A.07.23_-_Solicitation_W912DW-17-Q-0046_Lab_Analysis_Revised_20170512_.pdf

This is a combined synopsis/solicitation for commercial service items prepared in accordance with the format in FAR Subpart 12.6, as supplemented with additional information included in this notice. The announcement constitutes the only solicitation. Solicitation No. W912DW-17-Q-0046 is being issued as a Request For Quote (RFQ) with the intent to award as commercial acquisition. This procurement is 100% small business set-aside. The NAICS Code for this procurement is 541380 with a size standard of $15M the U.S. Army Corps of Engineers (USACE), Seattle District (NWS) has need for an analytical laboratory to provide timely chemical analysis of Soil, Water, Sediment, Air, Biota, Chemical products, and Solid Materials in accordance with the Performance Work Statement (PWS).

Unit Unit

ItemNo. DESCRIPTION QTY of Price Amount Measure

0001 Lab testing and Data Analysis (Base) 1 GROUP $_ N/A $

0002 Lab testing and Data Analysis (Option Year 1) 1 GROUP $_ N/A $

0003 Lab testing and Data Analysis (Option Year 2) 1 GROUP $_ N/A $

0004 Lab testing and Data Analysis (Option Year 3) 1 GROUP $_ N/A $

0005 Lab testing and Data Analysis (Option Year 4) 1 GROUP $_ N/A $

Notes:

TOTAL ITEMS (0001-0005) $

1. To better facilitate the receipt and quote process, all revisions to quotes are to be submitted on copies of the latest Price Schedules as published in the solicitation or the latest amendment thereto. In lieu of indicating additions/deductions to line items, all Offerors should state their revised prices for each item.

2. Offerors must insert a price on all numbered items of the Price Schedule. Failure to include pricing for all line items will result in the offer being unacceptable.

3. For questions: Please post all questions to PROJNET. Telephone and email inquiries will NOT be accepted. Instructions for submitting questions to PROJNET are below.

Project: (SATOC IDIQ) NWS IDIQ FY17 NAI10 NAIC 541380 Environmental

Laboratory Services (17Q0046) ProjNet‐BID: W912DW‐17‐Q‐0046

BID KEY: ASW3RH-6MXDSQ

All inquiries regarding this solicitation are to be submitted via ProjNet-Bid. Telephone and email inquiries will NOT be accepted. ProjNet-Bid is a web-based program that allows bidders to post questions regarding the solicitation and to view all questions by other bidders and answers by USACE.

ProjNet-Bid can be accessed through ProjNet at https://www.projnet.org To access the ProjNet-Bid website the first time:

1) Click the Quick Add menu in the upper right.

2) Enter the following information for access:

2.a) Select USACE as the Agency.

2.b) Input BID Key: ASW3RH-6MXDSQ http://www.projnet.org/ http://www.projnet.org/ http://www.projnet.org/

2.c) Your email address.

3) Enter valid business contact information (e.g. First and Last Name, Company name, city and state, phone number, email address). (Required on first project only.)

4) Establish Secret Question and Answer which will be used as a password (required on first project only).

5) For subsequent access use your email address, the Key and response to the Secret Question to access the ProjNet-BID Module.

6) Submit technical questions by clicking Post a New Inquiry. When an answer is posted to a question, the question and answer is then available for all other bidders to review.

7) For questions about ProjNet-BID, please contact the Call Center help desk toll free at 1-800- 428-

HELP (4357), which operates from 8AM to 5PM (Central US time zone).

No inquiries will be accepted after 2 p.m. Pacific Time on the fifth business day preceding the solicitation due date.

All bidders will be held to have reviewed the questions and responses in ProjNet-Bidsm prior to bid submission. All changes to this solicitation will be issued as an official modification.

4. Responses will be accepted via Email or Hard Copy. Email responses to: kelly.l.gunn@usace.army.mil Additional contact information is included in the combined Synopsis/Solicitation posting. For mailed or hand-delivered responses, see instructions below:

Marking of Quote Envelopes:

Envelopes shall be plainly marked as follows:

Quote for: LABORATORY TESTING AND DATA ANALYSIS

Request for Quote No.: W912DW-17-Q-0046

Closing Date and Time: 22 JUNE 2017, 2:00PM., Pacific Time

AMENDMENTS NUMBERED_ HAVE BEEN RECEIVED

Hand carried quote submittal procedures have changed. When dropping off all hand carried proposals, the official delivery location is now the guard station in the main foyer of Federal Center South, located at 4735 E. Marginal Way South where the official time clock is also located. Notify the guard on duty that you have a quote for Contracting Division. The point of contact will be notified and a representative from Contracting Division will sign in your package(s) and transport them to Contracting Division. Please allow sufficient time for these procedures when submitting hand carried quotes. All other quote submittal procedures remain the same.

5. PROSPECTIVE OFFERORS: Contractors are required to be registered in the System for Awards Management (SAM) for consideration of solicitations, awards and payment. Registration is required prior to award of any contract, basic agreement, basic ordering agreement, or blanket purchase agreement from a solicitation. LACK OF REGISTRATION IN THE SAM DATABASE WILL MAKE AN OFFER INELIGIBLE FOR AWARD. The web site may be accessed at www.sam.gov.

6. Award shall be made to the responsive, responsible, most technically capable offeror whose offer will be most advantageous to the Government (Refer to FAR Clause 52.212-2).

mailto:kelly.l.gunn@usace.army.mil http://www.sam.gov/

7. Required Submittals:

a) Instruction Page (2 pages)

• Must acknowledge any/all amendments to the solicitation.

• Must fill in all company information requested

• All submittals as required by evaluation criteria

b) Fill in all pricing information.

All of these must be filled in and returned in order to be eligible for evaluation.

DO NOT return the rest of the solicitation form.

8. The contractor is required to provide the following information with the quote:

Federal Taxpayer’s ID Number:

DUNS Number:

Cage Code Number:

This requires registration in SAM, web site for registration is www.sam.gov.

Remit to Address:

Company Name:

Address:

City/State/Zip:

Phone & Fax Numbers:

Point of Contact:

E-Mail Address:

The offeror must provide pricing for all items in the solicitation for its quote to be acceptable to the Government.

All quoted items must meet the requirements of the Request for Quote (RFQ) including specifications stated in all attachments.

Multiple quotes are not accepted for this RFQ. If multiple quotes are received only one quote (as determined by the Contracting Officer) will be evaluated by the Government. The quote shall be determined acceptable based on the date and time received.

The contractor should list any special features or warranty information applicable to the quoted product(s).

http://www.sam.gov/

ANNOUNCEMENT TO OFFERORS

Due to recent national events Seattle District US Army Corps of Engineers shall be conducting business under heightened security for the foreseeable future.

Access to Federal Center South, 4735 E Marginal Way S, Building 1202, Seattle, WA 98124 will be through the front lobby only. The building is under Federal Protective Service, which means that persons entering the facility are subject to inspection; including purses, packages, etc. All deliveries shall be thoroughly inspected. In addition, visitors may be required to be escorted by Corps personnel while in the building.

For any questions please contact the Contract Specialist assigned to your project or check our website at www.nws.usace.army.mil for up-to-date information.

http://www.nws.usace.army.mil/

X

SOLICITATION/CONTRACT/ORDER FOR COMMERCIAL ITEMS

OFFEROR TO COMPLETE BLOCKS 12, 17, 23, 24, AND 30

1. REQUISITION NUMBER PAGE 1 OF 64

2. CONTRACT NO. 3.AWARD/EFFECTIVEDATE 4. ORDER NUMBER 5.SOLICITATION NUMBER 6. SOLICITATION ISSUE DATE

W912DW-17-Q-0046 24-Apr-2017

7. FORSOLICITATION

INFORMATIONCALL:

a. NAME

KELLY L GUNN

b. TELEPHONE NUMBER

206-764-6575 (No Collect Calls) 8. OFFER DUE DATE/LOCALTIME

02:00 PM 24 May 2017

9. ISSUED BY

USA ENGINEER DISTRICT, SEATTLE

ATTN: CECT-NWS

CODE W912DW 10. THIS ACQUISITION IS

SMALL BUSINESS

UNRESTRICTED OR X SET ASIDE: 100 % FOR:

WOMEN-OWNED SMALL

BUSINESS (WOSB)

4735 EAST MARGINAL WAY SOUTH, BLDG. 1202

SEATTLE WA 98134-2388 HUBZONE SMALL

BUSINESS

TEL: SERVICE-DISABLED

ECONOMICALLY DISADVANTAGED

WOMEN-OWNED SMALL BUSINESS

(EDWOSB)

NAICS:

541380

VETERAN-OWNED 8(A) SIZE STANDARD:

FAX:

11. DELIVERY FOR FOB DESTINA-

TION UNLESS BLOCK IS

MARKED

12. DISCOUNT TERMS

SMALL BUSINESS

13a. THIS CONTRACT IS A

RATED ORDER UNDER

13b. RATING

15M

SEE SCHEDULE

DPAS (15 CFR 700) 14. METHOD OF SOLICITATION

X RFQ IFB RFP

15. DELIVER TO CODE 16. ADMINISTERED BY CODE

17a.CONTRACTOR/ CODE FACILITY

OFFEROR CODE

18a. PAY MENT WILL BE MADE BY CODE

TELEPHONE NO.

