Attachment C_Previous_TCLP_Analytical_Report.pdf

May 17, 2023

Dear Order No:

RE:

Analytical Environmental Services, Inc. received samples on for the analyses presented in following report.

“No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in the report or QC Summary. Additionally, all results for the associated Quality Control samples were within

EPA and/or AES established limits.

AES’s accreditations are as follows:

-NELAP/State of Florida Laboratory ID E87582 for analysis of Non-Potable Water, Solid & Chemical

Materials, Air & Emissions Volatile Organics, and Drinking Water Microbiology & Metals, effective

07/01/22-06/30/23.

State of Georgia, Department of Natural Resources ID #800 for analysis of Drinking Water Metals, effective through 06/30/23 and Total Coliforms/ E. coli, effective 04/25/23-04/24/24.

-AIHA LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Metals and PCM Asbestos), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct

Examination, effective until 11/01/23.

These results relate only to the items tested as received. This report may only be reproduced in full.

If you have any questions regarding these test results, please feel free to call.

Sincerely, Project Manager

2305C95

Daphne B. Little Athens-Clarke Co Unified Government

J.G.Beacham WTP & Bobby Snipes WRC Athens GA 30601

NOWRF Influent Wet Well

Eben Buchanan

May 10, 2023 12:36 pm

Daphne B. Little:

17-May-23Date:Analytical Environmental Services, Inc

Client:

Case NarrativeNOWRF Influent Wet Well

ATHENS CLARKE CO WRC

Lab ID:

Project:

2305C95

Sample Receiving Nonconformance:

Sample(s) for pH analysis by Method SM4500 H+ B were received and analyzed outside Method specified holding time of

“immediate or 15 minutes”.

TCLP Analysis by Method 8081/1311:

LCS-1-356151 recovery for Methoxychlor was outside control limits biased high. Target analyte was not detected in the analytical samples and data is reportable with high bias.

2305C95-001

Analyses Date Analyzed Dilution

Factor BatchIDUnitsQual

Reporting

Limit Result

Client:

Waste Water

5/9/2023 11:09:00 AM

NOWRF INFLUENT WET WELL

Matrix:

Collection Date:

Client Sample ID:

NOWRF Influent Wet Well

Athens-Clarke Co Unified Government

Lab ID:

Project Name:

Analyst

(SW5030B)VOLATILES, TCLP SW1311/8260D

1,1-Dichloroethene BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

1,2-Dichloroethane BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

2-Butanone BRL 0.20 mg/L 356252 20 05/12/2023 17:40 AV

Benzene BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Carbon tetrachloride BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Chlorobenzene BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Chloroform BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Tetrachloroethene BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Trichloroethene BRL 0.10 mg/L 356252 20 05/12/2023 17:40 AV

Vinyl chloride BRL 0.040 mg/L 356252 20 05/12/2023 17:40 AV

Surr: 4-Bromofluorobenzene 92.6 78-117 %REC 356252 20 05/12/2023 17:40 AV

Surr: Dibromofluoromethane 90.5 77.2-124 %REC 356252 20 05/12/2023 17:40 AV

Surr: Toluene-d8 99 80-120 %REC 356252 20 05/12/2023 17:40 AV

(SW7.3.4.2)Sulfide, Reactive SW846-7.3

Sulfide, Reactive BRL 100 mg/Kg 356308 1 05/15/2023 14:22 AA

(SW3510C)SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

1,4-Dichlorobenzene BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

2,4,5-Trichlorophenol BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

2,4,6-Trichlorophenol BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

2,4-Dinitrotoluene BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Hexachlorobenzene BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Hexachlorobutadiene BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Hexachloroethane BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH m,p-Cresol 0.17 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Nitrobenzene BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH o-Cresol BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Pentachlorophenol BRL 0.50 mg/L 356029 1 05/12/2023 21:13 YH

Pyridine BRL 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Cresols, Total 0.17 0.10 mg/L 356029 1 05/12/2023 21:13 YH

