TCLP 2.1.22.pdf
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- Solicitation number
- 191BWC22R0010
About this file
This document contains a combined synopsis and solicitation for sludge hauling services at the Nogales International Wastewater Treatment Plant in Rio Rico, Arizona. The solicitation is issued by the United States section of the International Boundary and Water Commission as a request for quote set aside for small businesses. The associated NAICS code is 562111 for solid waste collection with a small business size standard of $41.5 million. Quotes are due by 2:00 PM Mountain time on October 24, 2022 and shall be emailed to the point of contact. The solicitation seeks regular removal of sludge from the filter press at the wastewater treatment plant to an approved landfill during normal business hours. Offerors shall provide a technical approach narrative and past performance references for similar projects. Pricing shall be provided for line items 001 through 010 for sludge transport and landfill fees for the base year and option year one. The contract will be awarded based on lowest price technically acceptable to the responsible offeror meeting the solicitation requirements.
Attachments include forms SF1449, the quality assurance surveillance plan, equipment list, wage determination, and statement of work further outlining the requirements.
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RE: Annual TCLP Biosolids
Rio Rico, AZ 85648
865 E Frontage Rd
Michael Dionne
Mary Whaley
Client Services Representative
Legend Technical Services of Arizona, Inc. is pleased to provide the enclosed analytical results for the aforementioned project. These results relate only to the items tested. This cover letter and the accompanying pages represent the full report for these analyses and should only be reproduced in full .
Samples for this project were received by the laboratory on 02/02/22 13:20.
The samples were processed in accordance with the Chain of Custody document and the results presented relate only to the samples tested. The Chain of Custody is considered part of this report.
All samples will be retained by LEGEND for 30 days from the date of this report and then discarded unless other arrangements are made. Due to hold-time and method sample volume requirements, microbiological samples are not retained unless other arrangements are made.
This entire report was reviewed and approved for release by the undersigned. If you have any questions concerning this report, please feel free to contact me.
Sincerely, LEGEND TECHNICAL SERVICES OF ARIZONA, INC.
25 February 2022
International Boundary and Water Commission(IBWC)
Laboratory Work Order No.: 22B0419
This laboratory report is confidential and is intended for the sole use of LEGEND and it's client.
(602) 324-6100
4585 S. Palo Verde Rd., Ste. 423 � Tucson, AZ 85714
P (520) 327-1234 � F (520) 327-0518 www.legend-group.com
Project:
Project Number:
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date ReceivedType
1600-001-A-AZP 22B0419-01 02/01/22 15:00 02/02/22 13:20Solid Composite
This report contains data that were produced by a subcontracted laboratory certified for the fields of testing performed.
Pace Analytical National (fka ESC) AZ0612
Daphne Richards
800.767.5859
Legend Technical Services, St. Paul AZ0557
Bach Pham
651.221.4062
The recoveries for 8081 TCLP surrogate Decachlorobiphenyl were above acceptable limits in the sample and the batch B2B1522
Blank/LCS/MS/MSD due to the use of a deteriorated standard. The recoveries for Endrin were above acceptable limits in the 8081 TCLP batch B2B1522 MS/MSD due to the use of a deteriorated standard. The MS/MSD source sample was 22B0419-01.
Case Narrative:
Holding Times: All holding times were met unless otherwise qualified.
QA/QC Criteria: All analyses met method requirements unless otherwise qualified.
Certifications: AZ(PHX)0004, AZ(TUC)OOO4, AIHA#102982, CDC ELITE Member.
Accreditation is applicable only to the test methods specified on each scope of accreditation held by LEGEND.
Comments: There were no problems encountered during the processing of the samples, unless otherwise noted.
All samples were analyzed on a "wet" basis unless designated as "dry weight".
Containers Intact
Custody Seals
COC/Labels Agree Preservation Confirmed
Received On Ice
4.40°CSamples Received at:
No
No
No
No
No
Sample Condition Upon Receipt:
Temperature: 4.40 C
All samples were received in acceptable condition unless noted otherwise in the case narrative.
