B08_Appendix_D_-_Methods_with_Reporting_Requirements.xlsx

XLSX spreadsheet 151 KB Posted Feb 9, 2024

Attached to: GENERAL CHEMICAL ANALYTICAL SERVICES Federal contract opportunity
Solicitation number: 140G0224R0001
Issued by: Department of the Interior US Geological Survey Office of Acquisitions and Grants

About this file

Written by GovTribe AI · Feb 9, 2024

This document contains an Excel spreadsheet listing analytical methods and their associated requirements for chemical analyses required under the Department of the Interior US Geological Survey solicitation for general chemical analytical services. The solicitation seeks testing services for over 100 analytes using methods including ICP, ICP-MS, ion chromatography, colorimetry, gas chromatography and mass spectrometry. Required capabilities include MDL studies, proficiency testing, and subcontracting where necessary to meet method requirements. Analytes cover inorganic and organic parameters in water, soil, tissue and other sample types, including metals, anions, nutrients, cyanide, mercury, volatile and semi-volatile organic compounds. Reporting limits, preparation methods, and quality control procedures are specified for each test method.

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Gen Chem

Line Item

Test (Insert a row for multiple analyte information)

Description of Item

Method

Proposed Method number(s)

Contract Laboratory Method Name

Contract Laboratory Capability: Published Method Modification Y/N

Is the Modification 40 CFR Approved?

Primary Lab Testing Y/N

MDL Study Date Completion

MDL Concentration

MDL Units

Reporting Limit

Reporting Limit Units

Date of Acceptable PT

PT Provider

Comments for any failed analyte

Corrective Action Estimated Date of Completion

Date of PT Retake with acceptable results

Subcontractor: MDL Study Date Completion

Subcontractor: MDL Concentration

Subcontractor: MDL Units

Subcontractor: Reporting Limit

Subcontractor: Reporting Limit Units

Subcontractor: Date of Acceptable PT

Subcontractor: PT Provider

Subcontractor: Comments for any failed analyte

Subcontractor: Corrective Action Estimated Date of Completion

Subcontractor: Date of PT Retake with acceptable results

Screen for metals by ICP. Screen includes: Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn, Mo, Ni, P, K, Se, Ag, Na, Sr, Tl, Sn, Ti, V, Zn

Screen for metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

Screen for metals by ICP. Screen includes: Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn

Screen for metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

1 Metal by ICP

1 individual metal by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

1 Metal by ICP

1 individual metal by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

2 Metals by ICP

2 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

2 Metals by ICP

2 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

3 Metals by ICP

3 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

3 Metals by ICP

3 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

4 Metals by ICP

4 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

4 Metals by ICP

4 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

7 Metals by ICP

7 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

7 Metals by ICP

7 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

12 Metals by ICP

12 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma

200.7

12 Metals by ICP

12 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma

6010D

Screen for metals by ICP/MS. Screen includes: Al, Sb, As, Ba, Be, Cd, Cr, Co, Cu, Pb, Mn, Mo, Ni, Se, Ag, Tl, Th, U, V and Zn

Screen for metals by USEPA Method 200.8 for trace elements by ICP/MS

200.8

Screen for metals by ICP/MS. Screen includes: Al, Sb, As, Ba, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Ni, K, Se, Ag, Na, Tl, V and Zn

Screen for metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

1 Metal by ICP-MS

1 individual metal by USEPA Method 200.8 for metals by ICP/MS

200.8

1 Metal by ICP-MS

1 individual metal by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

2 Metals by ICP-MS

2 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

2 Metals by ICP-MS

2 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

3 Metals by ICP-MS

3 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

3 Metals by ICP-MS

3 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

4 Metals by ICP-MS

4 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

4 Metals by ICP-MS

4 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

7 Metals by ICP-MS

7 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

7 Metals by ICP-MS

7 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

11 Metals by ICP-MS

11 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

11 Metals by ICP-MS

11 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

13 Metals by ICP-MS

13 individual metals by USEPA Method 200.8 for metals by ICP/MS

200.8

13 Metals by ICP-MS

13 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS

6020B

Preparation of water samples for dissolved analytes

USEPA Method 3005A for acid digestion of aqueous samples for total recoverable or dissolved metals, if not included in the method charge

3005A

Preparation of aqueous samples for total or recoverable metals

USEPA Method 3010A for acid digestion of aqueous samples and extracts total metals, if not included in the method charge

3010A

Preparation of solid samples for total metals

USEPA Method 3050B for acid digestion of sediments, sludges, and soils

3050B

Preparation of biological samples for total metal analysis

Preparation of biological samples for total metal analysis such as filleting fish or grinding samples. Preparation to be followed by one or more of the digestion procedures listed above.