17b. CHECK IF REMITTANCE IS DIFFERENT AND PUT 18b. SUBMIT INVOICES TO ADDRESS SHOWN IN BLOCK 18a. UNLESS BLOCK

SUCH ADDRESS IN OFFER BELOW IS CHECKED SEE ADDENDUM

19. 20. 21. 22. 23. 24.

ITEM NO. SCHEDULE OF SUPPLIES/ SERVICES QUANTITY UNIT UNIT PRICE AMOUNT

25. ACCOUNTING AND APPROPRIATION DATA 26. TOTAL AWARD AMOUNT (For Gov t. Use Only )

27a. SOLICITATION INCORPORATES BY REFERENCE FAR 52.212-1. 52.212-4. FAR 52.212-3. 52.212-5 ARE ATTACHED. ADDENDA ARE ARE NOT ATTACHED

27b. CONTRACT/PURCHASE ORDER INCORPORATES BY REFERENCE FAR 52.212-4. FAR 52.212-5 IS ATTACHED.

ADDENDA

ARE

ARE NOT ATTACHED

28. CONTRACTOR IS REQUIRED TO SIGN THIS DOCUMENT AND RETURN 1 29. AWARD OF CONTRACT: REF.

COPIES TO ISSUING OFFICE. CONTRACTOR AGREES TO FURNISH AND OFFER DATED . Y OUR OFFER ON SOLICITATION

DELIVER ALL ITEMS SET FORTH OR OTHERWISE IDENTIFIED ABOVE AND ON ANY

ADDITIONAL SHEETS SUBJECT TO THE TERMS AND CONDITIONS SPECIFIED.

(BLOCK 5), INCLUDING ANY ADDITIONS OR CHANGES WHICH ARE

SET FORTH HEREIN, IS ACCEPTED AS TO ITEMS:

30a. SIGNATURE OF OFFEROR/CONTRACTOR 31a.UNITED STATES OF AMERICA (SIGNATUREOFCONTRACTINGOFFICER)

30b. NAME AND TITLEOF SIGNER 30c. DATE SIGNED 31b. NAME OF CONTRACTING OFFICER

(TYPE OR PRINT)

(TYPE OR PRINT) 31c. DATE SIGNED

TEL:

EMAIL:

AUTHORIZED FOR LOCAL REPRODUCTION

PREVIOUS EDITION IS NOT USABLE

STANDARD FORM 1449 (REV. 2/2012)

Prescribed by GSA – FAR (48 CFR) 53.212

X

SOLICITATION/CONTRACT/ORDER FOR COMMERCIAL ITEMS

(CONTINUED)

PAGE 2 OF64

19.

ITEM NO.

20.

SCHEDULE OF SUPPLIES/ SERVICES

21.

QUANTITY

22.

UNIT

23.

UNIT PRICE

24.

AMOUNT

32a. QUANTITY IN COLUMN 21 HAS BEEN

RECEIVED INSPECTED

ACCEPTED, AND CONFORMS TO THE CONTRACT, EXCEPT AS NOTED:

32b. SIGNATURE OF AUTHORIZED GOVERNMENT

REPRESENTATIVE

32c. DATE 32d. PRINTED NAME AND TITLE OF AUTHORIZED GOVERNMENT

REPRESENTATIVE

32e. MAILING ADDRESS OF AUTHORIZED GOVERNMENT REPRESENTATIVE 32f . TELEPHONE NUMBER OF AUTHORIZED GOVERNMENT REPRESENTATIVE

32g. E-MAIL OF AUTHORIZED GOVERNMENT REPRESENTATIVE

33. SHIP NUMBER 34. VOUCHER NUMBER 35. AMOUNT VERIFIED

CORRECT FOR

36. PAYMENT

COMPLETE PARTIAL FINAL

37. CHECK NUMBER

PARTIAL FINAL

38. S/R ACCOUNT NUMBER 39. S/R VOUCHER NUMBER 40. PAID BY

41a. I CERTIFY THIS ACCOUNT IS CORRECT AND PROPER FOR PAYMENT 42a. RECEIVED BY (Print)

41b. SIGNATURE AND TITLE OF CERTIFYING OFFICER 41c. DATE

42b. RECEIVED AT (Location)

42c. DATE REC'D (YY/MM/DD) 42d. TOTAL CONTAINERS

AUTHORIZED FOR LOCAL REPRODUCTION

PREVIOUS EDITION IS NOT USABLE

STANDARD FORM 1449 (REV. 2/2012) BACK

Prescribed by GSA – FAR (48 CFR) 53.212

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Base Year Base Year Base Year Line Item Description Method Price ($) Price ($) Price ($)

0001 - Waste Characterization and TCLP Parameters 1-5 Samples 6-10 Samples +11 Samples 0001A Corrosivity pH EPA 9045 0001B Ignitability EPA 1010 / 1030 0001C Paint Filter Liquid Test (Free Liquids) EPA 9095 0001D Filtration - Liquid Samples (Solids <0.5%) 1312 0001E Zero Headspace Extraction (VOC's Only) SW 1311 or SW 1312

TOTAL $

0002 - TCLP/SPLP Group Parameters (Including Extraction) 0002A TCLP Herbicides SW1311/8151 0002B TCLP Pesticides SW1311/8081 0002C

TCLP RCRA Metals

SW 1311/6010 &

7740/7471/245

0002D TCLP Volatiles SW 1311/8260 0002E TCLP Semivolatiles SW 1311/8270

TOTAL $

0003 - Petroleum Hydrocarbons Parameters 0003A Hydrocarbon Identification/NWTPH-HCID Publication No. ECY 97-602 0003B "GRO" Gasoline Range Organics /NWTPH-Gx, water Publication No. ECY 97-602 0003C "GRO" Gasoline Range Organics /NWTPH-Gx, soil (includes 5035 kit) Publication No. ECY 97-602 0003D

"GRO" Gasoline Range Organics + BTEX/NWTPH-Gx Modified

Publication No. ECY 97-602;

EPA 8021

0003E

"GRO" Gasoline Range Organics + BTEX/NWTPH-Gx Modified, soil (includes 5035 kit)

EPA 8021

0003F "DRO" Diesel Range Organics and Heavy Oils/NWTPH-Dx, soil or water Publication No. ECY 97-602 0003G VPH Fractions Publication No. ECY 97-602 0003H EPH Fractions Publication No. ECY 97-602 0003I TPH (GRO) CA Mod. 8015D 0003J TPH (DRO) CA Mod. 8015D 0003K TPH (ORO) CA Mod. 8015D 0003L VPH Fractions MADEP 0003M EPH Fractions MADEP

TOTAL $

0004 - Conventional / Wet Chemistry Parameters 0004A Acidity (titrimetric) (water) SM 2310B/305.1 0004B Alkalinity, as CaCO3 (water) EPA 310.1/SM 2320B 0004C Anions (individual) EPA 300.0 0004D Anions (Standard Scan), (Br, Cl, PO4, F, S04, NO2-N and NO3-N) EPA 300.0 0004E Biochemical Oxygen Demand, 5-Day SM 5210B/EPA 405.1 0004F

Chemical Oxygen Demand (water)

EPA 410.1/EPA 410.2/EPA

410.3/EPA 410.4/SM 5220D

0004G Chemical Oxygen Demand (soil) PSEP 0004H Chloride EPA 300.0 0004I Chlorine, Total Residual (water) EPA 330.4/EPA 330.5 0004J Coliform, Total SM 9221D 0004K Coliform, Fecal (water or soil) SM 9221E 0004L Color EPA 110.2/SM 2120B 0004M