Surr: 2,4,6-Tribromophenol 57.7 52.7-137 %REC 356029 1 05/12/2023 21:13 YH

Surr: 2-Fluorobiphenyl 54.5 47.1-121 %REC 356029 1 05/12/2023 21:13 YH

Surr: 2-Fluorophenol 56.2 42.3-120 %REC 356029 1 05/12/2023 21:13 YH

Surr: 4-Terphenyl-d14 55 50.9-127 %REC 356029 1 05/12/2023 21:13 YH

Surr: Nitrobenzene-d5 57.9 48.3-119 %REC 356029 1 05/12/2023 21:13 YH

Surr: Phenol-d5 52.6 45.6-120 %REC 356029 1 05/12/2023 21:13 YH

(SW3510C)PESTICIDES, TCLP SW1311/8081B

Chlordane BRL 0.0050 mg/L 356151 1 05/12/2023 18:39 ST

Endrin BRL 0.0010 mg/L 356151 1 05/12/2023 18:39 ST gamma-BHC BRL 0.00050 mg/L 356151 1 05/12/2023 18:39 ST

Heptachlor BRL 0.00050 mg/L 356151 1 05/12/2023 18:39 ST

Heptachlor epoxide BRL 0.00050 mg/L 356151 1 05/12/2023 18:39 ST

Methoxychlor BRL 0.0050 mg/L 356151 1 05/12/2023 18:39 ST

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

F Analyzed in the lab which is a deviation from the method

< Less than Result value

> Greater than Result value J Estimated value detected below Reporting Limit

2305C95-001

Analyses Date Analyzed Dilution

Factor BatchIDUnitsQual

Reporting

Limit Result

Client:

Waste Water

5/9/2023 11:09:00 AM

NOWRF INFLUENT WET WELL

Matrix:

Collection Date:

Client Sample ID:

NOWRF Influent Wet Well

Athens-Clarke Co Unified Government

Lab ID:

Project Name:

Analyst

(SW3510C)PESTICIDES, TCLP SW1311/8081B

Toxaphene BRL 0.050 mg/L 356151 1 05/12/2023 18:39 ST

Surr: Decachlorobiphenyl 86.6 48.2-122 %REC 356151 1 05/12/2023 18:39 ST

Surr: Tetrachloro-m-xylene 64.8 41-123 %REC 356151 1 05/12/2023 18:39 ST

(SW7470A)MERCURY, TCLP SW1311/7470A

Mercury BRL 0.00400 mg/L 356161 1 05/12/2023 16:46 GR

Ignitability / Flashpoint SW1010B

Ignitability 180 0 > °F R516016 1 05/11/2023 00:00 AY

(SW3010A)ICP METALS, TCLP SW1311/6010D

Arsenic BRL 0.250 mg/L 356204 1 05/12/2023 17:37 EO

Barium BRL 0.500 mg/L 356204 1 05/12/2023 17:37 EO

Cadmium BRL 0.0250 mg/L 356204 1 05/12/2023 17:37 EO

Chromium BRL 0.0500 mg/L 356204 1 05/12/2023 17:37 EO

Lead BRL 0.0500 mg/L 356204 1 05/12/2023 17:37 EO

Selenium BRL 0.100 mg/L 356204 1 05/12/2023 17:37 EO

Silver BRL 0.0250 mg/L 356204 1 05/12/2023 17:37 EO

Hydrogen Ion (pH) by SM4500H+B-2011 pH 6.60 0.0100 H pH Units R516055 1 05/11/2023 13:41 AH

(SW3510C)HERBICIDES, TCLP SW1311/8151A

2,4,5-TP (Silvex) BRL 0.20 mg/L 356030 1 05/12/2023 18:30 TB

2,4-D BRL 0.20 mg/L 356030 1 05/12/2023 18:30 TB

Surr: DCAA 78.2 45-126 %REC 356030 1 05/12/2023 18:30 TB

(SW7.3.3.2)Cyanide, Reactive SW846-7.3

Cyanide, Reactive BRL 0.980 mg/Kg 356117 1 05/15/2023 13:45 AA

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

F Analyzed in the lab which is a deviation from the method

< Less than Result value

> Greater than Result value J Estimated value detected below Reporting Limit

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Dates Report Lab Order:

