A02_28_Soil_Analysis_Report_0001.pdf

PDF 387 KB Posted Nov 3, 2023

Attached to: SCHAAKE HAZARDOUS WASTE DISPOSAL Federal contract opportunity
Solicitation number: 140R1724Q0010
Issued by: Department of the Interior Bureau of Reclamation

About this file

Written by GovTribe AI · Dec 20, 2023

This is a soil analysis report from Analyticallaboratories providing results of testing samples from the Schaake hazardous waste disposal site under solicitation number 140R1724Q0010 issued by the Department of the Interior Bureau of Reclamation. The report details results of testing four samples from the site for semi-volatile organic compounds using EPA method 8270D, and toxic characteristic leaching procedure analysis using EPA method 6020B. Sample 1 showed low level detections of 1,4-dichlorobenzene, 1,3-dichlorobenzene, and 1,2-dichlorobenzene. Sample 2 had similar results. Sample 3 detected phenanthrene in addition to the dichlorobenzenes. Sample 4 detected pyrene at the reporting limit. Quality control samples were within acceptance criteria. Barium and barium were detected at low levels in the TCLP analysis across samples.

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Sol_140R1724Q0010_Amd_0002.pdf	PDF	Nov 8, 2023
A02_28_Current_Waste_Profile_0001.pdf	PDF	Nov 3, 2023
Sol_140R1724Q0010_Amd_0001.pdf	PDF	Nov 3, 2023
C05_01_Pic_3.pdf	PDF	Nov 2, 2023
C05_01_Pic_4.pdf	PDF	Nov 2, 2023
C05_01_Pic_2.pdf	PDF	Nov 2, 2023
Sol_140R1724Q0010.pdf	PDF	Nov 2, 2023
C05_01_Pic_1.pdf	PDF	Nov 2, 2023

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1804 N. 33rd Street

Boise, Idaho 83703

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Laboratory Analysis Report

Lab/Sample Number: 2310410-01

Sample Location: SCHAAKE SAMPLE 1 - BIN

Date Printed: 06/14/2023 13:35

Report To:

Phone: (208) 860-9649

BOISE, ID 83706

Date Received: 05/25/2023

Collection Date/Time: 05/24/2023 15:00

Collector's Name: HEIDI MCMASTER e-mail: hmcmaster@usbr.gov

Copy:

US BUREAU OF RECLAMATION

HEIDI MCMASTER

1150 N CURTIS RD STE 100

Transported By: HEIDI MCMASTER

Temp C Received at Lab:

pH:

Temp C: Free Chlorine mg/L:

Total Chlorine mg/L: DO mg/L:

Flow g/min:

Field Measurements

Analyte Result MDL Analyzed MethodUnits Analyst NotesMCLMRL

Semivolatiles

EPA 8270D6/7/23 19:54 CG0.025Pyridine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodimethylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,4-Dichlorobenzene mg/kg 0.0250.052

EPA 8270D6/7/23 19:54 CG0.0251,3-Dichlorobenzene mg/kg 0.0250.116

EPA 8270D6/7/23 19:54 CG0.0251,2-Dichlorobenzene mg/kg 0.0250.259

EPA 8270D6/7/23 19:54 CG0.025Benzyl alcohol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroisopropyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodi-n-propylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253+4-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachloroethane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Nitrobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Isophorone mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dimethylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethoxy)methane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,2,4-Trichlorobenzene mg/kg 0.0250.068

EPA 8270D6/7/23 19:54 CG0.025Naphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobutadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloro-3-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylnaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorocyclopentadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,6-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,5-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chloronaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dimethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,6-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Acenaphthylene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253-Nitroaniline mg/kg 0.025ND

Page 1 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Semivolatiles (Continued)

2310410-01

EPA 8270D6/7/23 19:54 CG0.025Acenaphthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzofuran mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Diethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chlorophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluorene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254,6-Dinitro-2-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodiphenylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Azobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Bromophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pentachlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenanthrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Carbazole mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-butyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzyl Butyl Phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253,3'-Dichlorobenzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.050Di(2-ethylhexyl)phthalate mg/kg 0.0500.074

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Chrysene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-octyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[b]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[k]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzo(a,h)anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Indeno(1,2,3-cd)pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo(g,h,i)perylene mg/kg 0.025ND

Surrogate: 2-Fluorophenol 37.3 %2-190

Surrogate: Phenol-d5 44.3 %10-190

Surrogate: Nitrobenzene-d5 40.0 %10-190

Surrogate: 2-Fluorobiphenyl 36.0 %10-190

Surrogate: 2,4,6-Tribromophenol 94.0 %10-190

Surrogate: p-Terphenyl-d14 138 %10-190

TCLP

EPA 6020B6/2/23 13:10 JH50.20TCLP Arsenic, As mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH1000.20TCLP Barium, Ba mg/L 0.200.43

EPA 6020B6/2/23 13:10 JH10.20TCLP Cadmium, Cd mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Chromium, Cr mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Lead, Pb mg/L 0.20ND

SW 846 74706/9/23 15:30 JD0.20.02TCLP Mercury, Hg mg/L 0.02ND

EPA 6020B6/2/23 13:10 JH10.20TCLP Selenium, Se mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Silver, Ag mg/L 0.20ND

Page 2 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Laboratory Analysis Report

Lab/Sample Number: 2310410-02

Sample Location: SCHAAKE SAMPLE 2 - BIN

Date Printed: 06/14/2023 13:35

Report To:

