Attachment 2- Summary of Technical Specifications for 600 MHz Spectrometer System.xlsx

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600 MHz Spectrometer System
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N0017326RFIMR11
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This is a technical specifications document for a 600 MHz Nuclear Magnetic Resonance (NMR) Spectrometer System being sought by the Naval Research Laboratory (NRL). The specification details the required components of a high-field spectrometer console, including a minimum of 3 RF transmitter channels with 12.5 nanosecond timing resolution across a 15 to 600 MHz frequency range, 1 GB pulse sequencer waveform memory, and four trigger inputs. The receiver must digitize signals from 10 to 600 MHz with up to 10 MHz spectral width and digital resolution capabilities of 17 and 19 bits, controllable gain greater than 60 dB in 6 dB steps, and recovery time under 3 milliseconds. The system requires two high-power RF amplifiers for 1H and 19F operations at 600 and 564 MHz with minimum 500 W peak power, plus additional lower-frequency amplifiers and multiple RF preamplifiers with varying noise figures and power capabilities to support various nuclei observations including 57Fe, 19F, 13C, and 2H.

The spectrometer must also include hardware accessories such as gradient amplifier equipment compatible with solution NMR probes, low-temperature operation capability down to 77 K, high-temperature operation up to 150°C, a microprocessor-based MAS pneumatic unit maintaining spinning accuracy within 0.1%, gas flow control systems, field lock equipment, and necessary RF filters. A superconducting magnet with standard 54 mm bore size and very high field stability with guaranteed drift rate specifications is required. Supporting computer and software requirements for spectrometer control, data processing, and pulse programming are referenced separately. This Sources Sought Notice (RFI N00173-26-RFI-MR11) was posted April 14, 2026, with responses due April 29, 2026, at 3pm EST to primary point of contact Maribel Ramirez, and represents pre-solicitation market research with no financial commitment or guarantee of competition on SAM.gov.

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Sheet1 Requirements for High Field 600 MHz Nuclear Magnetic Resonance Spectrometer

