B08_Appendix_A_-_Pricing_Schedule.xlsx
XLSX spreadsheet 1 MB Posted
- Attached to
- GENERAL CHEMICAL ANALYTICAL SERVICES Federal contract opportunity
- Solicitation number
- 140G0224R0001
About this file
This document contains a pricing schedule appendix for a federal solicitation seeking general chemical analytical services. The solicitation is seeking pricing for over 100 different chemical analytical testing methods to be performed on samples of water, soil, sediment, waste and tissue. Tests include metals analysis by ICP and ICP-MS, anion analysis by ion chromatography, mercury analysis, cyanide testing, nutrient analysis and various wet chemistry methods. Sample preparation and digestion procedures are also included. Pricing is provided for each analytical method for a five year period with estimated annual quantities and unit pricing for the base year and each option year. The solicitation number is 140G0224R0001 and was issued by the Department of the Interior US Geological Survey Office of Acquisitions and Grants to obtain general chemical analytical services.
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Other files for this federal contract opportunity
| File | Type | Posted |
|---|---|---|
| B08_Appendix_E_-_ASR.pdf | ||
| B08_Appendix_B_-__EDD_Example.xlsx | XLSX spreadsheet | |
| Sol_140G0224R0001.pdf | ||
| B08_Appendix_C_Daily_Sample_Receipt_-_Example.xlsx | XLSX spreadsheet | |
| B08_Appendix_D_-_Methods_with_Reporting_Requirements.xlsx | XLSX spreadsheet |
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Gen Chem
| Line Item | Test | Description of Item | Method number(s) | EST. Annual QUANTITY | Unit Price Year 1 | Estimated Total Year 1 | Estimated Annual Quantities Year 2 | Unit Price | |||||
| Year 2 | Estimated Total Year 2 | Estimated Annual Quantities Year 3 | Unit Price | ||||||||||
| Year 3 | Estimated Total Year 3 | Estimated Annual Quantities Year 4 | Unit Price | ||||||||||
| Year 4 | Estimated Total Year 4 | Estimated Annual Quantities Year 5 | Unit Price | ||||||||||
| Year 5 | Estimated Total Year 5 | Estimated Quantities 6 month Extention (Qty = hafl of the annual est only) | Unit Price | ||||||||||
| 6 month Extention | Estimated Total 6-month extention | ||||||||||||
| 1 | Screen for metals by ICP. Screen includes: Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn, Mo, Ni, P, K, Se, Ag, Na, Sr, Tl, Sn, Ti, V, Zn | Screen for metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 166 | 166 | 166 | 166 | 166 | 83 | ||||
| 2 | Screen for metals by ICP. Screen includes: Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn | Screen for metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 3 | 1 Metal by ICP | 1 individual metal by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 4 | 1 Metal by ICP | 1 individual metal by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 5 | 2 Metals by ICP | 2 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 350 | 350 | 350 | 350 | 350 | 175 | ||||
| 6 | 2 Metals by ICP | 2 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 40 | 40 | 40 | 40 | 40 | 20 | ||||
| 7 | 3 Metals by ICP | 3 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 8 | 3 Metals by ICP | 3 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 9 | 4 Metals by ICP | 4 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 70 | 70 | 70 | 70 | 70 | 35 | ||||
| 10 | 4 Metals by ICP | 4 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 11 | 7 Metals by ICP | 7 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 12 | 7 Metals by ICP | 7 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 13 | 12 Metals by ICP | 12 individual metals by USEPA Method 200.7 for trace elements by inductively coupled plasma | 200.7 | 166 | 166 | 166 | 166 | 166 | 83 | ||||
| 14 | 12 Metals by ICP | 12 individual metals by USEPA Method 6010D (SW-846) for trace elements by inductively coupled plasma | 6010D | 40 | 40 | 40 | 40 | 40 | 20 | ||||
| 15 | Screen for metals by ICP/MS. Screen includes: Al, Sb, As, Ba, Be, Cd, Cr, Co, Cu, Pb, Mn, Mo, Ni, Se, Ag, Tl, Th, U, V and Zn | Screen for metals by USEPA Method 200.8 for trace elements by ICP/MS | 200.8 | 100 | 100 | 100 | 100 | 100 | 50 | ||||
| 16 | Screen for metals by ICP/MS. Screen includes: Al, Sb, As, Ba, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Ni, K, Se, Ag, Na, Tl, V and Zn | Screen for metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 20 | 20 | 20 | 20 | 40 | 10 | ||||
| 17 | 1 Metal by ICP-MS | 1 individual metal by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 160 | 160 | 160 | 160 | 160 | 80 | ||||
| 18 | 1 Metal by ICP-MS | 1 individual metal by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 19 | 2 Metals by ICP-MS | 2 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 200 | 200 | 200 | 200 | 200 | 100 | ||||
| 20 | 2 Metals by ICP-MS | 2 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 12 | 20 | 20 | 20 | 20 | 10 | ||||
| 21 | 3 Metals by ICP-MS | 3 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 12 | 12 | 12 | 12 | 12 | 6 | ||||
| 22 | 3 Metals by ICP-MS | 3 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 23 | 4 Metals by ICP-MS | 4 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 300 | 300 | 300 | 300 | 300 | 150 | ||||
| 24 | 4 Metals by ICP-MS | 4 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 25 | 7 Metals by ICP-MS | 7 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 12 | 12 | 12 | 12 | 12 | 6 | ||||
| 26 | 7 Metals by ICP-MS | 7 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 27 | 11 Metals by ICP-MS | 11 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 28 | 11 Metals by ICP-MS | 11 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 29 | 13 Metals by ICP-MS | 13 individual metals by USEPA Method 200.8 for metals by ICP/MS | 200.8 | 120 | 120 | 120 | 120 | 120 | 60 | ||||
| 30 | 13 Metals by ICP-MS | 13 individual metals by USEPA Method 6020B (SW-846) for trace elements by ICP/MS | 6020B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 31 | Preparation of water samples for dissolved analytes | USEPA Method 3005A for acid digestion of aqueous samples for total recoverable or dissolved metals, if not included in the method charge | 3005A | 160 | 160 | 160 | 160 | 160 | 80 | ||||
| 32 | Preparation of aqueous samples for total or recoverable metals | USEPA Method 3010A for acid digestion of aqueous samples and extracts total metals, if not included in the method charge | 3010A | 500 | 500 | 500 | 500 | 500 | 250 | ||||