Project Name:

Lab Sample ID Client Sample ID Test NameCollection Date Matrix TCLP Date Prep Date Analysis Date

2305C95

NOWRF Influent Wet Well

Athens-Clarke Co Unified Government

2305C95-001A NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water VOLATILES, TCLP Leached 05/11/2023 5/12/2023 1:56:00 PM 05/12/2023

2305C95-001B NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water TCLP SEMIVOLATILES ORGANICS 05/11/2023 5/12/2023 11:34:41 AM 05/12/2023

2305C95-001B NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water HERBICIDES, TCLP Leached 05/11/2023 5/12/2023 11:30:05 AM 05/12/2023

2305C95-001B NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water MERCURY, TCLP Leached 05/11/2023 5/12/2023 9:33:06 AM 05/12/2023

2305C95-001B NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water ICP METALS, TCLP Leached 05/11/2023 5/12/2023 2:05:00 PM 05/12/2023

2305C95-001B NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water PESTICIDES, TCLP Leached 05/11/2023 5/12/2023 7:46:47 AM 05/12/2023

2305C95-001C NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water Cyanide, Reactive 5/12/2023 12:55:00 PM 05/15/2023

2305C95-001C NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water Sulfide, Reactive 5/15/2023 1:02:00 PM 05/15/2023

2305C95-001D NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water IGNITABILITY 05/11/2023

2305C95-001E NOWRF INFLUENT WET WELL5/9/2023 11:09:00AM Waste Water Hydrogen Ion (pH) by SM4500 H+ B 05/11/2023

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356029

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356029MBLK 05/12/2023SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516285MB-356029

12174155

1,4-Dichlorobenzene 0.10BRL

2,4,5-Trichlorophenol 0.10BRL

2,4,6-Trichlorophenol 0.10BRL

2,4-Dinitrotoluene 0.10BRL

Cresols, Total 0.10BRL

Hexachlorobenzene 0.10BRL

Hexachlorobutadiene 0.10BRL

Hexachloroethane 0.10BRL m,p-Cresol 0.10BRL

Nitrobenzene 0.10BRL o-Cresol 0.10BRL

Pentachlorophenol 0.50BRL

Pyridine 0.10BRL

Surr: 2,4,6-Tribromophenol 00.6101 1.000 61.0 52.7 137

Surr: 2-Fluorobiphenyl 00.3287 0.5000 65.7 47.1 121

Surr: 2-Fluorophenol 00.5898 1.000 59.0 42.3 120

Surr: 4-Terphenyl-d14 00.3322 0.5000 66.4 50.9 127

Surr: Nitrobenzene-d5 00.3347 0.5000 66.9 48.3 119

Surr: Phenol-d5 00.5512 1.000 55.1 45.6 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356029LCS 05/12/2023SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516285LCS-356029

12174156

1,4-Dichlorobenzene 0.100.6675 1.000 66.8 60.1 125

2,4,5-Trichlorophenol 0.100.7134 1.000 71.3 55.3 135

2,4,6-Trichlorophenol 0.100.7412 1.000 74.1 62.2 137

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356029

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356029LCS 05/12/2023SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516285LCS-356029

12174156

2,4-Dinitrotoluene 0.100.6346 1.000 63.5 58.1 137

Cresols, Total 0.101.962 3.000 65.4 56.5 130

Hexachlorobenzene 0.100.6828 1.000 68.3 64.2 135

Hexachlorobutadiene 0.100.7325 1.000 73.2 61.8 133

Hexachloroethane 0.100.6373 1.000 63.7 57.1 134 m,p-Cresol 0.101.289 2.000 64.5 55.5 128