Custom

Hexavalent chromium

USEPA Method 218.6 for hexavalent chromium in drinking water, natural surface water or groundwater, or wastewater effluents by ion chromatography

218.6

Hexavalent chromium

USEPA Method 7196A (SW-846) determination of hexavalent chromium (colorimetric)

7196A

Mercury in water

USEPA Method 245.1 for mercury in water by cold-vapor atomic absorption spectrometry

245.1

Mercury in water

USEPA Method 7470A (SW-846) determination of mercury in liquid waste (manual cold-vapor technique)

7470A

Mercury in solids (sediments, sludges, or soil)

USEPA Method 245.1 for mercury in solids (sediments, sludges, or soil) samples

245.1

Mercury in solids (sediments, sludges, or soil)

USEPA Method 7470A (SW-846) determination of mercury in in solids (sediments, sludges, or soil) samples

7470A

Mercury by cold vapor atomic fluorescence spectrometry

Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry

1631E

Mercury in tissue, low-level

1631E

Acidity

Acidity by titration

305.1/ 2310B

IC anions (Br, Cl, F, NO3, NO2, PO4-P, SO4)

USEPA Method 300.1 for anions by ion chromatography (IC), basic screen: Br, Cl, F, NO3, NO2, PO4-P, SO4

300.1

IC anions (Cl, F, Br, NO3, NO2, PO4, SO4)

USEPA Method 9056A (SW-846) for anions by ion chromatography (IC), basic screen: Cl, F, Br, NO3, NO2, PO4, SO4

9056A

Inividiual anion

1 individual anion by USEPA Method 300.1 for anions by ion chromatography (IC), basic screen: Br, Cl, F, NO3, NO2, PO4-P, SO4

300.1

Bromide, low-level

USEPA Method 300.1 for Bromide by ion chromatography (IC), low-level

300.1

Inividiual anion

1 individual anion by USEPA Method 9056A (SW-846) for anions by ion chromatography (IC), basic screen: Cl, F, Br, NO3, NO2, PO4, SO4

9056A

Prep of solids for anions

Sample prep of solids/leachate for anion analysis

Abestos

Determination of asbestos structures over 10um in length in drinking water

100.2

Chemical oxygen on demand (COD)

The Determination of COD by Semi-Automated Colorimetry

410.4

Coliform, fecal

Thermotolerant (Fecal) Coliform Membrane Filter

9222D

Coliform, total

Standard Total Coliform Membrane Filter

9222B

Cyanide, amenable to chlorination (water)

Cyanide, amenable to chlorination

SM 4500-CN-G or USEPA 9012B

Cyanide, available (water)

UESPA method OIA-1677 or ASTM D6888 for available cyanide by ligand exchange and flow injection analysis

USEPA OIA-1677 or ASTM D6888

Cyanide, total

Colorimetric Method for Cyanide in Distillate

SM 4500-CN-E

Cyanide, weak acid dissociable

Weak Acid Dissociable Cyanide

SM 4500-CN-I

Hardness by calculation

Hardness in Water by Calculation

SM 2340B

Ammonia

Determination of ammonia nitrogen by semi-automated colorimetry

350.1

Nitrogen, Ammonia, low-level (LL)4

Determination of ammonia nitrogen low-level (LL)4

350.1 LL

Nitrogen, total kjeldahl

Determination of Total Kjeldahl Nitrogen by Semi-Automated Colorimetry

351.2

Nitrogen, nitrite

Nitrogen, nitrite - Spectrophotometric

354.1

Nitrite (only)

Determination of Nitrate-Nitrite Nitrogen by Automated Colorimetry

353.2

Nitrogen, nitrate

Automated Hydrazine Reduction Method

SM 4500-NO3-H

Nitrate plus nitrite

Determination of Nitrate-Nitrite Nitrogen by Automated Colorimetry

353.2

Nitrogen, nitrate plus nitrite, low-level (LL)4

353.2 LL

Total nitrogen by calculation

USEPA Methods 351.2 and 353.2 for total nitrogen by calculation (TKN plus nitrate/nitrite)

351.2 or 353.2

Dissolved organic carbon

Determination of Total Organic Carbon and Specific UV Absorbance at 254 nm in Source Water and Drinking Water

415.3

Total organic carbon (high-temp combustion)

Determination of total organic carbon (TOC) from water and wastewater by a high-temperature combustion method

SM 5310B

Total organic carbon

Determination of total organic carbon by combustion or oxidation

415.1

Total organic carbon

Determine the concentration of organic carbon in ground water, surface and saline waters, and domestic and industrial wastes (SW-846)

9060A

Total organic carbon

Determination of Total Organic Carbon in solids and semi solids

Lloyd Kahn

Total organic carbon

Determining low concentrations of organic carbon in soils using dichromate oxidation method

