IRPOD_NSN_1H_6810-00-043-0758_X2.pdf

05/16/2016

ITEM NAMENATIONAL STOCK NUMBER

DRAWING PREPARER/MANUFACTURER

REVISION

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1.0 SCOPE

THIS DOCUMENT PROVIDES THE REQUIREMENTS FOR THE PROCUREMENT OF

SODIUM PHOSPHATE, TRIBASIC DODECAHYDRATE

2.0 LIST OF APPLICABLE DOCUMENTS

IF A SUPPLIER QUOTES TO A LATER REVISION OF THE DRAWING (OR CATALOG ITEM) THAN

SPECIFIED BELOW, SUBMITTAL OF QUOTE SHALL INCLUDE TWO (2) COPIES OF THE REVISED

DOCUMENT AND AN EVALUATION OF THE INTERCHANGEABILITY. THE FOLLOWING DOCUMENTS AND

CHANGE DATA ARE APPLICABLE TO THE EXTENT SPECIFIED IN THIS IRPOD, THE DRAWINGS, OR

OTHER DOCUMENTS INVOKED BY THIS IRPOD. CONTRACTING AGENCY APPROVAL IS REQUIRED TO

USE EARLIER SPECIFICATION VERSIONS THAN THOSE LISTED HEREIN, EXCEPT AS IDENTIFIED

BELOW. IF NO DOCUMENT VERSION IS LISTED, THEN ANY VERSION OF THE DOCUMENT MAY BE

USED.

RAW MATERIAL REQUIRED HEREIN MAY HAVE BEEN PROCESSED OR TESTED (FOR EXAMPLE, HEAT

TREATED OR ULTRASONICALLY TESTED) AS REQUIRED BY THE RAW MATERIAL SPECIFICATION

PRIOR TO RECEIPT OF THIS ORDER USING PREVIOUS VERSIONS OF PROCESSING OR TESTING

SPECIFICATIONS. THIS PROCESSING AND TESTING NEED NOT BE REPEATED IF:

1.IT COMPLIED WITH THE APPLICABLE REQUIREMENTS OF THE

PROCESSING/TESTING SPECIFICATION VERSIONS IN EFFECT AT THE TIME OF

THE ACTUAL PROCESSING OR TESTING AND

2.ALL REQUIREMENTS OF THE RAW MATERIAL SPECIFICATION VERSION LISTED

HEREIN HAVE BEEN SATISFIED.

SECTION 6.0 IDENTIFIES SPECIAL REQUIREMENTS FOR SUBMITTAL OF THE PROCEDURES USED

FOR COMPLETED PROCESSING AND TESTING. ALL PROCESSING AND TESTING PERFORMED AFTER

RECEIPT OF THIS ORDER SHALL CONFORM TO THE PROCESSING/TESTING SPECIFICATION

VERSIONS LISTED HEREIN.

DOCUMENT NUMBER VERSION TITLE

FEDERAL SPECIFICATIONS

PPP-C-186 C NOTICE 1 CONTAINERS, PACKAGING AND PACKING FOR DRUGS,

CHEMICALS, AND PHARMACEUTICALS

PPP-C-2020 A, NOTICE 1 CHEMICALS, LIQUID, DRY, AND PASTE, PACKAGING

OF

FEDERAL STANDARDS

FED-STD-313 D, NOTICE 1 MATERIAL SAFETY DATA, TRANSPORTATION SAFETY

DATA AND DISPOSAL DATA FOR HAZARDOUS

MATERIAL FURNISHED TO GOVERNMENT ACTIVITIES

FED-STD-595 B COLORS USED IN GOVERNMENT PROCUREMENT

MILITARY STANDARDS

DRAWING PREPARER/MANUFACTURER

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MIL-STD-129 P MARKING FOR SHIPMENT AND STORAGE (PART 1 OF

4 PARTS)

DRAWINGS

5577B18 - BECHTEL BETTIS, INC. METAL CAN FOR

PACKAGING SODIUM PHOSPHATE, TRIBASIC

(1H 6810-00-043-0758X2)

OTHERS

TITLE 29 OCCUPATIONAL SAFETY AND HEALTH

ADMINISTRATION REQUIREMENTS

CODE OF FEDERAL REGULATIONS

CHAPTER XVII

TITLE 49 DEPARTMENT OF TRANSPORTATION CODE OF FEDERAL

REGULATIONS

HAZARDOUS MATERIAL REGULATIONS

PARTS 100 - 199

AMERICAN CHEMICAL 10TH EDITION REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

SOCIETY (ACS) REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

PUBLICATION REAGENT CHEMICALS, AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS

UNIFORM FREIGHT NATIONAL RAILROAD FREIGHT COMMITTEE

CLASSIFICATION RULES NATIONAL RAILROAD FREIGHT COMMITTEE

NATIONAL CLASSIFICA- NATIONAL MOTOR FREIGHT CLASSIFICATION

TION BOARD RULES NATIONAL MOTOR FREIGHT CLASSIFICATION

3.0 TECHNICAL REQUIREMENTS

SODIUM PHOSPHATE TR 8723-0112

NON-DEFINITIVE UNIT OF ISSUE

CONTAINER - 112 OUNCE

3.1 MATERIAL REQUIREMENTS

SODIUM PHOSPHATE TR 8723-0112

THE MATERIAL SHALL CONFORM TO THE REQUIREMENTS FOR SODIUM

PHOSPHATE, TRIBASIC, DODECAHYDRATE, OF THE AMERICAN CHEMICAL

SOCIETY (ACS) SPECIFICATIONS FOR REAGENT CHEMICALS.