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Laboratory Work Order No.: 22B0419
Page 2 of 16Page 2 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
ResultAnalyte PQL Batch Prepared Analyzed Method Notes DilutionUnits
1600-001-A-AZP (22B0419-01) Solid (Composite) Sampled: 02/01/22 15:00 Received: 02/02/22 13:20
Legend Technical Services, Inc. #AZ0557
TCLP SVOC
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:252,4,5-Trichlorophenol
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:252,4,6-Trichlorophenol
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:252,4-Dinitrotoluene
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:252-Methylphenol
EPA 1311/8270Dmg/L B2B152110.20<0.20 02/15/22 08:42 02/18/22 05:253&4-Methylphenol
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Hexachlorobenzene
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Hexachlorobutadiene
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Hexachloroethane
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Nitrobenzene
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Pentachlorophenol
EPA 1311/8270Dmg/L B2B152110.10<0.10 02/15/22 08:42 02/18/22 05:25Pyridine
Surrogate: 2,4,6-Tribromophenol EPA
1311/8270D
B2B1521 02/15/22 02/18/22 61.9-15599.2 %
Surrogate: 2-Fluorobiphenyl EPA
1311/8270D
B2B1521 02/15/22 02/18/22 45-90.265.2 %
Surrogate: 2-Fluorophenol EPA
1311/8270D
B2B1521 02/15/22 02/18/22 30-78.443.3 %
Surrogate: Nitrobenzene-d5 EPA
1311/8270D
B2B1521 02/15/22 02/18/22 41.9-94.470.8 %
Surrogate: Phenol-d6 EPA
1311/8270D
B2B1521 02/15/22 02/18/22 30-78.750.5 %
Surrogate: Terphenyl-d14 EPA
1311/8270D
B2B1521 02/15/22 02/18/22 58-12079.6 %
TCLP PESTICIDES
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05alpha-Chlordane
EPA 1311/8081Bmg/L B2B152210.0080<0.0080 02/15/22 08:46 02/16/22 16:05Chlordane (tech)
EPA 1311/8081Bmg/L B2B152210.0040 L3<0.0040 02/15/22 08:46 02/16/22 16:05Endrin
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05gamma-BHC (Lindane)
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05gamma-Chlordane
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05Heptachlor
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05Heptachlor epoxide
EPA 1311/8081Bmg/L B2B152210.0040<0.0040 02/15/22 08:46 02/16/22 16:05Methoxychlor
EPA 1311/8081Bmg/L B2B152210.010<0.010 02/15/22 08:46 02/16/22 16:05Toxaphene
Surrogate: Decachlorobiphenyl EPA
1311/8081B
B2B1522 02/15/22 02/16/22 N166.5-121132 %
Surrogate: Tetrachloro-meta-xylene EPA
1311/8081B
B2B1522 02/15/22 02/16/22 61-11579.0 %
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 3 of 16Page 3 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
ResultAnalyte PQL Batch Prepared Analyzed Method Notes DilutionUnits
1600-001-A-AZP (22B0419-01) Solid (Composite) Sampled: 02/01/22 15:00 Received: 02/02/22 13:20
Legend Technical Services of Arizona, Inc.
