Attachment 2 PWS.pdf

Performance Work Statement

LABORATORY ANALYTICAL SUPPORT SERVICES

1. SCOPE OF WORK. Work to be performed consists of laboratory analysis in support of various analytical requirements, including, but not limited to:

Routine wastewater discharge monitoring as required by permit.

Monthly Storm Water Monitoring

Special water and wastewater studies (short or long term).

Hazardous waste analysis.

Soil analysis.

Asbestos sample analyses, both air and bulk, and third party air monitoring for asbestos abatement projects.

Air samples associated with industrial hygiene monitoring.

2. GENERAL DESCRIPTION OF WORK

2.1 Contractor shall, from time to time, be required to provide sample collection and/or analytical support for routine monitoring requirements, emergency requirements and various projects/studies shown in paragraph 1 and others as may be needed. This support will be on an "as needed" basis as requested by the contracting officer or his designated representative. Parameters to be analyzed, sample pickup location and any special requirements will be provided at the time of the request.

2.2 Other Provisions

2.2.1. Written results for all samples shall be provided to the contracting officer and the contracting officer representative on the analytical report form shown in Attachment 1 to this PWS, or equivalent, within ten

(10) days of sample pickup (except for asbestos samples, see below) unless authorized otherwise. Written reports shall contain the information shown on the aforementioned form plus any remarks indicating any departure from standard procedure or anything unusual about the sample which might indicate a questionable result.

2.2.1.1. Asbestos reporting - Asbestos sample results shall be provided within five (5) days of sample pickup, or, in the case of mailed samples, within five (5) days of receipt. Results of asbestos Transmission Electron Microscopy (TEM) sample analyses shall be provided within forty-eight (48) hours of sample pickup, or, if mailed, sample receipt. The technician performing the analysis shall sign all asbestos laboratory reports of analyses.

2.2.2. Some samples may require a 24-hour turnaround due to the critical nature of information to support construction and operational programs and emergencies. In this case, telephonic (verbal) or electronic facsimile results are acceptable. However, formal written results must be submitted within the time frames indicated in paragraph 2.2.1.

2.2.3. Approved Analyses - Unless otherwise authorized, all analyses shall be performed in accordance with methods approved by the Environmental Protection Agency.

2.2.4. Laboratory/Laboratory Technician Certification

2.2.4.1. Water - Contractor’s laboratory and any subcontract laboratory expected to perform analyses under this contract shall be certified in the applicable categories by the Oklahoma Department of Environmental Quality (ODEQ).

2.2.4.2. Asbestos Laboratory – The contractor’s laboratory and any subcontract laboratory expected to perform asbestos analyses under this contract shall:

(1) For bulk asbestos analysis:

(A) Be certified by the National Voluntary Laboratory Accreditation Program for laboratories providing bulk analyses, or

(B) Participate in the AIHA Bulk Asbestos Proficiency Testing Program and have received a minimum score of 75% correct on the latest two rounds.

(2) For NIOSH Method 7400 (PCM) fiber counting analysis:

(A) Participate in the AIHA Proficiency Analytical Testing (PAT) program and have been rated proficient for the latest two rounds, or

(B) Have all individual analysts participate in the AIHA Asbestos Analyst Registry (AAR) program and have been rated proficient for each analyst.

(3) For TEM analysis, the laboratory shall participate in the National Voluntary Laboratory Accreditation Program for laboratories providing fiber-counting analyses using TEM.

2.2.4.3. Asbestos Laboratory Technician Requirements - The laboratory shall also utilize only laboratory technicians who have successfully completed State of Oklahoma Department of Labor (DOL) approved courses in the type of analyses performed by the technician. All technicians performing PCM analysis shall have successfully completed the NIOSH course No. 582 on "Sampling and Analysis of Airborne Asbestos Dust," or DOL approved equivalent. All technicians performing bulk analyses must have successfully completed a four-day course, or DOL approved equivalent, in the bulk analysis of asbestos-containing materials. Required courses shall have been provided by a government agency or an educational institution.

2.2.4.4. Asbestos Sampling Technician Requirements - Technicians collecting bulk samples shall have a valid Oklahoma AHERA Asbestos Inspector's license. Technicians performing routine air monitoring shall have successfully completed the NIOSH course No. 582 on "Sampling and Analysis of Airborne Asbestos Dust," or another DOL approved course on asbestos air monitoring techniques and procedures. Technicians performing air monitoring for asbestos abatement projects shall have the following minimum qualifications:

(1) Have successfully completed the NIOSH course No. 582 on "Sampling and Analysis of Airborne Asbestos Dust," or a DOL approved equivalent.

(2) For entry into contained work areas, have a current medical examination and clearance to wear a respirator.

(3) Have been fit tested for a respirator and be familiar with personal protection procedures required for abatement activities.