SHELF LIFE OF THIS ITEM IS FORTY-EIGHT MONTHS.

THIS ITEM SHALL BE SUPPLIED WITH AT LEAST 85 PERCENT OF ITS

SHELF LIFE REMAINING AT TIME OF SHIPMENT.

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3.2 MANUFACTURING AND PROCESS REQUIREMENTS

SODIUM PHOSPHATE TR 8723-0112

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A. MERCURY CONTAMINATION

THIS PRODUCT SHALL NOT CONTAIN AND SHALL NOT BE CONTAMINATED

BY MERCURY NOR MERCURY COMPOUNDS. DURING THE MANUFACTURING

PROCESS, TESTS, AND INSPECTIONS, THE PRODUCT SHALL NOT HAVE COME

IN DIRECT CONTACT WITH MERCURY, NOR ANY OF ITS COMPOUNDS, NOR ANY

MERCURY CONTAINING DEVICE EMPLOYING A SINGLE BOUNDARY OF

CONTAINMENT. THE SPECIFIC LIMIT IS THAT THIS ITEM SHALL CONTAIN

LESS THAN OR EQUAL TO 50 PPB MERCURY WHEN TESTED AS SPECIFIED IN

SECTION 4.6 OF THIS IRPOD.

B. FOREIGN MATERIAL EXCLUSION

THE SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE MATERIAL SHALL

BE UNIFORM AND SHALL CONFORM TO THE FOREIGN MATERIAL INSPECTION

REQUIREMENTS OF SECTION 4.6 OF THIS IRPOD. EXAMPLES OF FOREIGN

MATERIAL INCLUDE, BUT ARE NOT LIMITED TO, RUST, GLASS OR DIRT

PARTICLES; PLASTIC, CERAMIC, WOOD OR METAL CHIPS, CARDBOARD

FIBERS, CLOTH FIBERS, BRUSH BRISTLES AND PAINT CHIPS. PRODUCTION

OPERATIONS AND INSPECTION PROCEDURES SHALL BE CONDUCTED SO AS TO

PREVENT THE INTRODUCTION OF FOREIGN MATERIAL.

SUCH OPERATIONS MAY INCLUDE, BUT ARE NOT LIMITED TO, THE FOLLOWING

PRECAUTIONS: ENSURING THAT THE CANS ARE FREE FROM FOREIGN MATERIAL

PRIOR TO FILL, PROVIDING AN AREA FOR FILL OPERATIONS WHICH IS FREE

OF DIRT AND DEBRIS, AND MAINTAINING THE FILL EQUIPMENT IN A CLEAN

CONDITION.

INSPECTION FOR FOREIGN MATERIAL SHALL BE CONDUCTED IN ACCORDANCE

WITH SECTION 4.6.C OF THIS IRPOD. IN THE EVENT FOREIGN MATERIAL IS

DETECTED, THIS FINDING SHALL NOT PRECLUDE CONDUCTING ALL OTHER

REQUIRED INSPECTIONS AND TESTS. DISPOSITION OF THE LOT WITH

RESPECT TO FOREIGN MATERIAL SHALL BE DETERMINED IN ACCORDANCE

WITH THE FOREIGN MATERIAL EXCLUSION REQUIREMENTS OF SECTION 4.6.C.8.

C. CONTAINER REQUIREMENTS

THE CONTAINER SHALL CONFORM TO THE SPECIFICATIONS OF BECHTEL

BETTIS, INC. DRAWING 5577B18 WHICH INCLUDES THE FOLLOWING

SIGNIFICANT REQUIREMENTS:

1. MATERIAL

THE METAL CONTAINER SHALL CONSIST OF 135 POUND, 0.50

ELECTROLYTIC TINPLATE.

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2. CONSTRUCTION

THE METAL CAN SHALL BE A ROUND CORNERED, SQUARE

CROSS-SECTION CAN, WITH A SQUARE SLIP COVER AS SHOWN IN

BECHTEL BETTIS, INC. DRAWING 5577B18. THE BODY SHALL HAVE A

WELDED VERTICAL SEAM AND SHALL BE BEADED JUST BELOW THE

COVEREDGE. THE TOP EDGES SHALL BE HEMMED INSIDE. THE BOTTOM

SHALL BE DOUBLE SEAMED TO THE BODY. THE SQUARE SLIP

COVER SHALL BE TIGHT FITTING WITH HEMMED EDGES.

3. DIMENSIONS

THE WALL THICKNESS OF THE CAN, THE CAN BOTTOM, AND THE SLIP

COVER SHALL NOT BE LESS THAN 0.014 INCH THICK. THE INSIDE

BODY SHALL BE A NOMINAL 5.0 INCHES BY 5.0 INCHES IN CROSS

SECTION BY 10.0 INCHES IN HEIGHT. THE SQUARE SLIP COVER

TOP SHALL BE A NOMINAL 0.50 INCH IN HEIGHT.

4. INSIDE COATING

THE INSIDE OF THE CAN AND THE SLIP COVER SHALL BE COATED

WITH CLEAR PHENOLIC LACQUER.

