BUT ARE NOT LIMITED TO RUST, GLASS

OR DIRT PARTICLES, PLASTIC, CERAMIC, WOOD OR METAL CHIPS;

CARDBOARD FIBERS, CLOTH FIBERS, BRUSH BRISTLES AND PAINT

CHIPS. PRODUCTION OPERATIONS SHALL BE CONDUCTED SO AS TO

ASSURE THE REQUIRED LEVEL OF CLEANLINESS.

SUCH OPERATIONS MAY INCLUDE, BUT ARE NOT LIMITED TO THE

FOLLOWING PRECAUTIONS: ENSURING THAT THE BOTTLES ARE FREE

FROM FOREIGN MATERIAL PRIOR TO FILL, PROVIDING AN AREA FOR

FILL OPERATIONS THAT IS FREE OF DIRT AND DEBRIS, AND

MAINTAINING THE FILL EQUIPMENT IN A CLEAN CONDITION.

C. CONTAINER REQUIREMENTS

THE BOTTLE AND CLOSURE SHALL BE GOVERNMENT FURNISHED MATERIAL (GFM)

CONFORMING TO THE GENERAL SPECIFICATIONS OF PPP-C-2020 AND TO

THE FOLLOWING SPECIFIC REQUIREMENTS OF PPP-C-186:

CLASSIFICATION DESCRIPTION

GROUP A BOTTLE (NSN 1H 8125-01-493-7259X3)

TYPE-OTHER (SEE BELOW)

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CLASS 1 GLASS

STYLE 1 NARROW MOUTH

GRADE 2 NON-LIGHT RESISTANT

CLOSURE A PLASTIC SCREW CAP WITH CONE SHAPED

POLYETHYLENE LINER

(NSN 1H 8125 01-612-8910X3)

SEAL A PRESSURE SENSITIVE VINYL TAPE

BOTTLE TYPE: THE BOTTLE SHALL BE MADE FROM BOROSILICATE GLASS

CONFORMING TO ASTM E 438, TYPE 1, CLASS "A", WITH AN EXTERNAL

PLASTIC COATING TO PROVIDE PROTECTION FROM BREAKAGE. THE

BOTTLE IS SUPPLIED UNDER NSN 1H 8125-01-493-7259X3. THE

BOTTLE SHALL HAVE AN OUTSIDE DIAMETER NOT TO EXCEED

4-3/8 INCHES, A HEIGHT NOT TO EXCEED 8-1/4 INCHES, AND AN

INSIDE DIAMETER (TOP OF NECK) OF 0.71 INCH NOMINAL.

BOTTLES SHALL NOT BE FILLED WITH CHEMICAL UNLESS LABELS (SEE

SECTION 5.3.C) ARE AVAILABLE FOR IMMEDIATE APPLICATION.

CONTAINERS SHALL BE LABELED IMMEDIATELY FOLLOWING FILL.

LABELED CONTAINERS SHALL THEN BE PROMPTLY PACKED IN

INTERMEDIATE AND EXTERIOR SHIPPING CONTAINERS. FILLING,

LABELING, AND PACKAGING OPERATIONS SHALL NOT BE PERFORMED

UNLESS THE DEFENSE CONTRACT MANAGEMENT AGENCY (DCMA) QUALITY

ASSURANCE REPRESENTATIVE (QAR) HAVING COGNIZANCE IS PRESENT

TO WITNESS THESE OPERATIONS.

D. UNIT OF ISSUE

ONE (1) ONE-QUART PLASTIC COATED BOTTLE. EACH BOTTLE SHALL

BE FILLED WITH AN AMOUNT WHICH CAN BE SAFELY CONTAINED, BUT

NO LESS THAN 910 MILLILITERS (ML).

E. SHELF LIFE

THE DESIGNATED SHELF LIFE IS SIXTY (60) MONTHS. THIS ITEM

SHALL BE SUPPLIED WITH AT LEAST EIGHTY-FIVE (85) PERCENT

(FIFTY-ONE (51) MONTHS) SHELF LIFE REMAINING AT THE TIME OF

DRAWING PREPARER/MANUFACTURER

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SHIPMENT.

