2023 S_T J153256-1 Std_Tal_L4 Final Report_Part7.pdf

Sample Report

4/1/2023 6:54 AM

Sample Name 180-151590-c-2-e @10

File Name 104SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 5:45:05 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 62.839 2.6 103783.687 3000

Be 9 6 No Gas 0.274 11.8 135.333 3600

(B) 10 103 No Gas 170.361 3.3 8126.673 3600

B 11 103 No Gas 163.081 5.4 41162.800 3600

Si 28 45 H2 146.492 0.9 3943.877 10000

Fe 56 45 H2 30496.262 1.3 41424979.467 625000

Se 78 45 H2 3.492 3.8 231.253 2250

(Sn) 118 115 H2 121.069 1.1 231491.123 5400

Na 23 45 He 3278.298 0.6 378009.133 625000

{Mg} 24 45 He 6316.375 0.4 362173.937 625000

{Mg} 25 45 He 6338.606 0.2 54103.180 625000

Mg 26 45 He 6253.828 1.0 69056.823 625000

Al 27 45 He 7235.752 0.8 159161.827 225000

P 31 45 He 740.324 3.5 1261.173 15000

K 39 45 He 1781.594 0.3 132682.063 625000

{Ca} 43 45 He 59112.385 3.0 10618.317 625000

Ca 44 45 He 59713.330 0.8 185993.510 625000

Ti 47 45 He 2217.351 0.5 51791.930 6750

V 51 45 He 25.787 1.5 20926.110 11250

Cr 52 45 He 98.075 0.5 100263.850 11250

(Cr) 53 45 He 98.920 0.5 12285.200 11250

Mn 55 103 He 169.820 1.7 98626.977 22050

Co 59 103 He 66.745 1.3 117100.080 6750

Ni 60 103 He 241.114 0.9 113906.090 11250

(Cu) 63 103 He 3742.561 0.4 4900334.387 11250

Cu 65 103 He 3766.563 1.1 2435510.667 11250

Zn 66 103 He 1191.581 0.9 250270.980 11250

(Zn) 68 103 He 1269.938 1.3 198036.047 11250

As 75 103 He 88.036 0.3 12503.733 2250

(Se) 78 103 He 3.696 21.9 121.333 2250

(Se) 82 103 He 0.487 206.9 53.337 2250

Sr 88 103 He 111.850 1.0 90242.790 11250

(Mo) 95 103 He 80.923 1.5 52836.800 6750

Mo 98 103 He 80.677 0.3 87995.080 6750

Ag 107 103 He 18.152 2.5 38037.810 600

(Ag) 109 103 He 18.331 0.1 36940.490 600

4/1/2023 6:54 AM

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 0.468 2.9 166.333 6750

(Cd) 114 115 He 3.010 3.4 2395.207 6750

Sn 118 115 He 121.122 1.0 84621.637 5400

Sb 121 115 He 16.040 2.0 13718.993 5400

(Sb) 123 115 He 16.140 2.1 10844.243 5400

Ba 137 159 He 1063.874 1.2 358465.293 11250

(Tl) 203 209 He -0.062 N/A 91.110 9000

Tl 205 209 He -0.044 N/A 220.000 9000

[Pb] 206 209 He 142.055 1.3 192624.823 11250

[Pb] 207 209 He 139.886 1.7 164690.167 11250

Pb 208 209 He 139.741 1.6 759765.487 11250

Th 232 209 He 0.573 1.7 3200.410 4500

U 238 209 He 0.532 2.1 2779.207 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 194669.260 0.3 202714.773333333 96.03 30 150

Sc (IS) 45 No Gas 1315766.673 1.0 1182756.31 111.25 30 150

Rh (IS) 103 No Gas 2658093.917 0.6 2107039.5 126.15 30 150

Sc (IS) 45 H2 347845.107 1.1 318888.686666667 109.08 30 150

Rh (IS) 103 H2 98985.100 0.9 98679.7966666667 100.31 30 150

115In 115 H2 530362.220 2.7 421564.323333333 125.81 30 150

Sc (IS) 45 He 83205.963 0.4 74004.76 112.43 30 150

Rh (IS) 103 He 2135001.790 1.4 1819840.96666667 117.32 30 150

115In 115 He 164232.513 1.3 143763.77 114.24 30 150

Tb (IS) 159 He 184751.503 1.9 151792.613333333 121.71 30 150

Ho (IS) 165 He 184923.627 0.7 151670.6 121.92 30 150

Bi (IS) 209 He 1980372.423 1.7 1551684.83333333 127.63 30 150

4/1/2023 6:43 AM

Sample Name 180-151590-c-3-e

File Name 105SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 5:48:44 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

FailISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 1036.377 4.5 1506790.503 3000

Be 9 6 No Gas 3.701 4.5 1392.070 3600

(B) 10 103 No Gas 2112.440 3.2 86425.293 3600

B 11 103 No Gas 1992.966 3.8 429864.973 3600

Si 28 45 H2 1534.356 0.4 38690.230 10000

Fe 56 45 H2 402384.832 1.3 548953987.073 625000

Se 78 45 H2 54.588 1.3 3548.040 2250

(Sn) 118 115 H2 1802.248 0.3 3869533.797 5400

Na 23 45 He 84877.604 2.9 9463253.513 625000

{Mg} 24 45 He 83350.923 0.8 4726798.980 625000

{Mg} 25 45 He 81998.068 1.7 692189.280 625000

Mg 26 45 He 81487.682 2.2 889764.097 625000

Al 27 45 He 109234.635 2.3 2378943.583 225000

P 31 45 He 15839.979 0.9 23953.803 15000 LDR HIGH

K 39 45 He 31702.796 2.5 1888909.857 625000

{Ca} 43 45 He 702831.611 2.8 124996.693 625000 LDR HIGH

Ca 44 45 He 717476.802 1.7 2212079.080 625000 LDR HIGH

Ti 47 45 He 29888.635 2.6 691440.063 6750 LDR HIGH

V 51 45 He 386.385 2.0 310287.913 11250

Cr 52 45 He 1908.929 2.6 1922839.297 11250

(Cr) 53 45 He 1898.757 3.3 232495.853 11250

Mn 55 103 He 2596.422 1.4 1417876.160 22050

Co 59 103 He 728.266 1.4 1202573.353 6750

Ni 60 103 He 3012.264 2.1 1339020.087 11250

(Cu) 63 103 He 34113.104 2.5 42078070.553 11250 LDR HIGH

Cu 65 103 He 34807.398 2.0 21205295.827 11250 LDR HIGH

Zn 66 103 He 28158.850 2.0 5564988.807 11250 LDR HIGH

(Zn) 68 103 He 29306.443 1.0 4301237.053 11250 LDR HIGH

As 75 103 He 1275.707 1.9 170532.733 2250

(Se) 78 103 He 86.725 2.6 961.697 2250

(Se) 82 103 He 57.825 4.9 325.563 2250

Sr 88 103 He 1730.665 1.6 1314708.557 11250

(Mo) 95 103 He 1179.332 1.7 725010.543 6750

Mo 98 103 He 1189.052 2.4 1220994.707 6750

Ag 107 103 He 172.679 1.4 340626.780 600

(Ag) 109 103 He 175.689 2.7 333198.973 600

4/1/2023 6:43 AM

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 93.803 0.9 28114.907 6750

(Cd) 114 115 He 118.487 1.7 100811.793 6750

Sn 118 115 He 1780.509 2.0 1350783.417 5400

Sb 121 115 He 426.856 1.4 396094.687 5400

(Sb) 123 115 He 431.662 1.1 314768.583 5400

Ba 137 159 He 14314.787 1.0 4851509.833 11250 LDR HIGH

(Tl) 203 209 He 0.385 4.2 2204.640 9000

Tl 205 209 He 0.352 4.3 4730.863 9000

[Pb] 206 209 He 1675.051 1.5 5901089.490 11250

[Pb] 207 209 He 1692.384 0.8 5177587.990 11250

Pb 208 209 He 1650.256 0.5 23313952.273 11250

Th 232 209 He 3.616 2.3 48147.627 4500

U 238 209 He 3.011 2.6 40557.773 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 195224.427 1.8 202714.773333333 96.3 30 150

Sc (IS) 45 No Gas 1301307.790 0.7 1182756.31 110.02 30 150

Rh (IS) 103 No Gas 2457056.420 0.4 2107039.5 116.61 30 150

Sc (IS) 45 H2 349428.343 0.3 318888.686666667 109.58 30 150

Rh (IS) 103 H2 88005.613 0.8 98679.7966666667 89.18 30 150

115In 115 H2 597162.650 2.4 421564.323333333 141.65 30 150

Sc (IS) 45 He 82433.833 1.6 74004.76 111.39 30 150

Rh (IS) 103 He 2011782.280 1.1 1819840.96666667 110.55 30 150

115In 115 He 178820.210 0.4 143763.77 124.38 30 150

Tb (IS) 159 He 185813.590 0.5 151792.613333333 122.41 30 150

Ho (IS) 165 He 189089.530 1.6 151670.6 124.67 30 150

Bi (IS) 209 He 5147739.380 0.2 1551684.83333333 331.75 30 150 ISTD Failed

4/1/2023 6:55 AM

Sample Name CCV 5280846

File Name 108_CCV.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 5:59:41 PMAcq Time

