140P1318Q0002__Powerline_Removal.Lab_report.pdf
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Laboratory Analytical Report
Big Bend National Park
RE: Abandoned Utility Line MM/11
Big Bend National Park, TX 79834 P.O. Box 129
Mr. Michael Orr
Russell Britten
President
Enclosed are the results of analyses for samples received by the laboratory on 03/07/14 09:09. If you have any questions concerning this report, please feel free to contact me.
Sincerely, 12 March 2014 4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
WO: E4C0100
Project:
Project Number:
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
ResultAnalyte Reporting Limit Batch Analyzed Method Qualifiers DilutionUnits
UP001 (Utility Pole)
E4C0100-01 (Solid) - Sampled: 03/06/14 09:37
Analyst
Environmental Testing, Inc.
TCLP Extraction by EPA 1311
03/10/14 17:00N/A ECC0148 EPA 1311Completed JDZ1TCLP Extraction
TCLP Metals by 6000/7000 Series Methods
03/11/14 14:28mg/L ECC0176 EPA 6010C<0.100 JDZ10.100Silver
03/11/14 14:280.100 mg/L ECC0176 EPA 6010C18.5 JDZ1Arsenic
03/11/14 14:280.100 mg/L ECC0176 EPA 6010C0.144 JDZ1Barium
03/11/14 14:28mg/L ECC0176 EPA 6010C<0.100 JDZ10.100Cadmium
03/11/14 14:28mg/L ECC0176 EPA 6010C<0.100 JDZ10.100Chromium
03/11/14 14:28mg/L ECC0176 EPA 6010C<0.100 JDZ10.100Lead
03/11/14 14:28mg/L ECC0176 EPA 6010C<0.200 JDZ10.200Selenium
03/11/14 14:53mg/L ECC0175 EPA 7470A<0.00200 JDZ10.00200Mercury
03/11/14 09:30N/A ECC0176 EPA 3010ACompleted JDZ1Metals Digestion
03/11/14 09:00N/A ECC0175 EPA 7470ACompleted JDZ1Mercury Digestion
TCLP Semivolatile Organic Compounds by EPA Method 8270
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Pyridine
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.09301,4-Dichlorobenzene
03/10/14 16:380.930 mg/L ECC0143 EPA 8270D1.76 CDH46.5o-Cresol
03/10/14 16:380.930 mg/L ECC0143 EPA 8270D5.97 CDH46.5m+p-Cresols
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Hexachloroethane
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Nitrobenzene
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Hexachlorobutadiene
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.09302,4,6-Trichlorophenol
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.09302,4,5-Trichlorophenol
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.09302,4-Dinitrotoluene
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Hexachlorobenzene
03/10/14 15:19mg/L ECC0143 EPA 8270D<0.0930 CDH4.650.0930Pentachlorophenol
03/10/14 15:191-8956 %Surrogate: 2-Fluorophenol ECC0143 EPA 8270DCDH
03/10/14 15:195-9879 %Surrogate: Phenol-d5 ECC0143 EPA 8270DCDH
03/10/14 15:1919-10560 %Surrogate: Nitrobenzene-d5 ECC0143 EPA 8270DCDH
03/10/14 15:1922-10176 %Surrogate: 2-Fluorobiphenyl ECC0143 EPA 8270DCDH
03/10/14 15:1947-14467 %Surrogate: 2,4,6-Tribromophenol ECC0143 EPA 8270DCDH
03/10/14 15:1920-145104 %Surrogate: Terphenyl-d14 ECC0143 EPA 8270DCDH
03/11/14 08:29N/A ECC0143 EPA 3510CCompleted FJM1.16Liquid-Liquid Extraction
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted otherwise. This analytical report must be reproduced in its entirety.
Page 1 of 9Page 2 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Result Reporting Limit Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qualifiers Analyte
TCLP Extraction by EPA 1311 - Quality Control
Environmental Testing, Inc.
Batch ECC0148 - EPA 1311
Blank (ECC0148-BLK1) Prepared & Analyzed: 03/07/14
TCLP Extraction N/ACompleted
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 2 of 9Page 3 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Result Reporting Limit Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qualifiers Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Environmental Testing, Inc.
