B08_Appendix_D_Methods_with_Reporting_Requirements.xlsx
XLSX spreadsheet 39 KB Posted
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- RADCHEM TESTING
- Solicitation number
- 140G0225R0019
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This Excel file is an appendix detailing Quality Assurance and Quality Control (QAQC) information for radiochemistry testing methods across multiple analytes and sample types. The document comprehensively outlines testing requirements for various radioactive isotopes including gross alpha and beta radioactivity, radium, uranium, strontium, thorium, americium, plutonium, cesium, and others, specifying testing methods for water, sediment, and core samples using techniques like alpha spectrometry, gamma spectrometry, beta counting, and liquid scintillation.
The appendix provides extensive methodological details for each analyte, including EPA and DOE method citations, testing parameters such as minimum detectable concentrations, reporting limits, hold times, frequency of quality control measurements (like matrix spikes, duplicates, and blanks), and specific analytical approaches for filtered and unfiltered samples across different environmental media. The document appears to be a technical reference for a radiochemistry testing protocol, potentially supporting the US Geological Survey's RADCHEM TESTING solicitation (140G0225R0019), which is an Indefinite Delivery, Indefinite Quantity (IDIQ) contract for radiochemistry analysis services.
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Other files
| File | Type | Posted |
|---|---|---|
| Sol_140G0225R0019_Amd_0001.pdf | ||
| Sol_140G0225R0019.pdf | ||
| B08_Appendix_A_Pricing_Schedule.xlsx | XLSX spreadsheet | |
| B08_Appendix_C_Daily_Sample_Receipt_-_Example.xlsx | XLSX spreadsheet | |
| B08_Appendix_B_EDD_File_Example.xlsx | XLSX spreadsheet | |
| B08_Appendix_E_ASR.pdf |
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QAQC Information per analyte
| Test and Analyte description | Method Citation | Analytes included (insert one row per analyte) | Modified Y/N (if Y, indicate documentation of method modification) | Description/Comments | |||||||||||||
| (Short title and/or the modification) | Minimum Detectable Concentration (MDC) | Last date of MDL Study | Current MDL concentration per analyte (one row per analyte) | Reporting Limit (ssLC) per analyte | Units | Last Acceptable PT Date | Name of PT provider | LCS with every batch (Y/N) | LCSD (duplicate) frequency? (Every batch, every 10 samples, on request, etc.) | Blank with every batch ran (Y/N) | Reporting of blank values outside of 3*SD? (Y/N) If Y, how reported? | RL verification standard with every batch (y/N) | Matrix Spike every 10 samples (y/N) | Matrix Spike every 20 samples (y/N) | Duplicate ran with every 10 samples (y/N) | Duplicate ran with every 20 samples (y/N) | Hold time |
| Gross alpha radioactivity, Thorium-230 curve, water, filtered, pCi/L | EPA-NERL: 900.0 | ||||||||||||||||
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L | EPA-NERL: 900.0 |
| Gross alpha radioactivity, Thorium-230 curve, water, unfiltered,pCi/L | EPA-NERL: 900.0 |
| Gross-Beta radioactivity, Cesium-137 curve, water, unfiltered, pCi/L | EPA-NERL: 900.0 |
| Gross-Alpha,Thorium-230 curve, bed sediment, pCi/g | EPA-NERL: 900.0 + ORISE-AP1 |
| Gross-Beta, Cesium-137 curve, bed sediment, pCi/g, | EPA-NERL: 900.0 + ORISE-AP1 |
| Gross alpha radioactivity, Thorium-230 curve, water, filtered, pCi/L, 72 hours | EPA-NERL: 900.0 | < 72 hours |
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L, 72 hours | EPA-NERL: 900.0 | < 72 hours |
| Gross alpha radioactivity, Thorium-230 curve, water, filtered, pCi/L, 30 day recount | EPA-NERL: 900.0 | |
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L, 30 day recount | EPA-NERL: 900.0 |
| Gross alpha radioactivity, Thorium-230 curve, water, unfiltered, pCi/L, 72 hours | EPA-NERL: 900.0 | < 72 hours |
| Gross beta radioactivity, Cesium-137 curve, water, unfiltered, pCi/L, 72 hours | EPA-NERL: 900.0 | < 72 hours |
| Gross alpha radioactivity, Thorium-230 curve, water, unfiltered, pC'/L, 30 day recount | EPA-NERL: 900.0 | |
| Gross beta radioactivity, Cesium-137 curve, water, unfiltered, pCi/L, 30 day recount | EPA-NERL: 900.0 |
| Gross alpha radioactivity,Thorium-230 curve, water, filtered, pCi/L high solids | USEPA 00-02 |
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L, high solids | USEPA 00-02 |
| Gross alpha radioactivity, Thorium-230 curve, water, unfiltered, pCi/L, high solids | USEPA 00-02 |
| Gross beta radioactivity, Cesium-137 curve, water, unfiltered, pCi/L, high solids | USEPA 00-02 |
| Gross alpha radioactivity, Thorium-230 curve,water, filtered, pCi/L 72 hours, high solids | USEPA 00-02 | < 72 hours |