| 33 | Preparation of solid samples for total metals | USEPA Method 3050B for acid digestion of sediments, sludges, and soils | 3050B | 150 | 150 | 150 | 150 | 150 | 75 | ||||
| 34 | Preparation of biological samples for total metal analysis | Preparation of biological samples for total metal analysis such as filleting fish or grinding samples. Preparation to be followed by one or more of the digestion procedures listed above. | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 35 | Hexavalent chromium | USEPA Method 218.6 for hexavalent chromium in drinking water, natural surface water or groundwater, or wastewater effluents by ion chromatography | 218.6 | 50 | 50 | 50 | 50 | 50 | 25 | ||||
| 36 | Hexavalent chromium | USEPA Method 7196A (SW-846) determination of hexavalent chromium (colorimetric) | 7196A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 37 | Mercury in water | USEPA Method 245.1 for mercury in water by cold-vapor atomic absorption spectrometry | 245.1 | 50 | 50 | 50 | 50 | 50 | 25 | ||||
| 38 | Mercury in water | USEPA Method 7470A (SW-846) determination of mercury in liquid waste (manual cold-vapor technique) | 7470A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 39 | Mercury in solids (sediments, sludges, or soil) | USEPA Method 245.1 for mercury in solids (sediments, sludges, or soil) samples | 245.1 | 200 | 200 | 200 | 200 | 200 | 100 | ||||
| 40 | Mercury in solids (sediments, sludges, or soil) | USEPA Method 7470A (SW-846) determination of mercury in in solids (sediments, sludges, or soil) samples | 7470A | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 41 | Mercury by cold vapor atomic fluorescence spectrometry | Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry | 1631E | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 42 | Mercury in tissue, low-level | Mercury in tissue, low-level | 1631E | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 43 | Acidity | Acidity by titration | 305.1/ 2310B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 44 | IC anions (Br, Cl, F, NO3, NO2, PO4-P, SO4) | USEPA Method 300.1 for anions by ion chromatography (IC), basic screen: Br, Cl, F, NO3, NO2, PO4-P, SO4 | 300.1 | 100 | 100 | 100 | 100 | 100 | 50 | ||||
| 45 | IC anions (Cl, F, Br, NO3, NO2, PO4, SO4) | USEPA Method 9056A (SW-846) for anions by ion chromatography (IC), basic screen: Cl, F, Br, NO3, NO2, PO4, SO4 | 9056A | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 46 | Inividiual anion | 1 individual anion by USEPA Method 300.1 for anions by ion chromatography (IC), basic screen: Br, Cl, F, NO3, NO2, PO4-P, SO4 | 300.1 | 500 | 500 | 500 | 500 | 500 | 250 | ||||
| 47 | Bromide, low-level | USEPA Method 300.1 for Bromide by ion chromatography (IC), low-level | 300.1 | 100 | 100 | 100 | 100 | 100 | 50 | ||||
| 48 | Inividiual anion | 1 individual anion by USEPA Method 9056A (SW-846) for anions by ion chromatography (IC), basic screen: Cl, F, Br, NO3, NO2, PO4, SO4 | 9056A | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 49 | Prep of solids for anions | Sample prep of solids/leachate for anion analysis | NA | 40 | 40 | 40 | 40 | 40 | 20 | ||||
| 50 | Abestos | Determination of asbestos structures over 10um in length in drinking water | 100.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 51 | Chemical oxygen on demand (COD) | The Determination of COD by Semi-Automated Colorimetry | 410.4 | 210 | 210 | 210 | 210 | 210 | 105 | ||||
| 52 | Coliform, fecal | Thermotolerant (Fecal) Coliform Membrane Filter | 9222D | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 53 | Coliform, total | Standard Total Coliform Membrane Filter | 9222B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 54 | Cyanide, amenable to chlorination (water) | Cyanide, amenable to chlorination | SM 4500-CN-G or USEPA 9012B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 55 | Cyanide, available (water) | UESPA method OIA-1677 or ASTM D6888 for available cyanide by ligand exchange and flow injection analysis | USEPA OIA-1677 or ASTM D6888 | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 56 | Cyanide, total | Colorimetric Method for Cyanide in Distillate | SM 4500-CN-E | 200 | 200 | 200 | 200 | 200 | 100 | ||||
| 57 | Cyanide, weak acid dissociable | Weak Acid Dissociable Cyanide | SM 4500-CN-I | 22 | 22 | 22 | 22 | 22 | 11 | ||||
| 58 | Hardness by calculation | Hardness in Water by Calculation | SM 2340B | 304 | 304 | 304 | 304 | 304 | 152 | ||||
| 59 | Ammonia | Determination of ammonia nitrogen by semi-automated colorimetry | 350.1 | 350 | 350 | 350 | 350 | 350 | 175 | ||||
| 60 | Nitrogen, Ammonia, low-level (LL)4 | Determination of ammonia nitrogen low-level (LL)4 | 350.1 LL | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 61 | Nitrogen, total kjeldahl | Determination of Total Kjeldahl Nitrogen by Semi-Automated Colorimetry | 351.2 | 310 | 310 | 310 | 310 | 310 | 155 | ||||
| 62 | Nitrogen, nitrite | Nitrogen, nitrite - Spectrophotometric | 354.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 63 | Nitrite (only) | Determination of Nitrate-Nitrite Nitrogen by Automated Colorimetry | 353.2 | 450 | 450 | 450 | 450 | 450 | 225 | ||||
| 64 | Nitrogen, nitrate | Automated Hydrazine Reduction Method | SM 4500-NO3-H | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 65 | Nitrate plus nitrite | Determination of Nitrate-Nitrite Nitrogen by Automated Colorimetry | 353.2 | 500 | 500 | 500 | 500 | 500 | 250 | ||||
| 66 | Nitrogen, nitrate plus nitrite, low-level (LL)4 | Nitrogen, nitrate plus nitrite, low-level (LL)4 | 353.2 LL | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 67 | Total nitrogen by calculation | USEPA Methods 351.2 and 353.2 for total nitrogen by calculation (TKN plus nitrate/nitrite) | 351.2 or 353.2 | 164 | 164 | 164 | 164 | 164 | 82 | ||||
| 68 | Dissolved organic carbon | Determination of Total Organic Carbon and Specific UV Absorbance at 254 nm in Source Water and Drinking Water | 415.3 | 28 | 28 | 28 | 28 | 28 | 14 | ||||
| 69 | Total organic carbon (high-temp combustion) | Determination of total organic carbon (TOC) from water and wastewater by a high-temperature combustion method | SM 5310B | 298 | 298 | 298 | 298 | 298 | 149 | ||||
| 70 | Total organic carbon | Determination of total organic carbon by combustion or oxidation | 415.1 | 176 | 176 | 176 | 176 | 176 | 88 | ||||