F. LOT

ALL SPECIAL ZINC OXIDE/AMMONIUM HYDROXIDE PRODUCED AT ONE (1) TIME,

BY ONE (1) MANUFACTURER, AT ONE (1)PLANT, FROM THE SAME MATERIALS,

AND UNDER ESSENTIALLY THE SAME MANUFACTURING CONDITIONS PROVIDED

THE OPERATION IS CONTINUOUS. IN THE EVENT THE PROCESS IS A

BATCH OPERATION, EACH BATCH (SEE 3.2.G BELOW) SHALL CONSTITUTE

A LOT. EVEN IF A BATCH IS LARGER, EACH LOT PACKAGED FOR

DELIVERY SHALL BE LIMITED TO A MAXIMUM OF FIVE HUNDRED (500)

BOTTLES OF SPECIAL ZINC OXIDE/AMMONIUM HYDROXIDE.

G. BATCH

THAT QUANTITY OF MATERIAL WHICH HAS BEEN MANUFACTURED BY SOME

UNIT CHEMICAL PROCESS, OR SUBJECTED TO SOME PHYSICAL MIXING

OPERATION, INTENDED TO MAKE THE FINAL PRODUCT SUBSTANTIALLY

UNIFORM.

4.0 QUALITY ASSURANCE PROVISIONS

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4.1 INSPECTION SYSTEM

THE VENDOR SHALL MAINTAIN COMPLETE RECORDS FOR ALL INSPECTIONS

AND TESTS PERFORMED ON THE FINAL BOTTLES AND THEIR CONTENTS.

THE RECORDS SHALL BE TRACEABLE BY THE VENDOR'S LOT OR BATCH

NUMBER. THE VENDOR SHALL RETAIN THESE RECORDS FOR FIVE (5)

YEARS FOLLOWING DELIVERY TO THE GOVERNMENT. THE RECORDS

SHALL BE MADE AVAILABLE FOR GOVERNMENT REVIEW UPON WRITTEN

REQUEST DURING THIS PERIOD. THESE RECORDS SHALL INDICATE THE

NATURE AND NUMBER OF OBSERVATIONS MADE, THE NUMBER AND TYPE OF

DEFICIENCIES FOUND, THE QUANTITIES APPROVED AND REJECTED, AND

THE SPECIFIC ACTIONS TAKEN TO CORRECT THE DEFICIENCIES.

4.2 TEST EQUIPMENT

ALL GAGES, MEASURING AND TEST EQUIPMENT USED IN THE TESTS,

INSPECTION AND PROCESSING OF FILLED BOTTLES UNDER THIS IRPOD

SHALL BE CALIBRATED TO CERTIFIED STANDARDS THAT HAVE KNOWN,

VALID RELATIONSHIPS TO NATIONALLY ACCEPTED INDUSTRY STANDARDS.

THE CALIBRATION FREQUENCY FOR EACH DEVICE SHALL BE BASED ON

ITS STABILITY, PURPOSE AND USAGE. A POSITIVE MEANS (SUCH AS

STICKERS) SHALL BE PROVIDED TO IDENTIFY THE CALIBRATION

INTERVAL, LAST DATE OF CALIBRATION AND DATE CALIBRATION IS DUE

FOR EACH DEVICE. COMPLETE WRITTEN RECORDS OF CALIBRATION

DATA TRACEABLE TO THE INDIVIDUAL TEST DEVICES SHALL BE

AVAILABLE FOR GOVERNMENT REVIEW FOR UP TO FIVE YEARS FOLLOWING

DELIVERY OF FILLED BOTTLES TESTED WITH THE CALIBRATED

EQUIPMENT.

4.3 RESPONSIBILITIES

THE VENDOR IS RESPONSIBLE FOR THE PERFORMANCE OF ALL

INSPECTION AND TEST REQUIREMENTS IN SECTIONS 4.4 AND 4.6 OF

THIS SPECIFICATION. THE NUMBER OF SAMPLES TO BE TESTED

SHALL BE IN ACCORDANCE WITH TABLE 1 OF SECTION 4.4 OF THIS IRPOD.

THE VENDOR MAY USE HIS OWN OR ANY OTHER FACILITIES SUITABLE

FOR THE PERFORMANCE OF THE REQUIRED INSPECTIONS AND TESTS.