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L, 72 hours, high solids | USEPA 00-02 | < 72 hours |
| Gross alpha radioactivity, Thorium-230 curve, water, filtered, pCi/L, 30 day recount, high solids | USEPA 00-02 | |
| Gross beta radioactivity, Cesium-137 curve, water, filtered, pCi/L, 30 day recount, high solids | USEPA 00-02 |
Radium, total alpha isotopes, water, bed sediment, pCi/L, by alpha counting USEPA 903.0 tc={AE895E3E-1FE9-4571-8ACD-37EA010D879C}: [Threaded comment]
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Comment:
| ORISE, ORAU. 2001. “Method AP7: Determination of Radium-226 in Water and Soil Samples Using Alpha Spectroscopy.” Laboratory Procedures Manual for the Environmental Survey and Site Assessment Program. https://www.epa.gov/esam/orise-method-ap7-determination-radium-226-water-and-soil-samples-using-alpha-spectroscopy | < 96 hours | |||
| Radium-226, bed sediment, pCi/g, by gamma spectrometry | ASTM C 1402 or or EPA-HQ-OW-2018-0558-0048 (adapted for sediment) | Water: | ||
| Radium-228, bed sediment, pCi/g, by gamma spectrometry | Standard Method 7500-Ra (adapted for sediment) or EPA-HQ-OW-2018-0558-0048 (adapted for sediment) | EPA-HQ-OW-2018-0558-0048 |
| Radium, total alpha isotopes, water, filtered, pCi/L, by alpha counting | USEPA 903.0 | < 96 hours |
| Radium-224, water, filtered, pCi/L, by alpha spectrometry | USEPA 402-r-10 |
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Comment:
| epa_402-r-10-001. https://www.epa.gov/sites/default/files/2015-06/documents/ra-226_in_water_rev_0_1_epa_402-r-10-001c.pdf | < 96 hours | ||
| Radium-226, water, filtered, pCi/L, by alpha spectrometry | USEPA 402-r-10 |
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Comment:
epa_402-r-10-001. https://www.epa.gov/sites/default/files/2015-06/documents/ra-226_in_water_rev_0_1_epa_402-r-10-001c.pdf Radium-228, water, filtered, pCi/L, by beta counting USEPA 904.0
| Radium, total alpha isotopes, water, unfiltered, pCi/L, by alpha counting | USEPA 903.0 | < 96 hours |
| Radium-224, water, unfiltered, pCi/L, by alpha spectrometry | USEPA 402-r-10 | < 96 hours |
| Radium-226, water, unfiltered, pCi/L, by alpha spectrometry | USEPA 402-r-10 |
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Comment:
ORISE, ORAU. 2001. “Method AP7: Determination of Radium-226 in Water and Soil Samples Using Alpha Spectroscopy.” Laboratory Procedures Manual for the Environmental Survey and Site Assessment Program. https://www.epa.gov/esam/orise-method-ap7-determination-radium-226-water-and-soil-samples-using-alpha-spectroscopy Radium-228, water, unfiltered, pCi/L, by beta counting USEPA 904.0
| Uranium-234, water, filtered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-235, water, filtered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-238, water, filtered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-234, water, unfiltered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-235, water, unfiltered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-238, water, unfiltered, pCi/L, by alpha spectrometry | ASTM D 3972 |
| Uranium-234, suspended sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Uranium-235, suspended sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Uranium-238, suspended sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Uranium-234, bed sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Uranium-235, bed sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Uranium-238, bed sediment, pCi/g, by alpha spectrometry | ASTM D 3972 |
| Strontium-90, water, filtered, pCi/L. by chemical separation and beta counting | DoE HASL-300 Sr-02-RC |
| Strontium-90, water, unfiltered, pCi/L, by chemical separation and beta counting | DoE HASL-300 Sr-02-RC |
| Strontium-90, suspended sediment, pCi/g, by chemical seperation beta counting | DoE HASL-300 Sr-02-RC |
| Strontium-90, bed sediment, pCi/g, by chemical separation and beta counting | DoE HASL-300 Sr-02-RC |
Strontium-89 and -90, water, filtered, pCi/L, by beta counting USEPA 905.0 tc={AAE7C2B1-4400-48D0-ABFF-39735885F50C}: [Threaded comment]
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Comment:
Also available: Eichrom (beta or scintillation) SRW01-15 Reply:
Microsoft Word - SRW01-15_Sr-water-VBS.docx
| Strontium-89 and -90, water, unfiltered, pCi/L, by beta counting | USEPA 905.0 |
| Strontium-89 and -90, suspended sediment, pCi/g, by beta counting | USEPA 905.0 |
| Strontium-89 and -90, bed sediment, pCi/g, by beta counting | USEPA 905.0 |
Gamma-scan, water, filtered, pCi/L, by gamma spectrometry EPA-NERL: 901.1 tc={069855EA-F0E5-453F-8007-0CA2A62C1B39}: [Threaded comment]
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Comment:
Alternative: American Society for Testing and Materials (ASTM) D3649. Standard Test Method for High�Resolution Gamma-Ray Spectrometry of Water, 1991. West Conshohocken, PA.
