Attachment 1 Sand Analysis results.pdf

PDF 1 MB Posted Nov 17, 2025

Attached to: NFPC Sand Disposal
Solicitation number: N6449826Q50030001
Issued by: Department of the Navy Naval Sea Systems Command

About this file

Written by GovTribe AI · Nov 17, 2025

This is a Certificate of Analysis (COA) from ALS Environmental laboratory for Tradebe Environmental Services, LLC, documenting TCLP (Toxicity Characteristic Leaching Procedure) EPA 1311 metal analysis on six oil/other samples collected on 06/11/2025. The samples were collected by CBC (presumably a client representative) and received by the lab on 06/19/2025.

The analytical results detected varying levels of metals across the samples, including barium (ranging from non-detect to 0.29 mg/L), lead (ranging from non-detect to 0.043 mg/L), cadmium (ranging from non-detect to 0.065 mg/L), and chromium (ranging from non-detect to 0.049 mg/L). The analysis was performed using SW846 methods 6010C (for metals) and 7470A (for mercury), with all samples processed using EPA method 1311 leaching procedure. The lab is NELAP (National Environmental Laboratory Accreditation Program) accredited and the report includes detailed quality control data, preparation methods, and analytical batch information.

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Main Site: 301 Fulling Mill Road | Middletown, PA 17057 | Phone: 717-944-5541 | www.alsglobal.com

Associated Site: 20 Riverside Drive | Spring City, PA 19475 | Phone: 610-948-4903 |

NELAP Certifications: NJ PA010 , NY 11759 , PA 22-293 DoD ELAP: PJLA 74618

State Certifications: FL E871113 , WA C999 , MD 128 , VA 460157 , WV DW 9961-C , WV 343, NJ PA101

25F6068 MLK PSY

3421555Workorder

Certificate of Analysis

Project

Tradebe Environmental Services, LLCAnalytical Results Report For

436998 on 7/9/2025Report ID

Enclosed are the analytical results for samples received by the laboratory on Jun 19, 2025.

The ALS Environmental laboratory in Middletown, Pennsylvania is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet the requirements of NELAP.

If you have any questions regarding this certificate of analysis, please contact Susan Scherer (Project Coordinator) at (717) 944-5541.

Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state requirements.

The test results meet requirements of the current NELAP standards or state requirements, where applicable. For a specific list of accredited analytes, refer to the certifications section of the ALS website at www.alsglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads.

This laboratory report may not be reproduced, except in full, without the written approval of ALS Global.

ALS Middletown: 301 Fulling Mill Road, Middletown, PA 17057 : 717-944-5541.

Recipient(s):

Justin Gelvin - Tradebe Environmental Services

Report Distribution - Tradebe Environmental Services

Scott Sanabria - Tradebe Environmental Services LLC

This page is included as part of the Analytical Report and must be retained as a permanent record thereof.

Susan Scherer

Project Coordinator

Susan Scherer (ALS Digital Signature)

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 1 of 19 http://www.alsglobal.com

25F6068 MLK PSY

3421555

Project

Workorder

Sample Summary

Collection CompanyLab ID Sample ID Matrix Date Collected Date Received Collector

3421555001 Oil/Other 06/11/2025 08:00 06/19/2025 10:12 CBCSample 1-5148 Collected By Client

3421555002 Oil/Other 06/11/2025 08:00 06/19/2025 10:12 CBCSample 2-5148 Collected By Client

3421555003 Oil/Other 06/11/2025 08:00 06/19/2025 10:12 CBCSample 3-5148 Collected By Client

3421555004 Oil/Other 06/11/2025 08:00 06/19/2025 10:12 CBCSample 4-5148 Collected By Client

3421555005 Oil/Other 06/11/2025 08:05 06/19/2025 10:12 CBCSample 5-BLDG 20 Collected By Client

3421555006 Oil/Other 06/11/2025 08:05 06/19/2025 10:12 CBCSample 6-BLDG 28 Collected By Client

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 2 of 19

Project

Workorder

Reference

Notes

Samples collected by ALS personnel are done so in accordance with the procedures set forth in the ALS Field Sampling Plan (20 - Field

Services Sampling Plan).