THE FINAL PRODUCT SHALL ALSO BE MADE AVAILABLE FOR GOVERNMENT

TESTING AND INSPECTION. IN ADDITION TO THE SPECIFIED TESTS

AND INSPECTIONS IN THIS SPECIFICATION, THE GOVERNMENT RESERVES

THE RIGHT TO PERFORM ANY ADDITIONAL INSPECTIONS AND TESTS

DEEMED NECESSARY TO ASSURE SUPPLIES AND SERVICES CONFORM TO

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PRESCRIBED REQUIREMENTS. THE VENDOR SHALL ALSO PROVIDE THE

FOLLOWING:

A. THE GOVERNMENT WILL PROVIDE THE VENDOR WITH A CERTIFICATE

OF ANALYSIS FOR THE ZINC OXIDE MATERIAL WHICH SHALL BE

INCLUDED WITH THE VENDOR'S CERTIFICATION PACKAGE.

ADDITIONALLY, THE MATERIAL SHALL BE CERTIFIED TO BE FREE

FROM FOREIGN MATERIAL AS SPECIFIED IN SECTION 3.2.B OF

THIS IRPOD. THE VENDOR SHALL DOCUMENT RECEIPT OF ALL ZINC

OXIDE MATERIAL SUPPLIED AS GFM AND SHALL RETURN TO THE GFM

SUPPLIER ANY ZINC OXIDE MATERIAL NOT USED IN PREPARING THE

SPECIAL ZINC OXIDE AMMONIMUM HYDROXIDE.

B. A WRITTEN CERTIFICATION IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE THAT EACH MANUFACTURER'S LOT OF SPECIAL

ZINC OXIDE/AMMONIUM HYDROXIDE MEETS ALL THE REQUIREMENTS

OF THE AMERICAN CHEMICAL SOCIETY SPECIFICATIONS FOR

AMMONIUM HYDROXIDE, EXCEPT THAT THE SPECIAL ZINC OXIDE/

AMMONIUM HYDROXIDE SOLUTION MAY CONTAIN UP TO 0.004% CARBON

DIOXIDE AND THE RESIDUE AFTER IGNITION TEST IS NOT

REQUIRED.

C. CERTIFIED TEST RESULTS IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE SHOWING THAT THE APPROPRIATE NUMBER OF

REPRESENTATIVE SAMPLES OF EACH LOT OF FINISHED PRODUCT WERE

SELECTED IN ACCORDANCE WITH SECTION 4.4 OF THIS IRPOD AND

WERE TESTED AND FOUND TO MEET THE REQUIREMENTS LISTED IN

SECTION 4.6 OF THIS IRPOD.

D. A WRITTEN CERTIFICATION IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE THAT THE ITEMS ANALYZED AND OFFERED FOR

DELIVERY ARE THE SAME, AND THE ITEMS OFFERED FOR DELIVERY

MEET ALL THE REQUIREMENTS OF THE IRPOD.

4.4 INSPECTION OF PREPARATION FOR DELIVERY

SAMPLING FOR INSPECTION OF PREPARATION FOR DELIVERY SHALL BE

FROM PACKAGED UNITS OFFERED FOR DELIVERY. SAMPLES SHALL BE

CHOSEN RANDOMLY AND IN ACCORDANCE WITH TABLE 1.

TABLE 1

SAMPLING FOR INSPECTION AND TESTING

LOT SIZE NUMBER OF BOTTLES

~LT~ OR = 25 2

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26 TO 150 3

151 TO 500 5

ANY REMAINING OPEN PACKAGES SHALL BE REPACKED BY THE VENDOR

INTO WHOLE UNITS OF ISSUE READY FOR SHIPMENT.

EACH SELECTED BOTTLE SHALL BE INSPECTED FOR CONFORMANCE WITH

THE REQUIREMENTS SPECIFIED IN SECTION 3.2.C, CONTAINER

REQUIREMENTS, SECTION 3.2.B, FOREIGN MATERIAL EXCLUSION, AND

SECTION 5.0, PREPARATION FOR DELIVERY, OF THIS IRPOD. FAILURE

OF ANY ONE (1) BOTTLE CONSTITUTES FAILURE OF THE ENTIRE LOT. A

REJECTED LOT MAY BE RESUBMITTED FOR INSPECTION PROVIDED THE

CONTRACTOR HAS CORRECTED ALL THE NON-CONFORMING ATTRIBUTES.