TCLP
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:561,1-Dichloroethene
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:561,2-Dichloroethane
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:561,4-Dichlorobenzene
EPA 8260B/EPA
mg/L B2B0343100.100<0.100 02/10/22 11:30 02/10/22 13:562-Butanone
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Benzene
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Carbon tetrachloride
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Chlorobenzene
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Chloroform
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Tetrachloroethene
EPA 8260B/EPA
mg/L B2B0343100.0200<0.0200 02/10/22 11:30 02/10/22 13:56Trichloroethene
EPA 8260B/EPA
mg/L B2B0343100.00500<0.00500 02/10/22 11:30 02/10/22 13:56Vinyl chloride
Surrogate: 1,2-Dichlorobenzene-d4 EPA
8260B/EPA
B2B0343 02/10/22 02/10/22 80-120114 %
Surrogate: 1,2-Dichloroethane-d4 EPA
8260B/EPA
B2B0343 02/10/22 02/10/22 80-12094 %
Surrogate: 4-Bromofluorobenzene EPA
8260B/EPA
B2B0343 02/10/22 02/10/22 78-12084 %
Surrogate: Pentafluorobenzene EPA
8260B/EPA
B2B0343 02/10/22 02/10/22 80-120103 %
EPA
6010C/EPA1311
mg/L B2B025610.20<0.20 02/08/22 16:23 02/09/22 18:26Arsenic
EPA
6010C/EPA1311
B2B0256mg/L 10.0100.12 02/08/22 16:23 02/09/22 18:26Barium
EPA
6010C/EPA1311
mg/L B2B025610.0040<0.0040 02/08/22 16:23 02/09/22 18:26Cadmium
EPA
6010C/EPA1311
mg/L B2B025610.0050<0.0050 02/08/22 16:23 02/09/22 18:26Chromium
EPA
6010C/EPA1311
mg/L B2B025610.10<0.10 02/08/22 16:23 02/09/22 18:26Lead
EPA 7470A/EPA
mg/L B2B035410.0002<0.0002 02/09/22 09:03 02/09/22 14:47Mercury
EPA
6010C/EPA1311
mg/L B2B025610.20<0.20 02/08/22 16:23 02/09/22 18:26Selenium
EPA
6010C/EPA1311
mg/L B2B025610.010<0.010 02/08/22 16:23 02/09/22 18:26Silver
ESC AZ0612
8151ATCLP
8151ATCLPmg/l WG181477610.00200ND 02/09/22 08:49 02/10/22 18:002,4,5-TP (Silvex)
8151ATCLPmg/l WG181477610.00200ND 02/09/22 08:49 02/10/22 18:002,4-D
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 4 of 16Page 4 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
ResultAnalyte PQL Batch Prepared Analyzed Method Notes DilutionUnits
1600-001-A-AZP (22B0419-01) Solid (Composite) Sampled: 02/01/22 15:00 Received: 02/02/22 13:20
ESC AZ0612
8151ATCLP
Surrogate: 2,4-Dichlorophenyl Acetic Acid 8151ATCLPWG18147
02/09/22 02/10/22 14.0-15867.2 %
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 5 of 16Page 5 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Quality Control
Legend Technical Services of Arizona, Inc.
Batch B2B0256 - TCLP by EPA3010A
Blank (B2B0256-BLK1) Prepared: 02/08/22 Analyzed: 02/09/22
Arsenic mg/L0.20<0.20
Barium mg/L0.010<0.010
Cadmium mg/L0.0040<0.0040
Chromium mg/L0.0050<0.0050
Lead mg/L0.10<0.10
Selenium mg/L0.20<0.20
Silver mg/L0.010<0.010
Blank (B2B0256-BLK2) Prepared: 02/08/22 Analyzed: 02/09/22
Arsenic mg/L0.20<0.20
Barium mg/L0.010<0.010
Cadmium mg/L0.0040<0.0040
Chromium mg/L0.0050<0.0050
Lead mg/L0.10<0.10
Selenium mg/L0.20<0.20
Silver mg/L0.010<0.010
LCS (B2B0256-BS1) Prepared: 02/08/22 Analyzed: 02/09/22
Arsenic mg/L0.20 2.00 80-120982.0
Barium mg/L0.010 1.00 80-1201011.0
Cadmium mg/L0.0040 0.400 80-120970.39
Chromium mg/L0.0050 0.500 80-120980.49
Lead mg/L0.10 1.00 80-120960.96
Selenium mg/L0.20 1.00 80-120940.94
Silver mg/L0.010 0.500 80-1201030.51
LCS Dup (B2B0256-BSD1) Prepared: 02/08/22 Analyzed: 02/09/22
Arsenic mg/L0.20 2.00 2080-12099 12.0
Barium mg/L0.010 1.00 2080-120101 0.021.0
Cadmium mg/L0.0040 0.400 2080-12098 0.50.39
Chromium mg/L0.0050 0.500 2080-12098 0.50.49
Lead mg/L0.10 1.00 2080-12097 0.90.97
Selenium mg/L0.20 1.00 2080-12094 0.20.94
Silver mg/L0.010 0.500 2080-120105 20.53
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 6 of 16Page 6 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Quality Control
Legend Technical Services of Arizona, Inc.