(4) Have a valid Oklahoma Asbestos Abatement Worker's License.

Required courses shall have been provided by a government agency or an educational institution.

2.2.5. Sample Holding Times - Contractor shall ensure that samples are analyzed within the appropriate holding times for each parameter.

2.2.6. Chain-of-Custody Forms - Chain-of-custody forms shall be completed and submitted by the contractor with sample results. The forms shown in Attachment 2 to this PWS, or equivalent, shall be used for this purpose. The sampling technician will indicate the time of arrival on site and time of departure on the form. The contracting officer's representative will verify that the times are correct by initialing the form upon completion of sampling, before the technician leaves the Aeronautical Center.

2.2.7. Quality Control Plan (QCP) - Contractor and any subcontract lab expected to perform analyses under this contract shall have an active, written quality control plan. This plan must address, at a minimum, the items shown in Attachment 3 to this PWS.

2.2.8. Emergency Response Plan (ERP) - Contractor shall prepare an Emergency Response Plan that explains how the contractor will meet the 24-hr/ 7 days per week basis. The plan must show what means of transportation will be used to get contractor personnel on site, estimated sample taking times, method of packing and packaging of samples, transportation methods to return samples to contractors testing facilities, testing times, and method of getting results back to the site. (Note: The possibility exists that a given sample could not be shipped by air under DOT Hazardous Material Transportation Regulations (49 CFR).

Contractors that rely on air transportation to meet time requirements must explain fully how these samples will be transported.)

2.2.9. Records Retention - The contractor and all subcontract labs shall retain sample results and all quality control data generated relative to any test (e.g. blanks, duplicates, spikes and standards) for at least 60 days after submission of results to the FAA. The Contracting Officer may request submission of such quality control data at any time within that time frame.

2.2.10. Subcontract Lab - Contractor shall not utilize a subcontract lab for any analyses without prior approval of the contracting officer. Any subcontract lab selected shall meet the same quality control standards as are required of the contractor as specified in paragraphs 2.2.1. through 3

3. Security Requirements - All contractors associated with this contract will be required to complete and pass a security back ground check for badging purposes in order to complete all required work at the

MMAC.

3.1 The Contracting Officer Representatives for this contract will be Robert Griffin (Primary) and Vicki Ray (alternate) from the Facility Services AMP-100 Environmental Occupational Health and Safety (EOSH) Division.

Attachment 1

Example Analytical Report Form

Laboratory Analytical Result Form

Client: FAA Mike Monroney Aeronautical Center, AMP-100 Date Received:

Address: 6500 S. MacArthur Blvd Analyst Completed:

Oklahoma City, OK 73125 Analyst:

Project: Received By:

Req. By: Lab Log. No:

Sampling Location:

Field Sample ID

Parameter Media/Collection Method Method Detection Limit

Result Units

ND = Not Detected NA = Not Applicable

Reported By: _____________________ Reviewed By: _____________________ (Analyst)

Attachment 2

CHAIN OF CUSTODY RECORD

Page __1__ of ___1__

Samples From: FAA - MMAC - AMP-100 Contact: Date:

Address: P.O. Box 25082 City: Oklahoma City State: Oklahoma Zip: 73125 Phone: (405) 954-0784

Sampled By: Project I.D.: Fax: (405) 954-0013

Number Of Samples Received: Method of Payment (P.O.,VISA, MC, AmEx) : Contract P.O.#:

Item Sample Number

Sample Description

Lab Number

P

A

R

A

M

E

T

E

R

S

Remarks

Relinquished By: Date: Time: Received By: Parameters: Parameters: Parameters:

A. Organics (specify)

H. Metals (total)

O. Asbestos (plm)

B. GRO (C6 to C110) I. Metals (tclp) P. Asbestos (pcm)

C. DRO(C10 to C28 ) J. Metals (specify)

Q. Asbestos (tem)

D. Pesticides K. pH R. SEM (specify)

E. PCB’s L. TDS S.

F. Flashpoint M. TSS T.

G. Other N. Other U. Other

Attachment 3 to PWS

QUALITY CONTROL PLAN

Contractor shall provide a Quality Control Plan (QCP) for itself and any subcontract lab expected to perform any analyses under this contract. Contractor's QCP must demonstrate conformity with EPA recommended laboratory quality control procedures as described in such documents as 40 CFR 136 and EPA's "Handbook for Analytical Quality Control in Water and Wastewater Laboratories," September 1982.