Phone: (208) 860-9649

BOISE, ID 83706

Date Received: 05/25/2023

Collection Date/Time: 05/24/2023 15:02

Collector's Name: HEIDI MCMASTER e-mail: hmcmaster@usbr.gov

Copy:

US BUREAU OF RECLAMATION

HEIDI MCMASTER

1150 N CURTIS RD STE 100

Transported By: HEIDI MCMASTER

Temp C Received at Lab:

pH:

Temp C: Free Chlorine mg/L:

Total Chlorine mg/L: DO mg/L:

Flow g/min:

Field Measurements

Analyte Result MDL Analyzed MethodUnits Analyst NotesMCLMRL

Semivolatiles

EPA 8270D6/7/23 19:54 CG0.025Pyridine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodimethylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,4-Dichlorobenzene mg/kg 0.0250.069

EPA 8270D6/7/23 19:54 CG0.0251,3-Dichlorobenzene mg/kg 0.0250.150

EPA 8270D6/7/23 19:54 CG0.0251,2-Dichlorobenzene mg/kg 0.0250.235

EPA 8270D6/7/23 19:54 CG0.025Benzyl alcohol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroisopropyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodi-n-propylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253+4-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachloroethane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Nitrobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Isophorone mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dimethylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethoxy)methane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,2,4-Trichlorobenzene mg/kg 0.0250.090

EPA 8270D6/7/23 19:54 CG0.025Naphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobutadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloro-3-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylnaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorocyclopentadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,6-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,5-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chloronaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dimethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,6-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Acenaphthylene mg/kg 0.025ND

Page 3 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Semivolatiles (Continued)

2310410-02

EPA 8270D6/7/23 19:54 CG0.025Acenaphthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzofuran mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Diethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chlorophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluorene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254,6-Dinitro-2-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodiphenylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Azobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Bromophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pentachlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenanthrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Carbazole mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-butyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzyl Butyl Phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253,3'-Dichlorobenzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.050Di(2-ethylhexyl)phthalate mg/kg 0.0500.067

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Chrysene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-octyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[b]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[k]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzo(a,h)anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Indeno(1,2,3-cd)pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo(g,h,i)perylene mg/kg 0.025ND

Surrogate: 2-Fluorophenol 41.7 %2-190

Surrogate: Phenol-d5 50.8 %10-190

Surrogate: Nitrobenzene-d5 46.6 %10-190

Surrogate: 2-Fluorobiphenyl 38.6 %10-190

Surrogate: 2,4,6-Tribromophenol 95.0 %10-190

Surrogate: p-Terphenyl-d14 138 %10-190

TCLP

EPA 6020B6/2/23 13:10 JH50.20TCLP Arsenic, As mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH1000.20TCLP Barium, Ba mg/L 0.200.53

EPA 6020B6/2/23 13:10 JH10.20TCLP Cadmium, Cd mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Chromium, Cr mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Lead, Pb mg/L 0.20ND

SW 846 74706/9/23 15:30 JD0.20.02TCLP Mercury, Hg mg/L 0.02ND

EPA 6020B6/2/23 13:10 JH10.20TCLP Selenium, Se mg/L 0.20ND

Page 4 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Laboratory Analysis Report

Lab/Sample Number: 2310410-03

Sample Location: SCHAAKE SAMPLE 3 - BIN

Date Printed: 06/14/2023 13:35

Report To:

Phone: (208) 860-9649

BOISE, ID 83706

Date Received: 05/25/2023

Collection Date/Time: 05/24/2023 15:05

Collector's Name: HEIDI MCMASTER e-mail: hmcmaster@usbr.gov

Copy:

US BUREAU OF RECLAMATION

HEIDI MCMASTER

1150 N CURTIS RD STE 100

Transported By: HEIDI MCMASTER

Temp C Received at Lab:

pH:

Temp C: Free Chlorine mg/L:

Total Chlorine mg/L: DO mg/L:

Flow g/min:

Field Measurements

Analyte Result MDL Analyzed MethodUnits Analyst NotesMCLMRL

Semivolatiles

EPA 8270D6/7/23 19:54 CG0.025Pyridine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodimethylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,4-Dichlorobenzene mg/kg 0.0250.096

EPA 8270D6/7/23 19:54 CG0.0251,3-Dichlorobenzene mg/kg 0.0250.249

EPA 8270D6/7/23 19:54 CG0.0251,2-Dichlorobenzene mg/kg 0.0250.718

EPA 8270D6/7/23 19:54 CG0.025Benzyl alcohol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroisopropyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodi-n-propylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253+4-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachloroethane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Nitrobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Isophorone mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dimethylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethoxy)methane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,2,4-Trichlorobenzene mg/kg 0.0250.228

EPA 8270D6/7/23 19:54 CG0.025Naphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobutadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloro-3-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylnaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorocyclopentadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,6-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,5-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chloronaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dimethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,6-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Acenaphthylene mg/kg 0.025ND

Page 5 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Semivolatiles (Continued)

2310410-03

EPA 8270D6/7/23 19:54 CG0.025Acenaphthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzofuran mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Diethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chlorophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluorene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254,6-Dinitro-2-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodiphenylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Azobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Bromophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pentachlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenanthrene mg/kg 0.0250.040