Cyanide, total (water, soil)

SM 4500-CN-C/EPA

335.4/EPA 335.2/SW 9010

0004N

Cyanide, Amenable to Chlorination (soil, water)

EPA 335.4/SM 4500-CN-

G/SW 9010M/EPA 335.1/ SW

0004O Cyanide, Free (water) ASTM D4282-95M 0004P Cyanide, Weak and Dissociable (water, soil) SM 4500-CN I 0004Q Dissolved Oxygen (Lab/Probe) 106.2 0004R Hardness (as CaCO3) EPA 130.2 / 200.8/6010 0004S Hardness (Ca, MG calculation) 200.7/6010 0004T

Kjeldahl, Total (TKN) (water or soil)

EPA 351.2/ EPA 351.3/EPA

351.4/SM 4500-Norg

0004U Nitrogen, Nitrite-N (water) EPA 300.0/EPA 353.2 0004V Nitrogen, Nitrate-N (water) EPA 300.0/EPA 353.2 0004W Nitrogen, Nitrite-N (soil) EPA 300.0/EPA 353.2 0004X

Nitrogen, Natrate-N (soil)

SM 353.2/SM 4500-NO3

F/EPA 300.0

0004Y

Nitrogen, Nitrate + Nitrite-N (water)

0004Z

Nitrogen, Nitrate + Nitrite-N (soil)

0004AA

Nitrogen, Ammonia-N (water)

EPA 350.1/EPA 350.2/EPA

350.3

0004AB

Nitrogen, Ammonia-N (soil)

350.3

0004AC Nitrogen, Total Organic (calculation) EPA 350.1/351.4 0004AD Oil and Grease (Hexane Extractables) (water or soil) EPA 1664 0004AE Oil and Grease (Silica Gel treated Hexane Extractables) (water or soil) EPA 1664 0004AF Orthophosphate (water or soil) EPA 365.3 0004AG Perchlorate (water) SW 6860 0004AH Perchlorate (soil) SW 6860

0004AI

pH (water)

EPA 9045/EPA 150.1/SM

4500−H+

0004AJ pH (soil) EPA 9045/EPA 9040

0004AK

Phenolics (Manual Distillation) (water, soil)

EPA 420.1/SM 5530D/EPA

0004AL Phosphorus – Total (water) EPA 365.1 0004AM Settleable Solids SM 2540F/EPA 160.5

0004AN

Specific Conductance (water or soil)

EPA 120.1/SW 9050/SM 2510

Base Year (0000) 1 of 25

0004AO Sulfate (water or soil) EPA 300.0 0004AP Sulfide (Titrimetric) (water) SM 4500-S2-F/EPA 376.1 0004AQ Sulfide (Colormetric) (water) EPA 376.2/4500−S2 D 0004AR Sulfide (PSEP Total) (water or soil) PSEP 0004AS Sulfide (Reactivity) SW 7.3.4.2/ 0004AT Sulfur, Total (water or soil) EPA 300.0 0004AU Sulfur, Total (soil) ASTM D129 0004AV Surfactants (MBAS) (water) SM 5540C/EPA 425.1 0004AW Total Dissolved Solids (TDS) (water) SM 2540C/EPA 160.1 0004AX Total Suspended Solids (TSS) (water) EPA 160.2 0004AY Total Volatile Solids (TVS) (water or soil) EPA 106.4 0004AZ Total Organic Carbon (TOC) (water), triplicate SM 5310-D/9060/415.1

0004AAA

Total Organic Carbon (TOC) (soil), triplicate

ASTM D4129-82 M/Plumb

0004AAB Total Organic Carbon (TOC), quadruplicate (water) EPA 9060 0004AAC Total Organic Carbon (TOC), quadruplicate ( soil) EPA 9060 0004AAD Total Organic Carbon Walkley-Black 0004AAE Total Organic Halides (TOX) Single Replicate EPA 9076/EPA 9020 (Mod)

0004AAF

Volatile Fatty Acids

Performanced Based Method (EPA 300 Mod.)

0004AAG Hexane Extractable Material, silica treated (water) EPA 1664-SGT 0004AAH Total Phosphorus (colorimetric) (water or soil) EPA 365.1 0004AAI Total Solids EPA 160.3/SM 2540B 0004AAJ Total Suspended Solids (TSS) EPA 160.2/SM 2540D 0004AAK Total Dissolved Solids EPA 160.1/SM 2540C 0004AAL Total Volatile Solids EPA 160.4/SM 2540E 0004AAM Total Volatile Suspended Solids EPA 160.4/SM 2540E 0004AAN Turbidity EPA 180.1/SM 2130B

TOTAL $

0005 - Metals Parameters ICP (includes digestion) 0005A Metals EPA 200.7/SW 6010 ICP/MS (includes digestion) 0005B Metals EPA 200.8/SW 6020 Metals Regulatory Packages

0005C

Priority Pollutant Metals, water or soil (ICP/MS: Sb, As, Be, Cd, Cr, Cu, Pb, Ni, Se, Ag, Tl, Zn) (CVAA: Hg)

SW 6020

EPA 7471/7470

0005D

Priority Pollutant Metals, water

EPA 200.8/SW 6020

EPA 245.1/7470

0005E

CAM 17 Metals (CA Title 22) (ICP: Ba, Be, Cr, Co, Cu, Ni, Ag, V, Zn) (ICP/MS: Sb, As, Cd, Pb, Mo, SE, Tl)

EPA 200.7/SW 6010

0005F

CLP Target Analyte List (TAL) Metals (ICP: Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, K, Ag, Na, V, Zn) (ICP/MS: Sb, As, Cd, Pb, Tl)

SW 6010

0005G

RCRA List as Total Metals (ICP: As, Ba, Cd, Cr, Pb, Ag, Se)

0005H

RCRA List to Meet MTCA Limits, water

0005I

RCRA List to Meet MTCA Limits, soil

Other Metals

0005J

Chromium, Hexavalent (water)

EPA 7196

SM3500-Cr D

0005K Chromium, Hexavalent (soil) EPA 3060/7196 0005L Chromium, Hexavalent (water) EPA 7199 0005M Chromium, Hexavalent (water) EPA 218.6 0005N

Mercury

EPA 245.1/ SW 7470 /SW

0005O Mercury, cold vapor, 20 ng/L detection limit (water) SW 7470/EPA 1613 0005P

Mercury, Low Level (water or soil)

SW 7470M/EPA 1631/ SW

0005Q FULL IOC TEST Multiple TOTAL $ 0006 – Volatile Organic Parameters (5035 kit priced separately) 0006A Volatile Organics, DOD-QSM Std. List SW 8260/EPA 524.2 0006B Volatile Organics, PSDDA List SW 8260 SIM 0006C Volatile Organics, SDWA List EPA 524.2 0006D Volatile Organics, Priority Pollutant List EPA 624 0006E SIM analyses, for the first 1-5 compounds of concern SW 8260 0006F SIM analyses, for a total of six (6) or more compounds of concern SW 8260 0006G Method 8011 analyses of 1,2-Dibromo-3-chloropropane and/or Ethylene Dibromide SW 8011/EPA 504 0006H BTEX (GC/MS) + MTBE SW 8260 0006I Oxygenates (MTBE, TAME, ETBE, diisopropyl ether, tertbutanol SW8260 0006J Nonhalogenated Volatiles SW 8015 0006K Library Search (price per TIC) SW 8260 0006L Methane, Ethane & Ethene RSK 175 0006M F-Listed Solvents SW 8260/8270/8015 0006N Haloacetic Acids (HAA5) EPA 524.2/EPA 552.3 0006O Total Trihalomethanes (TTHMs) EPA 524.2