| Gamma-scan, water, unfiltered, pCi/L, by gamma spectrometry | EPA-NERL: 901.1 | |
| Gamma-scan, suspended sediment, pCi/g, by gamma spectrometry | ASTM C 1402-09 | ASTM C1402-09. (2009). Standard Guide for High-Resolution Gamma-Ray Spectrometry of Soil Samples. |
| Gamma-scan, bed sediment, pCi/g, by gamma spectrometry | ASTM C 1402-09 |
| Lead-210, core samples, pCi/g, by gamma spectrometry (Lead-210 dating) | Cutshall, N.H., Larsen, I.L., and Olsen, C.R., 1983, Direct analysis of 210 Pb in sediment samples—Self-absorption corrections: Nuclear Instruments and Methods in Physics Research, v. 206, issues 1–2, p. 309–312. https://doi.org/10.1016/0167-5087(83)91273-5.; Jodłowski, P., 2016, A revision factor to the Cutshall self-attenuation correction in (210)Pb gamma-spectrometry measurements. Applied radiation and isotopes, 109, 566-569 . https://doi.org/10.1016/j.apradiso.2015.11.092 |
| Radium-226, core samples, pCi/L, by gamma spectrometry (Lead-210 dating) | Cutshall, N.H., Larsen, I.L., and Olsen, C.R., 1983, Direct analysis of 210 Pb in sediment samples—Self-absorption corrections: Nuclear Instruments and Methods in Physics Research, v. 206, issues 1–2, p. 309–312. https://doi.org/10.1016/0167-5087(83)91273-5.; Jodłowski, P., 2016, A revision factor to the Cutshall self-attenuation correction in (210)Pb gamma-spectrometry measurements. Applied radiation and isotopes, 109, 566-569 . https://doi.org/10.1016/j.apradiso.2015.11.092 |
| Cesium-137, core samples, pCi/L, by gamma spectrometry (Lead-210 dating) | Cutshall, N.H., Larsen, I.L., and Olsen, C.R., 1983, Direct analysis of 210 Pb in sediment samples—Self-absorption corrections: Nuclear Instruments and Methods in Physics Research, v. 206, issues 1–2, p. 309–312. https://doi.org/10.1016/0167-5087(83)91273-5.; Jodłowski, P., 2016, A revision factor to the Cutshall self-attenuation correction in (210)Pb gamma-spectrometry measurements. Applied radiation and isotopes, 109, 566-569 . https://doi.org/10.1016/j.apradiso.2015.11.092 |
| Lead-210, water, filtered, pCi/L, by eichrom/scintillation | PBW01-21 |
| Lead-210, water, unfiltered, pCi/L, by eichrom/scintillation | PBW01-21 |
| Lead-210, suspended sediment, pCi/g, by gamma spectrometry | Cutshall, N.H., Larsen, I.L., and Olsen, C.R., 1983, Direct analysis of 210 Pb in sediment samples—Self-absorption corrections: Nuclear Instruments and Methods in Physics Research, v. 206, issues 1–2, p. 309–312. https://doi.org/10.1016/0167-5087(83)91273-5.; Jodłowski, P., 2016, A revision factor to the Cutshall self-attenuation correction in (210)Pb gamma-spectrometry measurements. Applied radiation and isotopes, 109, 566-569 . https://doi.org/10.1016/j.apradiso.2015.11.092 |
| Lead-210, bed sediment, pCi/g, by gamma spectrometry | Cutshall, N.H., Larsen, I.L., and Olsen, C.R., 1983, Direct analysis of 210 Pb in sediment samples—Self-absorption corrections: Nuclear Instruments and Methods in Physics Research, v. 206, issues 1–2, p. 309–312. https://doi.org/10.1016/0167-5087(83)91273-5.; Jodłowski, P., 2016, A revision factor to the Cutshall self-attenuation correction in (210)Pb gamma-spectrometry measurements. Applied radiation and isotopes, 109, 566-569 . https://doi.org/10.1016/j.apradiso.2015.11.092 |
| Polonium-210, water, filtered, pCi/L, by alpha spectrometry | DOE EML: Po-01-RC |
| Polonium-210, water, unfiltered, pCi/L, pCi/L,, by alpha spectrometry | DOE EML: Po-01-RC |
| Polonium-210, suspended sediment, pCi/g,, by alpha spectrometry | DOE EML: Po-02-RC |
| Polonium-210, bed sediment, pCi/g, by alpha spectrometry | DOE EML: Po-02-RC |