EPA 8270D6/7/23 19:54 CG0.025Anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Carbazole mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-butyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzyl Butyl Phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253,3'-Dichlorobenzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.050Di(2-ethylhexyl)phthalate mg/kg 0.0500.189

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Chrysene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-octyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[b]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[k]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzo(a,h)anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Indeno(1,2,3-cd)pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo(g,h,i)perylene mg/kg 0.025ND

Surrogate: 2-Fluorophenol 24.3 %2-190

Surrogate: Phenol-d5 28.9 %10-190

Surrogate: Nitrobenzene-d5 26.7 %10-190

Surrogate: 2-Fluorobiphenyl 28.1 %10-190

Surrogate: 2,4,6-Tribromophenol 89.5 %10-190

Surrogate: p-Terphenyl-d14 120 %10-190

TCLP

EPA 6020B6/2/23 13:10 JH50.20TCLP Arsenic, As mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH1000.20TCLP Barium, Ba mg/L 0.200.42

EPA 6020B6/2/23 13:10 JH10.20TCLP Cadmium, Cd mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Chromium, Cr mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Lead, Pb mg/L 0.20ND

SW 846 74706/9/23 15:30 JD0.20.02TCLP Mercury, Hg mg/L 0.02ND

EPA 6020B6/2/23 13:10 JH10.20TCLP Selenium, Se mg/L 0.20ND

Page 6 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Laboratory Analysis Report

Lab/Sample Number: 2310410-04

Sample Location: SCHAAKE SAMPLE 4 - CONTROL

Date Printed: 06/14/2023 13:35

Report To:

Phone: (208) 860-9649

BOISE, ID 83706

Date Received: 05/25/2023

Collection Date/Time: 05/24/2023 15:08

Collector's Name: HEIDI MCMASTER e-mail: hmcmaster@usbr.gov

Copy:

US BUREAU OF RECLAMATION

HEIDI MCMASTER

1150 N CURTIS RD STE 100

Transported By: HEIDI MCMASTER

Temp C Received at Lab:

pH:

Temp C: Free Chlorine mg/L:

Total Chlorine mg/L: DO mg/L:

Flow g/min:

Field Measurements

Analyte Result MDL Analyzed MethodUnits Analyst NotesMCLMRL

Semivolatiles

EPA 8270D6/7/23 19:54 CG0.025Pyridine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodimethylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,4-Dichlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,3-Dichlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,2-Dichlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzyl alcohol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroisopropyl)ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodi-n-propylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253+4-Methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachloroethane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Nitrobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Isophorone mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dimethylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Bis(2-chloroethoxy)methane mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0251,2,4-Trichlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Naphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobutadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chloro-3-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Methylnaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorocyclopentadiene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,6-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4,5-Trichlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Chloronaphthalene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dimethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,6-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Acenaphthylene mg/kg 0.025ND

Page 7 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Semivolatiles (Continued)

2310410-04

EPA 8270D6/7/23 19:54 CG0.025Acenaphthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzofuran mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0252,4-Dinitrotoluene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitrophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Diethyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Chlorophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluorene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Nitroaniline mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254,6-Dinitro-2-methylphenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025N-Nitrosodiphenylamine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Azobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0254-Bromophenyl phenyl ether mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Hexachlorobenzene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pentachlorophenol mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Phenanthrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Carbazole mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-butyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Pyrene mg/kg 0.0250.030

EPA 8270D6/7/23 19:54 CG0.025Benzyl Butyl Phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.0253,3'-Dichlorobenzidine mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.050Di(2-ethylhexyl)phthalate mg/kg 0.0500.086

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Chrysene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Di-n-octyl phthalate mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[b]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[k]fluoranthene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo[a]pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Dibenzo(a,h)anthracene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Indeno(1,2,3-cd)pyrene mg/kg 0.025ND

EPA 8270D6/7/23 19:54 CG0.025Benzo(g,h,i)perylene mg/kg 0.025ND

Surrogate: 2-Fluorophenol 27.8 %2-190

Surrogate: Phenol-d5 36.1 %10-190

Surrogate: Nitrobenzene-d5 34.9 %10-190

Surrogate: 2-Fluorobiphenyl 35.3 %10-190

Surrogate: 2,4,6-Tribromophenol 93.4 %10-190

Surrogate: p-Terphenyl-d14 51.2 %10-190

TCLP

EPA 6020B6/2/23 13:10 JH50.20TCLP Arsenic, As mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH1000.20TCLP Barium, Ba mg/L 0.200.56

EPA 6020B6/2/23 13:10 JH10.20TCLP Cadmium, Cd mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Chromium, Cr mg/L 0.20ND

EPA 6020B6/2/23 13:10 JH50.20TCLP Lead, Pb mg/L 0.20ND

SW 846 74706/9/23 15:30 JD0.20.02TCLP Mercury, Hg mg/L 0.02ND

EPA 6020B6/2/23 13:10 JH10.20TCLP Selenium, Se mg/L 0.20ND

Page 8 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Authorized Signature, James Hibbs, Client Manager

This report shall not be reproduced except in full, without the written approval of the laboratory

The results reported relate only to the samples indicated.