TOTAL $

Base Year (0000) 2 of 25

0007 – Semivolatile Organic Compounds 0007A Semivolatile Compounds, DOD-QSM Std List SW 8270/EPA 525.2 0007B Semivolatile Compounds (SIM), DOD-QSM Std List SW 8270 - SIM 0007C Semivolatile Compounds (SIM), PSDDA List SW 8270 - SIM 0007D Semivolatile Compounds (low-level) SW 8270 - SIM 0007E Polyaromatic Hydrocarbons SW 8270 0007F Polyaromatic Hydrocarbons (low-level) SW 8270-SIM 0007G Polyaromatic Hydrocarbons (0.01 μg/L) SW 8270-SIM Modified 0007H PAHs (NOAA list) NOAA Status & Trends 0007I Alkyl PAHs SW 8270-SIM 0007J 1,4-Dioxane as SVOC analyte SW 8270 0007K Nitramines & Nitroaromatics SW 8330 0007L Nitroglycerin & PETN EPA 8332 0007M Library Search (≥ 10 TICs) SW 8270 0007N Library Search (≥ 20 TICs) SW 8270 0007O Dioxins/Furans by HRGC/HRMS EPA 8290/1613A 0007P TCDD/TCDF by HRGC/HRMS EPA 8290/1613A 0007Q Polychlorinated Biphenyl Ethers (PBDEs) by HRGS/HRMS EPA 1664 0007R

Semivolatile Organics (benzo(a)pyrene, dimethyl nitrosamine, hexachlorobenzene, hexachlorobutadiene)

SW 8270

0007S Semivolatile Organics, Priority Polluntant List EPA 625 0007T PBDE Congeners (15, 28/33, 46,47,66,57,99,100,119,153,154,155,209) SW 8082

TOTAL $

0008 - Dioxin + PCB (TEFs) 0008A

Chemical Activated Luciferase Gene Expression (Dioxin and PCB TEFs), 1-5 analyses (price per analyses)

EPA 4435 (CALUX)

0008B

Chemical Activated Luciferase Gene Expression (Dioxin and PCB TEFs), >5 analyses (price per

0008C 1,4-Dioxane EPA 522

TOTAL $

0009 - Pesticide and Polychlorinated Biphenyl Parameters (include permangenate and sulfur cleanup in cost for analysis) 0009A Organochlorine Pesticides SW 8081/EPA 608 0009B Organochlorine Pesticides (low-level) SW 8081 0009C Organochlorine Pesticides (NOAA Status and Trends) SW 8081 0009D Organophosphorus Pesticides SW 8141/8270-SIM 0009E PCBs (water or soil) SW 8082/EPA 608 0009F PCBs utlra low-level (water, soil) SW 8082/EPA 608 0009G PCBs (oil) SW 8082 0009H PCB (wipes with cleanups) SW 8082 0009I PCB Congerers (209 full list) EPA 1668 0009J PCB Congerers (WHO full list) EPA 1668 0009K Herbicides (water) EPA 515.1 0009L General pesticides (water) EPA 525.2 0009M Insecticide (water) EPA 531.1 0009N EDB and other soil fumigants EPA 504 0009O Endothall EPA 547.1 0009P Diquat EPA 548.1 0009Q Glyphosphate EPA 249.1 0009R PCBs (caulk/paint) SW8082 0009S Pesticides and PCBs Priority Pollutant List EPA 625

TOTAL $

0010 - Herbicide Parameters 0010A Herbicides SW 8151 Mod 0010B Herbicides (PCP only) SW 8151/SW8041

TOTAL $

0011 - Asbestos Parameters 0011A PCM (air) NIOSH 7400 0011B PLM bulk EPA 600/R-93/116 0011C PLM bulk - Point count EPA Point Count 400 0011D TEM (air) NIOSH 7402 0011E

TEM (dust)

MICROVAC ASTM-D-5755-

0011F Asbestos (water) EPA 100.1/100.2

TOTAL $

0012 - Biological Parameters 0012A WETT Acute Tox Testing: Fathead minnow, Pemephales promelas EPA 821-R-02-012 0012B WETT Acute Tox Testing Daphid, Ceriodaphnia dubia, Daphnia pulex or Daphnia magna EPA 821-R-02-012 0012C

WETT Chronic Tox Testing: Top smelt (Atherinops affinis) or Silverside minnow (Menidia beryllina)

EPA 600/R-95-136

0012D WETT Chronic Tox Testing: Mysid shrimp (Holmesimysis costata or Mysidopsis bahia) EPA 821-R-02-014 0012E Salmonella (compost) Method TMECC 07.02

TOTAL $

0013 - Bioassay Parameters Amphipod Bioassay Description 0013A Rhepoxynius, series of 3 to 5 tests PSEP 0013B Rhepoxynius, series of 6 to 10 tests PSEP 0013C Ampelisca, series of 3 to 5 tests PSEP 0013D Ampelisca, series of 6 to 10 tests PSEP 0013E Eohaustorius, series of 3 to 5 tests PSEP 0013F Eohaustorius, series of 6 to 10 tests PSEP Sediment Larval Bioassay Tests

Base Year (0000) 3 of 25

0013G

Echinoderm/bivalve, series of 3 to 5 tests (Dendraster exentricus/Mytilus galloprovincialis or Dendraster exentricus /Crassostrea gigas)

PSEP

0013H

Echinoderm/bivalve, series of 6 to 10 tests

Juvenile Infaunal Bioassay Tests 0013I Neanthes arenaceodentata 20-day-Growth Test, series of 6 to 10 tests PSEP Bioaccumulation

0013J

Bioaccumulation (Macoma nasuta, Nephthys caecoides), series of 3 to 5 tests. 45-day test exposure.

DMMP Protocol Update http://www.nws.usace.army.mi l/PublicMenu/documents/DM MO/bioac_00-erratum_09.pdf

0014 - Sample Preparation and Cleanup Procedures 0014A Alumina SW 3610 0014B Alumina SW 3611B 0014C Florisil SW 3620 0014D Silica Gel SW 3630 0014E Gel Permeation SW 3640 0014F Sulfur Clean-up SW 3660 0014G Sulfuric Acid / Permangenate SW 3665 0014H Drying Grinding and Sieving SW 8330B Appendix A 0014I Tissue (shucking, filleting, grinding, drying) PSEP 0014J Lipids Bligh/Dyer 0014K Total Solids PSEP

TOTAL $

0015 - Air Parameters 0015A Phenols & Methylphenols (Cresols), blank not included EPA TO8 0015B Polynuclear Aromatic Hydrocarbons EPA TO13 0015C Volatile Organic Compounds (Collected in Summa Canister or Tedlar Bag) EPA TO15 0015D Volatile Organic Compounds (thermal desorption), blank not included EPA TO17 0015E Lead (air) NIOSH 7082

TOTAL $

0016 - Radionuclide Parameters 0016A Gross Alpha particle activity (drinking water) EPA 900.0 0016B Ra-226(drinking water) EPA 903.1 0016C Ra-228 (drinking water) EPA 904.0 0016D Uranium (mass & activity) ASTM D5174

TOTAL $

0017 - Various Analytical Suites

0017A

Unregulated Contaminated Monitoring Rule 3 List 1 (Entry Point)

EPA 524.3/EPA 522/EPA

200.8/EPA 300.1/EPA 537

Rev 1.1

0017B

Unregulated Contaminated Monitoring Rule 3 List 1 (DSMRT)

0017C

WAC 173-351 App I&II

SW 6020/SW 8260/EPA

310/SM 2320B/EPA

350.1/EPA 300/EPA 160.1/SM

0017D

WAC 173-351 App IV

SW 6020/EPA 415.1/EPA

410.1/SM 5310-D/SM

5210B/SM 4500-CN-C/SM

9221D

0017E

WAC 173-350-500

SW 6010/SW 9060/SM

2450C/SM 2320B/SM

5310D/EPA 160.1/EPA

300/EPA 310.1/EPA

350.1/EPA 350.2/ EPA 350.3/

0018 - Perfluorinated Compounds 0018A Perfluorinated Compounds (including PFOAs and PFOCs) EPA 537 0018B Perchlorate EPA 6850

TOTAL $

0019 - Collection Media and Equipment (prices include one way shipping) 0019E 6-L Summa Canister Rental and Prep Service (per week) 0019F 1-L Summa Canister Rental and Prep Service (per week) 0019G 6-L Certified Summa Canister Rental and Prep Service (per week) 0019H 1-L Certified Summa Canister (per week) 0019I 1-L Tedlar Bag 0019J 3-L Tedlar Bag 0019K 5-L Tedlar Bag 0019L 10-L Tedlar Bag 0019M PUF/XAD Cartridge (TO-13A, high volume) 0019N PUF/XAD Cartridge (TO-13A, low volume) 0019O PUF Cartridge (TO-4A, high volume) 0019P PUF Cartridge (TO-4A, low volume) 0019Q Thermal Desobption Tube 0019R Flow Controller