Except as qualified, Clean Water Act sample analyses are consistent with methodology requirements in 40 CFR Part 136, including but not limited to the following EPA Method reference revisions:

EPA 300.1 Rev. 1.0-1997

EPA 300.0 Rev. 2.1-1993

EPA 353.2 Rev. 2.0-1993

EPA 410.4 Rev. 1.0-1993

EPA 420.4 Rev. 1.0-1993

EPA 365.1 Rev. 2.0-1993

EPA 200.7 Rev. 4.4-1994

EPA 200.8 Rev. 5.4-1994

EPA 245.1 Rev. 3.0-1994

Except as qualified, Safe Drinking Water Act sample analyses are consistent with methodology requirements in 40 CFR Part 141.

The Chain of Custody document is included as part of this report.

All Library Search analytes should be regarded as tentative identifications based on the presumptive evidence of the mass spectra.

Concentrations reported are estimated values.

Parameters identified as "analyze immediately" require analysis within 15 minutes of collection. Any "analyze immediately" parameters not listed under the header "Field Parameters" are preformed in the laboratory and are therefore analyzed out of hold time.

Method references listed on this report beginning with the prefix “S” followed by a method number (such as S2310B-97) refer to methods from “Standard Methods for the Examination of Water and Wastewater”.

For microbiological analyses, the "Prepared" value is the date/time into the incubator and the "Analyzed" value is the date/time out the incubator.

An Analysis-Prep Method Cross Reference Table is included after Analytical Results & Qualifiers section in this report.

Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis.

Standard Acronyms/Flags

Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyteJ

Indicates that the analyte was Not Detected (ND) above the MDLU

Indicates presumptive evidence of the presence of a compoundN

Method Detection LimitMDL

Practical Quantitation LimitPQL

Practical Quantitation Limit for this ProjectRDL

Not Detected - indicates that the analyte was Not DetectedND

Analysis was performed using this containerCntr

Regulatory LimitRegLmt

Laboratory Control SampleLCS

Matrix SpikeMS

Matrix Spike DuplicateMSD

Sample DuplicateDUP

Percent Recovery%Rec

Relative Percent DifferenceRPD

DoD Limit of DetectionLOD

DoD Limit of QuantitationLOQ

DoD Detection LimitDL

Indicates reported value is greater than or equal to the Method Detection Limit (MDL) but less than the Report Detection Limit (RDL)I

Surrogate Compound(S)

Not CalculatedNC

Result outside of QC limits*

Please reference the result in the Results Section for analyte-level flags.#

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 3 of 19

Project

Workorder

Project Notations

Sample Notations

Sample IDLab ID

Notation Ref.

Result Notations

The QC type CRDL for method SW846 6010B was outside the control limits for the analyte

Arsenic. The % RSD was reported as 28.77 and the control limits were 0 to 20. MSY

7/1/25

The QC type CRDL for method SW846 6010B was outside the control limits for the analyte

Selenium. The % RSD was reported as 20.25 and the control limits were 0 to 20. MSY

7/1/25

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 4 of 19

Project

Workorder

Detected Results Summary

3421555001Lab Sample ID

Sample 1-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

Not applicable for this WO.

Result MethodCompound Units RDL Flag

TCLP EPA 1311 METALS

Barium, Total mg/L 0.0500.070 #SW846 6010C

Lead, Total mg/L 0.0300.037 #SW846 6010C

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 5 of 19

Project

Workorder

Detected Results Summary

3421555002Lab Sample ID

Sample 2-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

Not applicable for this WO.

Result MethodCompound Units RDL Flag

TCLP EPA 1311 METALS

Barium, Total mg/L 0.0500.060 #SW846 6010C

Lead, Total mg/L 0.0300.030 #SW846 6010C

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 6 of 19

Project

Workorder

Detected Results Summary

3421555003Lab Sample ID

Sample 3-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

Not applicable for this WO.

Result MethodCompound Units RDL Flag

TCLP EPA 1311 METALS

Barium, Total mg/L 0.0500.069 #SW846 6010C

Cadmium, Total mg/L 0.00990.012 #SW846 6010C

Chromium, Total mg/L 0.0250.030 #SW846 6010C

Lead, Total mg/L 0.0300.043 #SW846 6010C

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 7 of 19

Project

Workorder

Detected Results Summary

3421555005Lab Sample ID

Sample 5-BLDG 20Client Sample ID 06/11/2025 08:05

06/19/2025 10:12

Collected

Lab Receipt

Not applicable for this WO.