ND - Non Detect

MCL - Maximum Contaminant Level

MDL - Method Detection Limit

MRL - Method Reporting Limit

Page 9 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data

Semivolatiles

Batch: BCE1405 - Organics

Prepared: 5/31/2023 Analyzed: 6/7/2023Blank (BCE1405-BLK1)

Pyridine ND 0.025 mg/kg

N-Nitrosodimethylamine ND 0.025 mg/kg

Phenol ND 0.025 mg/kg

Bis(2-chloroethyl)ether ND 0.025 mg/kg

2-Chlorophenol ND 0.025 mg/kg

1,4-Dichlorobenzene ND 0.025 mg/kg

1,3-Dichlorobenzene ND 0.025 mg/kg

1,2-Dichlorobenzene ND 0.025 mg/kg

Benzyl alcohol ND 0.025 mg/kg

Bis(2-chloroisopropyl)ether ND 0.025 mg/kg

2-Methylphenol ND 0.025 mg/kg

N-Nitrosodi-n-propylamine ND 0.025 mg/kg

3+4-Methylphenol ND 0.025 mg/kg

Hexachloroethane ND 0.025 mg/kg

Nitrobenzene ND 0.025 mg/kg

Isophorone ND 0.025 mg/kg

2-Nitrophenol ND 0.025 mg/kg

2,4-Dimethylphenol ND 0.025 mg/kg

Bis(2-chloroethoxy)methane ND 0.025 mg/kg

2,4-Dichlorophenol ND 0.025 mg/kg

1,2,4-Trichlorobenzene ND 0.025 mg/kg

Naphthalene ND 0.025 mg/kg

4-Chloroaniline ND 0.025 mg/kg

Hexachlorobutadiene ND 0.025 mg/kg

4-Chloro-3-methylphenol ND 0.025 mg/kg

2-Methylnaphthalene ND 0.025 mg/kg

Hexachlorocyclopentadiene ND 0.025 mg/kg

2,4,6-Trichlorophenol ND 0.025 mg/kg

2,4,5-Trichlorophenol ND 0.025 mg/kg

2-Chloronaphthalene ND 0.025 mg/kg

2-Nitroaniline ND 0.025 mg/kg

Dimethyl phthalate ND 0.025 mg/kg

2,6-Dinitrotoluene ND 0.025 mg/kg

Acenaphthylene ND 0.025 mg/kg

3-Nitroaniline ND 0.025 mg/kg

Acenaphthene ND 0.025 mg/kg

2,4-Dinitrophenol ND 0.025 mg/kg

Dibenzofuran ND 0.025 mg/kg

2,4-Dinitrotoluene ND 0.025 mg/kg

4-Nitrophenol ND 0.025 mg/kg

Diethyl phthalate ND 0.025 mg/kg

4-Chlorophenyl phenyl ether ND 0.025 mg/kg

Fluorene ND 0.025 mg/kg

4-Nitroaniline ND 0.025 mg/kg

4,6-Dinitro-2-methylphenol ND 0.025 mg/kg

N-Nitrosodiphenylamine ND 0.025 mg/kg

Azobenzene ND 0.025 mg/kg

4-Bromophenyl phenyl ether ND 0.025 mg/kg

Hexachlorobenzene ND 0.025 mg/kg

Pentachlorophenol ND 0.025 mg/kg

Phenanthrene ND 0.025 mg/kg

Anthracene ND 0.025 mg/kg

Carbazole ND 0.025 mg/kg

Di-n-butyl phthalate ND 0.025 mg/kg

Fluoranthene ND 0.025 mg/kg

Benzidine ND 0.025 mg/kg

Page 10 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data (Continued)

Semivolatiles (Continued)

Batch: BCE1405 - Organics (Continued)

Prepared: 5/31/2023 Analyzed: 6/7/2023Blank (BCE1405-BLK1)

Pyrene ND 0.025 mg/kg

Benzyl Butyl Phthalate ND 0.025 mg/kg

3,3'-Dichlorobenzidine ND 0.025 mg/kg

Di(2-ethylhexyl)phthalate 0.047 0.025 mg/kg

Benzo[a]anthracene ND 0.025 mg/kg

Chrysene ND 0.025 mg/kg

Di-n-octyl phthalate ND 0.025 mg/kg

Benzo[b]fluoranthene ND 0.025 mg/kg

Benzo[k]fluoranthene ND 0.025 mg/kg

Benzo[a]pyrene ND 0.025 mg/kg

Dibenzo(a,h)anthracene ND 0.025 mg/kg

Indeno(1,2,3-cd)pyrene ND 0.025 mg/kg

Benzo(g,h,i)perylene ND 0.025 mg/kg

40.0 2-190Surrogate: 2-Fluorophenol 36.414.6 mg/kg

40.0 10-190Surrogate: Phenol-d5 45.518.2 mg/kg

40.0 10-190Surrogate: Nitrobenzene-d5 45.818.3 mg/kg

40.0 10-190Surrogate: 2-Fluorobiphenyl 36.514.6 mg/kg

40.0 10-190Surrogate: 2,4,6-Tribromophenol 56.922.8 mg/kg

40.0 10-190Surrogate: p-Terphenyl-d14 52.120.8 mg/kg

Prepared: 5/31/2023 Analyzed: 6/7/2023LCS (BCE1405-BS1)