0020 - Data Validation 1

0020A Stage 2A Pesticides SW1311/SW8081 0020B Stage 4 Pesticides SW1311/SW8081 0020C Stage 2A Herbicides SW1311/SW8151 0020D Stage 4 Herbicides SW1311/SW8151 0020E Stage 2A Petroleum Hydrocarbons Publication No. ECY 97-602

Base Year (0000) 4 of 25 http://www.nws.usace.army.mi/

0020F Stage 4 Petroleum Hydrocarbons Publication No. ECY 97-602 0020G Stage 2A Metals EPA 200.8/SW 6020 0020H Stage 4 Metals EPA 200.8/SW 6020 0020I Stage 2A Volatile Organic Compounds SW 8260 0020J Stage 4 Volatile Organic Compounds SW 8260 0020K Stage 2A Semi-Volatile Organic Compounds SW 8270 0020L Stage 4 Semi-Volatile Organic Compounds SW 8270 0020M Stage 2A Nitramines & Nitroaromatics SW 8330 0020N Stage 4 Nitramines & Nitroaromatics SW 8330 0020O Stage 2A PCBs SW 8082 0020P Stage 4 PCBs SW 8082 0021 - Sample Turn-Around Time (note – time refers to calendar days ;standard turn-around-time is 14 days; isotope dilution methods are 40 days) 0021A 1-2 Day Turn-around-Time Factor 0021B 3 Day Turn-Around-Time Factor 0021C 4 -5 Day Turn-Around-Time Factor 0021D 6 - 9 Day Turn-Around-Time Factor 0021E 10 - 13 Day Turn-Around-Time Factor 0021F 20 Day Turn-Around-Time Factor for Isotope Dilution Methods 0021G Emergency Sampling NTE $3,000.00 $ 3,000.00 $ 3,000.00

0022 - Miscellaneous

0022A Methanol or Na2HSO4 Kit VOCs in soil 0022B Routine Courier Services (minimum $60.00)

TOTAL $

0023 - Deliverables 0023A SEDD or ADR (A1/A3) including checks 0023B EQuIS EDP checks (% of analysis cost) 0024 - Test Panel Analysis 0024A Test Panel Report of Analysis

0025 - UCMR4

0025A Unregulated Contaminants-UCMR4. UCMR4 list will be updated in 40 CFR 141.40 once the rule is finalized. Sampling will begin in March of 2018.

EPA Method 546; EPA Method 544; EPA Method 545; EPA Method 200.8; EPA Mehtod 525.3; EPA Method

552.3 or 557; EPA method 541; EPA Method 530

0026 - Benthic Macroinvertebrate Sampling Analysis 0026A Benthic Macroinvertebrate Sampling Analysis. 500-count sample: surber/hess-collected sample or other similar protocol.

ASTM, 2010, Method 10500

Notes:

At times a “Focused Data Validation” may be necessary. For the purpose of this contract, a focused data validation is a detailed investigation of particular data records identified by either the data validator or the government that 1 need special interpretation or review by the data validator. When known, the government shall alert the subcontracted data validator of anticipated problems before the data validation is performed.

The government may also request a focused data validation based on instances such as:

o Errors or omissions in the data or data validation report, o Anomalies noted during review of the data and data validation report, and o Anomalies noted during the data quality assessment process.

The above table will be used by the government to determine if prices are balanced.

Base Year (0000) 5 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 1 Option Year 1 Option Year 1

1001 - Waste Characterization and TCLP Parameters 1-5 Samples 6-10 Samples +11 Samples 1001A Corrosivity pH EPA 9045 1001B Ignitability EPA 1010 / 1030 1001C Paint Filter Liquid Test (Free Liquids) EPA 9095 1001D Filtration - Liquid Samples (Solids <0.5%) 1312 1001E Zero Headspace Extraction (VOC's Only) SW 1311 or SW 1312

TOTAL $

1002 - TCLP/SPLP Group Parameters (Including Extraction) 1002A TCLP Herbicides SW1311/8151 1002B TCLP Pesticides SW1311/8081 1002C

7740/7471/245

1002D TCLP Volatiles SW 1311/8260 1002E TCLP Semivolatiles SW 1311/8270

TOTAL $

1003 - Petroleum Hydrocarbons Parameters 1003A Hydrocarbon Identification/NWTPH-HCID Publication No. ECY 97-602 1003B "GRO" Gasoline Range Organics /NWTPH-Gx, water Publication No. ECY 97-602 1003C "GRO" Gasoline Range Organics /NWTPH-Gx, soil (includes 5035 kit) Publication No. ECY 97-602 1003D

1003E

EPA 8021

1003F "DRO" Diesel Range Organics and Heavy Oils/NWTPH-Dx, soil or water Publication No. ECY 97-602 1003G VPH Fractions Publication No. ECY 97-602 1003H EPH Fractions Publication No. ECY 97-602 1003I TPH (GRO) CA Mod. 8015D 1003J TPH (DRO) CA Mod. 8015D 1003K TPH (ORO) CA Mod. 8015D 1003L VPH Fractions MADEP 1003M EPH Fractions MADEP

TOTAL $

1004 - Conventional / Wet Chemistry Parameters 1004A Acidity (titrimetric) (water) SM 2310B/305.1 1004B Alkalinity, as CaCO3 (water) EPA 310.1/SM 2320B 1004C Anions (individual) EPA 300.0 1004D Anions (Standard Scan), (Br, Cl, PO4, F, S04, NO2-N and NO3-N) EPA 300.0 1004E Biochemical Oxygen Demand, 5-Day SM 5210B/EPA 405.1 1004F

410.3/EPA 410.4/SM 5220D

1004G Chemical Oxygen Demand (soil) PSEP 1004H Chloride EPA 300.0 1004I Chlorine, Total Residual (water) EPA 330.4/EPA 330.5 1004J Coliform, Total SM 9221D 1004K Coliform, Fecal (water or soil) SM 9221E 1004L Color EPA 110.2/SM 2120B 1004M

1004N

1004O Cyanide, Free (water) ASTM D4282-95M 1004P Cyanide, Weak and Dissociable (water, soil) SM 4500-CN I 1004Q

Dissolved Oxygen (Lab/Probe)

SM 4500-O-C/EPA 360.1/EPA

106.2

1004R Hardness (as CaCO3) EPA 130.2 / 200.8/6010 1004S Hardness (Ca, MG calculation) 200.7/6010 1004T

351.4/SM 4500-Norg

1004U Nitrogen, Nitrite-N (water) EPA 300.0/EPA 353.2 1004V Nitrogen, Nitrate-N (water) EPA 300.0/EPA 353.2 1004W Nitrogen, Nitrite-N (soil) EPA 300.0/EPA 353.2 1004X

1004Y

1004Z

1004AA

1004AB

350.3

1004AC Nitrogen, Total Organic (calculation) EPA 350.1/351.4 1004AD Oil and Grease (Hexane Extractables) (water or soil) EPA 1664 1004AE Oil and Grease (Silica Gel treated Hexane Extractables) (water or soil) EPA 1664 1004AF Orthophosphate (water or soil) EPA 365.3 1004AG Perchlorate (water) SW 6860 1004AH Perchlorate (soil) SW 6860

1004AI

4500−H+

1004AJ pH (soil) EPA 9045/EPA 9040

1004AK

1004AL Phosphorus – Total (water) EPA 365.1 1004AM Settleable Solids SM 2540F/EPA 160.5

1004AN

Option Year 1 (1000) 6 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 1 Option Year 1 Option Year 1

1004AO Sulfate (water or soil) EPA 300.0 1004AP Sulfide (Titrimetric) (water) SM 4500-S2-F/EPA 376.1 1004AQ Sulfide (Colormetric) (water) EPA 376.2/4500−S2 D 1004AR Sulfide (PSEP Total) (water or soil) PSEP 1004AS Sulfide (Reactivity) SW 7.3.4.2/ 1004AT Sulfur, Total (water or soil) EPA 300.0 1004AU Sulfur, Total (soil) ASTM D129 1004AV Surfactants (MBAS) (water) SM 5540C/EPA 425.1 1004AW Total Dissolved Solids (TDS) (water) SM 2540C/EPA 160.1 1004AX Total Suspended Solids (TSS) (water) EPA 160.2 1004AY Total Volatile Solids (TVS) (water or soil) EPA 106.4 1004AZ Total Organic Carbon (TOC) (water), triplicate SM 5310-D/9060/415.1

1004AAA

1004AAB Total Organic Carbon (TOC), quadruplicate (water) EPA 9060 1004AAC Total Organic Carbon (TOC), quadruplicate ( soil) EPA 9060 1004AAD Total Organic Carbon Walkley-Black 1004AAE Total Organic Halides (TOX) Single Replicate EPA 9076/EPA 9020 (Mod)

1004AAF

(EPA 300 Mod.)