#Description
1Spectrometer Console: all electronics except NMR probes
1aTransmitter
A minimum of 3 RF transmitter channels
Minimum of 12.5 ns timing resolution on each channel
Synchronicity on all channels within 12.5 ns
Frequency range for each channel of 15 to 600 MHz (41K to 1H)
1 GB pulse sequencer waveform memory with specific minimum capabiliites of amplitude, phase, and frequency switching--see Table 1.
4 trigger inputs with 12.5 ns resolution
2 high frequency high power RF amplifiers for 1H and 19F observe and decoupling at 600 and 564 MHz respectively with minimum RF peak power of 500 W
2 low frequency high power RF amplifiers for X observe and decoupling at 15 to 600 MHz with minimum RF peak power of 500 W
1bReceiver--Note that the RF channels may transmit and receive
Capable of digitizing signals in the frequency range of 10 to 600 MHz 15-242 MHz (41K to 31P)
Up to a 10 MHz spectral width and a digital resolution of 17 and 19 bits for SWH < 5 MHz and 1 MHz respectively
The gain within the receiver console must be controllable over a range greater than 60 dB in ≤6 dB steps.
The recovery time from end of blanked pulse to linear operation within the receiver console much be less than 3 ms.
Two high power high frequency RF preamplifiers for 1H and 19F observe, 1H and 19F decoupling and 19F lock operation featuring ~1.0 dB system noise figure, maximum 4 kW peak power RF capability, active transmit/receive switch and built-in RF power detector
Two high power high frequency RF preamplifiers for observe and decoupling of nuclei from 57Fe up to 19F with built-in 1H Stop RF filter featuring ~1 dB system noise figure, maximum 4 kW peak power RF capability, active transmit/receive switch
Preamplifier for observe and decoupling of nuclei from 57Fe up to 19F with built-in 1H Stop RF filter featuring ~1.4 dB system noise figure, maximum 500 W peak power RF capability, active transmit/receive switch
Preamplifier for 13C observe and decoupling operation featuring ~1.4 dB system noise figure, maximum 500 W peak power RF capability, active transmit/receive switch and built-in RF power detector
High power RF preamplifier for 2H observe, 2H decoupling and 2H lock operation featuring ~1.4 dB system noise figure, maximum 500 W peak power RF capability, active transmit/receive switch and built-in RF power detector
1cHardware accessories
Gradient amplifier equipment compatible with solution NMR probe
Low temperature equipment including digital control unit to allow operation down to 77 K
High temperature equipment including digital control unit to allow operation up to 150 °C
Microprocessor based MAS pneumatic unit capable of maintaining spinning accuracy to < 0.1% over entire temperature operation range for all probes purchased.
Gas flow system to control sample insert/eject and variable temperatures within probes
Field lock equipment
RF filters necessary to achieve the full acquisition capabilities of the Spectrometer and the NMR probes, e.g., High pass RF filter with Pass Band 1H and Stop Band < 31P and 19F ; Low Pass RF filter with Pass Band < 31P and Stop Band 1H - 19F
1dComputer and software
A detailed description of the computer used to control the Spectrometer and the software requirements for processing and pulse programming are provided separately.
2Superconducting Magnet
Standard Bore (SB) with 54 mm bore size
Very high field stability with a guaranteed drift rate of <10 ppb/hr
Low loss cryostat with 365-day (1-year) helium hold time under stabilized conditions (T=20 °C, p=1030 mbar)
Small fringe field in vertical and horizontal direction--5 Gauss line must be within 3 m in all directions
Cryogenically cooled high order shim system with 14 shim gradients
Room temperature shim system with 36 shim gradients, current sources, B0 coils, and temperature sensor
Magnet stand with damping system
Helium flow system with one-way check valve for safe operation
Helium level measurement system including alarm functions for low helium levels
Nitrogen level sensor with direct display function
Helium transfer line for standard ceiling height.
3NMR probes
3aSolution NMR probe optimized for direct X-nuclei observation with 1H and/or 19F decoupling and for 1H observation (indirect detection).
X-nuclei frequency range 19F (564 MHz), 31P (243 MHz)-109Ag (28 MHz) excluding 171Yb (106 MHz)-9Be (84 MHz)
Designed for 1H and/or 19F decoupling
Minimum 19F background
Compatible with 2H lock
Incorporates Z-gradient with 5 G/A*cm when used with gradient amplifier equipment
Variable temperatue (VT) range: -150 °C to +150 °C
Automatic tuning and matching.
3bDouble resonance X/F-H 0.7 mm CP-MAS probe for solid state NMR probe with maximum rotation frequency of 111 kHz
Maximum rotation frequency equal to 111 kHz or greater
X tuning range from 15N to (61 MHz) to 31P (243 MHz).
High power 1H or 19F decoupling
Active sample volume: 0.35 ul
Variable temperature range: 5 °C to 50 °C
Rotor test station for checking the spinning properties of 0.7 mm MAS rotors before NMR measurements--includes base station and module optimized for 0.7 mm rotors
0.7 mm MAS ZrO2 Rotors and related tools
Stereo Microscope 40x magnification used to support packing of 0.7 mm MAS rotors
3bHFXY MAS probe for solid state NMR with interchangeable probe heads
600 MHz HFXY probe base module compatible with Standarcd Bore (SB) magnet
600 MHz 1.6 mm HFXY NB Probe Head with 1.6 mm Vespel Spinning System and X/Y Channel Tuning Plug-ins--see document for detailed specifications
600 MHz 2.5 mm HFXY NB Probe Head with 2.5 mm Vespel Spinning System and X/Y Channel Tuning Plug-ins--see document for detailed specifications
1.6 mm packing tools and rotors--minimum of 15 rotor assemblies
2.5 mm packing tools and rotors--minimum of 15 rotor assemblies
Low gamma tuning Kit which extends tuning to ~12MHz (required for 41K)
Light illumination capability

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