| Thorium-228, water, filtered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-230, water, filtered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-232, water, filtered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-228, water, unfiltered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-230, water, unfiltered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-232, water, unfiltered, pCi/L, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-228, suspended sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-230, suspended sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-232, suspended sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-228, bed sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-230, bed sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Thorium-232, bed sediment, pCi/g, by alpha spectrometry | EPA Method EMSL-33 |
| Americium-241, water, filtered, pCi/L, by alpha spectrometry | DOE EML: Am-04-RC |
| Americium-241, water, unfiltered, pCi/L, by alpha spectrometry | DOE EML: Am-04-RC |
| Americium-241, suspended sediment, pCi/g, by alpha spectrometry | Pu-12-RC / DOE EML: Am-04-RC |
| Americium-241, bed sediment, pCi/g, by alpha spectrometry | Pu-12-RC / DOE EML: Am-04-RC |
| Plutonium-238, water, filtered, pCi/L by alpha spectrometry | DOE EML: Pu-12-RC or Se-03 |
| Plutonium-239/240, water, filtered, pCi/L by alpha spectrometry | DOE EML: Pu-12-RC or Se-03 |
| Plutonium-238, water, unfiltered, pCi/L, by alpha spectrometry | DOE EML: Pu-12-RC or Se-03 |
| Plutonium-239/240, water, unfiltered, pCi/L, by alpha spectrometry | DOE EML: Pu-12-RC or Se-03 |
| Plutonium-238, suspended sediment, pCi/g, by alpha spectrometry | Pu-12-RC / Pu-11-RC |
| Plutonium-239/240, suspended sediment, pCi/g, by alpha spectrometry | Pu-12-RC / Pu-11-RC |
| Plutonium-238, bed sediment, pCi/g, by alpha spectrometry | Pu-12-RC / Pu-11-RC |
| Plutonium-239/240, bed sediment, pCi/g, by alpha spectrometry | Pu-12-RC / Pu-11-RC |
| Cesium-134 and -137, water, filtered, pCi/L, by gamma spectrometry | USEPA 901.0 |
| Cesium-134 and -137, water, unfiltered, pCi/L, by gamma spectrometry | USEPA 901.0 modified |
| Cesium-134 and -137, bed sediment, pCi/g, by gamma spectrometry | USEPA 901.0 modified |
| Cesium-134 and -137, core samples, pCi/g, by gamma spectrometry | USEPA 901.0 modified |
| Radon-222, pCi/L, water, unfiltered, pCi/L, by liquid scintillation | ASTM D 5072 |
| Chlorine-36, pCi/L, water, filtered, pCi/L | EPA 902.0 |
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Accelerator Mass Spectrometry in absence of methodology in 902.0 tc={91BDD246-8B7C-4E8C-81E1-93E37D08BFEC}: [Threaded comment]
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| epa_402-r-10-001. https://www.epa.gov/sites/default/files/2015-06/documents/ra-226_in_water_rev_0_1_epa_402-r-10-001c.pdf | Iodine-129, pCi/L, water, filtered, pCi/L, beta or gamma spectrometry | EPA 902.0 |
| Chlorine-36, pCi/L, water, unfiltered, pCi/L | EPA 902.0 |
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Accelerator Mass Spectrometry in absence of methodology in 902.0 tc={A2D936E3-B5E4-4BA1-9F6C-1357D6A1FCB7}: [Threaded comment]
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epa_402-r-10-001. https://www.epa.gov/sites/default/files/2015-06/documents/ra-226_in_water_rev_0_1_epa_402-r-10-001c.pdf tc={069855EA-F0E5-453F-8007-0CA2A62C1B39}: [Threaded comment]
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Comment:
Alternative: American Society for Testing and Materials (ASTM) D3649. Standard Test Method for High�Resolution Gamma-Ray Spectrometry of Water, 1991. West Conshohocken, PA.