Nitrobenzene 0.100.6837 1.000 68.4 58.9 131 o-Cresol 0.100.6726 1.000 67.3 57.7 134

Pentachlorophenol 0.500.5188 1.000 51.9 51 135

Pyridine 0.100.1590 1.000 15.9 12.7 120

Surr: 2,4,6-Tribromophenol 00.7706 1.000 77.1 52.7 137

Surr: 2-Fluorobiphenyl 00.3754 0.5000 75.1 47.1 121

Surr: 2-Fluorophenol 00.7045 1.000 70.4 42.3 120

Surr: 4-Terphenyl-d14 00.3711 0.5000 74.2 50.9 127

Surr: Nitrobenzene-d5 00.3595 0.5000 71.9 48.3 119

Surr: Phenol-d5 00.6628 1.000 66.3 45.6 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356029MS 05/12/2023SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5162852305E55-002BMS

12174371

1,4-Dichlorobenzene 0.100.5236 1.000 52.4 45.1 119

2,4,5-Trichlorophenol 0.100.2756 1.000 27.6 51.1 127 S

2,4,6-Trichlorophenol 0.100.2815 1.000 28.2 50.1 133 S

2,4-Dinitrotoluene 0.100.5427 1.000 54.3 50.8 134

Cresols, Total 0.100.7726 3.000 25.8 47.6 123 S

Hexachlorobenzene 0.100.5625 1.000 56.2 51.7 130

Hexachlorobutadiene 0.100.5982 1.000 59.8 50 128

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356029

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356029MS 05/12/2023SEMIVOLATILES ORGANICS, TCLP SW1311/8270E

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5162852305E55-002BMS

12174371

Hexachloroethane 0.100.5052 1.000 50.5 49.8 124 m,p-Cresol 0.100.4977 2.000 24.9 47.1 122 S

Nitrobenzene 0.100.5708 1.000 57.1 51.2 124 o-Cresol 0.100.2749 1.000 27.5 49.2 125 S

Pentachlorophenol 0.50BRL 1.000 24.8 42.6 129 S

Pyridine 0.100.3537 1.000 35.4 10 120

Surr: 2,4,6-Tribromophenol 00.3004 1.000 30.0 52.7 137 S

Surr: 2-Fluorobiphenyl 00.2986 0.5000 59.7 47.1 121

Surr: 2-Fluorophenol 00.2151 1.000 21.5 42.3 120 S

Surr: 4-Terphenyl-d14 00.2980 0.5000 59.6 50.9 127

Surr: Nitrobenzene-d5 00.2881 0.5000 57.6 48.3 119

Surr: Phenol-d5 00.2065 1.000 20.6 45.6 120 S

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356030

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356030MBLK 05/12/2023HERBICIDES, TCLP SW1311/8151A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/11/2023 516186MB-356030

12171094

2,4,5-TP (Silvex) 0.20BRL

2,4-D 0.20BRL

Surr: DCAA 00.2903 0.5000 58.1 45 126

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356030LCS 05/12/2023HERBICIDES, TCLP SW1311/8151A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/11/2023 516186LCS-356030

12171095

2,4,5-TP (Silvex) 0.200.3202 0.5000 64.0 46.9 120

2,4-D 0.200.3109 0.5000 62.2 48.3 120

Surr: DCAA 00.2670 0.5000 53.4 45 126

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356030MS 05/12/2023HERBICIDES, TCLP SW1311/8151A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/11/2023 5161862305943-001AMS

12171098

2,4,5-TP (Silvex) 0.200.3309 0.5000 66.2 49.3 120

2,4-D 0.200.3324 0.5000 66.5 47.9 120

Surr: DCAA 00.3252 0.5000 65.0 45 126

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356117

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356117MBLK 05/11/2023Cyanide, Reactive SW846-7.3

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/11/2023 516073MB-356117

12166900

Cyanide, Reactive 1.00BRL

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356117LCS 05/11/2023Cyanide, Reactive SW846-7.3