Batch ECC0175 - EPA 7470 TCLP
Blank (ECC0175-BLK1) Prepared & Analyzed: 03/11/14
Mercury 0.00200 mg/L<0.00200
Mercury Digestion N/ACompleted
LCS (ECC0175-BS1) Prepared & Analyzed: 03/11/14
Mercury 0.00200 0.0200 80-120108mg/L0.0215
Mercury Digestion 0-200N/ACompleted
Matrix Spike (ECC0175-MS1) Prepared & Analyzed: 03/11/14 Source: E4C0042-01
Mercury 0.00200 0.0200 ND 75-12581mg/L0.0162
Mercury Digestion 0.00 0-200N/ACompleted
Matrix Spike Dup (ECC0175-MSD1) Prepared & Analyzed: 03/11/14 Source: E4C0042-01
Mercury 0.00200 0.0200 ND 2075-12578 4mg/L0.0156
Mercury Digestion 0.00 2000-200N/ACompleted
Batch ECC0176 - EPA 3005 TCLP
Blank (ECC0176-BLK1) Prepared & Analyzed: 03/11/14
Arsenic 0.100 mg/L<0.100
Barium 0.100 mg/L<0.100
Cadmium 0.100 mg/L<0.100
Chromium 0.100 mg/L<0.100
Lead 0.100 mg/L<0.100
Silver 0.100 mg/L<0.100
Selenium 0.200 mg/L<0.200
Metals Digestion N/ACompleted
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 3 of 9Page 4 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Result Reporting Limit Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qualifiers Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Environmental Testing, Inc.
Batch ECC0176 - EPA 3005 TCLP
LCS (ECC0176-BS1) Prepared & Analyzed: 03/11/14
Arsenic 0.100 10.0 80-120107mg/L10.7
Barium 0.100 10.0 80-120108mg/L10.8
Cadmium 0.100 10.0 80-120106mg/L10.6
Chromium 0.100 10.0 80-120107mg/L10.7
Lead 0.100 10.0 80-120108mg/L10.8
Silver 0.100 10.0 80-120108mg/L10.8
Selenium 0.200 10.0 80-120106mg/L10.6
Metals Digestion 0-200N/ACompleted
Duplicate (ECC0176-DUP1) Prepared & Analyzed: 03/11/14 Source: E4C0042-01
Arsenic 0.100 ND 20mg/L<0.100
Barium 0.100 0.209 208mg/L0.226
Cadmium 0.100 ND 20mg/L<0.100
Chromium 0.100 ND 20mg/L<0.100
Lead 0.100 ND 20mg/L<0.100
Silver 0.100 ND 20mg/L<0.100
Selenium 0.200 ND 20mg/L<0.200
Metals Digestion 0.00 200N/ACompleted
Matrix Spike (ECC0176-MS1) Prepared & Analyzed: 03/11/14 Source: E4C0042-01
Arsenic 0.100 10.0 ND 75-125107mg/L10.7
Barium 0.100 10.0 0.209 75-125103mg/L10.5
Cadmium 0.100 10.0 ND 75-125104mg/L10.4
Chromium 0.100 10.0 ND 75-125102mg/L10.2
Lead 0.100 10.0 ND 75-125101mg/L10.1
Silver 0.100 10.0 ND 75-125104mg/L10.4
Selenium 0.200 10.0 ND 75-125107mg/L10.7
Metals Digestion 0.00 0-200N/ACompleted
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 4 of 9Page 5 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Result Reporting Limit Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qualifiers Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Environmental Testing, Inc.
Batch ECC0176 - EPA 3005 TCLP
Matrix Spike Dup (ECC0176-MSD1) Prepared & Analyzed: 03/11/14 Source: E4C0042-01
Arsenic 0.100 10.0 ND 2075-125108 0.9mg/L10.8
Barium 0.100 10.0 0.209 2075-125103 0.05mg/L10.5
Cadmium 0.100 10.0 ND 2075-125104 0.4mg/L10.4
Chromium 0.100 10.0 ND 2075-125103 1mg/L10.3
Lead 0.100 10.0 ND 2075-125101 0.3mg/L10.1
Silver 0.100 10.0 ND 2075-125104 0.3mg/L10.4
Selenium 0.200 10.0 ND 2075-125106 0.8mg/L10.6
Metals Digestion 0.00 2000-200N/ACompleted
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 5 of 9Page 6 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Result Reporting Limit Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qualifiers Analyte
TCLP Semivolatile Organic Compounds by EPA Method 8270 - Quality Control
Environmental Testing, Inc.