Sample Type CCV

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 198.855 1.1 334269.217 200

Be 9 6 No Gas 203.093 0.8 82982.500 200

(B) 10 103 No Gas 528.651 2.7 22821.767 500

B 11 103 No Gas 503.695 2.3 114780.173 500

Si 28 45 H2 1898.409 1.2 50515.360 2000

Fe 56 45 H2 52888.495 0.1 76262701.417 50000

Se 78 45 H2 209.203 0.6 14351.307 200

(Sn) 118 115 H2 205.219 0.8 390223.627 200

Na 23 45 He 52980.022 3.1 6291363.640 50000

{Mg} 24 45 He 53353.188 1.6 3221032.997 50000

{Mg} 25 45 He 52295.187 1.1 470024.113 50000

Mg 26 45 He 51750.063 1.9 601608.170 50000

Al 27 45 He 50458.539 1.8 1169981.957 50000

P 31 45 He 2436.343 2.8 4045.013 2500

K 39 45 He 52555.707 1.4 3315190.283 50000

{Ca} 43 45 He 53171.545 1.6 10073.480 50000

Ca 44 45 He 52539.709 1.4 172597.563 50000

Ti 47 45 He 207.162 0.6 5105.560 200

V 51 45 He 207.381 1.5 177312.830 200

Cr 52 45 He 205.429 1.6 220828.907 200

(Cr) 53 45 He 205.155 1.2 26803.417 200

Mn 55 103 He 201.636 1.8 118700.027 200

Co 59 103 He 203.356 3.2 361377.107 200

Ni 60 103 He 201.734 1.4 96659.587 200

(Cu) 63 103 He 200.877 1.2 267167.273 200

Cu 65 103 He 202.277 2.6 132838.023 200

Zn 66 103 He 104.645 1.9 22617.627 100

(Zn) 68 103 He 117.327 1.6 18789.997 100 >+\-10%

As 75 103 He 202.851 1.6 29192.373 200

(Se) 78 103 He 198.468 1.0 2262.517 200

(Se) 82 103 He 213.616 8.0 1154.497 200

Sr 88 103 He 198.760 1.8 162527.250 200

(Mo) 95 103 He 209.971 1.2 138946.873 200

Mo 98 103 He 208.262 2.1 230177.453 200

Ag 107 103 He 104.305 1.1 221434.507 100

(Ag) 109 103 He 105.719 1.4 215780.090 100

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 204.955 1.8 66077.437 200

(Cd) 114 115 He 205.108 0.7 163862.327 200

Sn 118 115 He 203.958 1.0 145545.037 200

Sb 121 115 He 200.243 0.8 174534.400 200

(Sb) 123 115 He 203.248 0.9 139207.840 200

Ba 137 159 He 198.083 1.7 66980.887 200

(Tl) 203 209 He 208.474 1.2 331923.617 200

Tl 205 209 He 206.488 1.1 784027.087 200

[Pb] 206 209 He 206.269 1.1 262808.480 200

[Pb] 207 209 He 206.560 1.6 228513.920 200

Pb 208 209 He 205.781 1.6 1051296.633 200

Th 232 209 He 104.792 0.4 496238.243 100

U 238 209 He 103.390 1.9 502645.483 100

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 217424.370 1.0 202714.773333333 107.26 30 150

Sc (IS) 45 No Gas 1360329.353 1.3 1182756.31 115.01 30 150

Rh (IS) 103 No Gas 2541514.543 2.2 2107039.5 120.62 30 150

Sc (IS) 45 H2 369268.607 1.3 318888.686666667 115.8 30 150

Rh (IS) 103 H2 103696.730 1.0 98679.7966666667 105.08 30 150

115In 115 H2 527999.057 1.9 421564.323333333 125.25 30 150

Sc (IS) 45 He 87759.927 1.8 74004.76 118.59 30 150

Rh (IS) 103 He 2165018.247 2.0 1819840.96666667 118.97 30 150

115In 115 He 167942.990 1.3 143763.77 116.82 30 150

Tb (IS) 159 He 185382.597 1.5 151792.613333333 122.13 30 150

Ho (IS) 165 He 187050.010 1.4 151670.6 123.33 30 150

Bi (IS) 209 He 1861183.330 1.6 1551684.83333333 119.95 30 150

Sample Name CCB

File Name 109_CCB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:03:20 PMAcq Time