5. OUTSIDE COATING

THE TOP, BOTTOM AND SIDES, INCLUDING THE VERTICAL SEAM AREA

SHALL BE PAINTED WITH ONE COLOR OF PAINT THAT SHALL BE

RESISTANT TO PEELING AND CHIPPING. THE COLOR OF THE PAINT

SHALL BE APPROXIMATELY NUMBER 25109, SEMIGLOSS BLUE OF

FEDERAL STANDARD 595. THE PAINT THAT IS USED SHALL BE

ACCEPTABLE FOR APPLICATION OF LETTERING BY A SILK SCREENING

PROCESS.

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6. LETTERING

THE LETTERING SHALL BE STANDARD BLOCK PRINT THAT WILL NOT

FADE OR RUB OFF. THE LETTERING MAY BE APPLIED BY A SILK

SCREENING PROCESS, OR MAY BE LITHOGRAPHED WHEN THE OUTSIDE

COATING IS APPLIED. THE LETTERING SHALL BE IN BLACK EXCEPT

THAT THE DESTROY DATE SHALL BE APPROXIMATELY NUMBER 22246

SEMIGLOSS ORANGE OF FEDERAL STANDARD 595. THE LOT OR BATCH

NUMBER SHALL BE EITHER BLACK OR ORANGE.

ALL LETTERING SHALL BE SUFFICIENTLY ADHERENT THAT NO

SMUDGING OCCURS. THE SIZES AND ARRANGEMENTS OF THE

LETTERING AND THE LOCATION OF THE SIDE SEAM OF THE CAN

SHALL BE IN ACCORDANCE WITH BECHTEL BETTIS, INC. DRAWING

5577B18 WITH THE LETTERING CENTERED TO THE FULLEST EXTENT

PRACTICABLE.

7. PACKAGING

THE SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE MATERIAL

SHALL BE PACKAGED IN A POLYETHYLENE BAG CONFORMING TO GROUP F,

CLASS 2 OF FEDERAL SPECIFICATION PPP-C-186 SEALED WITH ARE

SEALABLE TWIST TYPE SEALING STRIP. EACH BAG SHALL

CONTAIN 7.0 +/- 0.25 POUNDS OF SODIUM PHOSPHATE, TRIBASIC,

DODECAHYDRATE MATERIAL. THE POLYETHYLENE BAG SHALL THEN

BE CONTAINED IN THE ABOVE DESCRIBED CAN WITH THE LID OF THE

CAN SEALED WITH VINYL TAPE.

D. UNIT OF ISSUE

SEVEN (7) POUNDS OF SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE, IN

A POLYETHYLENE BAG IN A METAL CAN.

E. SHELF LIFE

THE DESIGNATED SHELF LIFE IS FORTY-EIGHT (48) MONTHS. THIS

ITEM SHALL BE SUPPLIED WITH AT LEAST EIGHTY-FIVE (85) PERCENT

(FORTY-ONE (41) MONTHS) SHELF LIFE REMAINING AT TIME OF

SHIPMENT.

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F. LOT

ALL SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE, PRODUCED AT

ONE (1) TIME, BY ONE (1) MANUFACTURER, AT ONE (1) PLANT, FROM

THE SAME MATERIALS, AND UNDER ESSENTIALLY THE SAME MANUFACTURING

CONDITIONS PROVIDED THE OPERATION IS CONTINUOUS. IN THE EVENT

THE PROCESS IS A BATCH OPERATION, EACH BATCH (SEE 3.2.G BELOW)

SHALL CONSTITUTE A LOT. EVEN IF A BATCH IS LARGER, EACH LOT

PACKAGED FOR DELIVERY SHALL BE LIMITED TO A MAXIMUM OF FIVE

HUNDRED (500) CANS OF SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE.

G. BATCH

THAT QUANTITY OF MATERIAL WHICH HAS BEEN MANUFACTURED BY SOME

UNIT CHEMICAL PROCESS, OR SUBJECTED TO SOME PHYSICAL MIXING

OPERATION, INTENDED TO MAKE THE FINAL PRODUCT SUBSTANTIALLY

UNIFORM.

4.0 QUALITY ASSURANCE PROVISIONS

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4.1 INSPECTION SYSTEM

THE VENDOR SHALL MAINTAIN COMPLETE RECORDS FOR ALL INSPECTIONS AND

TESTS PERFORMED ON THE FINAL CONTAINERS AND THEIR CONTENTS. THE

RECORDS SHALL BE TRACEABLE BY THE VENDOR'S LOT OR BATCH NUMBER.

THE VENDOR SHALL RETAIN THESE RECORDS FOR FOUR (4) YEARS FOLLOWING

DELIVERY TO THE GOVERNMENT. THE RECORDS SHALL BE MADE AVAILABLE

FOR GOVERNMENT REVIEW UPON WRITTEN REQUEST DURING THIS PERIOD.

THESE RECORDS SHALL INDICATE THE NATURE AND NUMBER OF OBSERVATIONS

MADE, THE NUMBER AND TYPE OF DEFICIENCIES FOUND, THE QUANTITIES

APPROVED AND REJECTED, AND THE SPECIFIC ACTIONS TAKEN TO CORRECT

THE DEFICIENCIES. THESE RECORDS SHALL INCLUDE HIGH MAGNIFICATION

(AT LEAST 45X) DIGITAL PHOTOGRAPHS OF ANY FOREIGN MATERIAL

IDENTIFIED DURING INSPECTION THAT CLEARLY INDICATE THE SIZE OF THE

FOREIGN MATERIAL (E.G., A LINEAR SCALE IS INCLUDED IN THE

PHOTOGRAPH).