Pyridine 9.60 0.025 10.0 50-15096.0mg/kg

N-Nitrosodimethylamine 9.82 0.025 10.0 50-15098.2mg/kg

Phenol 10.0 0.025 10.0 50-150100mg/kg

Bis(2-chloroethyl)ether 9.92 0.025 10.0 50-15099.2mg/kg

2-Chlorophenol 9.85 0.025 10.0 50-15098.5mg/kg

1,4-Dichlorobenzene 10.0 0.025 10.0 50-150100mg/kg

1,3-Dichlorobenzene 9.56 0.025 10.0 50-15095.6mg/kg

1,2-Dichlorobenzene 9.68 0.025 10.0 50-15096.8mg/kg

Benzyl alcohol 9.61 0.025 50-150mg/kg

Bis(2-chloroisopropyl)ether 9.70 0.025 10.0 50-15097.0mg/kg

2-Methylphenol 9.89 0.025 10.0 50-15098.9mg/kg

N-Nitrosodi-n-propylamine 9.55 0.025 10.0 50-15095.5mg/kg

3+4-Methylphenol 9.70 0.025 10.0 50-15097.0mg/kg

Hexachloroethane 9.81 0.025 10.0 50-15098.1mg/kg

Nitrobenzene 9.43 0.025 10.0 50-15094.3mg/kg

Isophorone 9.91 0.025 10.0 50-15099.1mg/kg

2-Nitrophenol 9.76 0.025 10.0 50-15097.6mg/kg

2,4-Dimethylphenol 9.68 0.025 10.0 50-15096.8mg/kg

Bis(2-chloroethoxy)methane 9.30 0.025 10.0 50-15093.0mg/kg

2,4-Dichlorophenol 9.75 0.025 10.0 50-15097.5mg/kg

1,2,4-Trichlorobenzene 9.62 0.025 10.0 50-15096.2mg/kg

Naphthalene 9.32 0.025 10.0 50-15093.2mg/kg

4-Chloroaniline 9.70 0.025 10.0 50-15097.0mg/kg

Hexachlorobutadiene 9.23 0.025 10.0 50-15092.3mg/kg

4-Chloro-3-methylphenol 9.39 0.025 10.0 50-15093.9mg/kg

2-Methylnaphthalene 9.10 0.025 10.0 50-15091.0mg/kg

Hexachlorocyclopentadiene 6.83 0.025 10.0 50-15068.3mg/kg

2,4,6-Trichlorophenol 9.78 0.025 10.0 50-15097.8mg/kg

2,4,5-Trichlorophenol 9.46 0.025 10.0 50-15094.6mg/kg

2-Chloronaphthalene 9.76 0.025 10.0 50-15097.6mg/kg

2-Nitroaniline 9.99 0.025 10.0 50-15099.9mg/kg

Dimethyl phthalate 9.43 0.025 10.0 50-15094.3mg/kg

2,6-Dinitrotoluene 9.84 0.025 10.0 50-15098.4mg/kg

Acenaphthylene 9.47 0.025 10.0 50-15094.7mg/kg

3-Nitroaniline 9.99 0.025 10.0 50-15099.9mg/kg

Page 11 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data (Continued)

Semivolatiles (Continued)

Batch: BCE1405 - Organics (Continued)

Prepared: 5/31/2023 Analyzed: 6/7/2023LCS (BCE1405-BS1)