| 71 | Total organic carbon | Determine the concentration of organic carbon in ground water, surface and saline waters, and domestic and industrial wastes (SW-846) | 9060A | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 72 | Total organic carbon | Determination of Total Organic Carbon in solids and semi solids | Lloyd Kahn | 50 | 50 | 50 | 50 | 50 | 25 | ||||
| 73 | Total organic carbon | Determining low concentrations of organic carbon in soils using dichromate oxidation method | Walkley-Black | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 74 | Total inorganic carbon (TIC) | Total inorganic carbon (TIC) in water | 9060A | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 75 | Inorganic carbon, dissolved (DIC) | Inorganic carbon, dissolved (DIC) | SM 5310B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 76 | Total organic halides (TOX) | Determines Total Organic Halides (TOX) as chloride in drinking water and ground waters | 9020B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 77 | Orthophosphate, low-level | USEPA Method 365.1 for orthophosphate by semi-automated colorimetry–low-level | 365.1 LL | 308 | 308 | 308 | 308 | 308 | 154 | ||||
| 78 | Orthophosphate | orthophosphate by colorimetry | 365.3 | 300 | 300 | 300 | 300 | 300 | 150 | ||||
| 79 | Oxygen, dissolved | Oxygen, dissolved | 360.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 80 | Particulate carbon (PC) & particulate nitrogen (PN) [analysis price includes glass or membrane fiber filter] | Determination of carbon and nitrogen in sediments and particulatesof estuarine/coastal waters using elemental analysis | 440 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 81 | pH of aqueous samples | USEPA method 9040C (SW-846) for pH in water by electronic measurement | 9040C | 298 | 298 | 298 | 298 | 298 | 149 | ||||
| 82 | pH of aqueous samples | pH measurement in water by potentiometry using a standard hydrogen electrode | SM 4500-HB | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 83 | pH of solid samples | USEPA 9045D (SW-846) for pH in soil and wastewater | 9045D | 78 | 78 | 78 | 78 | 78 | 39 | ||||
| 84 | Total phenols | Determination of Total Recoverable Phenolics by Semi-Automated Colorimetry | 420.4 | 9 | 9 | 9 | 9 | 9 | 5 | ||||
| 85 | Total phenols | USEPA 9066 (SW-846) for phenolics | 9066 | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 86 | Phosphorus, low-level | USEPA Method 365.1 for phosphorus by semi-automated colorimetry, low-level | 365.1 LL | 315 | 315 | 315 | 315 | 315 | 158 | ||||
| 87 | Total phosphorus | Phosphorus by Automated Ascorbic Acid Reduction | SM 4500-PF | 216 | 216 | 216 | 216 | 216 | 108 | ||||
| 88 | Residue, total (total solids) | Total Residue by Drying Oven | 160.3 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 89 | Volatile suspended solids | Volatile Residue by Muffle Furnace | 160.4 | 180 | 180 | 180 | 180 | 180 | 90 | ||||
| 90 | Settleable solids | Determination Settleable Matter in Water Using an Imhoff cone | 160.5 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 91 | Specific conductance/Conductivity | USEPA method 9050A (SW-846) for specific conductance | 9050A | 358 | 358 | 358 | 358 | 358 | 179 | ||||
| 92 | Sulfide | Determination of sulfide by titrimetry | 376.1 | 22 | 22 | 22 | 22 | 22 | 11 | ||||
| 93 | Sulfide | USEPA method 9030B (SW-846) for acid-soluble and acid-insoluble sulfides: distillation | 9030B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 94 | Turbidity | Turbidity by nephelometry | 180.1 | 298 | 298 | 298 | 298 | 298 | 149 | ||||
| 95 | VOCs by GC/MS | USEPA method 8260C (SW-846) for volatile organic compounds by gas chromatography-mass spectrometry (GC/MS) with library search up to ten (10) tentatively identified compounds (TICs) upon request; target analytes include CLP target list plus methyl tert-butyl ether and cis- and trans-1,2-dischloroethene | 8260C | 194 | 194 | 194 | 194 | 194 | 97 | ||||
| 96 | VOCs by GC/MS (7 or fewer analytes) | USEPA method 8260C (SW-846) for volatile organic compounds by gas chromatography-mass spectrometry (GC/MS) for seven (7) or fewer analytes | 8260C | 61 | 61 | 61 | 61 | 61 | 31 | ||||
| 97 | Purgeable VOCs by GC/MS for wastewater | USEPA method 624 for purgeable volatile organic compounds, with library search up to ten (10) tentatively identified compounds (TICs) upon request | 624 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 98 | Oxygenates including ethers: DIPE, ETBE, MTBE, TAME and alcohols: methanol, ethanol, and t-butanol (TBA) | Oxygenates including ethers: DIPE, ETBE, MTBE, TAME and alcohols: methanol, ethanol, and t-butanol (TBA) | 8260C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 99 | Aromatic and halogenated volatiles by GC | USEPA method 8021B (SW-846) for solids for aromatic and halogenated volatiles by gas chromatography using photoionization and/or electrolytic conductivity detectors | 8021B | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 100 | 1,2,3-Trichloropropane, low-level: RL < 0.005 ug/L | 1,2,3-Trichloropropane, low-level: RL < 0.005 ug/L | 1625C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 101 | SVOCs by GC/MS | USEPA method 8270E (SW-846) for semivolatile organic compounds by gas chromatography/mass spectrometry, with library search of up to 15 tentatively identified compounds (TICs) | 8270E | 80 | 80 | 80 | 80 | 80 | 40 | ||||
| 102 | Sample prep of tissue samples for SVOC analyses | Preparation of biological samples for semivolatile organics analysis such as filleting fish or grinding samples. | NA | 200 | 200 | 200 | 200 | 200 | 100 | ||||
| 103 | 1,4-dioxane by GC/MS SIM, low-level | USEPA method 8260 SIM (SW_846) for low-level 1,4-dioxane by gas chromatography/mass spectrometry (RLs<2.0 µg/L) | 8260 SIM | 20 | 20 | 20 | 20 | 20 | 10 | ||||
| 104 | N-Nitrosodimethylamine (NDMA), low-level | Determination of N-Nitrosodimethylamine (NDMA) by GC/MS, low-level | 1625 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 105 | NDMA by GC/CI/MS/MS | Determination of Nitrosamines in drinking water by GC/CI/MS/MS | 521 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 106 | Organochlorine pesticides by GC | USEPA method 8081B (SW-846) for organochlorine pesticides by gas chromatography with electron-capture detector | 8081B | 38 | 38 | 38 | 38 | 38 | 19 | ||||