1004AAG Hexane Extractable Material, silica treated (water) EPA 1664-SGT 1004AAH Total Phosphorus (colorimetric) (water or soil) EPA 365.1 1004AAI Total Solids EPA 160.3/SM 2540B 1004AAJ Total Suspended Solids (TSS) EPA 160.2/SM 2540D 1004AAK Total Dissolved Solids EPA 160.1/SM 2540C 0004AAL Total Volatile Solids EPA 160.4/SM 2540E 0004AAM Total Volatile Suspended Solids EPA 160.4/SM 2540E 0004AAN Turbidity EPA 180.1/SM 2130B

TOTAL $

1005 - Metals Parameters ICP (includes digestion) 1005A Metals EPA 200.7/SW 6010 ICP/MS (includes digestion) 1005B Metals EPA 200.8/SW 6020

1005C

1005D

1005E

(ICP: Ba, Be, Cr, Co, Cu, Ni, Ag, V, Zn)

1005F

(ICP: Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, K, Ag, Na, V, Zn)

1005G

1005H

1005I

1005J

SM3500-Cr D

1005K Chromium, Hexavalent (soil) EPA 3060/7196 1005L Chromium, Hexavalent (water) EPA 7199 1005M Chromium, Hexavalent (water) EPA 218.6 1005N

1005O Mercury, cold vapor, 20 ng/L detection limit (water) SW 7470/EPA 1613 1005P

1005Q FULL IOC TEST Multiple TOTAL $ 1006 – Volatile Organic Parameters (5035 kit priced separately) 1006A Volatile Organics, DOD-QSM Std. List SW 8260/EPA 524.2 1006B Volatile Organics, PSDDA List SW 8260 SIM 1006C Volatile Organics, SDWA List EPA 524.2 1006D Volatile Organics, Priority Pollutant List EPA 624 1006E SIM analyses, for the first 1-5 compounds of concern SW 8260 1006F SIM analyses, for a total of six (6) or more compounds of concern SW 8260 1006G Method 8011 analyses of 1,2-Dibromo-3-chloropropane and/or Ethylene Dibromide SW 8011/EPA 504 1006H BTEX (GC/MS) + MTBE SW 8260 1006I Oxygenates (MTBE, TAME, ETBE, diisopropyl ether, tertbutanol SW8260 1006J Nonhalogenated Volatiles SW 8015 1006K Library Search (price per TIC) SW 8260 1006L Methane, Ethane & Ethene RSK 175 1006M F-Listed Solvents SW 8260/8270/8015 1006N Haloacetic Acids (HAA5) EPA 524.2/EPA 552.3 1006O Total Trihalomethanes (TTHMs) EPA 524.2

Option Year 1 (1000) 7 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 1 Option Year 1 Option Year 1

1007 – Semivolatile Organic Compounds 1007A Semivolatile Compounds, DOD-QSM Std List SW 8270/EPA 525.2 1007B Semivolatile Compounds (SIM), DOD-QSM Std List SW 8270 - SIM 1007C Semivolatile Compounds (SIM), PSDDA List SW 8270 - SIM 1007D Semivolatile Compounds (low-level) SW 8270 - SIM 1007E Polyaromatic Hydrocarbons SW 8270 1007F Polyaromatic Hydrocarbons (low-level) SW 8270-SIM 1007G Polyaromatic Hydrocarbons (0.01 μg/L) SW 8270-SIM Modified 1007H PAHs (NOAA list) NOAA Status & Trends 1007I Alkyl PAHs SW 8270-SIM 1007J 1,4-Dioxane as SVOC analyte SW 8270 1007K Nitramines & Nitroaromatics SW 8330 1007L Nitroglycerin & PETN EPA 8332 1007M Library Search (≥ 10 TICs) SW 8270 1007N Library Search (≥ 20 TICs) SW 8270 1007O Dioxins/Furans by HRGC/HRMS EPA 8290/1613A 1007P TCDD/TCDF by HRGC/HRMS EPA 8290/1613A 1007Q Polychlorinated Biphenyl Ethers (PBDEs) by HRGS/HRMS EPA 1664 1007R

1007S Semivolatile Organics, Priority Polluntant List EPA 625 1007T PBDE Congeners (15, 28/33, 46,47,66,57,99,100,119,153,154,155,209) SW 8082

TOTAL $

1008 - Dioxin + PCB (TEFs) 1008A

1008B

1008C 1,4-Dioxane EPA 522

TOTAL $

1009 - Pesticide and Polychlorinated Biphenyl Parameters (include permangenate and sulfur cleanup in cost for analysis) 1009A Organochlorine Pesticides SW 8081/EPA 608 1009B Organochlorine Pesticides (low-level) SW 8081 1009C Organochlorine Pesticides (NOAA Status and Trends) SW 8081 1009D Organophosphorus Pesticides SW 8141/8270-SIM 1009E PCBs (water or soil) SW 8082/EPA 608 1009F PCBs utlra low-level (water, soil) SW 8082/EPA 608 1009G PCBs (oil) SW 8082 1009H PCB (wipes with cleanups) SW 8082 1009I PCB Congerers (209 full list) EPA 1668 1009J PCB Congerers (WHO full list) EPA 1668 1009K Herbicides (water) EPA 515.1 1009L General pesticides (water) EPA 525.2 1009M Insecticide (water) EPA 531.1 1009N EDB and other soil fumigants EPA 504 1009O Endothall EPA 547.1 1009P Diquat EPA 548.1 1009Q Glyphosphate EPA 249.1 1009R PCBs (caulk/paint) SW8082 1009S Pesticides and PCBs Priority Pollutant List EPA 625

TOTAL $

1010 - Herbicide Parameters 1010A Herbicides SW 8151 Mod 1010B Herbicides (PCP only) SW 8151/SW8041

TOTAL $

1011 - Asbestos Parameters 1011A PCM (air) NIOSH 7400 1011B PLM bulk EPA 600/R-93/116 1011C PLM bulk - Point count EPA Point Count 400 1011D TEM (air) NIOSH 7402 1011E

1011F Asbestos (water) EPA 100.1/100.2

TOTAL $

1012 - Biological Parameters 1012A WETT Acute Tox Testing: Fathead minnow, Pemephales promelas EPA 821-R-02-012 1012B WETT Acute Tox Testing Daphid, Ceriodaphnia dubia, Daphnia pulex or Daphnia magna EPA 821-R-02-012 1012C

1012D WETT Chronic Tox Testing: Mysid shrimp (Holmesimysis costata or Mysidopsis bahia) EPA 821-R-02-014 1012E Salmonella (compost) Method TMECC 07.02

TOTAL $

1013 - Bioassay Parameters Amphipod Bioassay Description 1013A Rhepoxynius, series of 3 to 5 tests PSEP 1013B Rhepoxynius, series of 6 to 10 tests PSEP 1013C Ampelisca, series of 3 to 5 tests PSEP 1013D Ampelisca, series of 6 to 10 tests PSEP 1013E Eohaustorius, series of 3 to 5 tests PSEP 1013F Eohaustorius, series of 6 to 10 tests PSEP Sediment Larval Bioassay Tests

Option Year 1 (1000) 8 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 1 Option Year 1 Option Year 1

1013G

1013H

1013I Neanthes arenaceodentata 20-day-Growth Test, series of 6 to 10 tests PSEP

1013J

DMMP Protocol Update http://www.nws.usace.army.mi

1014 - Sample Preparation and Cleanup Procedures 1014A Alumina SW 3610 1014B Alumina SW 3611B 1014C Florisil SW 3620 1014D Silica Gel SW 3630 1014E Gel Permeation SW 3640 1014F Sulfur Clean-up SW 3660 1014G Sulfuric Acid / Permangenate SW 3665 1014H Drying Grinding and Sieving SW 8330B Appendix A 1014I Tissue (shucking, filleting, grinding, drying) PSEP 1014J Lipids Bligh/Dyer 1014K Total Solids PSEP