Walkley-Black

Total inorganic carbon (TIC)

Total inorganic carbon (TIC) in water

9060A

Inorganic carbon, dissolved (DIC)

SM 5310B

Total organic halides (TOX)

Determines Total Organic Halides (TOX) as chloride in drinking water and ground waters

9020B

Orthophosphate, low-level

USEPA Method 365.1 for orthophosphate by semi-automated colorimetry–low-level

365.1 LL

Orthophosphate

orthophosphate by colorimetry

365.3

Oxygen, dissolved

360.1

Particulate carbon (PC) & particulate nitrogen (PN) [analysis price includes glass or membrane fiber filter]

Determination of carbon and nitrogen in sediments and particulatesof estuarine/coastal waters using elemental analysis

440

pH of aqueous samples

USEPA method 9040C (SW-846) for pH in water by electronic measurement

9040C

pH of aqueous samples

pH measurement in water by potentiometry using a standard hydrogen electrode

SM 4500-HB

pH of solid samples

USEPA 9045D (SW-846) for pH in soil and wastewater

9045D

Total phenols

Determination of Total Recoverable Phenolics by Semi-Automated Colorimetry

420.4

Total phenols

USEPA 9066 (SW-846) for phenolics

9066

Phosphorus, low-level

USEPA Method 365.1 for phosphorus by semi-automated colorimetry, low-level

365.1 LL

Total phosphorus

Phosphorus by Automated Ascorbic Acid Reduction

SM 4500-PF

Residue, total (total solids)

Total Residue by Drying Oven

160.3

Volatile suspended solids

Volatile Residue by Muffle Furnace

160.4

Settleable solids

Determination Settleable Matter in Water Using an Imhoff cone

160.5

Specific conductance/Conductivity

USEPA method 9050A (SW-846) for specific conductance

9050A

Sulfide

Determination of sulfide by titrimetry

376.1

Sulfide

USEPA method 9030B (SW-846) for acid-soluble and acid-insoluble sulfides: distillation

9030B

Turbidity

Turbidity by nephelometry

180.1

VOCs by GC/MS

USEPA method 8260C (SW-846) for volatile organic compounds by gas chromatography-mass spectrometry (GC/MS) with library search up to ten (10) tentatively identified compounds (TICs) upon request; target analytes include CLP target list plus methyl tert-butyl ether and cis- and trans-1,2-dischloroethene

8260C

VOCs by GC/MS (7 or fewer analytes)

USEPA method 8260C (SW-846) for volatile organic compounds by gas chromatography-mass spectrometry (GC/MS) for seven (7) or fewer analytes

8260C

Purgeable VOCs by GC/MS for wastewater

USEPA method 624 for purgeable volatile organic compounds, with library search up to ten (10) tentatively identified compounds (TICs) upon request

624

Oxygenates including ethers: DIPE, ETBE, MTBE, TAME and alcohols: methanol, ethanol, and t-butanol (TBA)

8260C

Aromatic and halogenated volatiles by GC

USEPA method 8021B (SW-846) for solids for aromatic and halogenated volatiles by gas chromatography using photoionization and/or electrolytic conductivity detectors

8021B

100

1,2,3-Trichloropropane, low-level: RL < 0.005 ug/L

1625C

101

SVOCs by GC/MS

USEPA method 8270E (SW-846) for semivolatile organic compounds by gas chromatography/mass spectrometry, with library search of up to 15 tentatively identified compounds (TICs)

8270E

102

Sample prep of tissue samples for SVOC analyses

Preparation of biological samples for semivolatile organics analysis such as filleting fish or grinding samples.

103

1,4-dioxane by GC/MS SIM, low-level

USEPA method 8260 SIM (SW_846) for low-level 1,4-dioxane by gas chromatography/mass spectrometry (RLs<2.0 µg/L)

8260 SIM

104

N-Nitrosodimethylamine (NDMA), low-level

Determination of N-Nitrosodimethylamine (NDMA) by GC/MS, low-level

1625

105

NDMA by GC/CI/MS/MS

Determination of Nitrosamines in drinking water by GC/CI/MS/MS

521

106

Organochlorine pesticides by GC

USEPA method 8081B (SW-846) for organochlorine pesticides by gas chromatography with electron-capture detector

8081B

107

Polychlorinated biphenyls (PCBs) by GC

USEPA method 8082A (SW-846) for polychlorinated biphenyls (PCBs) by gas chromatograhpy

8082A

108

Polychlorinated biphenyls (PCBs) by GC, low-level

USEPA method 8082A (SW-846) for polychlorinated biphenyls (PCBs) by gas chromatograhpy, LL