4.5 GOVERNMENT TESTING

FOLLOWING COMPLETION OF SECTION 4.4, THE COGNIZANT DEFENSE

CONTRACT MANAGEMENT AGENCY (DCMA) QUALITY ASSURANCE

REPRESENTATIVE (QAR) WILL SUBMIT THE RANDOMLY SELECTED BOTTLES

FOR GOVERNMENT LABORATORY INSPECTION AND TESTING. THE VENDOR

SHALL REPACKAGE THE BOTTLES AS A UNIT OF ISSUE FOR DELIVERY IN

ACCORDANCE WITH THIS IRPOD AND SHALL SHIP THEM WITH FORM

DD-1222, A MATERIAL SAFETY DATA SHEET (MSDS), AND A COPY OF

THE DATA REQUIRED IN SECTION 4.3 TO THE FOLLOWING ADDRESS:

PUGET SOUND NAVAL SHIPYARD & IMF

CODE 134.03X BUILDING 59

1400 FARRAGUT AVE

BREMERTON, WA 98314-5001

THE GOVERNMENT INSPECTION AND TESTING MUST DEMONSTRATE

CONFORMANCE WITH THE REQUIREMENTS OF THIS IRPOD BEFORE THE LOT

OF MATERIAL WILL BE ACCEPTED. PUGET SOUND NAVAL SHIPYARD

SHALL PROVIDE NOTIFICATION OF RESULTS TO THE PROCURING

CONTRACTING OFFICER WHO WILL NOTIFY THE CONTRACTOR AND THE

DCMA QAR.

4.6 ACCEPTANCE TESTING

THE VENDOR MAY USE ALTERNATE TEST METHODS TO ENSURE THAT THE

DELIVERED PRODUCT CONFORMS TO THE IRPOD REQUIREMENTS.

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HOWEVER, IN THE EVENT OF A DISAGREEMENT BETWEEN THE VENDOR

AND THE GOVERNMENT, THE TEST METHOD IDENTIFIED HERE SHALL BE

USED AS THE REFEREE METHOD. ACCEPTANCE TESTING SHALL CONSIST

OF THE FOLLOWING:

A. CHEMICAL PURITY TESTING

EACH SELECTED SAMPLE SHALL BE TESTED FOR CONFORMANCE WITH THE

ACS SPECIFICATION FOR REAGENT CHEMICALS (8TH EDITION) FOR

AMMONIUM HYDROXIDE LISTED IN THE FOLLOWING TABLE EXCEPT FOR

CARBON DIOXIDE, FOR WHICH THE REVISED PROCEDURE/ACCEPTANCE

CRITERION ARE SPECIFIED BELOW, AND RESIDUE AFTER IGNITION,

WHICH IS NOT PERFORMED. ACCEPTANCE REQUIREMENTS ARE SPECIFIED

IN THE TABLE BELOW.

ANALYSIS REQUIREMENT

APPEARANCE COLORLESS AND FREE FROM

SUSPENDED MATTER OR SEDIMENT

ASSAY (AS NH3) 28.0 - 30.0%

CARBON DIOXIDE (CO2) 0.004% MAXIMUM

CHLORIDE (CL) 0.5 PPM MAXIMUM

PHOSPHATE (PO4) 2 PPM MAXIMUM

TOTAL SULFUR (AS SO4) 2 PPM MAXIMUM

HEAVY METALS (AS PB) 0.5 PPM MAXIMUM

IRON (FE) 0.2 PPM MAXIMUM

SUBSTANCES REDUCING

PERMANGANATE PASSES TEST

FOR CARBON DIOXIDE, DILUTE 10 GRAMS (11 ML) OF SAMPLE WITH

10 ML OF WATER FREE FROM CARBON DIOXIDE, AND ADD 5 ML OF

CLEAR, SATURATED, BARIUM HYDROXIDE SOLUTION. ANY TURBIDITY

SHOULD NOT BE GREATER THAN WHAT IS PRODUCED WHEN THE SAME

AMOUNT OF BARIUM HYDROXIDE SOLUTION IS ADDED TO 21 ML OF

WATER (FREE FROM CARBON DIOXIDE) CONTAINING 0.6 MG OF

CARBONATE STANDARD (0.4 MG OR 0.004% CARBON DIOXIDE).