Each QCP shall contain the following information:

a. Laboratory Organization and Responsibility - Indicate the personnel who will be involved in the analyses and what their responsibilities will be. Provide a brief resume for each person indicating his or her qualifications to perform the required work. The laboratory supervisor shall have a B.S. in either Chemistry or Chemical Engineering and at least three years experience in analytical techniques needed to perform the tests listed in the Performance Work Statement.

b. Quality Control Objectives for Measurement Data - Include a list of all parameters listed in Attachment 4, the reference of the method to be used (EPA or other) along with precision, accuracy and completion objectives as percent of samples analyzed.

c. Sample Custody and Holding Procedures - Describe how EPA holding times will be met, sample preservative preparation methodology, sample container identification such as marking and labeling, field tracking forms to be used, name and title of designated sample custodian, and how sample custody is maintained until completion of analysis.

d. Calibration Procedures and Frequency - Describe frequency and method of calibration of all instruments and equipment. Describe preparation of reagent standards to be used for laboratory analyses.

e. Data Reduction, Validation and Reporting - Briefly describe procedures used to reduce, validate and report data generated in the laboratory.

f. Internal Quality Control Checks and Frequency - Describe how spike, duplicate, blank and standard analyses are used to maintain quality control, generation frequency and method of constructing quality control charts, participation in EPA or state laboratory quality control programs and laboratory management review of quality control results.

g. Performance and System Audits and Frequency - Describe any external performance audits or inspections made on the laboratory by EPA or state inspectors within the past year and the results of these inspections. Also describe management review frequency and procedures for evaluating analytical procedures, facilities and sampling methodologies. Include the type and frequency of quality assurance reports submitted to laboratory management. Also, describe actions taken in the event that precision or accuracy data fall outside the boundaries of quality control chart limits.

h. Preventive Maintenance Procedures and Schedules - Describe preventive maintenance of laboratory equipment. Include such items as analytical balance, pH meter and water distillation unit.

i. Asbestos Microscope Requirements - The laboratory shall certify the following:

(1) That phase contrast microscopes used for fiber counting meet the specifications of NIOSH Method 7400, including verification of the microscope-resolving power by means of an HSE/NPL phase-shift test slide.

(2) That all microscopes have been checked with a phase-shift test slide.

(3) That all microscopes are checked with a phase-ring-centering telescope after having been moved.

Attachment 4 to PWS

ANALYTICAL TESTS

GAS CHROMATOGRAPHY/MASS SPECTROSCOPY (GC/MS)

1. Volatile Priority Pollutants

1a. Purgeable Halocarbons (EPA 601) 1b. Purgeable Aromatics (EPA 602) 1c. Acrolein and Acrylonitrile (EPA 603) 1d. Volatile Organics (EPA 624)

2. Acid Extractable Priority Pollutants

2a. Cresols 2b. Phenols

3. Base - Neutral Extractable Priority Pollutants

3a. Polynuclear Aromatic Hydrocarbons 3b. Halo Ethers 3c. Benzidines 3d. Chlorinated Hydrocarbons 3e. Nitroaromatics and Isophorone 3f. Phthalate Esters 3g. Nitrosamines 3h. 1,2-Diphenylhydrazine (as Azobenzene)

GAS CHROMATOTOGRAPHY/ELECTRON CAPTURE

DETECTOR (GC/ECD)

4. Pesticides, herbicides, polychlorinated biphenyl compounds (PCBs) 4a. In water (routine) 4b. In soil (routine) 4c. PCB's in soil (within 24 hours) 4d. PCB's in water (within 24 hours) 4e. PCB’s in oil (routine) 4f. PCB’s in oil (within 24 hours) 4g. PCB wipe test (report as mg/100 cm2

GAS CHROMATOGRAPHY/FLAME IONIZATION

DETECTOR (GC/FID)

5. Total petroleum hydrocarbons, gasoline, diesel 5a. In water: routine 5b. within 24 hours 5c. In soil: routine 5d. within 24 hours

6. Benzene-toluene-ethyl benzene-xylene (BTEX) 6a. In water: routine 6b. within 24 hours 6c. In soil: routine 6d. within 24 hours

ASBESTOS

7. Air samples - Transmission electron microscopy (NIOSH 7402, modified) 7a. routine (within 48 hours) 7b. blank

8. Phase contrast microscopy (PCM) (NIOSH 8a. routine 8b. within 24 hours 8c. blank

9. Bulk analysis 9a. routine 9b. within 24 hours 9.c. point counting

10. Water samples 10.a routine

DIOXINS

11. 2,3,7,8-Tetrachlorodibenzo-P-Dioxin

HAZARDOUS WASTE ANALYSES

12. Specific Gravity

13. Ignitability

14. Corrosivity

15. Reactivity

16. Toxicity Characteristic Leaching Procedure

(TCLP)

16a. Extraction procedure 16b. Metals analysis 16c. Pesticides analysis 16d. Organic analyses 16d.i Volatile organics 16d.ii Semi-volatile organics