8082A

109

Organochlorine pesticides and PCBs by GC

Determination of Organochlorine Pesticides in municipal and industrial wastewater by gas chromatography

608.1

110

Organophosphorus pesticides by GC

USEPA method 8141B (SW-846) for organophosphorus pesticides by gas chromatograpy

8141B

111

Chlorinated herbicides by GC

USEPA method 8151A (SW-846) for chlorinated herbicides by GC using methylation or pentafluorobenzylation derivatization

8151A

112

PAHs in water by HPLC

USEPA method 8310 (SW-846) for polynuclear aromatic hydrocarbons (PAHs) by HPLC

8310

113

PAHs in soil or water, low-level, by GC/MS SIM

USEPA method 8270 SIM (SW-846) for polynuclear aromatic hydrocarbons (PAHs) in soil and water by GC/MS SIM

8270E SIM LL

114

Gasoline-range organics (GRO), C6-C10 using GC-FID

USEPA method 8015B (SW-846) for nonhalogenated (gasoline-range) organics using GC/FID – C6 to C10

8015D

115

Diesel-range organics (DRO), C10-C28 using GC-FID

USEPA method 8015D (SW-846) for nonhalogenated organics using GC/FID – C10 to C28

8015D

116

Motor-oil-range organics (MRO), C28-C36 using GC-FID

USEPA method 8015D (SW-846) for nonhalogenated organics using GC/FID – C28 to C36

8015D

117

Dispersants of interest for oil spills / glycols by GC-FID

USEPA method 8015D (SW-846) with modifications for detection of dispersants of interest for oil spills (glycols) by gas chromatrography and flame-ionization detection

8015D with modifications

118

Dissolved gases (methane, ethane, and ethene) in headspace

Method RSK 175 for dissolved gases (methane, ethane, and ethene) in drinking water by purge and trap headspace analysis

RSK-175

119

Propane

RSK-175

120

Dissolved gases (C1–C6) in aqueous samples by headspace analysis, with isotopic analysis of methane (if present)

USEPA Method RSK 175 (modified) for dissolved gases (C1–C6) in drinking water by purge and trap headspace analysis, including isotopic analysis of methane if present. [If methane is not present, the isotopic analysis will not be performed; see next row]

RSK-175 modified

121

Dissolved gases (C1–C6) in aqueous samples by headspace analysis (compositional analysis only)

USEPA Method RSK 175 (modified) for dissolved gases (C1–C6) in drinking water by purge and trap headspace analysis (compositional analysis only).

RSK-175 modified

122

GRO plus benzene, toluene, ethylbenzene, and xylene (BTEX compounds) by GC/PID-FID

8015D or 8021B

123

n-Hexane-extractable material (oil and grease) in aqueous samples

USEPA method 1664B for n-hexane-extractable material (oil and grease) in aqueous samples by extraction and gravimetry

1664B

124

n-Hexane-extractable material (total petroleum hydrocarbons) in aqueous samples

USEPA method 1664B for n-hexane-extractable material (total petroleum hydrocarbons) in aqueous samples by extraction and gravimetry

1664B

125

n-Hexane-extractable material (total petroleum hydrocarbons) in sediment or solids

USEPA method 9071B (SW-846) n-hexane-extractable material (total petroleum hydrocarbons) in sludge, sediment, and solids samples

9071B

126

Methylene-blue-active substances (MBAS) in aqueous samples

USEPA method 425.1 for surfactants by colorimetry

425.1

127

Surfactants in soil

USEPA method 425.1 for surfactants in soil by colorimetry

425.1

128

Volatile Fatty Acids (metabolic acids) by IC: Acetic Acid, Butyric Acid, Formic Acid, Lactic Acid, Propionic Acid, Pyruvic Acid

Custom

129

Volatile organic compounds (VOCs) with library search up to 10 tentatively identified compounds (TICs) from 40 CFR part 264, ground-water monitoring list

Custom

130

SVOCs by GC-MS in aqueous samples

USEPA method 625.1 for Base/Neutrals and Acids by GC/MS in aqueous samples from 40 CFR part 264 groundwater monitoring list, with library search up to 20 tentatively identified compounds (TICs) upon request

625.1

131

Pesticides from 40 CFR part 264, ground-water monitoring list

Custom

132

Polychlorinated biphenyls (Arochlors) from 40 CFR part 264, ground-water monitoring list

Custom

133

Herbicides from 40 CFR part 264, ground-water monitoring list

Custom

134

Dioxins/Furans from 40 CFR part 264, ground-water monitoring list

Custom

135

Alumina cleanup

USEPA method 3610B (SW_846) Alumina cleanup

3610B

136

Florisil column clean-up for pesticide analysis of biological samples

3620A

137

Gel permeation column (GPC) clean-up for organic analysis of biological samples

3640A

138

Silica gel cleanup

3630C

139

Sulfur cleanup

3660B

140

Special closed system sample container (Encore) for volatile organics analysis of solid samples

Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples

5035

141

2,3,7,8-tetrachlorodibenzo-p-dioxin (only) by HRGC/LRMS

USEPA Method 8280B for 2,3,7,8-tetrachlorodibenzo-p-dioxin (only) by high-resolution gas chromatography with low-resolution mass spectrometry (HRGC/LRMS)

8280B

142

Polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by HRGC/HRMS

USEPA method 8290A (SW-846) for polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS)

8290A

143

Dioxins and furans by isotope-dilution HRGC/HRMS

Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS

1613B

144

2,3,7,8-TCDD only (screening test)

2,3,7,8-TCDD only (drinking water screen samples)

625.1

145

2,3,7,8-TCDD only (municipal and industrial discharge)

Determination of 2,3,7,8-TCDD in municipal and industrial discharge by GC/MS

613

146

PCB congeners by HRGC/HRMS (WHO list: 77, 81, 105, 114, 118, 123, 126, 156, 157, 167, 169, 170, 180, and 189)

USEPA Method 1668C for polychlorinated biphenyl (PCB) congeners designated as toxic by the World Health Organization (77, 81, 105, 114, 118, 123, 126, 156, 157, 167, 169, 170, 180, and 189) by high-resolution gas chromatography with high-resolution mass spectrometry (HRGC/HRMS)

1668C

147

PCB congeners by HRGC/HRMS (209 congeners)

USEPA Method 1668C for 209 polychlorinated biphenyl (PCB) congeners by high-resolution gas chromatography with high-resolution mass spectrometry (HRGC/HRMS)

1668C

148

BDEs (flame retardants) by HRGC/HRMS

USEPA method 1614A Brominated Diphenyl Ethers (BDEs) in water, soil, sediment, and tissue by HRGC/HRMS

1614A

149

Nitroaromatics, Nitramines, and Nitrate Esters (Explosives)

USEPA method 8330B (SW-846)for nitroaromatics, nitramines, and nitrate esters by High Performance Liquid Chromatography (HPLC)

8330B

150

Nitroaromatics, Nitramines, and Nitrate Esters (Explosives) in solids

USEPA method 8330B (SW-846)for nitroaromatics, nitramines, and nitrate esters in solids by High Performance Liquid Chromatography (HPLC)

8330B

151

Solvent-extractable nonvolatiles by HPLC (azo dyes, organophosphorus compounds, tris(2,3-dibromopropyl)phosphate, carbamates, and chlorinated phenoxyacids and their esters, etc.)

USEPA method 8321B (SW-846) for solvent-extractable nonvolatile compounds in solids or aqueous samples by High-Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) detection

8321B

152

Organophosphates

USEPA method 8321B (SW-846) for organophosphates in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection

8321B

153

Chlorinated herbacides

USEPA method 8321B (SW-846) for chlorinated herbacides in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection

8321B

154

Tebuthiuron and Bromacil

USEPA method 8321B (SW-846) for Tebuthiuron and Bromacil in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection

8321B

155

Perchlorate - aqueous

Determination of perchlorate in aqueous samples using Ion Chromatography

314.2

156

Perchlorate - solids

314

157

Perchlorate in aqueous samples by Inline Column Concentration/Matrix Elimination IC

Determination of perchlorate in aqueous samples using Inline Column Concentration/Matrix Elimination Ion Chromatography With Suppressed Conductivity Detection

314.1

158

Perchlorate in aqueous samples by LC-EI-MS

Determination of perchlorate in aqueous samples by Liquid Chromatography Electrospray Ionization Mass Specxtrometry (LC/ESI/MS)

331.0

159

Perchlorate in aqueous samples by IC-ESI/MS

Determination of perchlorate in aqueous samples by Ion Chromatography with Suppressed Conductivity and Electrospray Ionization Mass Spectometry

332.0

160

Perchlorate by LC/MS/MS

DoD SOP

161

Perchlorate in solids or aqueous samples by HPLC-ESI-MS or HPLC-ESI-MS/MS

USEPA method 6850 (SW-846) for perchlorate in water, soils and solid wastes using high performance liquid chromatography with electrospray-ionization (ESI) mass spectrometry or ESI with tandem mass spectrometry

6850

162

Perchlorate by IC/MS/MS

DoD SOP

163

Perchlorate in solids or aqueous samples by IC-ESI-MS or IC-ESI-MS/MS

USEPA method 6860 (SW-846) for perchlorate in water, soils and solid wastes using ion chromatography with electrospray-ionization (ESI) mass spectrometry or ESI with tandem mass spectrometry