TOTAL $

1015 - Air Parameters 1015A Phenols & Methylphenols (Cresols), blank not included EPA TO8 1015B Polynuclear Aromatic Hydrocarbons EPA TO13 1015C Volatile Organic Compounds (Collected in Summa Canister or Tedlar Bag) EPA TO15 1015D Volatile Organic Compounds (thermal desorption), blank not included EPA TO17 1015E Lead (air) NIOSH 7082

TOTAL $

1016 - Radionuclide Parameters 1016A Gross Alpha particle activity (drinking water) EPA 900.0 1016B Ra-226(drinking water) EPA 904.0 1016C Ra-228 (drinking water) EPA 903.1 1016D Uranium (mass & activity) ASTM D5174

TOTAL $

1017 - Various Analytical Suites

1017A

1017B

1017C

310/SM 2320B/EPA

1017D

410.1/SM 5310-D/SM

1017E

2450C/SM 2320B/SM

5310D/EPA 160.1/EPA

1018 - Perfluorinated Compounds 1018A Perfluorinated Compounds (including PFOAs and PFOCs) EPA 537 1018B Perchlorate EPA 6850

TOTAL $

1019 - Collection Media and Equipment (prices include one way shipping) 1019A 6-L Summa Canister Rental and Prep Service (per week) 1019B 1-L Summa Canister Rental and Prep Service (per week) 1019C 6-L Certified Summa Canister Rental and Prep Service (per week) 1019D 1-L Certified Summa Canister (per week) 1019E 1-L Tedlar Bag 1019F 3-L Tedlar Bag 1019G 5-L Tedlar Bag 1019H 10-L Tedlar Bag 1019I PUF/XAD Cartridge (TO-13A, high volume) 1019J PUF/XAD Cartridge (TO-13A, low volume) 1019K PUF Cartridge (TO-4A, high volume) 1019L PUF Cartridge (TO-4A, low volume) 1019M Thermal Desobption Tube 1019N Flow Controller

1020A Stage 2A Pesticides & Herbicides SW1311/SW8081 1020B Stage 4 Pesticides & Herbicides SW1311/SW8081 1020C Stage 2A Herbicides SW1311/SW8151 1020D Stage 4 Herbicides SW1311/SW8151 1020E Stage 2A Petroleum Hydrocarbons Publication No. ECY 97-602

Option Year 1 (1000) 9 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 1 Option Year 1 Option Year 1

1020F Stage 4 Petroleum Hydrocarbons Publication No. ECY 97-602 1020G Stage 2A Metals EPA 200.8/SW 6020 1020H Stage 4 Metals EPA 200.8/SW 6020 1020I Stage 2A Volatile Organic Compounds SW 8260 1020J Stage 4 Volatile Organic Compounds SW 8260 1020K Stage 2A Semi-Volatile Organic Compounds SW 8270 1020L Stage 4 Semi-Volatile Organic Compounds SW 8270 1020M Stage 2A Nitramines & Nitroaromatics SW 8330 1020N Stage 4 Nitramines & Nitroaromatics SW 8330 1020O Stage 2A PCBs SW 8082 1020P Stage 4 PCBs SW 8082 1021 - Sample Turn-Around Time (note – time refers to calendar days ;standard turn-around-time is 14 days; isotope dilution methods are 40 days) 1021A 1-2 Day Turn-around-Time Factor 1021B 3 Day Turn-Around-Time Factor 1021C 4 -5 Day Turn-Around-Time Factor 1021D 6 - 9 Day Turn-Around-Time Factor 1021E 10 - 13 Day Turn-Around-Time Factor 1021F 20 Day Turn-Around-Time Factor for Isotope Dilution Methods 1021G Emergency Sampling NTE $3,000.00 $ 3,000.00 $ 3,000.00

1022 - Miscellaneous

1022B Methanol or Na2HSO4 Kit VOCs in soil 1022D Routine Courier Services (minimum $60.00)

TOTAL $

1023 - Deliverables 1023A SEDD or ADR (A1/A3) including checks 1023B EQuIS EDP checks (% of analysis cost) 1024 - Test Panel Analysis 1024A Test Panel Report of Analysis

1025 - UCMR4

1025A Unregulated Contaminants-UCMR4. UCMR4 list will be updated in 40 CFR 141.40 once the rule is finalized. Sampling will begin in March of 2018.

EPA Method 546; EPA Method 544; EPA Method 545; EPA Method 200.8; EPA Mehtod 525.3; EPA Method

1026 - Benthic Macroinvertebrate Sampling Analysis 1026A Benthic Macroinvertebrate Sampling Analysis. 500-count sample: surber/hess-collected sample or other similar protocol.

ASTM, 2010, Method 10500

Notes:

At times a “Focused Data Validation” may be necessary. For the purpose of this contract, a focused data validation is a detailed investigation of particular data records identified by either the data validator or the government that 1 need special interpretation or review by the data validator. When known, the government shall alert the subcontracted data validator of anticipated problems before the data validation is performed.

Option Year 1 (1000) 10 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 2 Option Year 2 Option Year 2

2001 - Waste Characterization and TCLP Parameters 1-5 Samples 6-10 Samples +11 Samples 2001A Corrosivity pH EPA 9045 2001B Ignitability EPA 1010 / 1030 2001C Paint Filter Liquid Test (Free Liquids) EPA 9095 2001D Filtration - Liquid Samples (Solids <0.5%) 1312 2001E Zero Headspace Extraction (VOC's Only) SW 1311 or SW 1312

TOTAL $

2002 - TCLP/SPLP Group Parameters (Including Extraction) 2002A TCLP Herbicides SW1311/8151 2002B TCLP Pesticides SW1311/8081 2002C

7740/7471/245

2002D TCLP Volatiles SW 1311/8260 2002E TCLP Semivolatiles SW 1311/8270

TOTAL $

2003 - Petroleum Hydrocarbons Parameters 2003A Hydrocarbon Identification/NWTPH-HCID Publication No. ECY 97-602 2003B "GRO" Gasoline Range Organics /NWTPH-Gx, water Publication No. ECY 97-602 2003C "GRO" Gasoline Range Organics /NWTPH-Gx, soil (includes 5035 kit) Publication No. ECY 97-602 2003D

2003E

EPA 8021

2003F "DRO" Diesel Range Organics and Heavy Oils/NWTPH-Dx, soil or water Publication No. ECY 97-602 2003G VPH Fractions Publication No. ECY 97-602 2003H EPH Fractions Publication No. ECY 97-602 2003I TPH (GRO) CA Mod. 8015D 2003J TPH (DRO) CA Mod. 8015D 2003K TPH (ORO) CA Mod. 8015D 2003L VPH Fractions MADEP 2003M EPH Fractions MADEP

TOTAL $

2004 - Conventional / Wet Chemistry Parameters 2004A Acidity (titrimetric) (water) SM 2310B/305.1 2004B Alkalinity, as CaCO3 (water) EPA 310.1/SM 2320B 2004C Anions (individual) EPA 300.0 2004D Anions (Standard Scan), (Br, Cl, PO4, F, S04, NO2-N and NO3-N) EPA 300.0 2004E Biochemical Oxygen Demand, 5-Day SM 5210B/EPA 405.1 2004F

410.3/EPA 410.4/SM 5220D

2004G Chemical Oxygen Demand (soil) PSEP 2004H Chloride EPA 300.0 2004I Chlorine, Total Residual (water) EPA 330.4/EPA 330.5 2004J Coliform, Total SM 9221D 2004K Coliform, Fecal (water or soil) SM 9221E 2004L Color EPA 110.2/SM 2120B 2004M

2004N

2004O Cyanide, Free (water) ASTM D4282-95M 2004P Cyanide, Weak and Dissociable (water, soil) SM 4500-CN I 2004Q Dissolved Oxygen (Lab/Probe) 106.2 2004R Hardness (as CaCO3) EPA 130.2 / 200.8/6010 2004S Hardness (Ca, MG calculation) 200.7/6010 2004T

351.4/SM 4500-Norg

2004U Nitrogen, Nitrite-N (water) EPA 300.0/EPA 353.2 2004V Nitrogen, Nitrate-N (water) EPA 300.0/EPA 353.2 2004W Nitrogen, Nitrite-N (soil) EPA 300.0/EPA 353.2 2004X

2004Y

2004Z

2004AA

2004AB

350.3

2004AC Nitrogen, Total Organic (calculation) EPA 350.1/351.4 2004AD Oil and Grease (Hexane Extractables) (water or soil) EPA 1664 2004AE Oil and Grease (Silica Gel treated Hexane Extractables) (water or soil) EPA 1664 2004AF Orthophosphate (water or soil) EPA 365.3 2004AG Perchlorate (water) SW 6860 2004AH Perchlorate (soil) SW 6860

