A01_-_Revised_SOW_FOR_EQUIPMENT_PURCHASE.docx
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- Solicitation number
- W91ZLK-19-R-0007
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Requirements and Specifications
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| A02_-_Solicitation_W9ZLK-19-R-0007.docx | DOCX document |
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Statement of Work PURCHASE of a LC/MSD System with DAD (PR# 11208702)
1. Requirement. The contractor shall provide timely delivery of Government requested material to the address provided below unless otherwise specified by the Government. The Government is procuring one
(1) Liquid Chromatograph-Prep-Mass Spectrometer Detection System as specified below.
Line
Part Number
Part Description
Total Quantity
| 1 |
| G6125BW |
| LC/MSD Bundle Including LC/MSD and 1260 Infinity II LC System w/OpenLAB CDS ChemStation |
| 1 |
| 2 |
| N/A |
| Installation and Familiarization of Unit |
| 1 |
a. The items listed above shall be received approximately 25 days after award or sooner.
2. Government Furnished Property or Assistance. Not applicable. No requirement for Government Furnished Property.
3. DELIVERY/LOGISTICS.
3.1 The contractor shall deliver the data/supplies/services approximately 25 days after award to:
Attn: Nicole Rippeon U.S. Army, Edgewood Chemical Biological RDCB-DRC 8510 Ricketts Point Road
BLDG E3400
Gunpowder, MD 21010 410-436-7291
3.2 Inspection and Acceptance of the items will be conducted at destination by authorized ECBC government personnel.
4. Safety Security Considerations. None
5. Security Considerations. None
6. Government Point of Contact.
U.S. Army - RDECOM
RDCB-DRC
Nicole Rippeon Bldg E3400 5183 Blackhawk Road
APG, MD 21010-5424
410-436-7291
Specifications for LC/MSD System with DAD System
General System Specifications
| Single point of control |
| Single Point data system method capability with full control |
| Supported Data Systems |
| Must have OpenLab CDS ChemStation Edition and MassHunter Data Analysis capabilities |
| Time Programming |
| Must have: |
SIM Ion Selection Scan Functions Fragmentor Voltage External CAN valves MS Diverter Valve Drying Gas Glow Nebulizer Pressure Drying Gas Temperature Capillary Voltage (Positive) Capillary Voltage (Negative)
| Wide Range of Ionization Sources |
| Must have: |
Electrospray (ESI) Multimode Source (Simultaneous ESI and APCI) Atmospheric pressure chemical ionization (APCI) Atmospheric pressure photoionization (APPI)
| Detector |
| High energy conversion dynode and electron multiplier horn |
| Vacuum System |
| One Turbo-molecular pump with one mechanical pump |
| Parameter |
| Measure |
| Specification |
Mass Range
10-2,000 m/z
| SIM Sensitivity, ESI Positive |
| 1pg of reserpine injected on column, quantifying the m/z 609 ion |
| Signal-to-noise ration, RMS >100:1 |
| SIM Sensitivity, APCI Positive |
| 1pg of reserpine injected on column, quantifying the m/z 609 ion |
| Signal-to-noise ratio, RMS >30:1 |
| Maximum scan speed |
| u/sec (Da/sec) |
| 10,400 u/sec (Da/sec) |
| Polarity Switching |
| Switching time from positive to negative polarity |
| 300 msec |
| Mass resolution (Autotune) |
| Full width at half maximum |
| Unit resolution (< 0.7 u (Da)) |
| Mass stability (drift) |
| Over 12 hours |
| < 0.1 u (Da) or 100 ppm, whichever is larger |
Mass accuracy
+0.005 u (Da) (only applicable with optional Cerno MassWorks Accurate Mass Software for LC/MSD using OpenLab CDS ChemStation Edition
Minimum SIM dwell time
5 msec
Maximum SIM transitions
100 SIM ions per time segment
Dynamic Range
>6 x 106 (electronic)
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