6860

164

EDB,DCBP, and 123TCP in Water Using GCECD

1,2-Dibromoethane (EDB), 1,2-Dibromo-3-Chloro-Propane (DCBP), and 1,2,3-Trichloropropane (123TCP) in water by Microextraction and Gas Chromatography

504.1

165

Chlorinated Pesticides in Water Using GCECD

Determination of Chlorinated Pesticides in Water by Gas Chromatography with an Electron Capture Detector

508.1

166

Chlorinated herbicides in water by GC-ECD

Determination of chlorinated acids in aqueous samples by Liquid-liquid Microextraction Derivatization and Fast Gas Chromatography With Electron Capture Detection

515.4

167

Purgeable VOCs by GC-MS for drinking water

USEPA Method 524.2 for purgeable volatile organic compounds by gas chromatography-mass spectrometry (GC/MS)

524.2

168

Purgeable VOCs by GC-MS for drinking water–THMs only

USEPA Method 524.2 for purgeable volatile organic compounds (total trihalomethanes, only) by gas chromatography-mass spectrometry (GC/MS)

524.2

169

Semivolatile organic compounds by GC/MS

Determination of organic compounds in aqueous samples by liquid-solid extraction and capillary column GC/MS

525.2

170

Carbamates by HPLC

Determination of N-methylcarbamoyloximes and N-methylcarbamates (carbamates) in water by direct aqueous injection by HPLC with postcolumn derivization

531.2

171

Glyphosate and AMPA by HPLC

USEPA method 547 for glyphosate and aminomethylphosphonic acid (AMPA) in drinking water by direct-aqueous-injection and high performance liquid chromatography (HPLC) with post-column derivatization and fluorescence detection

547

172

Endothall in Water Using GCMS

Determination of Endothall in aqueous samples by Ion-Exchange Extraction, Acidic Methanol Methylation, and Gas Chromatography/Mass Spectrometry

548.1

173

Diquat and paraquat by HPLC

Determination of diquat and paraquat in aqueous samples by liquid-solid extraction and HPLC with UV detection

549.2

174

Haloacetic acids and Dalapon by GC-ECD

Determination of Haloacetic Acids and Dalapon in aqueous samples by Liquid-Liquid Microextraction, Derivatization, and Gas Chromatography with Electron Capture Detection

552.3

175

TCLP prep and extraction

USEPA methods 1311 (SW-846) for the toxicity characteristic leaching procedure (TCLP) and sample preparation

1311

176

SPLP prep and extraction

USEPA methods 1312 (SW-846) for the Synthetic precipitation leaching procedure (SPLP) and sample preparation

1312

177

Moisture content of sediment or soil

ASTM D2216-19 standard test method for laboratory determination of water (moisture) content of soil and rock by mass significance

D2216-19

178

Measurement of Hydraulic Conductivity of Saturated Porous Materials Using a Flexible Wall Permeameter

D5084

179

Density of Soils in Place by the Drive-Cylinder Method

D2937

180

Cyanide, total and amenable

USEPA method 9012B (SW-846) for total and amenable cyanide in distillates of aqueous samples by colorimetric method

9012B

181

Cyanide, free by microdiffusion

Standard Method D4282-89 for determination of free cyanide in water and wastewater by microdiffusion

D4282-89

182

Sulfide

ulfide (Colorimetric, Methylene Blue)

9034/376.2

183

Ferrous iron (dissolved) in aqueous samples

Standard Method 3500-Fe for dissolved ferrous and ferric iron in aqueous samples

SM 3500 Fe

184

Ferric iron (dissolved) in aqueous samples

Standard Method 3500-Fe for dissolved ferrous and ferric iron in aqueous samples

SM 3500 Fe

185

Alkalinity (total only)

Standard Method 2320B for alkalinty (total only) by titration

SM 2320B

186

Alkalinity (total, carbonate, bicarbonate, and hydroxide)

SM 2320B

187

Biochemical oxygen demand (BOD) 5-Day

USEPA method 405.1 or SM 5210B for 5-day biological oxygen demand (BOD)

405.1 or SM 5210B

188

BOD 30-day

405.1

189

Carbonaceous Biochemical Oxygen Demand (CBOD) 5-day

USEPA method 405.1 or SM 5210B for 5-day carbonaceous biological oxygen demand (CBOD)

405.1 or 5210B

190

Ultimate CBOD

405.1

191

Color in water

Color in Water by Visual Comparison Method

SM 2120B

192

Hardness by EDTA titration

Standard Method 2340C for hardness by EDTA titration

SM 2340C

193

Oxygen, dissolved

Oxygen by Membrane Electrode Method

SM 4500-O G

194

Residue, filterable (total dissolved solids: TDS)