| 107 | Polychlorinated biphenyls (PCBs) by GC | USEPA method 8082A (SW-846) for polychlorinated biphenyls (PCBs) by gas chromatograhpy | 8082A | 68 | 68 | 68 | 68 | 68 | 34 | ||||
| 108 | Polychlorinated biphenyls (PCBs) by GC, low-level | USEPA method 8082A (SW-846) for polychlorinated biphenyls (PCBs) by gas chromatograhpy, LL | 8082A | 88 | 88 | 88 | 88 | 88 | 44 | ||||
| 109 | Organochlorine pesticides and PCBs by GC | Determination of Organochlorine Pesticides in municipal and industrial wastewater by gas chromatography | 608.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 110 | Organophosphorus pesticides by GC | USEPA method 8141B (SW-846) for organophosphorus pesticides by gas chromatograpy | 8141B | 280 | 280 | 280 | 280 | 280 | 140 | ||||
| 111 | Chlorinated herbicides by GC | USEPA method 8151A (SW-846) for chlorinated herbicides by GC using methylation or pentafluorobenzylation derivatization | 8151A | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 112 | PAHs in water by HPLC | USEPA method 8310 (SW-846) for polynuclear aromatic hydrocarbons (PAHs) by HPLC | 8310 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 113 | PAHs in soil or water, low-level, by GC/MS SIM | USEPA method 8270 SIM (SW-846) for polynuclear aromatic hydrocarbons (PAHs) in soil and water by GC/MS SIM | 8270E SIM LL | 80 | 80 | 80 | 80 | 80 | 40 | ||||
| 114 | Gasoline-range organics (GRO), C6-C10 using GC-FID | USEPA method 8015B (SW-846) for nonhalogenated (gasoline-range) organics using GC/FID – C6 to C10 | 8015D | 72 | 72 | 72 | 72 | 72 | 36 | ||||
| 115 | Diesel-range organics (DRO), C10-C28 using GC-FID | USEPA method 8015D (SW-846) for nonhalogenated organics using GC/FID – C10 to C28 | 8015D | 38 | 38 | 38 | 38 | 38 | 19 | ||||
| 116 | Motor-oil-range organics (MRO), C28-C36 using GC-FID | USEPA method 8015D (SW-846) for nonhalogenated organics using GC/FID – C28 to C36 | 8015D | 35 | 35 | 35 | 35 | 35 | 18 | ||||
| 117 | Dispersants of interest for oil spills / glycols by GC-FID | USEPA method 8015D (SW-846) with modifications for detection of dispersants of interest for oil spills (glycols) by gas chromatrography and flame-ionization detection | 8015D with modifications | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 118 | Dissolved gases (methane, ethane, and ethene) in headspace | Method RSK 175 for dissolved gases (methane, ethane, and ethene) in drinking water by purge and trap headspace analysis | RSK-175 | 26 | 26 | 26 | 26 | 26 | 13 | ||||
| 119 | Propane | Propane | RSK-175 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 120 | Dissolved gases (C1–C6) in aqueous samples by headspace analysis, with isotopic analysis of methane (if present) | USEPA Method RSK 175 (modified) for dissolved gases (C1–C6) in drinking water by purge and trap headspace analysis, including isotopic analysis of methane if present. [If methane is not present, the isotopic analysis will not be performed; see next row] | RSK-175 modified | 67 | 67 | 67 | 67 | 67 | 34 | ||||
| 121 | Dissolved gases (C1–C6) in aqueous samples by headspace analysis (compositional analysis only) | USEPA Method RSK 175 (modified) for dissolved gases (C1–C6) in drinking water by purge and trap headspace analysis (compositional analysis only). | RSK-175 modified | 91 | 91 | 91 | 91 | 91 | 46 | ||||
| 122 | GRO plus benzene, toluene, ethylbenzene, and xylene (BTEX compounds) by GC/PID-FID | GRO plus benzene, toluene, ethylbenzene, and xylene (BTEX compounds) by GC/PID-FID | 8015D or 8021B | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 123 | n-Hexane-extractable material (oil and grease) in aqueous samples | USEPA method 1664B for n-hexane-extractable material (oil and grease) in aqueous samples by extraction and gravimetry | 1664B | 15 | 15 | 15 | 15 | 15 | 8 | ||||
| 124 | n-Hexane-extractable material (total petroleum hydrocarbons) in aqueous samples | USEPA method 1664B for n-hexane-extractable material (total petroleum hydrocarbons) in aqueous samples by extraction and gravimetry | 1664B | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 125 | n-Hexane-extractable material (total petroleum hydrocarbons) in sediment or solids | USEPA method 9071B (SW-846) n-hexane-extractable material (total petroleum hydrocarbons) in sludge, sediment, and solids samples | 9071B | 35 | 35 | 35 | 35 | 35 | 18 | ||||
| 126 | Methylene-blue-active substances (MBAS) in aqueous samples | USEPA method 425.1 for surfactants by colorimetry | 425.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 127 | Surfactants in soil | USEPA method 425.1 for surfactants in soil by colorimetry | 425.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 128 | Volatile Fatty Acids (metabolic acids) by IC: Acetic Acid, Butyric Acid, Formic Acid, Lactic Acid, Propionic Acid, Pyruvic Acid | Volatile Fatty Acids (metabolic acids) by IC: Acetic Acid, Butyric Acid, Formic Acid, Lactic Acid, Propionic Acid, Pyruvic Acid | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 129 | Volatile organic compounds (VOCs) with library search up to 10 tentatively identified compounds (TICs) from 40 CFR part 264, ground-water monitoring list | Volatile organic compounds (VOCs) with library search up to 10 tentatively identified compounds (TICs) from 40 CFR part 264, ground-water monitoring list | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 130 | SVOCs by GC-MS in aqueous samples | USEPA method 625.1 for Base/Neutrals and Acids by GC/MS in aqueous samples from 40 CFR part 264 groundwater monitoring list, with library search up to 20 tentatively identified compounds (TICs) upon request | 625.1 | 40 | 40 | 40 | 40 | 40 | 20 | ||||