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B. ZINC CONTENT

ZINC CONCENTRATION IN THE RANGE 4000 TO 5000 PPM BY WEIGHT

SHALL BE CONFIRMED ON EACH SELECTED SAMPLE USING ATOMIC

ABSORPTION SPECTROMETRY OR INDUCTIVELY COUPLED PLASMA (ICP).

AN ALTERNATE ANALYTICAL TECHNIQUE MAY BE USED WITH PRIOR

APPROVAL OF THE PROCURING ACTIVITY. ZINC STANDARD SOLUTIONS

USED FOR CALIBRATING THE ANALYTICAL TECHNIQUE MUST BE

CERTIFIED TRACEABLE TO THE NATIONAL INSTITUTE OF STANDARDS

AND TECHNOLOGY (NIST). THE SOLUTION MATRICES FOR THE DILUTED

ZINC STANDARD AND THE DILUTED SAMPLE SHALL CONTAIN THE SAME

AMOUNT OF AMMONIUM HYDROXIDE AND OTHER CONSTITUENTS (E.G.

SOLVENT FOR THE STANDARDS). IF THE DETERMINED ZINC

CONCENTRATION IS LESS THAN 4000 PPM OR GREATER THAN 5000 PPM

BY WEIGHT, THE SAMPLE SHALL BE REJECTED.

C. ISOTOPIC ANALYSIS

THE RELATIVE ISOTOPIC ABUNDANCE OF ZINC-64 IN THE PRODUCT

SHALL BE CONFIRMED BY MASS SPECTROMETRY NOT TO EXCEED

1.0 ATOM PERCENT ZINC-64. IF THE ABUNDANCE OF ZINC-64

EXCEEDS 1.0 ATOM PERCENT, THE SAMPLE SHALL BE REJECTED.

D. CONDUCTIVITY

THREE (3) ALIQUOTS FROM EACH SELECTED SAMPLE SHALL BE DILUTED

WITH CARBON DIOXIDE-FREE WATER TO YIELD SOLUTIONS HAVING A PH

IN THE FOLLOWING RANGES:

9.75 - 9.85

10.05 - 10.15

10.35 - 10.45

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THE SAMPLE TEMPERATURE SHALL BE ADJUSTED TO 25 DEGREES

CELSIUS AND CONDUCTIVITY MEASURED. THE PH AND CONDUCTIVITY

MEASUREMENTS SHALL BE IN ACCORDANCE WITH ASTM D 1293 AND

ASTM D 1125, RESPECTIVELY. THE CONDUCTIVITY OF THE THREE (3)

SOLUTIONS SHALL FALL WITHIN THE ALLOWED RANGE FOR THE MEASURED

PH AS DERIVED FROM THE FOLLOWING TABLE. IF NOT, THEN THE

SAMPLE SHALL BE REJECTED.

SAMPLE PH CONDUCTIVITY RANGE

(MICRO-MHO/CM)

9.75 9.6 TO 24.1

9.76 9.8 TO 24.6

9.77 10.0 TO 25.2

9.78 10.3 TO 25.8

9.79 10.5 TO 26.4

9.80 10.7 TO 27.0

9.81 11.0 TO 27.6

9.82 11.2 TO 28.3

9.83 11.5 TO 28.9

9.84 11.8 TO 29.6

9.85 12.0 TO 30.3

10.05 19.1 TO 47.9

10.06 19.5 TO 49.0

10.07 20.0 TO 50.2

10.08 20.5 TO 51.3

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10.09 20.9 TO 52.5

10.10 21.4 TO 53.8

10.11 21.9 TO 55.0

10.12 22.4 TO 56.3

10.13 23.0 TO 57.6

10.14 23.5 TO 58.9

10.15 24.0 TO 60.3

10.35 38.1 TO 95.5

10.36 39.0 TO 97.7

10.37 39.9 TO 100.0

10.38 40.8 TO 102.3

10.39 41.8 TO 104.7

10.40 42.8 TO 107.1

10.41 43.8 TO 109.6

10.42 44.8 TO 112.2

10.43 45.8 TO 114.8

10.44 46.9 TO 117.4

10.45 48.0 TO 120.2

E. MERCURY CONTENT

THE MERCURY CONTENT OF THIS CHEMICAL SHALL BE DETERMINED BY

ATOMIC ABSORPTION SPECTROMETRY USING ENVIRONMENTAL PROTECTION

AGENCY METHOD 7470 FOR LIQUIDS OR METHOD 7471 FOR SOLIDS.