Batch ECC0143 - EPA 3510 TCLP
Blank (ECC0143-BLK1) Prepared: 03/08/14 Analyzed: 03/10/14
Pyridine 0.0200 mg/L<0.0200
1,4-Dichlorobenzene 0.0200 mg/L<0.0200 o-Cresol 0.0200 mg/L<0.0200 m+p-Cresols 0.0200 mg/L<0.0200
Hexachloroethane 0.0200 mg/L<0.0200
Nitrobenzene 0.0200 mg/L<0.0200
Hexachlorobutadiene 0.0200 mg/L<0.0200
2,4,6-Trichlorophenol 0.0200 mg/L<0.0200
2,4,5-Trichlorophenol 0.0200 mg/L<0.0200
2,4-Dinitrotoluene 0.0200 mg/L<0.0200
Hexachlorobenzene 0.0200 mg/L<0.0200
Pentachlorophenol 0.0200 mg/L<0.0200
Liquid-Liquid Extraction N/ACompleted
0.200 1-89Surrogate: 2-Fluorophenol 350.0698 mg/L
0.200 5-98Surrogate: Phenol-d5 540.108 mg/L
0.100 19-105Surrogate: Nitrobenzene-d5 690.0692 mg/L
0.100 22-101Surrogate: 2-Fluorobiphenyl 780.0779 mg/L
0.200 47-144Surrogate: 2,4,6-Tribromophenol 820.164 mg/L
0.100 20-145Surrogate: Terphenyl-d14 900.0902 mg/L
LCS (ECC0143-BS1) Prepared: 03/08/14 Analyzed: 03/10/14
Pyridine 0.0100 0.0500 1-12455mg/L0.0274
1,4-Dichlorobenzene 0.0100 0.100 1-9547mg/L0.0469 o-Cresol 0.0100 0.0500 5-9563mg/L0.0315 m+p-Cresols 0.0100 0.100 1-16464mg/L0.0636
Hexachloroethane 0.0100 0.100 1-9142mg/L0.0417
Nitrobenzene 0.0100 0.100 36-11079mg/L0.0792
Hexachlorobutadiene 0.0100 0.100 1-10548mg/L0.0481
2,4,6-Trichlorophenol 0.0100 0.100 20-125109mg/L0.109
2,4,5-Trichlorophenol 0.0100 0.0500 1-14171mg/L0.0353
2,4-Dinitrotoluene 0.0100 0.100 37-134105mg/L0.105
Hexachlorobenzene 0.0100 0.100 23-11883mg/L0.0833
Pentachlorophenol 0.0100 0.100 1-11149mg/L0.0486
Liquid-Liquid Extraction 0-200N/ACompleted
0.100 1-89Surrogate: 2-Fluorophenol 300.0300 mg/L
0.100 5-98Surrogate: Phenol-d5 540.0543 mg/L
0.0500 19-105Surrogate: Nitrobenzene-d5 670.0335 mg/L
0.0500 22-101Surrogate: 2-Fluorobiphenyl 670.0334 mg/L
0.100 47-144Surrogate: 2,4,6-Tribromophenol 820.0823 mg/L
0.0500 20-145Surrogate: Terphenyl-d14 960.0482 mg/L
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 6 of 9Page 7 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Non-Certified Analyses included in this Report
Analyte
Certifications
Code Description Number Expires
E-10401Kansas Accredited 04/01/2014KDHE
10002NELAP Accredited 06/30/2014NELAP
2013-063Oklahoma Accredited 08/31/2014ODEQ
T104704498-13-3Texas Accredited 03/31/2014TCEQ
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 7 of 9Page 8 of 11
Project Manager:
Reported:
Big Bend National Park
P.O. Box 129 Utility Line
Mr. Michael Orr
Abandoned Utility Line MM/11
03/12/14 12:39Big Bend National Park TX, 79834
4619 N. Santa Fe
Oklahoma City, OK 73118
405.488.2400 Phone
405.488.2404 Fax
www.etilab.com
Qualifiers and Definitions
COM Completed
Sample results reported on a dry weight basis
Relative Percent DifferenceRPD dry
Not ReportedNR
Analyte NOT DETECTED at or above the reporting limitND
Analyte DETECTEDDET x Non-Certified analyte
Russell Britten, President
Environmental Testing, Inc. The results in this report apply to the samples analyzed in accordance with the chain of custody document and meet all laboratory accreditation requirements unless noted
Page 8 of 9Page 9 of 11
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