OTHER ANALYSES

17. Total dry solids

18. Volatile solids

19. pH

20. Thermal content (BTUs/unit weight)

21. Infrared spectra

22. Soil permeability

23. Total halogens (TOX, waste oil)

24. Total Metals (Method 6010A, Sw-846) 24.a. 26 metals 24.b. Single metal 24.c. Digestion

WATER/WASTEWATER

25. pH

26. Biochemical Oxygen Demand

27. Carbonaceous Biochemical Oxygen Demand

28. Chemical Oxygen Demand

29. Color

30. Fecal Coliform

31. Oil and Grease

32. Total Dissolved Solids

33. Total Organic Carbon

34. Total Suspended Solids

35. Turbidity

36. Ammonia nitrogen

37. Bromide

38. Chloride

39. Chlorine, total residual

40. Cyanide, free

41. Cyanide, total

42. Fluoride

43. Nitrate nitrogen

44. Nitrite nitrogen

45. Nitrate/nitrite

46. Nitrogen, kjeldahl

47. Nitrogen, organic

48. Phenols

49. Phosphates, Total as P

50. Sulfate

51. Sulfide, as S

52. Sulfite, as SO3

53. Surfactants

54. Aluminum

55. Antimony

56. Arsenic

57. Barium

58. Beryllium

59. Boron

60. Cadmium

61. Chromium, hexavalent

62. Chromium, total

63. Cobalt

64. Copper

65. Iron

66. Lead

67. Magnesium

68. Manganese

69. Mercury

70. Molybdenum

71. Nickel

72. Selenium

73. Silver

74. Thallium

75. Tin

76. Titanium

77. Zinc

Radioactivity:

78. Alpha, total

79. Beta, total

80. Radium, total

81. Radium 226, total

INDUSTRIAL HYGIENE SAMPLES - BIOLOGICAL

BioAerosols - Active Sampling

82. Report Mold-Colony-Forming Units 82.a. air 82.b. bulk 82.c. swipe

83. Report Bacteria-Colony Forming Units 83a. air 83b. bulk 83c. swipe

84. Microscopy 84.a. Allergenco slide analysis (spore trap-visual microscopic analysis) 84.b. Tape lift analysis

85. CFU Speciation (up to 8 Species) 85.a. air

85.b. bulk 85.c. swipe

INDUSTRIAL HYGIENE SAMPLES - ORGANIC

86. Formaldehyde analysis of sample 86.a. media1 86.b. air 86.c. swipe

87. Formaldehyde analysis of sample 87.a. media1 87.b. air 87.c. swipe

88. Gas Chromatography, air samples 88.a. Charcoal tube – 1st Parameter 88.b. Charcoal tube– Each Additional 88.c. Passive Badge – 3 Parameters 88.d. Passive Badge – Blank

89. Gas Chromatography/ Mass Spectroscopy (GC/MS) 89.a. Qualitative scan – air 89.b. Qualitative scan - bulk 89.c. Qualitative scan - swipe 89.d. Quantitative scan – air 89.e. Quantitative scan - bulk 89.f. Quantitative scan – swipe

90. High Pressure Liquid Chromatography (HPLC) 90.a. MDI2, TDI3, HDI4, NDI5 media1 90.b. MDI, TDI, HDI, NDI in air 90.c. Analysis of blank air sample

INDUSTRIAL HYGIENE SAMPLES – INORGANIC

91. High Pressure Liquid Chromatography (HPLC), air samples 91.a. Inorganic Acids 91.b. Anion Scan

1 250 milliliters of sample media 2 MDI = Methylenediphenyl isocyanate or diphenylmethane-4,4’-diisocyanate or methylenebisphenyl isocyanate.

3 TDI = 2,4-TDI (Toluene-2,4-diisocyanate) or

2,6-TDI (Toluene-2,6-diisocyanate) 4 HDI = Hexamethylene diisocyanate 5 NDI = Naphthylene diisocyanate

92. Scanning Electron Microscopy (SEM) 92.a. Analysis of sample, air 92.b. Analysis of sample, bulk 92.c. Analysis of sample, swipe 92.d. Photo documentation, per photo

93. Metals (including preparation), air samples 93.a. Analysis for first parameter 93.b. Each additional parameter 93.c. Analysis for special parameters

94. Metals – solids, bulk 94.a. Sample Preparation 94.b. Analysis for first parameter 94.c. Each additional parameter 94.d. Analysis for special parameters

INDUSTRIAL HYGIENE SAMPLES - PARTICULATE

95. Gravimetric Analysis, air 95.a. Total Particulates 95.b. Respirable Fraction

INDUSTRIAL HYGIENE SAMPLES - DRINKING WATER

96. Metals 96.a. Primary Standard for eight RCRA 96.b. Sample Preparation

97. Inorganic 97a. Secondary Standard parameters