Batch B2B0256 - TCLP by EPA3010A
Matrix Spike (B2B0256-MS1) Prepared: 02/08/22 Analyzed: 02/09/22 Source: 22B0419-01
Arsenic mg/L0.20 2.00 75-1251062.1 0.018
Barium mg/L0.010 1.00 75-1251041.2 0.12
Cadmium mg/L0.0040 0.400 75-125940.38 0.0009
Chromium mg/L0.0050 0.500 75-125970.49 0.0035
Lead mg/L0.10 1.00 75-125930.93 <0.10
Selenium mg/L0.20 1.00 75-1251031.0 0.012
Silver mg/L0.010 0.500 75-1251100.55 <0.010
Matrix Spike Dup (B2B0256-MSD1) Prepared: 02/08/22 Analyzed: 02/09/22 Source: 22B0419-01
Arsenic mg/L0.20 2.00 2075-125106 0.72.1 0.018
Barium mg/L0.010 1.00 2075-125104 0.031.2 0.12
Cadmium mg/L0.0040 0.400 2075-12594 00.38 0.0009
Chromium mg/L0.0050 0.500 2075-12597 0.20.49 0.0035
Lead mg/L0.10 1.00 2075-12592 0.40.92 <0.10
Selenium mg/L0.20 1.00 2075-125104 11.1 0.012
Silver mg/L0.010 0.500 2075-125111 0.020.55 <0.010
Batch B2B0343 - Default Prep VOC
Blank (B2B0343-BLK1) Prepared & Analyzed: 02/10/22
1,1-Dichloroethene mg/L0.0200<0.0200
1,2-Dichloroethane mg/L0.0200<0.0200
1,4-Dichlorobenzene mg/L0.0200<0.0200
2-Butanone mg/L0.100<0.100
Benzene mg/L0.0200<0.0200
Carbon tetrachloride mg/L0.0200<0.0200
Chlorobenzene mg/L0.0200<0.0200
Chloroform mg/L0.0200<0.0200
Tetrachloroethene mg/L0.0200<0.0200
Trichloroethene mg/L0.0200<0.0200
Vinyl chloride mg/L0.00500<0.00500
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 7 of 16Page 7 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Quality Control
Legend Technical Services of Arizona, Inc.
Batch B2B0343 - Default Prep VOC
LCS (B2B0343-BS1) Prepared & Analyzed: 02/10/22
1,1-Dichloroethene mg/L0.00200 0.0100 80-120890.00886
1,2-Dichloroethane mg/L0.00200 0.0100 80-120980.00982
1,4-Dichlorobenzene mg/L0.00200 0.0100 80-1201000.0100
2-Butanone mg/L0.0100 0.0400 72-1201120.0446
Benzene mg/L0.00200 0.0100 80-120970.00965
Carbon tetrachloride mg/L0.00200 0.0100 76-127970.00973
Chlorobenzene mg/L0.00200 0.0100 80-120970.00973
Chloroform mg/L0.00200 0.0100 80-120960.00955
Tetrachloroethene mg/L0.00200 0.0100 80-120930.00929
Trichloroethene mg/L0.00200 0.0100 80-120970.00969
Vinyl chloride mg/L0.000500 0.0100 75-123870.00873
LCS Dup (B2B0343-BSD1) Prepared & Analyzed: 02/10/22
1,1-Dichloroethene mg/L0.00200 0.0100 2080-12090 20.00901
1,2-Dichloroethane mg/L0.00200 0.0100 2080-12095 30.00950
1,4-Dichlorobenzene mg/L0.00200 0.0100 2080-120102 10.0102
2-Butanone mg/L0.0100 0.0400 2072-120102 90.0406
Benzene mg/L0.00200 0.0100 2080-12096 0.90.00956
Carbon tetrachloride mg/L0.00200 0.0100 2076-12797 0.80.00965
Chlorobenzene mg/L0.00200 0.0100 2080-12098 0.70.00980
Chloroform mg/L0.00200 0.0100 2080-12093 20.00932
Tetrachloroethene mg/L0.00200 0.0100 2080-12092 10.00919
Trichloroethene mg/L0.00200 0.0100 2080-12096 0.70.00962
Vinyl chloride mg/L0.000500 0.0100 2075-12390 30.00901
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 8 of 16Page 8 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Quality Control
Legend Technical Services of Arizona, Inc.