| 131 | Pesticides from 40 CFR part 264, ground-water monitoring list | Pesticides from 40 CFR part 264, ground-water monitoring list | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 132 | Polychlorinated biphenyls (Arochlors) from 40 CFR part 264, ground-water monitoring list | Polychlorinated biphenyls (Arochlors) from 40 CFR part 264, ground-water monitoring list | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 133 | Herbicides from 40 CFR part 264, ground-water monitoring list | Herbicides from 40 CFR part 264, ground-water monitoring list | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 134 | Dioxins/Furans from 40 CFR part 264, ground-water monitoring list | Dioxins/Furans from 40 CFR part 264, ground-water monitoring list | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 135 | Alumina cleanup | USEPA method 3610B (SW_846) Alumina cleanup | 3610B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 136 | Florisil column clean-up for pesticide analysis of biological samples | Florisil column clean-up for pesticide analysis of biological samples | 3620A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 137 | Gel permeation column (GPC) clean-up for organic analysis of biological samples | Gel permeation column (GPC) clean-up for organic analysis of biological samples | 3640A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 138 | Silica gel cleanup | Silica gel cleanup | 3630C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 139 | Sulfur cleanup | Sulfur cleanup | 3660B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 140 | Special closed system sample container (Encore) for volatile organics analysis of solid samples | Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples | 5035 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 141 | 2,3,7,8-tetrachlorodibenzo-p-dioxin (only) by HRGC/LRMS | USEPA Method 8280B for 2,3,7,8-tetrachlorodibenzo-p-dioxin (only) by high-resolution gas chromatography with low-resolution mass spectrometry (HRGC/LRMS) | 8280B | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 142 | Polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by HRGC/HRMS | USEPA method 8290A (SW-846) for polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS) | 8290A | 7 | 7 | 7 | 7 | 7 | 4 | ||||
| 143 | Dioxins and furans by isotope-dilution HRGC/HRMS | Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS | 1613B | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 144 | 2,3,7,8-TCDD only (screening test) | 2,3,7,8-TCDD only (drinking water screen samples) | 625.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 145 | 2,3,7,8-TCDD only (municipal and industrial discharge) | Determination of 2,3,7,8-TCDD in municipal and industrial discharge by GC/MS | 613 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 146 | PCB congeners by HRGC/HRMS (WHO list: 77, 81, 105, 114, 118, 123, 126, 156, 157, 167, 169, 170, 180, and 189) | USEPA Method 1668C for polychlorinated biphenyl (PCB) congeners designated as toxic by the World Health Organization (77, 81, 105, 114, 118, 123, 126, 156, 157, 167, 169, 170, 180, and 189) by high-resolution gas chromatography with high-resolution mass spectrometry (HRGC/HRMS) | 1668C | 15 | 15 | 15 | 15 | 15 | 8 | ||||
| 147 | PCB congeners by HRGC/HRMS (209 congeners) | USEPA Method 1668C for 209 polychlorinated biphenyl (PCB) congeners by high-resolution gas chromatography with high-resolution mass spectrometry (HRGC/HRMS) | 1668C | 59 | 59 | 59 | 59 | 59 | 30 | ||||
| 148 | BDEs (flame retardants) by HRGC/HRMS | USEPA method 1614A Brominated Diphenyl Ethers (BDEs) in water, soil, sediment, and tissue by HRGC/HRMS | 1614A | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 149 | Nitroaromatics, Nitramines, and Nitrate Esters (Explosives) | USEPA method 8330B (SW-846)for nitroaromatics, nitramines, and nitrate esters by High Performance Liquid Chromatography (HPLC) | 8330B | 30 | 30 | 30 | 30 | 30 | 15 | ||||
| 150 | Nitroaromatics, Nitramines, and Nitrate Esters (Explosives) in solids | USEPA method 8330B (SW-846)for nitroaromatics, nitramines, and nitrate esters in solids by High Performance Liquid Chromatography (HPLC) | 8330B | 17 | 17 | 17 | 17 | 17 | 9 | ||||
| 151 | Solvent-extractable nonvolatiles by HPLC (azo dyes, organophosphorus compounds, tris(2,3-dibromopropyl)phosphate, carbamates, and chlorinated phenoxyacids and their esters, etc.) | USEPA method 8321B (SW-846) for solvent-extractable nonvolatile compounds in solids or aqueous samples by High-Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) detection | 8321B | 7 | 7 | 7 | 7 | 7 | 4 | ||||
| 152 | Organophosphates | USEPA method 8321B (SW-846) for organophosphates in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection | 8321B | 15 | 15 | 15 | 15 | 15 | 8 | ||||
| 153 | Chlorinated herbacides | USEPA method 8321B (SW-846) for chlorinated herbacides in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection | 8321B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 154 | Tebuthiuron and Bromacil | USEPA method 8321B (SW-846) for Tebuthiuron and Bromacil in solids or aqueous samples by high performance liquid chromatography (HPLC) with thermospray-mass spectrometry (TS-MS) or ultraviolet (UV) detection | 8321B | 15 | 15 | 15 | 15 | 15 | 8 | ||||
| 155 | Perchlorate - aqueous | Determination of perchlorate in aqueous samples using Ion Chromatography | 314.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 156 | Perchlorate - solids | Perchlorate - solids | 314 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 157 | Perchlorate in aqueous samples by Inline Column Concentration/Matrix Elimination IC | Determination of perchlorate in aqueous samples using Inline Column Concentration/Matrix Elimination Ion Chromatography With Suppressed Conductivity Detection | 314.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 158 | Perchlorate in aqueous samples by LC-EI-MS | Determination of perchlorate in aqueous samples by Liquid Chromatography Electrospray Ionization Mass Specxtrometry (LC/ESI/MS) | 331.0 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 159 | Perchlorate in aqueous samples by IC-ESI/MS | Determination of perchlorate in aqueous samples by Ion Chromatography with Suppressed Conductivity and Electrospray Ionization Mass Spectometry | 332.0 | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 160 | Perchlorate by LC/MS/MS | Perchlorate by LC/MS/MS | DoD SOP | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 161 | Perchlorate in solids or aqueous samples by HPLC-ESI-MS or HPLC-ESI-MS/MS | USEPA method 6850 (SW-846) for perchlorate in water, soils and solid wastes using high performance liquid chromatography with electrospray-ionization (ESI) mass spectrometry or ESI with tandem mass spectrometry | 6850 | 125 | 125 | 125 | 125 | 125 | 63 | ||||
| 162 | Perchlorate by IC/MS/MS | Perchlorate by IC/MS/MS | DoD SOP | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 163 | Perchlorate in solids or aqueous samples by IC-ESI-MS or IC-ESI-MS/MS | USEPA method 6860 (SW-846) for perchlorate in water, soils and solid wastes using ion chromatography with electrospray-ionization (ESI) mass spectrometry or ESI with tandem mass spectrometry | 6860 | 24 | 24 | 24 | 24 | 24 | 12 | ||||