FAILURE OF ONE (1) OF THE SUBMITTED ACCEPTANCE SAMPLES TO MEET

THE MERCURY SPECIFICATION OF SECTION 3.2.A SHALL BE CAUSE FOR

REJECTION OF THE LOT.

5.0 PREPARATION FOR DELIVERY

DRAWING PREPARER/MANUFACTURER

REVISION

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ACTIVITY

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5.1 PACKAGING AND PACKING

PACKAGING AND PACKING SHALL CONFORM TO FEDERAL SPECIFICATION

PPP-C-2020 LEVEL B AND 49 CFR 100-199. THE PACKING OF THE

BOTTLES OF ZINC OXIDE/AMMONIMUM HYDROXIDE SHALL BE

SUFFICIENT TO PREVENT SHIFTING OF CONTENTS, BREAKAGE, DAMAGE,

OR SUBSTANTIAL DISTORTION DURING HANDLING, SHIPMENT, AND

INTERMEDIATE STORAGE. CONTAINERS SHALL CONFORM TO THE

UNIFORM FREIGHT CLASSIFICATION OR REGULATIONS OF OTHER

CARRIERS AS APPLICABLE TO THE MODE OF TRANSPORTATION.

A MATERIAL SAFETY DATA SHEET (MSDS) PREPARED PER FED-STD-313 SHALL

BE PROVIDED WITH EACH UNIT OF ISSUE AND AFFIXED/PACKAGED IN A

MANNER FOR EASY ACCESSIBILITY WITHOUT BEING LOST OR DAMAGED DURING

SHIPMENT AND STORAGE.

5.2 PRECAUTIONARY LABELS

NOT APPLICABLE

5.3 MARKING

A. MARKING FOR SHIPMENT AND STORAGE

INTERIOR PACKAGES AND EXTERIOR SHIPPING CONTAINERS SHALL BE

MARKED IN ACCORDANCE WITH MIL-STD-129, 49 CFR 100-199, AND

29 CFR 1910.1200.

BAR CODE MARKING SUITABLE FOR HAND SCANNING IS REQUIRED.

THE BAR CODE SHALL CONTAIN THE NSN, MFR/PN, AND THE

SUPPLIER'S CAGE CODE. THE BAR CODE SHALL BE APPLIED

DRAWING PREPARER/MANUFACTURER

REVISION

MANUFACTURER'S PART NO./DRAWING NO. RSP

ACTIVITY

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ON THE UNIT AND INTERMEDIATE PACK.

B. DISPOSAL OF EXCESS MATERIAL

THE VENDOR IS RESPONSIBLE FOR DISPOSAL OF ANY EXCESS SPECIAL

ZINC OXIDE/AMMONIUM HYDROXIDE SOLUTION MANUFACTURED PER THIS

SPECIFICATION. SUCH DISPOSAL SHALL BE IN ACCORDANCE WITH

DIRECTION FROM THE PROCURING CONTRACTING OFFICER (PCO).

C. SPECIAL MARKING

(1) IDENTIFICATION LABEL DATA - EACH UNIT, INTERMEDIATE AND

EXTERIOR SHIPPING CONTAINER (WITH THE EXCEPTION OF THE NET

CONTENTS ENTRY FOR THE EXTERIOR SHIPPING CONTAINER) SHALL

BE MARKED WITH THE FOLLOWING INFORMATION IN ACCORDANCE

WITH MIL-STD-129:

= NATIONAL STOCK NUMBER 1H 6810 01-386-5562X2 =

= NOMENCLATURE SPECIAL ZINC OXIDE/AMMONIUM =

= HYDROXIDE =

= NAME OF MANUFACTURER =

= CONTRACT NUMBER =

= LOT NUMBER =

= DATE OF MANUFACTURE (MONTH/YEAR =

= SHELF LIFE SIXTY (60) MONTHS =

= EXPIRATION DATE (MONTH/YEAR) =

= NET CONTENTS ONE (1) QUART =

THE EXPIRATION DATE IS COMPUTED BY ADDING THE SHELF LIFE

(SIXTY (60) MONTHS) TO THE DATE OF MANUFACTURE. THE DATE

OF MANUFACTURE SHALL BE WHEN THE REAGENTS ARE PLACED IN

THEIR END USE CONTAINERS. THIS DATE SHOULD CORRESPOND TO

THE TIME AT WHICH THE SPECIAL ZINC OXIDE/AMMONIUM HYDROXIDE

IS TESTED BY THE VENDOR FOR CERTIFICATION IT MEETS PURCHASE

SPECIFICATIONS AND THE PROCUREMENT CONTRACT.