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/11/2023 516073LCS-356117

12166901

Cyanide, Reactive 1.0010.65 12.50 85.2 54.8 130

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356117MS 05/11/2023Cyanide, Reactive SW846-7.3

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/11/2023 5160732305A64-001CMS

12166903

Cyanide, Reactive 0.98010.00 12.25 81.6 28.2 130

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356117MSD 05/11/2023Cyanide, Reactive SW846-7.3

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/11/2023 5160732305A64-001CMSD

12166904

Cyanide, Reactive 0.98010.34 23.812.25 84.4 28.2 130 10.00 3.37

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356151

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151MBLK 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516178MB-356151

12173304

Chlordane 0.0050BRL

Endrin 0.0010BRL gamma-BHC 0.00050BRL

Heptachlor 0.00050BRL

Heptachlor epoxide 0.00050BRL

Methoxychlor 0.0050BRL

Toxaphene 0.050BRL

Surr: Decachlorobiphenyl 00.005042 0.0050 101 48.2 122

Surr: Tetrachloro-m-xylene 00.004292 0.0050 85.8 41 123

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151LCS 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516178LCS-1-356151

12173305

Endrin 0.00100.009039 0.0080 113 65.4 132 gamma-BHC 0.000500.008098 0.0080 101 67.2 126

Heptachlor 0.000500.008738 0.0080 109 68.9 127

Heptachlor epoxide 0.000500.007642 0.0080 95.5 69.8 130

Methoxychlor 0.00500.03758 0.0300 125 55.3 121 S

Surr: Decachlorobiphenyl 00.005006 0.0050 100 48.2 122

Surr: Tetrachloro-m-xylene 00.004288 0.0050 85.8 41 123

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151LCS 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516178LCS-2-356151

12173306

Chlordane 0.00500.03337 0.0400 83.4 69.4 131

Toxaphene 0.0500.08082 0.0800 101 69.1 129

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356151

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151LCS 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516178LCS-2-356151

12173306

Surr: Decachlorobiphenyl 00.005035 0.0050 101 48.2 122

Surr: Tetrachloro-m-xylene 00.003947 0.0050 78.9 41 123

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151MS 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161782305E55-002BMS-1

12173309

Endrin 0.00100.009158 0.0080 114 60.1 136 gamma-BHC 0.000500.008127 0.0080 102 56.8 127

Heptachlor 0.000500.008981 0.0080 112 51.3 132

Heptachlor epoxide 0.000500.007710 0.0080 96.4 56 132

Methoxychlor 0.00500.03954 0.0300 132 43.9 127 S

Surr: Decachlorobiphenyl 00.004964 0.0050 99.3 48.2 122

Surr: Tetrachloro-m-xylene 00.004079 0.0050 81.6 41 123

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356151MS 05/12/2023PESTICIDES, TCLP SW1311/8081B

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161782305E55-002BMS-2

12173311

Chlordane 0.00500.03423 0.0400 85.6 63.5 132

Toxaphene 0.0500.08565 0.0800 107 62.9 133

Surr: Decachlorobiphenyl 00.005073 0.0050 101 48.2 122

Surr: Tetrachloro-m-xylene 00.004090 0.0050 81.8 41 123

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356161

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356161MBLK 05/12/2023MERCURY, TCLP SW1311/7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516151MB-356161

12171080

Mercury 0.00400BRL

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356161LCS 05/12/2023MERCURY, TCLP SW1311/7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516151LCS-356161

12171081

Mercury 0.004000.04062 0.0400 102 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356161MS 05/12/2023MERCURY, TCLP SW1311/7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161512305E55-001BMS

12171083

Mercury 0.004000.04129 0.0400 103 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356161MSD 05/12/2023MERCURY, TCLP SW1311/7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161512305E55-001BMSD

12171085

Mercury 0.004000.04139 200.0400 103 80 120 0.04129 0.242

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356204

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356204MBLK 05/12/2023ICP METALS, TCLP SW1311/6010D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516193MB-356204

