Attachment_15_Laboratory_Testing_Requirements__1.pdf

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NIH Water Treatment Program
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Attachment 15

Laboratory Test Protocols

1. Adenosine Tri - Phosphate (ATP) (Method described in “LuminUltra” ( user manual)

2. Calcium hardness, magnesium hardness, iron, copper, zinc, sodium, potassium, chloride, sulfate, silica, bromide, aluminum, barium, manganese, orthophosphate, phosphate. (Detection using ICP-AES, EPA 200.7 protocol)

3. Chloride (EPA Method 9252A)

4. Sulfate, phosphate, orthophosphate (ASTM Standard D4327 - 17, Standard Test Method for

Anions in Water by Suppressed Ion Chromatography)

5. Bromide (ASTM D1246-16, Standard Test Method for Bromide Ion in Water)

6. Nitrate (Either Cadmium reduction method or Nitrate electrode method by following EPA method 5.7 https://archive.epa.gov/water/archive/web/html/vms57.html)

7. Benzotriazole and tolytriazole (Contractor’s In- House High Performance Liquid

Chromatography (HPLC) method provided by contractor for review .)

8. Total suspended solids (Standard Methods (2005) 2540D and EPA (1983) Method 160.2)

9. Turbidity (The test is measured by a nephelometer, following EPA Method 180.1)

10. Monthly legionella test (ISO 11731 testing protocol)

11. Amine sampling in air (PV2016 by OSHA)

12. NPDES total and dissolved copper tests (EPA 200.8)

13. Particle size distribution analysis on side stream filters (ISO 21501-2 in compliance with ISO

17025) https://archive.epa.gov/water/archive/web/html/vms57.html

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