| 164 | EDB,DCBP, and 123TCP in Water Using GCECD | 1,2-Dibromoethane (EDB), 1,2-Dibromo-3-Chloro-Propane (DCBP), and 1,2,3-Trichloropropane (123TCP) in water by Microextraction and Gas Chromatography | 504.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 165 | Chlorinated Pesticides in Water Using GCECD | Determination of Chlorinated Pesticides in Water by Gas Chromatography with an Electron Capture Detector | 508.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 166 | Chlorinated herbicides in water by GC-ECD | Determination of chlorinated acids in aqueous samples by Liquid-liquid Microextraction Derivatization and Fast Gas Chromatography With Electron Capture Detection | 515.4 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 167 | Purgeable VOCs by GC-MS for drinking water | USEPA Method 524.2 for purgeable volatile organic compounds by gas chromatography-mass spectrometry (GC/MS) | 524.2 | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 168 | Purgeable VOCs by GC-MS for drinking water–THMs only | USEPA Method 524.2 for purgeable volatile organic compounds (total trihalomethanes, only) by gas chromatography-mass spectrometry (GC/MS) | 524.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 169 | Semivolatile organic compounds by GC/MS | Determination of organic compounds in aqueous samples by liquid-solid extraction and capillary column GC/MS | 525.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 170 | Carbamates by HPLC | Determination of N-methylcarbamoyloximes and N-methylcarbamates (carbamates) in water by direct aqueous injection by HPLC with postcolumn derivization | 531.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 171 | Glyphosate and AMPA by HPLC | USEPA method 547 for glyphosate and aminomethylphosphonic acid (AMPA) in drinking water by direct-aqueous-injection and high performance liquid chromatography (HPLC) with post-column derivatization and fluorescence detection | 547 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 172 | Endothall in Water Using GCMS | Determination of Endothall in aqueous samples by Ion-Exchange Extraction, Acidic Methanol Methylation, and Gas Chromatography/Mass Spectrometry | 548.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 173 | Diquat and paraquat by HPLC | Determination of diquat and paraquat in aqueous samples by liquid-solid extraction and HPLC with UV detection | 549.2 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 174 | Haloacetic acids and Dalapon by GC-ECD | Determination of Haloacetic Acids and Dalapon in aqueous samples by Liquid-Liquid Microextraction, Derivatization, and Gas Chromatography with Electron Capture Detection | 552.3 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 175 | TCLP prep and extraction | USEPA methods 1311 (SW-846) for the toxicity characteristic leaching procedure (TCLP) and sample preparation | 1311 | 11 | 11 | 11 | 11 | 11 | 6 | ||||
| 176 | SPLP prep and extraction | USEPA methods 1312 (SW-846) for the Synthetic precipitation leaching procedure (SPLP) and sample preparation | 1312 | 11 | 11 | 11 | 11 | 11 | 6 | ||||
| 177 | Moisture content of sediment or soil | ASTM D2216-19 standard test method for laboratory determination of water (moisture) content of soil and rock by mass significance | D2216-19 | 341 | 341 | 341 | 341 | 341 | 171 | ||||
| 178 | Measurement of Hydraulic Conductivity of Saturated Porous Materials Using a Flexible Wall Permeameter | Measurement of Hydraulic Conductivity of Saturated Porous Materials Using a Flexible Wall Permeameter | D5084 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 179 | Density of Soils in Place by the Drive-Cylinder Method | Density of Soils in Place by the Drive-Cylinder Method | D2937 | 164 | 164 | 164 | 164 | 164 | 82 | ||||
| 180 | Cyanide, total and amenable | USEPA method 9012B (SW-846) for total and amenable cyanide in distillates of aqueous samples by colorimetric method | 9012B | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 181 | Cyanide, free by microdiffusion | Standard Method D4282-89 for determination of free cyanide in water and wastewater by microdiffusion | D4282-89 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 182 | Sulfide | ulfide (Colorimetric, Methylene Blue) | 9034/376.2 | 27 | 27 | 27 | 27 | 27 | 14 | ||||
| 183 | Ferrous iron (dissolved) in aqueous samples | Standard Method 3500-Fe for dissolved ferrous and ferric iron in aqueous samples | SM 3500 Fe | 27 | 27 | 27 | 27 | 27 | 14 | ||||
| 184 | Ferric iron (dissolved) in aqueous samples | Standard Method 3500-Fe for dissolved ferrous and ferric iron in aqueous samples | SM 3500 Fe | 27 | 27 | 27 | 27 | 27 | 14 | ||||
| 185 | Alkalinity (total only) | Standard Method 2320B for alkalinty (total only) by titration | SM 2320B | 191 | 191 | 191 | 191 | 191 | 96 | ||||
| 186 | Alkalinity (total, carbonate, bicarbonate, and hydroxide) | Alkalinity (total, carbonate, bicarbonate, and hydroxide) | SM 2320B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 187 | Biochemical oxygen demand (BOD) 5-Day | USEPA method 405.1 or SM 5210B for 5-day biological oxygen demand (BOD) | 405.1 or SM 5210B | 359 | 359 | 359 | 359 | 359 | 180 | ||||
| 188 | BOD 30-day | BOD 30-day | 405.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 189 | Carbonaceous Biochemical Oxygen Demand (CBOD) 5-day | USEPA method 405.1 or SM 5210B for 5-day carbonaceous biological oxygen demand (CBOD) | 405.1 or 5210B | 200 | 200 | 200 | 200 | 200 | 100 | ||||
| 190 | Ultimate CBOD | Ultimate CBOD | 405.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 191 | Color in water | Color in Water by Visual Comparison Method | SM 2120B | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 192 | Hardness by EDTA titration | Standard Method 2340C for hardness by EDTA titration | SM 2340C | 28 | 28 | 28 | 28 | 28 | 14 | ||||
| 193 | Oxygen, dissolved | Oxygen by Membrane Electrode Method | SM 4500-O G | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 194 | Residue, filterable (total dissolved solids: TDS) | Standard Method 2540C Total Dissolved Solids Dried at 180oC | SM 2540C | 360 | 360 | 360 | 360 | 360 | 180 | ||||
| 195 | Residue, non-filterable (total suspended solids: TSS) | Standard Method 2540D for Total Suspended Solids Dried at 103-105oC | SM 2540D | 1065 | 1065 | 1065 | 1065 | 1065 | 533 | ||||