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Comment:
ORISE, ORAU. 2001. “Method AP7: Determination of Radium-226 in Water and Soil Samples Using Alpha Spectroscopy.” Laboratory Procedures Manual for the Environmental Survey and Site Assessment Program. https://www.epa.gov/esam/orise-method-ap7-determination-radium-226-water-and-soil-samples-using-alpha-spectroscopy Iodine-129, pCi/L, water, unfiltered, pCi/L, gamma spectrometry EPA 902.0 modified
| Alpha-emitting isotopes of Radium, water, filtered, pCi/L, by gas proportional counting | EPA-RCA: 9315 |
| Alpha-emitting isotopes of Radium, water, unfiltered, pCi/L, by gas proportional counting | EPA-RCA: 9315 |
| Alpha-emitting isotopes of Radium, suspended sediment, pCi/g, by gas proportional counting | EPA-RCA: 9315 (adapted for sediment) |
| Alpha-emitting isotopes of Radium, bed sediment, pCi/g, by gas proportional counting | SW-846 9315 (adapted for sediment) |
| Radium-226, water, filtered, pCi/L, by radon emanation | USEPA 903.1 |
| Radium-226, water, unfiltered, pCi/L, by radon emanation | DOE EML: Ra-02-RC |
| Radium-226, suspended sediment, pCi/g, by radon emanation | DOE-EML: Ra-04-RC |
| Radium-226, core samples, pCi/g, by gamma spectrometry | ASTM C 1402 |
| Radium-228, water, filtered, pCi/L, by radiochemical separation and beta counting | USEPA 904.0 |
| Radium-228, water, unfiltered, pCi/L, by radiochemical separation and beta counting | EPA-RCA: 9320 |
| Radium-228, suspended sediment, pCi/g, by beta counting | EPA-RCA: 9320 (adapted for sediment) |
| Radium-228 and Radium-226 in Drinking Water by Gamma Ray Spectrometry using HPGE or Ge(Li) Detectors | EPA-HQ-OW-2018-0558-0048 | https://www.regulations.gov/document/EPA-HQ-OW-2018-0558-0048 |
| Radium-224, Gamma-ray spectroscopy method | Standard Method 7500-Ra224 E. | 7500-Ra224 E. Gamma-ray spectroscopy method. (submitted) Standard Methods for the Examination of Water and Wastewater ( 21st Edition ). Published by the American Public Health Association, the American Water Works Association and the Water Environment Federation |
https://www.nemi.gov/methods/method_summary/4730/https://www.nemi.gov/methods/method_summary/4845/https://www.nemi.gov/methods/method_summary/4846/https://www.nemi.gov/methods/method_summary/4846/https://www.nemi.gov/methods/method_summary/4847/https://www.nemi.gov/methods/method_summary/4848/https://www.nemi.gov/methods/method_summary/9345/https://www.nemi.gov/methods/method_summary/4730/https://www.nemi.gov/methods/method_summary/4730/https://www.nemi.gov/methods/method_summary/4730/https://www.nemi.gov/methods/method_summary/4730/https://www.epa.gov/sites/default/files/2015-07/documents/eml-pu-12-rc.pdfhttps://www.epa.gov/sites/default/files/2015-07/documents/eml-pu-12-rc.pdfhttps://www.epa.gov/sites/default/files/2015-07/documents/eml-pu-12-rc.pdfhttps://www.nemi.gov/methods/method_summary/10004/https://www.nemi.gov/methods/method_summary/4854/https://doi.org/10.1016/0167-5087(83)91273-5https://doi.org/10.1016/0167-5087(83)91273-5https://doi.org/10.1016/0167-5087(83)91273-5https://doi.org/10.1016/0167-5087(83)91273-5https://doi.org/10.1016/0167-5087(83)91273-5https://www.nemi.gov/methods/method_summary/9345/https://www.nemi.gov/methods/method_summary/9344/https://www.nemi.gov/methods/method_summary/9344/https://www.regulations.gov/document/EPA-HQ-OW-2018-0558-0048https://www.nemi.gov/methods/method_summary/9344/https://www.nemi.gov/methods/method_summary/4854/https://www.nemi.gov/methods/method_summary/10004/https://www.nemi.gov/methods/method_summary/7391/https://www.nemi.gov/methods/method_summary/7391/https://www.nemi.gov/methods/method_summary/4845/
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