Batch B2B0343 - Default Prep VOC
Matrix Spike (B2B0343-MS1) Prepared & Analyzed: 02/10/22 Source: 22A3489-01
1,1-Dichloroethene mg/L0.0200 0.100 80-120990.0990 <0.0200
1,2-Dichloroethane mg/L0.0200 0.100 80-120980.0980 <0.0200
1,4-Dichlorobenzene mg/L0.0200 0.100 80-1201060.106 <0.0200
2-Butanone mg/L0.100 0.400 77-120990.458 0.0638
Benzene mg/L0.0200 0.100 80-1201030.103 <0.0200
Carbon tetrachloride mg/L0.0200 0.100 79-1221070.107 <0.0200
Chlorobenzene mg/L0.0200 0.100 80-1201050.105 <0.0200
Chloroform mg/L0.0200 0.100 72-1311030.103 <0.0200
Tetrachloroethene mg/L0.0200 0.100 80-120980.0984 <0.0200
Trichloroethene mg/L0.0200 0.100 80-1201030.103 <0.0200
Vinyl chloride mg/L0.00500 0.100 73-129920.0921 <0.00500
Matrix Spike Dup (B2B0343-MSD1) Prepared & Analyzed: 02/10/22 Source: 22A3489-01
1,1-Dichloroethene mg/L0.0200 0.100 2080-12099 0.10.0989 <0.0200
1,2-Dichloroethane mg/L0.0200 0.100 2080-12096 20.0964 <0.0200
1,4-Dichlorobenzene mg/L0.0200 0.100 2080-120104 20.104 <0.0200
2-Butanone mg/L0.100 0.400 2077-12093 50.436 0.0638
Benzene mg/L0.0200 0.100 2080-120104 10.104 <0.0200
Carbon tetrachloride mg/L0.0200 0.100 2079-122107 0.60.107 <0.0200
Chlorobenzene mg/L0.0200 0.100 2080-120104 0.20.104 <0.0200
Chloroform mg/L0.0200 0.100 2072-131103 00.103 <0.0200
Tetrachloroethene mg/L0.0200 0.100 2080-120100 20.0999 <0.0200
Trichloroethene mg/L0.0200 0.100 2080-120104 0.90.104 <0.0200
Vinyl chloride mg/L0.00500 0.100 2073-12997 50.0970 <0.00500
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 9 of 16Page 9 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Quality Control
Legend Technical Services of Arizona, Inc.
Batch B2B0354 - EPA 7470A Prep
Blank (B2B0354-BLK1) Prepared & Analyzed: 02/09/22
Mercury mg/L0.0002<0.0002
Blank (B2B0354-BLK2) Prepared & Analyzed: 02/09/22
Mercury mg/L0.0002<0.0002
LCS (B2B0354-BS1) Prepared & Analyzed: 02/09/22
Mercury mg/L0.0002 0.00100 80-1201020.0010
LCS Dup (B2B0354-BSD1) Prepared & Analyzed: 02/09/22
Mercury mg/L0.0002 0.00100 2080-120101 10.0010
Matrix Spike (B2B0354-MS1) Prepared & Analyzed: 02/09/22 Source: 22B0419-01
Mercury mg/L0.0002 0.00100 75-1251030.0010 <0.0002
Matrix Spike Dup (B2B0354-MSD1) Prepared & Analyzed: 02/09/22 Source: 22B0419-01
Mercury mg/L0.0002 0.00100 2075-125102 10.0010 <0.0002
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 10 of 16Page 10 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP SVOC - Quality Control
Legend Technical Services, Inc.