12171363

Arsenic 0.250BRL

Barium 0.500BRL

Cadmium 0.0250BRL

Chromium 0.0500BRL

Lead 0.0500BRL

Selenium 0.100BRL

Silver 0.0250BRL

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356204LCS 05/12/2023ICP METALS, TCLP SW1311/6010D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516193LCS-356204

12171364

Arsenic 0.2505.091 5.000 102 80 120

Barium 0.5004.920 5.000 98.4 80 120

Cadmium 0.02505.074 5.000 101 80 120

Chromium 0.05004.993 5.000 99.9 80 120

Lead 0.05004.995 5.000 99.9 80 120

Selenium 0.1005.181 5.000 104 80 120

Silver 0.02500.5013 0.5000 100 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356204MS 05/12/2023ICP METALS, TCLP SW1311/6010D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161932305944-002AMS

12171366

Arsenic 0.5005.464 5.000 0.2027 105 50 150

Barium 1.005.376 5.000 0.2208 103 50 150

Cadmium 0.05005.195 5.000 104 50 150

Chromium 0.1005.214 5.000 104 50 150

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356204

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356204MS 05/12/2023ICP METALS, TCLP SW1311/6010D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161932305944-002AMS

12171366

Lead 0.1001364 5.000 1295 1380 50 150 S

Selenium 0.2005.279 5.000 106 50 150

Silver 0.05000.5154 0.5000 103 50 150

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356204MSD 05/12/2023ICP METALS, TCLP SW1311/6010D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5161932305944-002AMSD

12171367

Arsenic 0.5005.634 305.000 0.2027 109 50 150 5.464 3.06

Barium 1.005.507 305.000 0.2208 106 50 150 5.376 2.41

Cadmium 0.05005.319 305.000 106 50 150 5.195 2.35

Chromium 0.1005.333 305.000 107 50 150 5.214 2.25

Lead 0.1001445 305.000 1295 3000 50 150 1364 S5.78

Selenium 0.2005.415 305.000 108 50 150 5.279 2.54

Silver 0.05000.5317 300.5000 106 50 150 0.5154 3.11

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356252

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252MBLK 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516243MB-356252

12172916

1,1-Dichloroethene 0.10BRL

1,2-Dichloroethane 0.10BRL

2-Butanone 0.20BRL

Benzene 0.10BRL

Carbon tetrachloride 0.10BRL

Chlorobenzene 0.10BRL

Chloroform 0.10BRL

Tetrachloroethene 0.10BRL

Trichloroethene 0.10BRL

Vinyl chloride 0.040BRL

Surr: 4-Bromofluorobenzene 00.9394 1.000 93.9 78 117

Surr: Dibromofluoromethane 00.9292 1.000 92.9 77.2 124

Surr: Toluene-d8 00.9986 1.000 99.9 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252LCS 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516243LCS-356252

12172915

1,1-Dichloroethene 0.100.8868 1.000 88.7 64.7 131

1,2-Dichloroethane 0.100.7622 1.000 76.2 63 129

2-Butanone 0.202.124 2.000 106 61.7 138

Benzene 0.101.020 1.000 102 76.4 118

Carbon tetrachloride 0.100.7838 1.000 78.4 66.9 136

Chlorobenzene 0.100.9464 1.000 94.6 79.4 117

Chloroform 0.100.8656 1.000 86.6 66.5 122

Tetrachloroethene 0.100.9200 1.000 92.0 75 127

Trichloroethene 0.101.005 1.000 100 77.1 123

Vinyl chloride 0.0400.9018 1.000 90.2 57.1 139

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356252

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252LCS 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 516243LCS-356252

12172915

Surr: 4-Bromofluorobenzene 00.9012 1.000 90.1 78 117

Surr: Dibromofluoromethane 00.8474 1.000 84.7 77.2 124

Surr: Toluene-d8 01.005 1.000 101 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252MS 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5162432305C00-005AMS