Acenaphthene 9.36 0.025 10.0 50-15093.6mg/kg

2,4-Dinitrophenol 10.1 0.025 10.0 50-150101mg/kg

Dibenzofuran 9.30 0.025 10.0 50-15093.0mg/kg

2,4-Dinitrotoluene 9.84 0.025 10.0 50-15098.4mg/kg

4-Nitrophenol 10.6 0.025 10.0 50-150106mg/kg

Diethyl phthalate 9.53 0.025 10.0 50-15095.3mg/kg

4-Chlorophenyl phenyl ether 9.14 0.025 10.0 50-15091.4mg/kg

Fluorene 9.20 0.025 10.0 50-15092.0mg/kg

4-Nitroaniline 10.8 0.025 10.0 50-150108mg/kg

4,6-Dinitro-2-methylphenol 9.94 0.025 10.0 50-15099.4mg/kg

N-Nitrosodiphenylamine 9.59 0.025 10.0 50-15095.9mg/kg

Azobenzene 9.79 0.025 10.0 50-15097.9mg/kg

4-Bromophenyl phenyl ether 9.08 0.025 10.0 50-15090.8mg/kg

Hexachlorobenzene 9.28 0.025 10.0 50-15092.8mg/kg

Pentachlorophenol 9.78 0.025 10.0 50-15097.8mg/kg

Phenanthrene 8.85 0.025 10.0 50-15088.5mg/kg

Anthracene 8.63 0.025 10.0 50-15086.3mg/kg

Carbazole 9.13 0.025 10.0 50-15091.3mg/kg

Di-n-butyl phthalate 9.21 0.025 10.0 50-15092.1mg/kg

Fluoranthene 8.81 0.025 10.0 50-15088.1mg/kg

Benzidine 13.7 0.025 10.0 50-150137mg/kg

Pyrene 9.86 0.025 10.0 50-15098.6mg/kg

Benzyl Butyl Phthalate 9.98 0.025 10.0 50-15099.8mg/kg

3,3'-Dichlorobenzidine 10.3 0.025 10.0 50-150103mg/kg

Di(2-ethylhexyl)phthalate 9.84 0.025 10.0 50-15098.4mg/kg

Benzo[a]anthracene 9.52 0.025 10.0 50-15095.2mg/kg

Chrysene 9.52 0.025 10.0 50-15095.2mg/kg

Di-n-octyl phthalate 9.71 0.025 10.0 50-15097.1mg/kg

Benzo[b]fluoranthene 11.1 0.025 10.0 50-150111mg/kg

Benzo[k]fluoranthene 11.2 0.025 10.0 50-150112mg/kg

Benzo[a]pyrene 9.73 0.025 10.0 50-15097.3mg/kg

Dibenzo(a,h)anthracene 8.30 0.025 10.0 50-15083.0mg/kg

Indeno(1,2,3-cd)pyrene 5.75 0.025 10.0 50-15057.5mg/kg

Benzo(g,h,i)perylene 9.04 0.025 10.0 50-15090.4mg/kg

10.0 2-190Surrogate: 2-Fluorophenol 10010.0 mg/kg

10.0 10-190Surrogate: Phenol-d5 10110.1 mg/kg

10.0 10-190Surrogate: Nitrobenzene-d5 97.39.73 mg/kg

10.0 10-190Surrogate: 2-Fluorobiphenyl 98.79.87 mg/kg

10.0 10-190Surrogate: 2,4,6-Tribromophenol 96.59.65 mg/kg

10.0 10-190Surrogate: p-Terphenyl-d14 98.69.86 mg/kg

Page 12 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data (Continued)

Semivolatiles (Continued)

Batch: BCE1405 - Organics (Continued)

Prepared: 5/31/2023 Analyzed: 6/7/2023LCS (BCE1405-BS2)

Pyridine 20.3 0.025 20.0 50-150101mg/kg

N-Nitrosodimethylamine 22.0 0.025 20.0 50-150110mg/kg

Phenol 21.2 0.025 20.0 50-150106mg/kg

Bis(2-chloroethyl)ether 21.4 0.025 20.0 50-150107mg/kg

2-Chlorophenol 21.1 0.025 20.0 50-150106mg/kg

1,4-Dichlorobenzene 19.8 0.025 20.0 50-15099.0mg/kg

1,3-Dichlorobenzene 19.8 0.025 20.0 50-15098.9mg/kg

1,2-Dichlorobenzene 19.0 0.025 20.0 50-15094.8mg/kg

Benzyl alcohol 24.2 0.025 50-150mg/kg

Bis(2-chloroisopropyl)ether 21.3 0.025 20.0 50-150107mg/kg

2-Methylphenol 21.1 0.025 20.0 50-150106mg/kg

N-Nitrosodi-n-propylamine 21.7 0.025 20.0 50-150108mg/kg

3+4-Methylphenol 19.3 0.025 20.0 50-15096.4mg/kg

Hexachloroethane 20.2 0.025 20.0 50-150101mg/kg

Nitrobenzene 21.2 0.025 20.0 50-150106mg/kg

Isophorone 20.2 0.025 20.0 50-150101mg/kg

2-Nitrophenol 22.0 0.025 20.0 50-150110mg/kg

2,4-Dimethylphenol 20.1 0.025 20.0 50-150100mg/kg

Bis(2-chloroethoxy)methane 18.6 0.025 20.0 50-15093.0mg/kg

2,4-Dichlorophenol 21.0 0.025 20.0 50-150105mg/kg

1,2,4-Trichlorobenzene 18.7 0.025 20.0 50-15093.6mg/kg

Naphthalene 12.5 0.025 20.0 50-15062.3mg/kg

4-Chloroaniline 27.4 0.025 20.0 50-150137mg/kg

Hexachlorobutadiene 17.8 0.025 20.0 50-15089.1mg/kg

4-Chloro-3-methylphenol 20.5 0.025 20.0 50-150102mg/kg

2-Methylnaphthalene 15.2 0.025 20.0 50-15076.1mg/kg

Hexachlorocyclopentadiene 12.1 0.025 20.0 50-15060.3mg/kg

2,4,6-Trichlorophenol 19.6 0.025 20.0 50-15098.1mg/kg

2,4,5-Trichlorophenol 19.3 0.025 20.0 50-15096.4mg/kg

2-Chloronaphthalene 15.3 0.025 20.0 50-15076.4mg/kg

2-Nitroaniline 20.6 0.025 20.0 50-150103mg/kg

Dimethyl phthalate 17.7 0.025 20.0 50-15088.4mg/kg

2,6-Dinitrotoluene 19.0 0.025 20.0 50-15095.1mg/kg

Acenaphthylene 13.5 0.025 20.0 50-15067.5mg/kg

3-Nitroaniline 20.6 0.025 20.0 50-150103mg/kg

Acenaphthene 14.2 0.025 20.0 50-15071.0mg/kg

2,4-Dinitrophenol 21.8 0.025 20.0 50-150109mg/kg

Dibenzofuran 13.1 0.025 20.0 50-15065.3mg/kg

2,4-Dinitrotoluene 19.0 0.025 20.0 50-15095.1mg/kg

4-Nitrophenol 26.2 0.025 20.0 50-150131mg/kg

Diethyl phthalate 14.4 0.025 20.0 50-15072.1mg/kg

4-Chlorophenyl phenyl ether 17.1 0.025 20.0 50-15085.5mg/kg

Fluorene 14.3 0.025 20.0 50-15071.4mg/kg

4-Nitroaniline 24.6 0.025 20.0 50-150123mg/kg

4,6-Dinitro-2-methylphenol 22.3 0.025 20.0 50-150111mg/kg

N-Nitrosodiphenylamine 15.0 0.025 20.0 50-15075.2mg/kg

Azobenzene 15.2 0.025 20.0 50-15075.8mg/kg

4-Bromophenyl phenyl ether 18.3 0.025 20.0 50-15091.7mg/kg

Hexachlorobenzene 18.4 0.025 20.0 50-15092.2mg/kg

Pentachlorophenol 23.9 0.025 20.0 50-150119mg/kg

Phenanthrene 13.2 0.025 20.0 50-15065.8mg/kg

Anthracene 12.8 0.025 20.0 50-15064.1mg/kg

Carbazole 14.4 0.025 20.0 50-15072.2mg/kg

Di-n-butyl phthalate 12.9 0.025 20.0 50-15064.3mg/kg

Fluoranthene 12.7 0.025 20.0 50-15063.7mg/kg

Benzidine 24.5 0.025 20.0 50-150122mg/kg

Page 13 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data (Continued)