| 196 | Sulfide, iodometric method | Sulfide, iodometric titration (water) | SM 4500-S F | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 197 | VOCs in air | USEPA method TO-15 for volatile organic compounds in air by gas chromatography and mass spectrometry | TO-15 | 229 | 229 | 229 | 229 | 229 | 115 | ||||
| 198 | VOCs in air | TO-15 SIM scan | TO-15 SUP | ||||||||||
| 199 | PCB congeners in air by HRGC/HRMS | USEPA Method 1668 (modified) for 19 target PCB congeners in air (PUF or XAD) by HRGC/HRMS with no totals | 1668 mod | 50 | 50 | 50 | 50 | 50 | 25 | ||||
| 200 | PAHs in ambient air by GC/MS | USEPA method TO-13A for polynuclear aromatic hydrocarbons (PAHs) in ambient air by GC/MS | TO-13A | 201 | 201 | 201 | 201 | 201 | 101 | ||||
| 201 | Dioxins and furans in air (PUF) by HRGC/HRMS | USEPA method 8290A (SW-846) for polychlorinated dibenzodioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) by high-resolution gas chromatography/high-resolution mass spectrometry in air (PUF) | 8290A | 50 | 50 | 50 | 50 | 50 | 25 | ||||
| 202 | Metals in ambient air | USEPA method 6020B (SW-846) for metals in ambient air by inductively coupled plasma with mass spectrometry | 6020B | 211 | 211 | 211 | 211 | 211 | 106 | ||||
| 203 | Total suspended particulate matter in air | Compendium Method IO-2.1 for total suspended particulate matter and PM10 in ambient air using high-volume sampler | IO-2.1 | 212 | 212 | 212 | 212 | 212 | 106 | ||||
| 204 | Clean-up of client-supplied SUMMA canister | Clean-up of client-supplied SUMMA canister | NA | 230 | 230 | 230 | 230 | 230 | 115 | ||||
| 205 | Certification of cleanliness of SUMMA canister | Certification of cleanliness of SUMMA canister | NA | 63 | 63 | 63 | 63 | 63 | 32 | ||||
| 206 | Preparation and QC check of PUF or XAD media for air sampling | Preparation and QC check of PUF or XAD media for air sampling | NA | 47 | 47 | 47 | 47 | 47 | 24 | ||||
| 207 | Corrosivity, RCRA | Corrosivity Toward Steel (SW-846), RCRA | 1110A | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 208 | Ignitability Characteristic (Setaflash closed cup method), RCRA | USEPA method 1020C (SW-846) for Standard Test Methods for Flash Point by Setaflash (Small Scale) Closed-Cup Apparatus, RCRA | 1020C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 209 | Methyl mercury in aqueous samples | USPEA method 1630 for methyl mercury in water by distillation, aqueous ethylation, purge and trap, and cold vapor atomic fluorescence spectrometry | 1630 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 210 | Arsenic III | Arsenic in aqueous samples and extracts by anodic stripping voltammetry (ASV) | 7063 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 211 | Arsenic V | Arsenic in aqueous samples and extracts by anodic stripping voltammetry (ASV) | 7063 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 212 | Sulfite | Sulfite by Titrimetry | 377.1 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 213 | Percent lipids in tissue samples | Determination of percent lipids in tissue samples by accelerated solvent extractor | 175 | 175 | 175 | 175 | 175 | 88 | |||||
| 214 | Pesticides and PCBs in Water GC-ECD | Analysis of Organochlorine Pesticides and Commercial Polychlorinated Biphenyl (PCB) Products in Water by Microextraction and Gas Chromatography | 505 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 215 | Mercury in Solid or Semisolid Wastes | Mercury in Solid or Semisolid Wastes (Manual Cold-Vapor Technique) | 7471B | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 216 | Ignitability 1010 | USEPA method 010B (SW-846) for Flash Point by Pensky-Martens Closed Cup Tester | 1010B | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 217 | Hydrogen cyanide | Hydrogen cyanide | SW-846, Chapter 7 | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 218 | Hydrogen sulfide | Hydrogen sulfide | SW-846, Chapter 7 | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 219 | Specific Gravity of Soils | Standard Test Method for Specific Gravity of Soil Solids by Gas Pycnometer | SM D5550 | 4 | 4 | 4 | 4 | 4 | 2 | ||||
| 220 | Amount of Materials in Soils Finer than No. 200 (75um) Sieve | Amount of Materials in Soils Finer than No. 200 (75um) Sieve | D1140 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 221 | Permeability of Granular Soils (sands/ gravels)--constant or falling head | Permeability of Granular Soils (sands/ gravels)--constant or falling head | D2434 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 222 | Moisture, ash, and organic matter of peats and other organic soils | ASTM D2974 standard test method for moisture, ash, and organic matter of peat and other organic soils used to determine the percent organic matter within soil and sediment | D2974 | 6 | 6 | 6 | 6 | 6 | 3 | ||||
| 223 | Liquid Limit, Plastic Limit, and Plasticity Index of Soils (Atterburg Limits) | Liquid Limit, Plastic Limit, and Plasticity Index of Soils (Atterburg Limits) | D4318 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 224 | VOCs in Ambient Air using Tenax adsorption tubes and by GC/MS | VOCs in Ambient Air using Tenax adsorption tubes and by GC/MS | TO-01 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 225 | VOCs in ambient air by GC-FID | USEPA Method TO-3 for hydrocarbons and oxygenated hydrocarbons, such as methanol and MTBE, in ambient air and gas samples by gas chromatograph (GC) flame ionization detector (FID) | TO-3 | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 226 | BTEX and TPH (only) in ambient air by GC-FID | USEPA Method TO-3 or Air-Phase Petroleum hydrocarbon (APH) method for BTEX and total petroleum hydrocarbons (only), in ambient air and gas samples (SUMMA canister) by gas chromatograph (GC) flame ionization detector (FID) | TO-3 or APH | 37 | 37 | 37 | 37 | 37 | 19 | ||||
| 227 | Organopesticides and PCBs in Ambient Air by GC/FID | Determination of pesticides and Polychlorinated Biphenyls (PCBs) in ambient air using high volume polyurethane foam (PUF) sampling followed by Gas Chromatographic/Multi-Detector Detection (GC/MD) | TO-4A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 228 | PAHs by GC/MS -- selective ion monitoring (SIM) [matrix: PUF/XAD] | PAHs by GC/MS -- selective ion monitoring (SIM) [matrix: PUF/XAD] | TO-13A SIM LL | 2 | 2 | 2 | 2 | 2 | 1 | ||||