Result MethodCompound Units RDL Flag

TCLP EPA 1311 METALS

Cadmium, Total mg/L 0.0200.065 #SW846 6010C

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 8 of 19

Project

Workorder

Detected Results Summary

3421555006Lab Sample ID

Sample 6-BLDG 28Client Sample ID 06/11/2025 08:05

06/19/2025 10:12

Collected

Lab Receipt

Not applicable for this WO.

Result MethodCompound Units RDL Flag

TCLP EPA 1311 METALS

Barium, Total mg/L 0.0500.29 #SW846 6010C

Chromium, Total mg/L 0.0250.049 #SW846 6010C

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com 7/9/2025 2:37 PM 9 of 19

Project

Workorder

Results

3421555001Lab Sample ID

Sample 1-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.050 SW846 6010CND ND,1 MSY A11 07/01/2025 13:28

Barium, Total mg/L 0.050 SW846 6010C0.070 MSY A11 07/01/2025 13:28

Cadmium, Total mg/L 0.0099 SW846 6010CND ND MSY A11 07/01/2025 13:28

Chromium, Total mg/L 0.025 SW846 6010CND ND MSY A11 07/01/2025 13:28

Lead, Total mg/L 0.030 SW846 6010C0.037 MSY A11 07/01/2025 13:28

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 16:26

Selenium, Total mg/L 0.099 SW846 6010CND ND,2 MSY A11 07/01/2025 13:28

Silver, Total mg/L 0.020 SW846 6010CND ND MSY A11 07/01/2025 13:28

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 10 of 19

Project

Workorder

Results

3421555002Lab Sample ID

Sample 2-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.050 SW846 6010CND ND MSY A11 07/01/2025 11:47

Barium, Total mg/L 0.050 SW846 6010C0.060 MSY A11 07/01/2025 11:47

Cadmium, Total mg/L 0.0099 SW846 6010CND ND MSY A11 07/01/2025 11:47

Chromium, Total mg/L 0.025 SW846 6010CND ND MSY A11 07/01/2025 11:47

Lead, Total mg/L 0.030 SW846 6010C0.030 MSY A11 07/01/2025 11:47

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 16:27

Selenium, Total mg/L 0.099 SW846 6010CND ND MSY A11 07/01/2025 11:47

Silver, Total mg/L 0.020 SW846 6010CND ND MSY A11 07/01/2025 11:47

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 11 of 19

Project

Workorder

Results

3421555003Lab Sample ID

Sample 3-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.050 SW846 6010CND ND MSY A11 07/01/2025 11:49

Barium, Total mg/L 0.050 SW846 6010C0.069 MSY A11 07/01/2025 11:49

Cadmium, Total mg/L 0.0099 SW846 6010C0.012 MSY A11 07/01/2025 11:49

Chromium, Total mg/L 0.025 SW846 6010C0.030 MSY A11 07/01/2025 11:49

Lead, Total mg/L 0.030 SW846 6010C0.043 MSY A11 07/01/2025 11:49

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 15:17

Selenium, Total mg/L 0.099 SW846 6010CND ND MSY A11 07/01/2025 11:49

Silver, Total mg/L 0.020 SW846 6010CND ND MSY A11 07/01/2025 11:49

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 12 of 19

Project

Workorder

Results

3421555004Lab Sample ID

Sample 4-5148Client Sample ID 06/11/2025 08:00

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.050 SW846 6010CND ND MSY A11 07/02/2025 13:03

Barium, Total mg/L 0.050 SW846 6010CND ND MSY A11 07/02/2025 13:03

Cadmium, Total mg/L 0.0099 SW846 6010CND ND MSY A11 07/02/2025 13:03

Chromium, Total mg/L 0.025 SW846 6010CND ND MSY A11 07/02/2025 13:03

Lead, Total mg/L 0.030 SW846 6010CND ND MSY A11 07/07/2025 18:07

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 15:20

Selenium, Total mg/L 0.099 SW846 6010CND ND MSY A11 07/02/2025 13:03

Silver, Total mg/L 0.020 SW846 6010CND ND MSY A11 07/02/2025 13:03

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 13 of 19

Project

Workorder

Results

3421555005Lab Sample ID

Sample 5-BLDG 20Client Sample ID 06/11/2025 08:05

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.099 SW846 6010CND ND MSY A12 07/02/2025 13:31