4.2 TEST EQUIPMENT

ALL GAGES, MEASURING AND TEST EQUIPMENT USED IN THE TESTS,

INSPECTION AND PROCESSING OF FILLED CANS UNDER THIS IRPOD

SHALL BE CALIBRATED TO CERTIFIED STANDARDS THAT HAVE KNOWN,

VALID RELATIONSHIPS TO NATIONALLY ACCEPTED INDUSTRY STANDARDS.

THE CALIBRATION FREQUENCY FOR EACH DEVICE SHALL BE BASED ON

ITS STABILITY, PURPOSE AND USAGE. A POSITIVE MEANS (SUCH AS

STICKERS) SHALL BE PROVIDED TO IDENTIFY THE CALIBRATION

INTERVAL, LAST DATE OF CALIBRATION AND DATE CALIBRATION IS DUE

FOR EACH DEVICE. COMPLETE WRITTEN RECORDS OF CALIBRATION

DATA TRACEABLE TO THE INDIVIDUAL TEST DEVICES SHALL BE

AVAILABLE FOR GOVERNMENT REVIEW FOR UP TO FOUR (4) YEARS FOLLOWING

DELIVERY OF FILLED CANS TESTED WITH THE CALIBRATED EQUIPMENT.

4.3 RESPONSIBILITIES

THE VENDOR IS RESPONSIBLE FOR THE PERFORMANCE OF ALL INSPECTIONS

AND TEST REQUIREMENTS IN SECTIONS 4.4 AND 4.6 OF THIS

SPECIFICATION. THE NUMBER OF SAMPLES TO BE TESTED SHALL BE IN

ACCORDANCE WITH TABLE 1 OF SECTION 4.4 OF THIS IRPOD. THE VENDOR

MAY USE HIS OWN OR ANY OTHER FACILITIES SUITABLE FOR THE

PERFORMANCE OF THE REQUIRED INSPECTIONS AND TESTS. THE FINAL

PRODUCT SHALL BE MADE AVAILABLE FOR GOVERNMENT TESTING AND

INSPECTION. IN ADDITION TO THE SPECIFIED TESTS AND INSPECTIONS IN

THIS SPECIFICATION, THE GOVERNMENT RESERVES THE RIGHT TO PERFORM

ANY ADDITIONAL INSPECTIONS AND TESTS DEEMED NECESSARY TO ASSURE

SUPPLIES AND SERVICES CONFORM TO PRESCRIBED REQUIREMENTS. THE

VENDOR SHALL ALSO PROVIDE THE FOLLOWING:

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A. A WRITTEN CERTIFICATION IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE THAT EACH MANUFACTURER'S LOT OF SODIUM

PHOSPHATE, TRIBASIC, DODECAHYDRATE MEETS ALL THE

REQUIREMENTS OF THE AMERICAN CHEMICAL SOCIETY

SPECIFICATIONS FOR REAGENT CHEMICALS.

IF THE VENDOR FOR THIS CHEMICAL IS NOT THE MANUFACTURER, THE

VENDOR SHALL SUBMIT THE CERTIFICATION DOCUMENTION PROVIDED BY

THE ACTUAL MANUFACTURER (DEFINED AS THE ENTITY WHO LAST

PROCESSED THE MATERIAL FROM THE LIQUID FORM TO THE FINAL DRY

MATERIAL). THE CERTIFICATION SHALL BE TRACEABLE BY LOT NUMBER

FROM THE MANUFACTURER TO THE SUPPLIER, AS ADDITIONAL

VERIFICATION THAT THIS LOT OF CHEMICAL MEETS THE REQUIREMENTS

FOR ACS GRADE CHEMICALS.

B. CERTIFIED TEST RESULTS IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE SHOWING THAT THE APPROPRIATE NUMBER OF

REPRESENTATIVE SAMPLES OF EACH LOT OF FINISHED PRODUCT WERE

SELECTED IN ACCORDANCE WITH SECTION 4.4 OF THIS IRPOD AND

WERE TESTED AND FOUND TO MEET THE REQUIREMENTS OF

SECTION 4.6 OF THIS IRPOD.

C. A WRITTEN CERTIFICATION IN ACCORDANCE WITH THE CONTRACT

DELIVERY SCHEDULE THAT THE ITEMS ANALYZED AND OFFERED FOR

DELIVERY ARE THE SAME, AND THE ITEMS OFFERED FOR DELIVERY

MEET ALL THE REQUIREMENTS OF THE IRPOD.

4.4 INSPECTION OF PREPARATION FOR DELIVERY

SAMPLING FOR INSPECTION OF PREPARATION FOR DELIVERY SHALL BE

FROM PACKAGED CANS OFFERED FOR DELIVERY. SAMPLES SHALL BE

CHOSEN RANDOMLY AND IN ACCORDANCE WITH TABLE 1.

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TABLE 1

SAMPLING FOR INSPECTION AND TESTING

LOT SIZE NUMBER OF CANS

LT~ OR = 25 4

26 TO 150 6

151 TO 500 10

EACH SELECTED CAN SHALL BE INSPECTED FOR CONFORMANCE WITH

THE REQUIREMENTS SPECIFIED IN SECTION 3.2.C, CONTAINER

REQUIREMENTS, SECTION 3.2.B, FOREIGN MATERIAL EXCLUSION,

AND SECTION 5.0, PREPARATION FOR DELIVERY, OF THIS IRPOD.