Batch B2B1521 - EPA 3510C (Sep Funnel)
Blank (B2B1521-BLK1) Prepared: 02/15/22 Analyzed: 02/17/22
2,4,5-Trichlorophenol mg/L0.10<0.10
2,4,6-Trichlorophenol mg/L0.10<0.10
2,4-Dinitrotoluene mg/L0.10<0.10
2-Methylphenol mg/L0.10<0.10
3&4-Methylphenol mg/L0.20<0.20
Hexachlorobenzene mg/L0.10<0.10
Hexachlorobutadiene mg/L0.10<0.10
Hexachloroethane mg/L0.10<0.10
Nitrobenzene mg/L0.10<0.10
Pentachlorophenol mg/L0.10<0.10
Pyridine mg/L0.10<0.10
LCS (B2B1521-BS1) Prepared: 02/15/22 Analyzed: 02/18/22
2,4,5-Trichlorophenol mg/L0.10 0.500 56.2-11074.30.371
2,4,6-Trichlorophenol mg/L0.10 0.500 71.2-96.980.50.403
2,4-Dinitrotoluene mg/L0.10 0.500 67.2-10180.50.403
2-Methylphenol mg/L0.10 0.500 56.5-88.877.50.388
3&4-Methylphenol mg/L0.20 1.00 48-87.865.20.652
Hexachlorobenzene mg/L0.10 0.500 70.1-11898.90.494
Hexachlorobutadiene mg/L0.10 0.500 61.6-97.571.50.358
Hexachloroethane mg/L0.10 0.500 55.3-92.968.00.340
Nitrobenzene mg/L0.10 0.500 37-10057.90.290
Pentachlorophenol mg/L0.10 0.500 64.1-11991.70.458
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 11 of 16Page 11 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP SVOC - Quality Control
Legend Technical Services, Inc.
Batch B2B1521 - EPA 3510C (Sep Funnel)
Matrix Spike (B2B1521-MS1) Prepared: 02/15/22 Analyzed: 02/18/22 Source: 2200668-01
2,4,5-Trichlorophenol mg/L0.10 0.500 52.2-11376.50.382 <0.10
2,4,6-Trichlorophenol mg/L0.10 0.500 56.7-10981.50.408 <0.10
2,4-Dinitrotoluene mg/L0.10 0.500 63.9-11083.10.416 <0.10
2-Methylphenol mg/L0.10 0.500 51.7-93.578.40.392 <0.10
3&4-Methylphenol mg/L0.20 1.00 30-10164.00.640 <0.20
Hexachlorobenzene mg/L0.10 0.500 64.6-12099.70.499 <0.10
Hexachlorobutadiene mg/L0.10 0.500 50.2-10669.70.349 <0.10
Hexachloroethane mg/L0.10 0.500 46.4-98.465.10.326 <0.10
Nitrobenzene mg/L0.10 0.500 38.2-98.258.60.293 <0.10
Pentachlorophenol mg/L0.10 0.500 52.6-13795.20.476 <0.10
Matrix Spike Dup (B2B1521-MSD1) Prepared: 02/15/22 Analyzed: 02/18/22 Source: 2200668-01
2,4,5-Trichlorophenol mg/L0.10 0.500 17.352.2-11371.7 6.450.359 <0.10
2,4,6-Trichlorophenol mg/L0.10 0.500 15.156.7-10978.2 4.220.391 <0.10
2,4-Dinitrotoluene mg/L0.10 0.500 15.463.9-11075.6 9.460.378 <0.10
2-Methylphenol mg/L0.10 0.500 18.351.7-93.578.2 0.3060.391 <0.10
3&4-Methylphenol mg/L0.20 1.00 16.530-10164.2 0.2690.642 <0.20
Hexachlorobenzene mg/L0.10 0.500 14.564.6-12094.9 4.990.474 <0.10
Hexachlorobutadiene mg/L0.10 0.500 18.250.2-10669.5 0.2750.348 <0.10
Hexachloroethane mg/L0.10 0.500 15.646.4-98.466.1 1.410.330 <0.10
Nitrobenzene mg/L0.10 0.500 13.438.2-98.258.1 0.8840.291 <0.10
Pentachlorophenol mg/L0.10 0.500 17.352.6-13789.5 6.200.447 <0.10
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 12 of 16Page 12 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP PESTICIDES - Quality Control
Legend Technical Services, Inc.