| 229 | VOCs using SUMMA canister sampling and by GC/MS | VOCs using SUMMA canister sampling and by GC/MS | TO-14A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 230 | Full list of SVOCs in Ambient Air by GC/MS | Full list of SVOCs in Ambient Air by GC/MS | TO-13A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 231 | PAHs in Ambient Air by GC/MS and high resolution liquid chromatography | PAHs in Ambient Air by GC/MS and high resolution liquid chromatography | TO-13A | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 232 | PAHs in Ambient Air by GC/SIM LL | PAHs in Ambient Air by GC/SIM LL | TO-13A LL | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 233 | PCB congeners in Ambient Air with no totals | PCB congeners in Ambient Air with no totals | 1668C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 234 | PCB congeners in Ambient Air with totals | PCB congeners in Ambient Air with totals | 1668C | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 235 | VOCs in Ambient Air by GC/MS (short list) <10 compounds | VOCs in Ambient Air by GC/MS (short list) <10 compounds | TO-15 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 236 | Pharmaceuticals and personal care products (PPCPs) | Pharmaceuticals and Personal Care Products in Water by HPLC/MS/MS | 1694 | 17 | 17 | 17 | 17 | 17 | 9 | ||||
| 237 | Pharmaceuticals and personal care products (PPCPs) | Pharmaceuticals and Personal Care Products in Soil, Sediment, and Biosolids by HPLC/MS/MS | 1694 | 46 | 46 | 46 | 46 | 46 | 23 | ||||
| 238 | Pharmaceuticals and Personal Care Products in Drinking Water | Determination of Pharmaceuticals and Personal Care Products in Drinking Water by Solid Phase Extraction and Liquid Chromatography Electrospray Ionization Tandem Mass Spectrometry | 542 | 46 | 46 | 46 | 46 | 46 | 23 | ||||
| 239 | Vitamin E | Vitamin E | Custom | 2 | 2 | 2 | 2 | 2 | 1 | ||||
| 240 | Alkylated PAHs by isotopic-dilution GC/MS | USEPA method 8270E (SW-846) for alkylated PAHs by isotopic-dilution gas chromatography and mass spectrometry | 8270E | 171 | 171 | 171 | 171 | 171 | 86 | ||||
| 241 | IsoFlask | IsoFlask | custom | 104 | 104 | 104 | 104 | 104 | 52 | ||||
| 242 | PCNs (polychlorinated Naphthalenes) | PCNs (polychlorinated Naphthalenes) | Custom | 5 | 5 | 5 | 5 | 5 | 3 | ||||
| 243 | Fixed gases by GC-TCD | ASTM D1946 for permanent gases in refinery samples using gas chromatography (GC) with a thermal conductivity detector (TCD) | D1946 | 29 | 29 | 29 | 29 | 29 | 15 | ||||
| 244 | Gaseous non-methane organic compounds | USEPA Method 25.1 for total gaseous nonmethane organic (TGNMO) compounds, as carbon | 25.1 | 39 | 39 | 39 | 39 | 39 | 20 | ||||
| 245 | Sulfur, Total | Determination of Total Sulfur by UVF | D5453 | 8 | 8 | 8 | 8 | 8 | 4 | ||||
| 246 | Free Cyanide | USEPA method 9014 (SW-846) for cyanide in waters and extracts using titrimetric and manual spectrophotometric procedures | 9014 | 19 | 19 | 19 | 19 | 19 | 10 | ||||
| 247 | Wound Glass Cannister Filters (4x2 1um) | Wound Glass Cannister Filters (4x2 1um) | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 248 | Flat Filter charge - 100 filters | Flat Filter charge - 100 filters | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 249 | Pesticides in Water, Soil, Sediment, Biosolids, and Tissue by HRGC/HRMS | Determines organochlorine, organophosphorus, triazine, and pyrethroid pesticides in environmental samples by high resolution gas chromatography/high resolution mass spectrometry (HRGC/HRMS) using isotope dilution | 1699 | 397 | 397 | 397 | 397 | 397 | 199 | ||||
| 250 | Tissue homoginization, >1500 grams | Tissue homoginization, >1500 grams | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 251 | IsoTubes (25 tubes/box) | IsoTubes (25 tubes/box) | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 252 | MG-2 | MG-2 | MG-2 | 100 | 17 | 17 | 17 | 17 | 9 | ||||
| 253 | Gamma Emitting Radionuclides in Drinking Water | Gamma Emitting Radionuclides in Water by Gamma Spectroscopy | 901.1 | 35 | 35 | 35 | 35 | 35 | 18 | ||||
| 254 | Speciated Se: SeCN + MeSe(IV) + SeMet + Se(VI) + Se (IV) + Unk Se Sp + Total Diss | Speciated Se: SeCN + MeSe(IV) + SeMet + Se(VI) + Se (IV) + Unk Se Sp + Total Diss | custom | 11 | 11 | 11 | 11 | 11 | 6 | ||||
| 255 | Flutolanil and Alpha-BHC in water | Flutolanil and Alpha BHC in water | custom | 17 | 17 | 17 | 17 | 17 | 9 | ||||
| 256 | Mestrione and Clopyralid in water | Mestrione and Clopyralid in water | LC/MS/MS | 17 | 17 | 17 | 17 | 17 | 9 | ||||
| 257 | Be-7 and Cesium-137 | Be-7 and Cesium-137 | Gamma Spec | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 258 | Steroids and Hormones in Water, Soil, Sediment, and Biosolids | Steroids and Hormones in Water, Soil, Sediment, and Biosolids by HRGC/HRMS | 1698 | 3 | 3 | 3 | 3 | 3 | 2 | ||||
| 259 | Grain Size + Hydrometer | Grain Size + Hydrometer | ASTM | 23 | 23 | 23 | 23 | 23 | 12 | ||||
| 260 | Metsulfuron-methyl and Aminopyralid | Determination of Selected Organic Contaminants in Drinking Water by DAI-LC/MS/MS | EPA 538 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 261 | NG-2 | NG-2 | custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 262 | Chemical Speciation of Arsenic in Water and Tissue | USEPA method 1632 for total inorganic arsenic, arsenite (As+3), arsenate (As+5), monomethylarsonate (MMA), and dimethylarsinate (DMA) | 1632 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 263 | Cation Exchange Capacity CEC | Cation Exchange Capacity CEC | SW846 EPA9081 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 264 | Anion Exchange Capacity AEC | Anion Exchange Capacity AEC | New Zealand P Retention | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 265 | Indaziflam, chlorsulfuron | Pesticides by LC/MS/MS | custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 266 | Aminopyralid | Pesticides by LC/MS/MS | custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 267 | 6PPD | 6PPD-quinone | EPA 1634 | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 268 | Data Management 1hr | Data Management per hr | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 269 | POCIS Extraction | POCIS Extraction | Custom | 10 | 10 | 10 | 10 | 10 | 5 | ||||
| 270 | Level 4 Data Package (per workorder) | Level 4 Data Package (per workorder) | 10 | 10 | 10 | 10 | 10 | 5 | |||||
| 271 | Saturday arrival and analysis per work order | Saturday arrival and analysis per work order for short holding times | 30 | 30 | 30 | 30 | 30 | 15 |
Data Package Descriptions image1.png
File details come from the government source that posted it. Updated .