FAILURE OF ANY ONE (1) CAN CONSTITUTES FAILURE OF THE ENTIRE LOT.

A REJECTED LOT MAY BE RESUBMITTED FOR INSPECTION PROVIDED THE

CONTRACTOR HAS CORRECTED ALL NON-CONFORMING ATTRIBUTES.

4.5 GOVERNMENT TESTING

FOLLOWING COMPLETION OF SECTION 4.4, THE COGNIZANT DEFENSE

CONTRACT MANAGEMENT AGENCY (DCMA) QUALITY ASSURANCE

REPRESENTATIVE (QAR) WILL SELECT RANDOM CANS FROM EACH LOT

IN ACCORDANCE WITH WITH TABLE 1 OF THIS IRPOD AND ONE (1)

ADDITIONAL RANDOM CAN FROM EACH LOT FOR RETENTION AS A LIBRARY

SAMPLE AT PSNS&IMF (CAN SHALL NOT BE OPENED BY THE QAR).

EACH SAMPLE CAN SELECTED IN ACCORDANCE WITH TABLE 1 SHALL BE

INDIVIDUALLY SUBSAMPLED INTO A ONE (1) POUND SAMPLE CONTAINED IN

A SEALED POLYETHYLENE BOTTLE FOR GOVERNMENT LABORATORY TESTING.

THE QAR SHALL WITNESS THE SUBSAMPLING AND PACKAGING OF THE

SUBSAMPLES. THE VENDOR SHALL PREPARE THE SELECTED

SAMPLES FOR DELIVERY IN ACCORDANCE WITH THIS IRPOD AND SHALL SHIP

THEM WITH FORM DD-1222, A MATERIAL SAFETY DATA SHEET (MSDS),

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AND A COPY OF THE DATA REQUIRED IN SECTION 4.3 TO THE

FOLLOWING ADDRESS:

PUGET SOUND NAVAL SHIPYARD & IMF

CODE 134.03X, BUILDING 59

1400 FARRAGUT AVE

BREMERTON, WA 98314-5001

ANY FOREIGN MATERIAL OBSERVED DURING THE SUBSAMPLING PROCESS

SHOULD BE REMOVED, RETAINED, AND SHIPPED TO PSNS&IMF WITH THE

SELECTED SUBSAMPLES.

THE GOVERNMENT INSPECTION AND TESTING MUST DEMONSTRATE

CONFORMANCE WITH THE REQUIREMENTS OF THIS IRPOD BEFORE THE LOT

OF MATERIAL WILL BE ACCEPTED. PUGET SOUND NAVAL SHIPYARD

SHALL PROVIDE NOTIFICATION OF RESULTS TO THE PROCURING

CONTRACTING OFFICER WHO WILL NOTIFY THE CONTRACTOR AND DCMA

QAR.

4.6 ACCEPTANCE TESTING

THE VENDOR MAY USE ALTERNATE TEST METHODS TO ENSURE THAT THE

DELIVERED PRODUCT CONFORMS TO THE IRPOD REQUIREMENTS.

HOWEVER, IN THE EVENT OF A DISAGREEMENT BETWEEN THE VENDOR

AND THE GOVERNMENT, THE TEST METHOD IDENTIFIED HERE SHALL BE

USED AS THE REFEREE METHOD. ACCEPTANCE TESTING SHALL CONSIST

OF THE TESTS DESCRIBED BELOW. 50% OF THE SAMPLES SHALL UNDERGO THE

TESTING IN PARAGRAPHS (A) AND (B), BELOW. ALL OF THE SAMPLES SHALL

UNDERGO THE TESTING IN PARAGRAPH (C).

A. GOVERNMENT TESTING SHALL CONSIST OF ALL THE TESTS SPECIFIED

IN THE AMERICAN CHEMICAL SOCIETY SPECIFICATIONS FOR REAGENT

CHEMICALS FOR SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE.

B. MERCURY CONTENT

THE MERCURY CONTENT OF THIS CHEMICAL SHALL BE DETERMINED BY

DRAWING PREPARER/MANUFACTURER

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ATOMIC ABSORPTION SPECTROMETRY USING ENVIRONMENTAL PROTECTION

AGENCY METHOD 7470 FOR LIQUIDS OR METHOD 7471 FOR SOLIDS.

FAILURE OF ONE (1) OF THE SUBMITTED ACCEPTANCE SAMPLES TO MEET

THE MERCURY SPECIFIACTION OF SECTION 3.2.A SHALL BE CAUSE FOR

REJECTION OF THE LOT.

C. VISUAL INSPECTION FOR FOREIGN MATERIAL

1. OBTAIN A REPRESENTATIVE SAMPLE OF APPROXIMATELY 250 GRAMS

(+5.0/- 0.0 GRAMS) OF MATERIAL.

A. REDUCE THE SAMPLE SIZE TO OBTAIN THE ABOVE QUANTITY FROM

LARGER RECEIVED SAMPLES EMPLOYING GOOD SAMPLING PRACTICES,

INCLUDING BUT NOT LIMITED TO CONING AND QUARTERING,

ROLLING AND QUARTERING, OR APPLICATION OF A MECHANICAL

SAMPLE SPLITTER, DIVIDER, OR RIFFLER.

2. SPREAD THE MATERIAL COMPRISING THE 250 GRAM SAMPLE, A SMALL

PORTION AT A TIME, ON A PIECE OF CLEAN, WHITE PAPER.