Batch B2B1522 - EPA 3510C (Sep Funnel)
Blank (B2B1522-BLK1) Prepared & Analyzed: 02/15/22 alpha-Chlordane mg/L0.0040<0.0040
Chlordane (tech) mg/L0.0080<0.0080
Endrin mg/L0.0040 L3<0.0040 gamma-BHC (Lindane) mg/L0.0040<0.0040 gamma-Chlordane mg/L0.0040<0.0040
Heptachlor mg/L0.0040<0.0040
Heptachlor epoxide mg/L0.0040<0.0040
Methoxychlor mg/L0.0040<0.0040
Toxaphene mg/L0.010<0.010
LCS (B2B1522-BS1) Prepared: 02/15/22 Analyzed: 02/16/22 alpha-Chlordane mg/L0.0040 0.0125 70-1301020.0128
Endrin mg/L0.0040 0.0125 L370-1301330.0166 gamma-BHC (Lindane) mg/L0.0040 0.0125 70-1301040.0130 gamma-Chlordane mg/L0.0040 0.0125 70-1301020.0128
Heptachlor mg/L0.0040 0.0125 70-13098.00.0122
Heptachlor epoxide mg/L0.0040 0.0125 70-1301000.0126
Methoxychlor mg/L0.0040 0.0125 70-1301050.0131
Matrix Spike (B2B1522-MS1) Prepared: 02/15/22 Analyzed: 02/18/22 Source: 22B0419-01 alpha-Chlordane mg/L0.0040 0.0125 70-1301030.0128 <0.0040
Endrin mg/L0.0040 0.0125 N170-1301380.0172 <0.0040 gamma-BHC (Lindane) mg/L0.0040 0.0125 70-1301070.0134 <0.0040 gamma-Chlordane mg/L0.0040 0.0125 70-1301020.0128 <0.0040
Heptachlor mg/L0.0040 0.0125 70-1301000.0126 <0.0040
Heptachlor epoxide mg/L0.0040 0.0125 70-1301020.0127 <0.0040
Methoxychlor mg/L0.0040 0.0125 70-1301120.0140 <0.0040
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 13 of 16Page 13 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP PESTICIDES - Quality Control
Legend Technical Services, Inc.
Batch B2B1522 - EPA 3510C (Sep Funnel)
Matrix Spike Dup (B2B1522-MSD1) Prepared: 02/15/22 Analyzed: 02/16/22 Source: 22B0419-01 alpha-Chlordane mg/L0.0040 0.0125 9.6970-130107 4.190.0134 <0.0040
Endrin mg/L0.0040 0.0125 8.37 N170-130144 3.980.0180 <0.0040 gamma-BHC (Lindane) mg/L0.0040 0.0125 11.570-130111 3.300.0138 <0.0040 gamma-Chlordane mg/L0.0040 0.0125 9.0270-130106 3.830.0133 <0.0040
Heptachlor mg/L0.0040 0.0125 1270-130105 4.670.0132 <0.0040
Heptachlor epoxide mg/L0.0040 0.0125 13.370-130106 4.620.0133 <0.0040
Methoxychlor mg/L0.0040 0.0125 8.3470-130120 6.870.0150 <0.0040
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 14 of 16Page 14 of 18
Project Manager:
Reported:865 E Frontage Rd Landfill Biosolids
Michael Dionne
Annual TCLP Biosolids
02/25/22 15:50Rio Rico, AZ 85648
International Boundary and Water Commission(IBWC)
Notes and Definitions
P RPD between the primary and confirmatory analysis exceeded 40%
N1 See case narrative.
L3 The associated blank spike recovery was above method acceptance limits.
Sample results reported on a dry weight basis
Relative Percent DifferenceRPD
Dry
Matrix Spike/DuplicateMS/Dup
Laboratory Control Sample/Laboratory Fortified Blank/DuplicateLCS/Dup
Method BlankBLK
Legend Technical Services of Arizona, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 15 of 16Page 15 of 18
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