Barium, Total mg/L 0.099 SW846 6010CND ND MSY A12 07/02/2025 13:31

Cadmium, Total mg/L 0.020 SW846 6010C0.065 MSY A12 07/02/2025 13:31

Chromium, Total mg/L 0.050 SW846 6010CND ND MSY A12 07/02/2025 13:31

Lead, Total mg/L 0.060 SW846 6010CND ND MSY A12 07/07/2025 18:09

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 15:22

Selenium, Total mg/L 0.20 SW846 6010CND ND MSY A12 07/02/2025 13:31

Silver, Total mg/L 0.040 SW846 6010CND ND MSY A12 07/02/2025 13:31

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 14 of 19

Project

Workorder

Results

3421555006Lab Sample ID

Sample 6-BLDG 28Client Sample ID 06/11/2025 08:05

06/19/2025 10:12

Collected

Lab Receipt

TCLP EPA 1311 METALS

Result MethodCompound Units RDLFlag By CntrDilution Analysis Date/Time

Arsenic, Total mg/L 0.050 SW846 6010CND ND MSY A11 07/02/2025 13:07

Barium, Total mg/L 0.050 SW846 6010C0.29 MSY A11 07/02/2025 13:07

Cadmium, Total mg/L 0.0099 SW846 6010CND ND MSY A11 07/02/2025 13:07

Chromium, Total mg/L 0.025 SW846 6010C0.049 MSY A11 07/02/2025 13:07

Lead, Total mg/L 0.030 SW846 6010CND ND MSY A11 07/07/2025 18:11

Mercury, Total mg/L 0.00050 SW846 7470AND ND JMS A1 07/07/2025 15:23

Selenium, Total mg/L 0.099 SW846 6010CND ND MSY A11 07/02/2025 13:07

Silver, Total mg/L 0.020 SW846 6010CND ND MSY A11 07/02/2025 13:07

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 15 of 19

Project

Workorder

Sample - Method Cross Reference Table

Lab ID Sample ID Analysis Method Preparation Method Leachate Method

3421555001 Sample 1-5148 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

3421555002 Sample 2-5148 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

3421555003 Sample 3-5148 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

3421555004 Sample 4-5148 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

3421555005 Sample 5-BLDG 20 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

3421555006 Sample 6-BLDG 28 SW846 1311SW846 3015ASW846 6010C

SW846 1311SW846 7470ASW846 7470A

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 16 of 19

Project

Workorder

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Lab ID Sample ID Preparation Method Prep Batch Anly BatchPrep Date/Time Analysis MethodBy

3421555001 Sample 1-5148 SW846 3015A SW846 6010C1448138 144975006/27/2025 11:54 RMH

SW846 7470A SW846 7470A1450162 145149307/07/2025 10:53 JMS

3421555002 Sample 2-5148 SW846 3015A SW846 6010C1448138 144975006/27/2025 11:54 RMH

SW846 7470A SW846 7470A1450162 145149307/07/2025 10:53 JMS

3421555003 Sample 3-5148 SW846 3015A SW846 6010C1448138 144975006/27/2025 11:54 RMH

SW846 7470A SW846 7470A1450163 145149407/07/2025 10:53 JMS

3421555004 Sample 4-5148 SW846 3015A SW846 6010C1448325 145023906/26/2025 10:48 J1K

SW846 3015A SW846 6010C1448325 144978506/26/2025 10:48 J1K

SW846 7470A SW846 7470A1450163 145149407/07/2025 10:53 JMS

3421555005 Sample 5-BLDG 20 SW846 3015A SW846 6010C1448325 145023906/26/2025 10:48 J1K

SW846 3015A SW846 6010C1448325 144978506/26/2025 10:48 J1K

SW846 7470A SW846 7470A1450163 145149407/07/2025 10:53 JMS

3421555006 Sample 6-BLDG 28 SW846 3015A SW846 6010C1448325 145023906/26/2025 10:48 J1K

SW846 3015A SW846 6010C1448325 144978506/26/2025 10:48 J1K

SW846 7470A SW846 7470A1450163 145149407/07/2025 10:53 JMS

ALS is one of the world’s largest and most diversified analytical testing service providers. To learn more visit us at: www.alsglobal.com

7/9/2025 2:37 PM 17 of 19

7/ 9/

Certificate of Analysis

Sample Summary

General Notations

Summary Results

Sample Results

Sample Method Reference

Sample Batch Reference

COC for SDG - 3421555

	2025-07-09T14:37:14-0400
ALS Middletown

File details come from the government source that posted it. Updated Nov 17, 2025.