A. BREAK UP CLUMPS, IF NECESSARY.

B. THE SAMPLE MAY BE SLOWLY POURED FROM THE CONTAINER TO FORM

A LAYER NO MORE THAN SEVERAL GRANULES THICK FOR INSPECTION.

C. SPREAD IN A THIN LAYER SO THAT NONE OF THE GRANULES ARE

HIDDEN FROM VIEW.

D. ENSURE THAT FOREIGN MATERIAL IS NOT INTRODUCED (CLOTHING,

ENVIRONMENT, UTENSILS) BY THIS INSPECTION PROCEDURE.

3. VIEW THE MATERIAL FROM NORMAL READING DISTANCE (APPROXIMATELY

35 CM) IN A LABORATORY ENVIRONMENT WITH CONVENTIONAL

FLUORESCENT OVER-HEAD LIGHTING, AND BY A PERSON WITH NORMAL

OR CORRECTED VISUAL ACUITY.

4. VIEW THE MATERIAL AT 90 DEGREES, 180 DEGREES, AND 270 DEGREES

RELATIVE TO THE INITIAL VIEWING DIRECTION.

5. CONTINUE VIEWING ALL PORTIONS OF THE SELECTED SAMPLE SIZE BY

REPETITION OF STEPS 2 THROUGH 4.

6. REMOVE ANY AND ALL VISIBLE FOREIGN MATERIAL FROM THE OBSERVED

SAMPLE SIZE AND DETERMINE THE INDIVIDUAL MASS, TOTAL MASS,

AND NUMBER OF FOREIGN PIECES COMPRISING THIS MASS.

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A. ISOLATE FOREIGN MATERIAL FROM CHEMICAL PARTICULATE AND USE

A BALANCE WITH RESOLUTION OF 0.1 MG TO DETERMINE THE MASS.

IF THE FOREIGN MATERIAL INDIVIDUAL MASS IS TOO SMALL TO

MEASURE, NOTE IT AS ~LT~0.1 MG.

B. FOR FOREIGN MATERIAL WITH INDIVIDUAL MASS THAT IS TOO SMALL

TO MEASURE, MEASURE A TOTAL MASS AND SPECIFY THE NUMBER

OF PIECES COMPRISING THIS MASS.

C. IF POSSIBLE, IN ADDITION TO SIZE, MASS, AND NUMBER,

CHARACTERIZE ANY FINDING OF FOREIGN MATERIAL FOUND WITHIN

THE 250 GRAM SAMPLE BY TYPE.

D. PRESERVE FOREIGN MATERIAL IN AN APPROPRIATE CONTAINER, FOR

FURTHER CHARACTERIZATION.

7. RESULTS FROM MULTIPLE 250 GRAM SAMPLES FOR A SINGLE LOT SHALL

BE REPORTED INDIVIDUALLY, AND NOT AVERAGED UNTIL THE

CONCLUSION OF THE INSPECTION PROCESS FOR ALL SAMPLES.

8. BASED ON THE COLLECTIVE FINDING OF FOREIGN MATERIAL

IDENTIFIED DURING SUBSAMPLING AND DURING THE DETAILED

VISUAL INSPECTION OF THE SUBSAMPLES, INDIVIDUAL LOTS OF

POWDERED CHEMICAL ARE ACCEPTABLE IF THE FOLLOWING CRITERIA

ARE MET:

A. THE NUMBER OF PARTICLES AND FIBERS OF FOREIGN MATERIAL

DETECTED DURING SUBSAMPLING OF UNIT-OF-ISSUE CONTAINERS

AND DURING VISUAL INSPECTION OF THE CORRESPONDING

SUBSAMPLES SHALL BE NO MORE THAN AN AVERAGE OF 2.0 PER

CONTAINER (E.G., AT MOST A TOTAL OF 20 PIECES OF FOREIGN

MATERIAL ARE IDENTIFIED IN TEN (10) CONTAINERS INSPECTED

FOR THE LARGEST LOT SIZE);

B. FROM THE TOTAL QUANTITY OF FOREIGN MATERIAL, THE SINGLE

LARGEST PARTICLE SHALL MEASURE NO MORE THAN THREE

MILLIMETERS IN MAJOR DIMENSION AND THE REMAINDER OF THE

PARTICLES SHALL HAVE A MAJOR DIMENSION OF 1.5 MILLIMETERS

OR LESS;

C. FROM THE TOTAL QUANTITY OF FOREIGN MATERIAL, ANY FIBERS

SHALL BE NO LONGER THAN SIX MILLIMETERS AND NO THICKER

THAN 50 MICROMETERS.

IF FOREIGN MATERIAL OR OTHER TEST REQUIREMENTS ARE NOT MET, THE LOT SHALL BE

REJECTED AND THE DOCUMENTATION FORWARDED TO NAVSUP WSS.

5.0 PREPARATION FOR DELIVERY

DRAWING PREPARER/MANUFACTURER

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5.1 PACKAGING AND PACKING

PACKAGING AND PACKING SHALL CONFORM TO FEDERAL SPECIFICATION

PPP-C-2020, LEVEL B, AND 49 CFR 100-199 WHERE APPLICABLE. THE

PACKING OF THE CANS OF SODIUM PHOSPHATE, TRIBASIC, DODECAHYDRATE

MATERIAL SHALL BE SUFFICIENT TO PREVENT SHIFTING OF CONTENTS,

BREAKAGE, DAMAGE, OR SUBSTANTIAL DISTORTION DURING HANDLING,

SHIPMENT, AND INTERMEDIATE STORAGE. CONTAINERS SHALL CONFORM TO

THE UNIFORM FREIGHT CLASSIFICATION OR REGULATIONS OF OTHER

CARRIERS AS APPLICABLE TO THE MODE OF TRANSPORTATION.