Semivolatiles (Continued)

Batch: BCE1405 - Organics (Continued)

Prepared: 5/31/2023 Analyzed: 6/7/2023LCS (BCE1405-BS2)

Pyrene 14.1 0.025 20.0 50-15070.7mg/kg

Benzyl Butyl Phthalate 17.6 0.025 20.0 50-15087.9mg/kg

3,3'-Dichlorobenzidine 19.9 0.025 20.0 50-15099.5mg/kg

Di(2-ethylhexyl)phthalate 14.9 0.025 20.0 50-15074.3mg/kg

Benzo[a]anthracene 19.4 0.025 20.0 50-15096.9mg/kg

Chrysene 16.4 0.025 20.0 50-15081.9mg/kg

Di-n-octyl phthalate 15.0 0.025 20.0 50-15075.0mg/kg

Benzo[b]fluoranthene 22.5 0.025 20.0 50-150113mg/kg

Benzo[k]fluoranthene 22.2 0.025 20.0 50-150111mg/kg

Benzo[a]pyrene 22.9 0.025 20.0 50-150114mg/kg

Dibenzo(a,h)anthracene 22.8 0.025 20.0 50-150114mg/kg

Indeno(1,2,3-cd)pyrene 21.8 0.025 20.0 50-150109mg/kg

Benzo(g,h,i)perylene 22.5 0.025 20.0 50-150112mg/kg

20.0 2-190Surrogate: 2-Fluorophenol 94.118.8 mg/kg

20.0 10-190Surrogate: Phenol-d5 93.918.8 mg/kg

20.0 10-190Surrogate: Nitrobenzene-d5 93.218.6 mg/kg

20.0 10-190Surrogate: 2-Fluorobiphenyl 66.613.3 mg/kg

20.0 10-190Surrogate: 2,4,6-Tribromophenol 97.319.5 mg/kg

20.0 10-190Surrogate: p-Terphenyl-d14 73.614.7 mg/kg

Prepared: 5/31/2023 Analyzed: 6/7/2023Source: 2310410-04Matrix Spike (BCE1405-MS1)