DRAWING PREPARER/MANUFACTURER

REVISION

MANUFACTURER'S PART NO./DRAWING NO. RSP

ACTIVITY

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(2) BOTTLE LABELS: LETTER COLOR SHALL BE BLACK ON A

FLUORESCENT PINK PAPER LABEL. THE LABEL SHALL EXTEND

NO MORE THAN 3/4 OF THE CIRCUMFERENCE OF THE BOTTLE.

PRINTED LABELS SHALL BE STORED IN A LOCKED CONTAINER

OR AREA UNTIL NEEDED. EXCESS LABLES SHALL BE DESTROYED.

(3) SHIPPING CONTAINERS SHALL BE MARKED WITH TAPE IMPRINTED

WITH THE WORDS "X2 CHEMICALS". THE TAPE SHALL BE WHITE

AND APPROXIMATELY 1.25 INCHES WIDE. THE RED BLOCK PRINTING

SHALL BE APPROXIMATELY 0.75 INCH TALL. THE RED BORDER SHALL

BE APPROXIMATELY 0.2 INCH WIDE. THE TAPE SHALL NOT COVER

ANY OTHER IDENTIFICATION MARKINGS ON THE CONTAINER. WHERE

THE EXTERIOR CONTAINER IS A BOX OR CARTON, A STRIP OF TAPE

SHALL BE PLACED ON ALL FOUR (4) LATERAL FACES TO ENSURE THAT

THE COMPLETE WORDS "X2 CHEMICALS" ARE REPEATED AT LEAST

TWICE ON EACH FACE.

NOTE: TAPE MAY BE PURCHASED FROM:

NADCO INC.

ONE WASHINGTON ST

DOVER, NH 03820

(P/N X2CHEM)

PHONE (800) 839-9018

5.4 SHIPPING

SPECIAL REQUIREMENTS FOR SHIPMENT OF CHEMICALS

IN ACCORDANCE WITH 29 CFR 1910.1200, ONE (1) COPY OF THE MSDS SHALL

BE PROVIDED WITH THE BILL OF LADING FOR EACH SHIPMENT OF MATERIAL.

IN ADDITION TO THE EXISTING REQUIREMENTS OF MIL-STD-129, THIS PART SHALL CONTAIN

BAR CODES THAT IDENTIFY SHELF LIFE INFORMATION (CURE DATE, SHELF LIFE CODE) ON THE

UNIT PACKING ONLY.

6.0 CONTRACT DATA REQUIREMENTS

THE SELLER MUST PROVIDE THE CONTRACTING AGENCY WITH ALL OF THE

SUBMITTALS LISTED BELOW. SUBMITTALS WHICH ARE REQUIRED BY A

SPECIFICATION, BUT WHICH ARE NOT LISTED BELOW, NEED NOT BE

SUBMITTED. ONLY THOSE SUBMITTALS LISTED BELOW ARE REQUIRED.

DRAWING PREPARER/MANUFACTURER

REVISION

MANUFACTURER'S PART NO./DRAWING NO. RSP

ACTIVITY

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HOWEVER, IF THE SELLER CONSIDERS A REQUIRED SUBMITTAL INAPPLICABLE

TO THIS PROCUREMENT, THE SELLER MUST SUBMIT A STATEMENT JUSTIFYING

THE EXCLUSION OF THE REQUIRED SUBMITTAL.