A MATERIAL SAFETY DATA SHEET (MSDS) PREPARED PER FED-STD-313

SHALL BE PROVIDED WITH EACH UNIT OF ISSUE AND AFFIXED/PACKAGED

IN A MANNER FOR EASY ACCESSIBILITY WITHOUT BEING LOST OR

DAMAGED DURING SHIPMENT AND STORAGE.

5.2 PRECAUTIONARY LABELS

NOT APPLICABLE

5.3 MARKING

A. MARKING FOR SHIPMENT AND STORAGE

INTERIOR PACKAGES AND EXTERIOR SHIPPING CONTAINERS SHALL BE

MARKED IN ACCORDANCE WITH MIL-STD-129, 49 CFR 100-199, AND

29 CFR 1910.1200.

BAR CODE MARKING SUITABLE FOR HAND SCANNING IS REQUIRED.

THE BAR CODE SHALL CONTAIN THE NSN, MFR/PN, AND THE

SUPPLIER'S CAGE CODE. THE BAR CODE SHALL BE APPLIED ON THE

UNIT AND INTERMEDIATE PACK.

B. SPECIAL MARKING

FOR CHEMICALS PACKAGED IN METAL CANS, THE LABELING

INFORMATION PRINTED ON THE CAN SHALL BE PRESENTED IN THE

MANNER SPECIFIED ON THE ENGINEERING DRAWING FOR THE CAN

(LISTED IN SECTION 2.0). ALL OTHER PACKAGING LABELING SHALL

BE PRESENTED ACCORDING TO THE FOLLOWING STANDARDIZED TABLE.

DRAWING PREPARER/MANUFACTURER

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(1) IDENTIFICATION LABEL DATA - EACH UNIT OF ISSUE, INTERMEDIATE AND

EXTERIOR SHIPPING CONTAINER (EXCEPT FOR NET CONTENTS)

SHALL BE MARKED WITH THE FOLLOWING INFORMATION IN

ACCORDANCE WITH MIL-STD-129:

= NATIONAL STOCK NUMBER 1H 6810-00-043-0758X2 =

= NOMENCLATURE SODIUM PHOSPHATE, TRIBASIC =

= NAME OF MANUFACTURER =

= CONTRACT NUMBER =

= LOT NUMBER =

= DATE OF MANUFACTURE (MONTH/YEAR) =

= SHELF LIFE 48 MONTHS =

= EXPIRATION DATE (MONTH/YEAR) =

= NET CONTENTS SEVEN POUNDS =

THE EXPIRATION DATE IS COMPUTED BY ADDING THE SHELF

LIFE (48 MONTHS) TO THE DATE OF MANUFACTURE. THE DATE

OF MANUFACTURE SHALL BE WHEN THE CHEMICAL POWDER IS PLACED IN

ITS END USE CONTAINERS. THIS DATE SHOULD CORRESPOND

TO THE TIME AT WHICH THE SODIUM PHOSPHATE, TRIBASIC,

DODECAHYDRATE MATERIAL IS TESTED BY THE VENDOR FOR

CERTIFICATION IT MEETS PURCHASE SPECIFICATIONS AND

THE PROCUREMENT CONTRACT.

DRAWING PREPARER/MANUFACTURER

REVISION

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(2) SHIPPING CONTAINERS SHALL BE MARKED WITH TAPE

IMPRINTED WITH THE WORDS "X2 CHEMICALS". THE TAPE

SHALL BE WHITE AND APPROXIMATELY 1.25 INCHES WIDE. THE

RED BLOCK PRINTING SHALL BE APPROXIMATELY 0.75 INCH

TALL. THE RED BORDER SHALL BE APPROXIMATELY 0.2 INCH

WIDE. THE TAPE SHALL NOT COVER ANY OTHER IDENTIFICATION

MARKINGS ON THE CONTAINER. WHERE THE EXTERIOR

CONTAINER IS A BOX OR CARTON, A STRIP OF TAPE SHALL

BE PLACED ON ALL FOUR (4) LATERAL FACES TO ENSURE THAT THE

COMPLETE WORDS "X2 CHEMICALS" ARE REPEATED AT LEAST

TWICE ON EACH FACE.

NOTE: TAPE MAY BE PURCHASED FROM:

NADCO, INC.

ONE WASHINGTON ST

DOVER, NH 03820

(P/N X2CHEM)

PHONE (800) 839-9018

5.4 SHIPPING

SPECIAL REQUIREMENTS FOR SHIPMENT OF CHEMICALS

IN ACCORDANCE WITH 29 CFR 1910.1200, ONE (1) COPY OF THE MSDS

SHALL BE PROVIDED WITH THE BILL OF LADING FOR EACH SHIPMENT OF

MATERIAL.

IN ADDITION TO THE EXISTING REQUIREMENTS OF MIL-STD-129, THIS PART SHALL CONTAIN

BAR CODES THAT IDENTIFY SHELF LIFE INFORMATION (CURE DATE, SHELF LIFE CODE) ON THE

UNIT PACKING ONLY.