Standard Method 2540C Total Dissolved Solids Dried at 180oC

SM 2540C

195

Residue, non-filterable (total suspended solids: TSS)

Standard Method 2540D for Total Suspended Solids Dried at 103-105oC

SM 2540D

196

Sulfide, iodometric method

Sulfide, iodometric titration (water)

SM 4500-S F

197

VOCs in air

USEPA method TO-15 for volatile organic compounds in air by gas chromatography and mass spectrometry

TO-15

198

VOCs in air

TO-15 SIM scan

TO-15 SUP

199

PCB congeners in air by HRGC/HRMS

USEPA Method 1668 (modified) for 19 target PCB congeners in air (PUF or XAD) by HRGC/HRMS with no totals

1668 mod

200

PAHs in ambient air by GC/MS

USEPA method TO-13A for polynuclear aromatic hydrocarbons (PAHs) in ambient air by GC/MS

TO-13A

201

Dioxins and furans in air (PUF) by HRGC/HRMS

USEPA method 8290A (SW-846) for polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by high-resolution gas chromatography/high-resolution mass spectrometry in air (PUF)

8290A

202

Metals in ambient air

USEPA method 6020B (SW-846) for metals in ambient air by inductively coupled plasma with mass spectrometry

6020B

203

Total suspended particulate matter in air

Compendium Method IO-2.1 for total suspended particulate matter and PM10 in ambient air using high-volume sampler

IO-2.1

204

Clean-up of client-supplied SUMMA canister

205

Certification of cleanliness of SUMMA canister

206

Preparation and QC check of PUF or XAD media for air sampling

207

Corrosivity, RCRA

Corrosivity Toward Steel (SW-846), RCRA

1110A

208

Ignitability Characteristic (Setaflash closed cup method), RCRA

USEPA method 1020C (SW-846) for Standard Test Methods for Flash Point by Setaflash (Small Scale) Closed-Cup Apparatus, RCRA

1020C

209

Methyl mercury in aqueous samples

USPEA method 1630 for methyl mercury in water by distillation, aqueous ethylation, purge and trap, and cold vapor atomic fluorescence spectrometry

1630

210

Arsenic III

Arsenic in aqueous samples and extracts by anodic stripping voltammetry (ASV)

7063

211

Arsenic V

Arsenic in aqueous samples and extracts by anodic stripping voltammetry (ASV)

7063

212

Sulfite

Sulfite by Titrimetry

377.1

213

Percent lipids in tissue samples

Determination of percent lipids in tissue samples by accelerated solvent extractor

214

Pesticides and PCBs in Water GC-ECD

Analysis of Organochlorine Pesticides and Commercial Polychlorinated Biphenyl (PCB) Products in Water by Microextraction and Gas Chromatography

505

215

Mercury in Solid or Semisolid Wastes

Mercury in Solid or Semisolid Wastes (Manual Cold-Vapor Technique)

7471B

216

Ignitability 1010

USEPA method 010B (SW-846) for Flash Point by Pensky-Martens Closed Cup Tester

1010B

217

Hydrogen cyanide

SW-846, Chapter 7

218

Hydrogen sulfide

SW-846, Chapter 7

219

Specific Gravity of Soils

Standard Test Method for Specific Gravity of Soil Solids by Gas Pycnometer

SM D5550

220

Amount of Materials in Soils Finer than No. 200 (75um) Sieve

D1140

221

Permeability of Granular Soils (sands/ gravels)--constant or falling head

D2434

222

Moisture, ash, and organic matter of peats and other organic soils

ASTM D2974 standard test method for moisture, ash, and organic matter of peat and other organic soils used to determine the percent organic matter within soil and sediment

D2974

223

Liquid Limit, Plastic Limit, and Plasticity Index of Soils (Atterburg Limits)

D4318

224

VOCs in Ambient Air using Tenax adsorption tubes and by GC/MS

TO-01

225

VOCs in ambient air by GC-FID

USEPA Method TO-3 for hydrocarbons and oxygenated hydrocarbons, such as methanol and MTBE, in ambient air and gas samples by gas chromatograph (GC) flame ionization detector (FID)

TO-3

226

BTEX and TPH (only) in ambient air by GC-FID

USEPA Method TO-3 or Air-Phase Petroleum hydrocarbon (APH) method for BTEX and total petroleum hydrocarbons (only), in ambient air and gas samples (SUMMA canister) by gas chromatograph (GC) flame ionization detector (FID)