REQUESTS FOR APPROVAL OF PROCEDURES USED PRIOR TO RECEIPT OF THIS

ORDER SHALL IDENTIFY THE PROCESSING/TESTING SPECIFICATION VERSION

APPLICABLE AND STATE THAT THE PROCESSING AND/OR TESTING WAS

PERFORMED PRIOR TO RECEIPT OF THE ORDER. IF THE PROCEDURE THAT WAS

USED IS NOT COMPLETE, TEST REPORTS, HEAT TREATMENT RECORDS, OR

OTHER DOCUMENTATION SHALL BE SUBMITTED WITH THE PROCEDURES TO

SUBSTANTIATE THAT ALL SPECIFICATION REQUIREMENTS WERE MET.

6.1 PROCEDURES AND REPORTS

THE SELLER SHALL PROVIDE THE FOLLOWING PROCEDURE(S) AND REPORT(S) TO THE PROCURING

ACTIVITY. SUPPLIER PROCEDURE SUBMITTALS REQUIRED BY MATERIAL AND PROCESS

SPECIFICATIONS NEED NOT BE RESUBMITTED FOR APPROVAL EACH TIME AN ORDER IS PLACED

FOR THE SAME IRPOD ITEM TO THE SAME VERSION (IE REVISION, AMENDMENT, CHANGE NOTICE

OR INTERIM CHANGE) OF THE SPECIFICATION OR STANDARD INVOKED. THE SELLER NEED ONLY

SUBMIT PROOF OF THE PRIOR APPROVAL FOR THAT ITEM AND SPECIFICATION REVISION.

ACCEPTABLE PROOF OF PRIOR APPROVAL WILL CONSIST OF A COORDINATED PROCEDURE REVIEW

SYSTEM (CPRS) APPROVAL LETTER. CPRS APPROVAL DOES NOT RELIEVE THE SELLER OF THE

RESPONSIBILITY TO COMPLY WITH ALL REQUIREMENTS IMPOSED ON ANY CURRENT AND FUTURE

PURCHASE ORDERS.

IF FIRST-TIER SUPPLIER RETESTING OF MATERIAL IS NECESSARY, USE OF BUYER APPROVED

PROCEDURES APPLICABLE TO THE SAME VERSION OF THE SPECIFICATION OR STANDARD INVOKED

ON THE IRPOD IS ACCEPTABLE IN LIEU OF OBTAINING THE RAW MATERIAL SUPPLIER OR

MATERIAL INSPECTION AND TEST PROCEDURES FOR APPROVAL.

WHERE ALTERNATIVE SPECIFICATIONS ARE SHOWN FOR A GIVEN ITEM, ONLY

THE DATA FOR THE SPECIFICATIONS USED IS REQUIRED. THE SELLER

SHALL SPECIFY THE FOLLOWING ON PROCEDURE(S)/REPORT(S) REQUIRING

SUBMITTAL, AS APPLICABLE, IN ORDER THAT THE PROCEDURE/REPORT CAN

BE READILY REVIEWED AGAINST THE APPROPRIATE ACCEPTANCE CRITERIA:

SPECIFICATION AND REVISION, INCLUDING AMENDMENTS, NOTICES, ETC

APPLICABLE PARAGRAPH OF THE SPECIFICATION

THE NAME OF THE SUBMITTAL

THE MATERIAL CONDITIONS (I.E., MATERIAL GRADE, CLASS, TYPE,

SIZE, COMPOSITION, ETC.).

6.1.3 PER THE CONTRACT DELIVERY SCHEDULE:

DRAWING PREPARER/MANUFACTURER

REVISION

MANUFACTURER'S PART NO./DRAWING NO. RSP

ACTIVITY

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SPL ZNCOXD/AMHYDROX 8714A12

FOR EACH SHIPMENT, THE SELLER SHALL PROVIDE TO THE GOVERNMENT

A REPORT DOCUMENTING THE RESULTS OF QUALITY ASSURANCE TESTING

AND INSPECTION SPECIFIED IN SECTION 4.3, AS WELL AS ANY

ADDITIONAL WRITTEN CERTIFICATIONS REQUIRED BY SECTION 4.3.

THESE REPORTS AND CERTIFICATIONS ARE DELIVERABLE IN ACCORDANCE

WITH THE CONTRACT DELIVERY SCHEDULE AND SHALL PROVIDE THE

QUANTITATIVE RESULTS (NUMERICAL RESULT OR PASS/FAIL AS

APPLICABLE) FOR EACH SAMPLE TESTED.

6.2 OTHER CONTRACT DATA REQUIREMENTS

INTENTIONALLY LEFT BLANK