6.0 CONTRACT DATA REQUIREMENTS

THE SELLER MUST PROVIDE THE CONTRACTING AGENCY WITH ALL OF THE

SUBMITTALS LISTED BELOW. SUBMITTALS WHICH ARE REQUIRED BY A

SPECIFICATION, BUT WHICH ARE NOT LISTED BELOW, NEED NOT BE

SUBMITTED. ONLY THOSE SUBMITTALS LISTED BELOW ARE REQUIRED.

DRAWING PREPARER/MANUFACTURER

REVISION

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HOWEVER, IF THE SELLER CONSIDERS A REQUIRED SUBMITTAL INAPPLICABLE

TO THIS PROCUREMENT, THE SELLER MUST SUBMIT A STATEMENT JUSTIFYING

THE EXCLUSION OF THE REQUIRED SUBMITTAL.

REQUESTS FOR APPROVAL OF PROCEDURES USED PRIOR TO RECEIPT OF THIS

ORDER SHALL IDENTIFY THE PROCESSING/TESTING SPECIFICATION VERSION

APPLICABLE AND STATE THAT THE PROCESSING AND/OR TESTING WAS

PERFORMED PRIOR TO RECEIPT OF THE ORDER. IF THE PROCEDURE THAT WAS

USED IS NOT COMPLETE, TEST REPORTS, HEAT TREATMENT RECORDS, OR

OTHER DOCUMENTATION SHALL BE SUBMITTED WITH THE PROCEDURES TO

SUBSTANTIATE THAT ALL SPECIFICATION REQUIREMENTS WERE MET.

6.1 PROCEDURES AND REPORTS

THE SELLER SHALL PROVIDE THE FOLLOWING PROCEDURE(S) AND REPORT(S) TO THE PROCURING

ACTIVITY. SUPPLIER PROCEDURE SUBMITTALS REQUIRED BY MATERIAL AND PROCESS

SPECIFICATIONS NEED NOT BE RESUBMITTED FOR APPROVAL EACH TIME AN ORDER IS PLACED

FOR THE SAME IRPOD ITEM TO THE SAME VERSION (IE REVISION, AMENDMENT, CHANGE NOTICE

OR INTERIM CHANGE) OF THE SPECIFICATION OR STANDARD INVOKED. THE SELLER NEED ONLY

SUBMIT PROOF OF THE PRIOR APPROVAL FOR THAT ITEM AND SPECIFICATION REVISION.

ACCEPTABLE PROOF OF PRIOR APPROVAL WILL CONSIST OF A COORDINATED PROCEDURE REVIEW

SYSTEM (CPRS) APPROVAL LETTER. CPRS APPROVAL DOES NOT RELIEVE THE SELLER OF THE

RESPONSIBILITY TO COMPLY WITH ALL REQUIREMENTS IMPOSED ON ANY CURRENT AND FUTURE

PURCHASE ORDERS.

IF FIRST-TIER SUPPLIER RETESTING OF MATERIAL IS NECESSARY, USE OF BUYER APPROVED

PROCEDURES APPLICABLE TO THE SAME VERSION OF THE SPECIFICATION OR STANDARD INVOKED

ON THE IRPOD IS ACCEPTABLE IN LIEU OF OBTAINING THE RAW MATERIAL SUPPLIER OR

MATERIAL INSPECTION AND TEST PROCEDURES FOR APPROVAL.

WHERE ALTERNATIVE SPECIFICATIONS ARE SHOWN FOR A GIVEN ITEM, ONLY

THE DATA FOR THE SPECIFICATIONS USED IS REQUIRED. THE SELLER

SHALL SPECIFY THE FOLLOWING ON PROCEDURE(S)/REPORT(S) REQUIRING

SUBMITTAL, AS APPLICABLE, IN ORDER THAT THE PROCEDURE/REPORT CAN

BE READILY REVIEWED AGAINST THE APPROPRIATE ACCEPTANCE CRITERIA:

SPECIFICATION AND REVISION, INCLUDING AMENDMENTS, NOTICES, ETC

APPLICABLE PARAGRAPH OF THE SPECIFICATION

THE NAME OF THE SUBMITTAL

THE MATERIAL CONDITIONS (I.E., MATERIAL GRADE, CLASS, TYPE,

SIZE, COMPOSITION, ETC.).

6.1.3 PER THE CONTRACT DELIVERY SCHEDULE:

DRAWING PREPARER/MANUFACTURER

REVISION

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SODIUM PHOSPHATE TR 8723-0112

FOR EACH SHIPMENT, THE SELLER SHALL PROVIDE TO THE GOVERNMENT

A REPORT DOCUMENTING THE RESULTS OF QUALITY ASSURANCE TESTING

AND INSPECTION SPECIFIED IN SECTION 4.3, AS WELL AS ANY

ADDITIONAL WRITTEN CERTIFICATIONS REQUIRED BY SECTION 4.3.

THESE REPORTS AND CERTIFICATIONS ARE DELIVERABLE IN ACCORDANCE

WITH THE CONTRACT DELIVERY SCHEDULE AND SHALL PROVIDE THE

QUANTITATIVE RESULTS (NUMERICAL RESULT OR PASS/FAIL AS

APPLICABLE) FOR EACH SAMPLE TESTED.

6.2 OTHER CONTRACT DATA REQUIREMENTS

INTENTIONALLY LEFT BLANK