CPyridine 0.431 0.025 10.0 ND 10-1904.31mg/kg

N-Nitrosodimethylamine 2.49 0.025 10.0 ND 10-19024.9mg/kg

Phenol 2.72 0.025 10.0 ND 10-19027.2mg/kg

Bis(2-chloroethyl)ether 3.13 0.025 10.0 ND 10-19031.3mg/kg

2-Chlorophenol 2.83 0.025 10.0 ND 10-19028.3mg/kg

1,4-Dichlorobenzene 2.76 0.025 10.0 ND 10-19027.6mg/kg

1,3-Dichlorobenzene 2.83 0.025 10.0 ND 10-19028.3mg/kg

1,2-Dichlorobenzene 2.81 0.025 10.0 ND 10-19028.1mg/kg

Benzyl alcohol 3.05 0.025 10.0 ND 10-19030.5mg/kg

Bis(2-chloroisopropyl)ether 2.81 0.025 10.0 ND 10-19028.1mg/kg

2-Methylphenol 3.07 0.025 10.0 ND 10-19030.7mg/kg

N-Nitrosodi-n-propylamine 3.17 0.025 10.0 ND 10-19031.7mg/kg

3+4-Methylphenol 3.35 0.025 10.0 ND 10-19033.5mg/kg

Hexachloroethane 1.20 0.025 10.0 ND 10-19012.0mg/kg

Nitrobenzene 2.76 0.025 10.0 ND 10-19027.6mg/kg

Isophorone 3.02 0.025 10.0 ND 10-19030.2mg/kg

2-Nitrophenol 2.86 0.025 10.0 ND 10-19028.6mg/kg

2,4-Dimethylphenol 3.05 0.025 10.0 ND 10-19030.5mg/kg

Bis(2-chloroethoxy)methane 2.99 0.025 10.0 ND 10-19029.9mg/kg

2,4-Dichlorophenol 2.81 0.025 10.0 ND 10-19028.1mg/kg

1,2,4-Trichlorobenzene 2.99 0.025 10.0 ND 10-19029.9mg/kg

Naphthalene 3.36 0.025 10.0 ND 10-19033.6mg/kg

4-Chloroaniline 1.94 0.025 10.0 ND 10-19019.4mg/kg

Hexachlorobutadiene 2.83 0.025 10.0 ND 10-19028.3mg/kg

4-Chloro-3-methylphenol 4.27 0.025 10.0 ND 10-19042.7mg/kg

2-Methylnaphthalene 3.37 0.025 10.0 ND 10-19033.7mg/kg

CHexachlorocyclopentadiene ND 0.025 10.0 ND 10-190mg/kg

2,4,6-Trichlorophenol 4.46 0.025 10.0 ND 10-19044.6mg/kg

2,4,5-Trichlorophenol 4.85 0.025 10.0 ND 10-19048.5mg/kg

2-Chloronaphthalene 3.61 0.025 10.0 ND 10-19036.1mg/kg

2-Nitroaniline 4.44 0.025 10.0 ND 10-19044.4mg/kg

Dimethyl phthalate 4.63 0.025 10.0 ND 10-19046.3mg/kg

2,6-Dinitrotoluene 4.56 0.025 10.0 ND 10-19045.6mg/kg

Acenaphthylene 4.40 0.025 10.0 ND 10-19044.0mg/kg

3-Nitroaniline 4.44 0.025 10.0 ND 10-19044.4mg/kg

Page 14 of 16 2310410_1 AL 06 14 23 1335

Phone (208) 342-5515 www.analyticallaboratories.com

Lab Federal ID# ID00020

Result

Reporting

Limit Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control Data (Continued)

Semivolatiles (Continued)

Batch: BCE1405 - Organics (Continued)

Prepared: 5/31/2023 Analyzed: 6/7/2023Source: 2310410-04Matrix Spike (BCE1405-MS1)

Acenaphthene 4.38 0.025 10.0 ND 10-19043.8mg/kg

Ca2,4-Dinitrophenol 0.432 0.025 10.0 ND 10-1904.32mg/kg

Dibenzofuran 4.76 0.025 10.0 ND 10-19047.6mg/kg

2,4-Dinitrotoluene 4.56 0.025 10.0 ND 10-19045.6mg/kg

4-Nitrophenol 4.66 0.025 10.0 ND 10-19046.6mg/kg

Diethyl phthalate 6.16 0.025 10.0 ND 10-19061.6mg/kg

4-Chlorophenyl phenyl ether 4.96 0.025 10.0 ND 10-19049.6mg/kg

Fluorene 5.45 0.025 10.0 ND 10-19054.5mg/kg

4-Nitroaniline 5.49 0.025 10.0 ND 10-19054.9mg/kg

4,6-Dinitro-2-methylphenol 1.67 0.025 10.0 ND 10-19016.7mg/kg

N-Nitrosodiphenylamine 6.18 0.025 10.0 ND 10-19061.8mg/kg

Azobenzene 5.60 0.025 10.0 ND 10-19056.0mg/kg

4-Bromophenyl phenyl ether 5.82 0.025 10.0 ND 10-19058.2mg/kg

Hexachlorobenzene 6.13 0.025 10.0 ND 10-19061.3mg/kg

Pentachlorophenol 5.30 0.025 10.0 ND 10-19053.0mg/kg

Phenanthrene 7.41 0.025 10.0 ND 10-19074.1mg/kg

Anthracene 7.12 0.025 10.0 ND 10-19071.2mg/kg

Carbazole 7.03 0.025 10.0 ND 10-19070.3mg/kg

Di-n-butyl phthalate 8.14 0.025 10.0 ND 10-19081.4mg/kg

Fluoranthene 7.96 0.025 10.0 ND 10-19079.6mg/kg

CaBenzidine 0.089 0.025 10.0 ND 10-1900.890mg/kg

Pyrene 8.32 0.025 10.0 0.030 10-19082.9mg/kg

Benzyl Butyl Phthalate 8.20 0.025 10.0 ND 10-19082.0mg/kg

3,3'-Dichlorobenzidine 14.3 0.025 10.0 ND 10-190143mg/kg

Di(2-ethylhexyl)phthalate 8.68 0.025 10.0 0.086 10-19085.9mg/kg

Benzo[a]anthracene 7.44 0.025 10.0 ND 10-19074.4mg/kg

Chrysene 7.53 0.025 10.0 ND 10-19075.3mg/kg

Di-n-octyl phthalate 7.45 0.025 10.0 ND 10-19074.5mg/kg

Benzo[b]fluoranthene 8.19 0.025 10.0 ND 10-19081.9mg/kg

Benzo[k]fluoranthene 7.62 0.025 10.0 ND 10-19076.2mg/kg

Benzo[a]pyrene 7.69 0.025 10.0 ND 10-19076.9mg/kg

Dibenzo(a,h)anthracene 7.49 0.025 10.0 ND 10-19074.9mg/kg

Indeno(1,2,3-cd)pyrene 6.13 0.025 10.0 ND 10-19061.3mg/kg

Benzo(g,h,i)perylene 7.60 0.025 10.0 ND 10-19076.0mg/kg

40.0 2-190Surrogate: 2-Fluorophenol 25.310.1 mg/kg

40.0 10-190Surrogate: Phenol-d5 32.312.9 mg/kg

40.0 10-190Surrogate: Nitrobenzene-d5 31.312.5 mg/kg

40.0 10-190Surrogate: 2-Fluorobiphenyl 31.312.5 mg/kg

40.0 10-190Surrogate: 2,4,6-Tribromophenol 74.729.9 mg/kg

40.0 10-190Surrogate: p-Terphenyl-d14 48.719.5 mg/kg

C Compound lost during the concentration step.

Ca Compound was lost during the concentration step.

Page 15 of 16 2310410_1 AL 06 14 23 1335

Page 16 of 16 2310410_1 AL 06 14 23 1335

File details come from the government source that posted it. Updated Nov 3, 2023.