2004AI

4500−H+

2004AJ pH (soil) EPA 9045/EPA 9040

2004AK

2004AL Phosphorus – Total (water) EPA 365.1 2004AM Settleable Solids SM 2540F/EPA 160.5

2004AN

Option Year 2 (2000) 11 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 2 Option Year 2 Option Year 2

2004AO Sulfate (water or soil) EPA 300.0 2004AP Sulfide (Titrimetric) (water) SM 4500-S2-F/EPA 376.1 2004AQ Sulfide (Colormetric) (water) EPA 376.2/4500−S2 D 2004AR Sulfide (PSEP Total) (water or soil) PSEP 2004AS Sulfide (Reactivity) SW 7.3.4.2/ 2004AT Sulfur, Total (water or soil) EPA 300.0 2004AU Sulfur, Total (soil) ASTM D129 2004AV Surfactants (MBAS) (water) SM 5540C/EPA 425.1 2004AW Total Dissolved Solids (TDS) (water) SM 2540C/EPA 160.1 2004AX Total Suspended Solids (TSS) (water) EPA 160.2 2004AY Total Volatile Solids (TVS) (water or soil) EPA 106.4 2004AZ Total Organic Carbon (TOC) (water), triplicate SM 5310-D/9060/415.1

2004AAA

2004AAB Total Organic Carbon (TOC), quadruplicate (water) EPA 9060 2004AAC Total Organic Carbon (TOC), quadruplicate ( soil) EPA 9060 2004AAD Total Organic Carbon Walkley-Black 2004AAE Total Organic Halides (TOX) Single Replicate EPA 9076/EPA 9020 (Mod)

2004AAF

(EPA 300 Mod.)

2004AAG Hexane Extractable Material, silica treated (water) EPA 1664-SGT 2004AAH Total Phosphorus (colorimetric) (water or soil) EPA 365.1 2004AAI Total Solids EPA 160.3/SM 2540B 2004AAJ Total Suspended Solids (TSS) EPA 160.2/SM 2540D 2004AAK Total Dissolved Solids EPA 160.1/SM 2540C 2004AAL Total Volatile Solids EPA 160.4/SM 2540E 2004AAM Total Volatile Suspended Solids EPA 160.4/SM 2540E 2004AAN Turbidity EPA 180.1/SM 2130B

TOTAL $

2005 - Metals Parameters ICP (includes digestion) 2005A 1 Metal EPA 200.7/SW 6010 2005B 2 Metals 2005C 3 Metals 2005D 4 Metals 2005E 5 - 8 Metals 2005F 9-12 Metals 2005G 13 or More Metals ICP/MS (includes digestion) 2005H 1 Metal EPA 200.8/SW 6020 2005I 2 Metals 2005J 3 Metals 2005K 4 Metals 2005L 5 - 8 Metals 2005M 9-12 Metals 2005N 13 or More Metals

2005O

2005P

2005Q

(ICP: Ba, Be, Cr, Co, Cu, Ni, Ag, V, Zn)

2005R

(ICP: Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, K, Ag, Na, V, Zn)

2005S

2005T

2005U

2005V

SM3500-Cr D

2005W Chromium, Hexavalent (soil) EPA 3060/7196 2005X Chromium, Hexavalent (water) EPA 7199 2005Y Chromium, Hexavalent (water) EPA 218.6

2005AA

2005AB Mercury, cold vapor, 20 ng/L detection limit (water) SW 7470/EPA 1613

2005AC

2005AD FULL IOC TEST Multiple

TOTAL $

2006 – Volatile Organic Parameters (5035 kit priced separately) 2006A Volatile Organics, DOD-QSM Std. List SW 8260/EPA 524.2 2006B Volatile Organics, PSDDA List SW 8260 SIM 2006C Volatile Organics, SDWA List EPA 524.2 2006D Volatile Organics, Priority Pollutant List EPA 624

Option Year 2 (2000) 12 of 25

2017 SEATTLE DISTRICT ANALYTICAL SERVICES CONTRACT - BID SCHEDULE Option Year 2 Option Year 2 Option Year 2

2006E SIM analyses, for the first 1-5 compounds of concern SW 8260 2006F SIM analyses, for a total of six (6) or more compounds of concern SW 8260 2006G Method 8011 analyses of 1,2-Dibromo-3-chloropropane and/or Ethylene Dibromide SW 8011/EPA 504 2006H BTEX (GC/MS) + MTBE SW 8260 2006I Oxygenates (MTBE, TAME, ETBE, diisopropyl ether, tertbutanol SW8260 2006J Nonhalogenated Volatiles SW 8015 2006K Library Search (price per TIC) SW 8260 2006L Methane, Ethane & Ethene RSK 175 2006M F-Listed Solvents SW 8260/8270/8015 2006N Haloacetic Acids (HAA5) EPA 524.2/EPA 552.3 2006O Total Trihalomethanes (TTHMs) EPA 524.2

TOTAL $

2007 – Semivolatile Organic Compounds 2007A Semivolatile Compounds, DOD-QSM Std List SW 8270/EPA 525.2 2007A Semivolatile Compounds (SIM), DOD-QSM Std List SW 8270 - SIM 2007A Semivolatile Compounds (SIM), PSDDA List SW 8270 - SIM 2007A Semivolatile Compounds (low-level) SW 8270 - SIM 2007E Polyaromatic Hydrocarbons SW 8270 2007F Polyaromatic Hydrocarbons (low-level SW 8270-SIM 2007G Polyaromatic Hydrocarbons (0.01 μg/L) SW 8270-SIM Modified 2007H PAHs (NOAA list) NOAA Status & Trends 2007I Alkyl PAHs SW 8270-SIM 2007J 1,4-Dioxane as SVOC analyte SW 8270 2007K Nitramines & Nitroaromatics SW 8330 2007L Nitroglycerin & PETN EPA 8332 2007M Library Search (≥ 10 TICs) SW 8270 2007N Library Search (≥ 20 TICs) SW 8270 2007O

Dioxins/Furans by HRGC/HRMS

EPA 8290/1613A

2007P TCDD/TCDF by HRGC/HRMS EPA 8290/1613A 2007Q Polychlorinated Biphenyl Ethers (PBDEs) by HRGS/HRMS EPA 1664 2007R hexachlorobutadiene) SW 8270 2007S Semivolatile Organics, Priority Polluntant List EPA 625 2007T PBDE Congeners (15, 28/33, 46,47,66,57,99,100,119,153,154,155,209) SW 8082

TOTAL $

2008 - Dioxin + PCB (TEFs) 2008A

2008B

2008C 1,4-Dioxane EPA 522

TOTAL $

(include permangenate and sulfur cleanup in cost for analysis) 2009A Organochlorine Pesticides SW 8081/EPA 608 2009B Organochlorine Pesticides (low-level) SW 8081 2009C Organochlorine Pesticides (NOAA Status and Trends) SW 8081 2009D Organophosphorus Pesticides SW 8141/8270-SIM 2009E PCBs (water or soil) SW 8082/EPA 608 2009F PCBs utlra low-level (water, soil) SW 8082/EPA 608 2009G PCBs (oil) SW 8082 2009H PCB (wipes with cleanups) SW 8082 2009I PCB Congerers (209 full list) EPA 1668 2009J PCB Congerers (WHO full list) EPA 1668 2009K Herbicides (water) EPA 515.1 2009L General pesticides (water) EPA 525.2 2009M Insecticide (water) EPA 531.1 2009N EDB and other soil fumigants EPA 504 2009O Endothall EPA 547.1 2009P Diquat EPA 548.1 2009Q Glyphosphate EPA 249.1 2009R PCBs (caulk/paint) SW8082 2009S Pesticides and PCBs Priority Pollutant List EPA 625

TOTAL $

2010 - Herbicide Parameters 2010A Herbicides SW 8151 Mod 2010B Herbicides (PCP only) SW 8151/SW8041 TOTAL $ 2011 - Asbestos Parameters 2011A PCM (air) NIOSH 7400 2011B PLM bulk EPA 600/R-93/116 2011C PLM bulk - Point count EPA Point Count 400 2011D TEM (air) NIOSH 7402 2011E

2011F Asbestos (water) EPA…