12172928

1,1-Dichloroethene 0.100.9362 1.000 93.6 69.4 138

1,2-Dichloroethane 0.100.8114 1.000 81.1 57.1 134

2-Butanone 0.202.103 2.000 105 64.2 135

Benzene 0.101.047 1.000 105 78.9 124

Carbon tetrachloride 0.100.8352 1.000 83.5 72.7 137

Chlorobenzene 0.101.004 1.000 100 81.5 122

Chloroform 0.100.9102 1.000 91.0 65 134

Tetrachloroethene 0.100.9910 1.000 99.1 80.6 129

Trichloroethene 0.101.055 1.000 106 82.4 132

Vinyl chloride 0.0401.021 1.000 102 64.1 135

Surr: 4-Bromofluorobenzene 00.9024 1.000 90.2 78 117

Surr: Dibromofluoromethane 00.8608 1.000 86.1 77.2 124

Surr: Toluene-d8 00.9974 1.000 99.7 80 120

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252DUP 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5162432305C00-005ADUP

12172926

1,1-Dichloroethene 0.10BRL 300 0

1,2-Dichloroethane 0.10BRL 300 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356252

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356252DUP 05/12/2023VOLATILES, TCLP SW1311/8260D

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 05/12/2023 5162432305C00-005ADUP

12172926

2-Butanone 0.20BRL 300 0

Benzene 0.10BRL 300 0

Carbon tetrachloride 0.10BRL 300 0

Chlorobenzene 0.10BRL 300 0

Chloroform 0.10BRL 300 0

Tetrachloroethene 0.10BRL 300 0

Trichloroethene 0.10BRL 300 0

Vinyl chloride 0.040BRL 300 0

Surr: 4-Bromofluorobenzene 00.9464 01.000 94.6 78 117 0.9284 0

Surr: Dibromofluoromethane 00.9432 01.000 94.3 77.2 124 0.9446 0

Surr: Toluene-d8 00.9906 01.000 99.1 80 120 0.9896 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

356308

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356308MBLK 05/15/2023Sulfide, Reactive SW846-7.3

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/15/2023 516341MB-356308

12175614

Sulfide, Reactive 100BRL

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356308MS 05/15/2023Sulfide, Reactive SW846-7.3

NOWRF INFLUENT WET WELL Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/15/2023 5163412305C95-001CMS

12175642

Sulfide, Reactive 100671.9 744.0 90.3 50.3 135

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 356308MSD 05/15/2023Sulfide, Reactive SW846-7.3

NOWRF INFLUENT WET WELL Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 05/15/2023 5163412305C95-001CMSD

12175648

Sulfide, Reactive 100671.9 22.3744.0 90.3 50.3 135 671.9 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

R516016

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: R516016LCS 05/11/2023Ignitability / Flashpoint SW1010B

Units: Prep Date:Sample ID: Client ID: Run No:°F 516016LCS-R516016

12167186

Ignitability 080.00 81.00 98.8 97.5 102.47

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: R516016DUP 05/11/2023Ignitability / Flashpoint SW1010B

Units: Prep Date:Sample ID: Client ID: Run No:°F 5160162305C80-001ADUP

12167188

Ignitability 0149.0 5150.0 >0.669

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

BatchID:Workorder:

Project Name:

ANALYTICAL QC SUMMARY REPORT

NOWRF Influent Wet Well

2305C95

Athens-Clarke Co Unified Government

R516055

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: R516055LCS 05/11/2023Hydrogen Ion (pH) by SM4500H+B-2011

Units: Prep Date:Sample ID: Client ID: Run No:pH Units 516055LCS-R516055

12166825 pH 0.01007.031 7.000 100 90 110

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: R516055DUP 05/11/2023Hydrogen Ion (pH) by SM4500H+B-2011

Units: Prep Date:Sample ID: Client ID: Run No:pH Units 5160552305D14-001BDUP

12166827 pH 0.01006.601 206.568 0.501

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

End of Report