TO-3 or APH

227

Organopesticides and PCBs in Ambient Air by GC/FID

Determination of pesticides and Polychlorinated Biphenyls (PCBs) in ambient air using high volume polyurethane foam (PUF) sampling followed by Gas Chromatographic/Multi-Detector Detection (GC/MD)

TO-4A

228

PAHs by GC/MS -- selective ion monitoring (SIM) [matrix: PUF/XAD]

TO-13A SIM LL

229

VOCs using SUMMA canister sampling and by GC/MS

TO-14A

230

Full list of SVOCs in Ambient Air by GC/MS

TO-13A

231

PAHs in Ambient Air by GC/MS and high resolution liquid chromatography

TO-13A

232

PAHs in Ambient Air by GC/SIM LL

TO-13A LL

233

PCB congeners in Ambient Air with no totals

1668C

234

PCB congeners in Ambient Air with totals

1668C

235

VOCs in Ambient Air by GC/MS (short list) <10 compounds

TO-15

236

Pharmaceuticals and personal care products (PPCPs)

Pharmaceuticals and Personal Care Products in Water by HPLC/MS/MS

1694

237

Pharmaceuticals and personal care products (PPCPs)

Pharmaceuticals and Personal Care Products in Soil, Sediment, and Biosolids by HPLC/MS/MS

1694

238

Pharmaceuticals and Personal Care Products in Drinking Water

Determination of Pharmaceuticals and Personal Care Products in Drinking Water by Solid Phase Extraction and Liquid Chromatography Electrospray Ionization Tandem Mass Spectrometry

542

239

Vitamin E

Custom

240

Alkylated PAHs by isotopic-dilution GC/MS

USEPA method 8270E (SW-846) for alkylated PAHs by isotopic-dilution gas chromatography and mass spectrometry

8270E

241

IsoFlask

custom

242

PCNs (polychlorinated Naphthalenes)

Custom

243

Fixed gases by GC-TCD

ASTM D1946 for permanent gases in refinery samples using gas chromatography (GC) with a thermal conductivity detector (TCD)

D1946

244

Gaseous non-methane organic compounds

USEPA Method 25.1 for total gaseous nonmethane organic (TGNMO) compounds, as carbon

25.1

245

Sulfur, Total

Determination of Total Sulfur by UVF

D5453

246

Free Cyanide

USEPA method 9014 (SW-846) for cyanide in waters and extracts using titrimetric and manual spectrophotometric procedures

9014

247

Wound Glass Cannister Filters (4x2 1um)

Custom

248

Flat Filter charge - 100 filters

Custom

249

Pesticides in Water, Soil, Sediment, Biosolids, and Tissue by HRGC/HRMS

Determines organochlorine, organophosphorus, triazine, and pyrethroid pesticides in environmental samples by high resolution gas chromatography/high resolution mass spectrometry (HRGC/HRMS) using isotope dilution

1699

250

Tissue homoginization, >1500 grams

Custom

251

IsoTubes (25 tubes/box)

Custom

252

MG-2

253

Gamma Emitting Radionuclides in Drinking Water

Gamma Emitting Radionuclides in Water by Gamma Spectroscopy

901.1

254

Speciated Se: SeCN + MeSe(IV) + SeMet + Se(VI) + Se (IV) + Unk Se Sp + Total Diss

custom

255

Flutolanil and Alpha-BHC in water

Flutolanil and Alpha BHC in water

custom

256

Mestrione and Clopyralid in water

LC/MS/MS

257

Be-7 and Cesium-137

Gamma Spec

258

Steroids and Hormones in Water, Soil, Sediment, and Biosolids

Steroids and Hormones in Water, Soil, Sediment, and Biosolids by HRGC/HRMS

1698

259

Grain Size + Hydrometer

ASTM

260

Metsulfuron-methyl and Aminopyralid

Determination of Selected Organic Contaminants in Drinking Water by DAI-LC/MS/MS

EPA 538

261

NG-2

custom

262

Chemical Speciation of Arsenic in Water and Tissue

USEPA method 1632 for total inorganic arsenic, arsenite (As+3), arsenate (As+5), monomethylarsonate (MMA), and dimethylarsinate (DMA)

1632

263

Cation Exchange Capacity CEC

SW846 EPA9081

264

Anion Exchange Capacity AEC

New Zealand P Retention

265

Indaziflam, chlorsulfuron

Pesticides by LC/MS/MS

custom

266

Aminopyralid

Pesticides by LC/MS/MS

custom

267

6PPD

6PPD-quinone

EPA 1634

268

Data Management 1hr

Data Management per hr

Custom

269

POCIS Extraction

Custom

270

Level 4 Data Package (per workorder)

271

Saturday arrival and analysis per work order

Saturday arrival and analysis per work order for short holding times

File details come from the government source that posted it. Updated Feb 9, 2024.