Sample Type CCB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas -0.013 N/A 15080.210 5

Be 9 6 No Gas -0.044 N/A 21.333 1

(B) 10 103 No Gas 51.090 8.7 2772.493 80

B 11 103 No Gas 49.736 1.8 14346.863 80

Si 28 45 H2 -6.117 N/A 151.113 500

Fe 56 45 H2 6.526 5.9 24239.007 50

Se 78 45 H2 -0.037 N/A 3.507 5

(Sn) 118 115 H2 0.240 35.0 1110.070 5

Na 23 45 He -16.960 N/A 7842.090 500

{Mg} 24 45 He -5.127 N/A 373.340 500

{Mg} 25 45 He -3.909 N/A 62.223 500

Mg 26 45 He -4.623 N/A 77.777 500

Al 27 45 He 4.960 16.4 185.333 30

P 31 45 He -60.585 N/A 47.777 500

K 39 45 He -88.190 N/A 22897.763 500

{Ca} 43 45 He 55.109 113.5 15.557 500

Ca 44 45 He 9.892 82.4 184.447 500

Ti 47 45 He 0.802 15.4 21.667 5

V 51 45 He 0.037 33.6 52.220 1

Cr 52 45 He -0.062 N/A 514.457 2

(Cr) 53 45 He -0.013 N/A 60.003 2

Mn 55 103 He -0.097 N/A 175.557 5

Co 59 103 He -0.025 N/A 106.667 0.5

Ni 60 103 He -0.183 N/A 78.890 1

(Cu) 63 103 He 0.849 14.6 1630.100 2

Cu 65 103 He 0.862 8.7 806.693 2

Zn 66 103 He 0.032 718.1 370.007 15

(Zn) 68 103 He 0.288 64.3 304.447 15

As 75 103 He 0.008 376.3 15.333 1

(Se) 78 103 He -0.919 N/A 72.333 5

(Se) 82 103 He -1.365 N/A 44.443 5

Sr 88 103 He 0.010 59.7 68.887 5

(Mo) 95 103 He 0.127 17.8 129.333 5

Mo 98 103 He 0.152 17.7 238.667 5

Ag 107 103 He 0.080 23.4 218.893 1

(Ag) 109 103 He 0.079 19.1 205.560 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He -0.032 N/A 7.667 1

(Cd) 114 115 He -0.011 N/A 36.667 1

Sn 118 115 He 0.331 7.6 484.457 5

Sb 121 115 He 0.238 17.7 258.893 2

(Sb) 123 115 He 0.305 22.0 244.447 2

Ba 137 159 He 0.369 26.1 133.333 10

(Tl) 203 209 He -0.030 N/A 134.447 1

Tl 205 209 He -0.013 N/A 318.897 1

[Pb] 206 209 He 0.172 14.6 330.007 1

[Pb] 207 209 He 0.147 25.7 242.227 1

Pb 208 209 He 0.153 7.5 1176.693 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 218538.540 0.2 202714.773333333 107.81 30 150

Sc (IS) 45 No Gas 1359987.113 1.1 1182756.31 114.98 30 150

Rh (IS) 103 No Gas 2557174.077 1.3 2107039.5 121.36 30 150

Sc (IS) 45 H2 369686.117 0.6 318888.686666667 115.93 30 150

Rh (IS) 103 H2 106295.833 1.8 98679.7966666667 107.72 30 150

115In 115 H2 522338.933 3.1 421564.323333333 123.9 30 150

Sc (IS) 45 He 87404.343 1.2 74004.76 118.11 30 150

Rh (IS) 103 He 2163324.707 0.4 1819840.96666667 118.87 30 150

115In 115 He 166745.783 0.2 143763.77 115.99 30 150

Tb (IS) 159 He 178578.423 1.0 151792.613333333 117.65 30 150

Ho (IS) 165 He 178290.817 1.5 151670.6 117.55 30 150

Bi (IS) 209 He 1827001.870 1.4 1551684.83333333 117.74 30 150

4/1/2023 6:48 AM

Sample Name 180-151590-c-3-e @10

File Name 112SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:14:17 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 122.978 1.5 203381.907 3000

Be 9 6 No Gas 0.357 1.5 177.333 3600

(B) 10 103 No Gas 266.129 1.4 11340.980 3600

B 11 103 No Gas 252.106 1.5 56811.287 3600

Si 28 45 H2 175.287 3.6 4831.920 10000

Fe 56 45 H2 43815.310 1.0 61703290.880 625000

Se 78 45 H2 5.980 3.1 406.437 2250

(Sn) 118 115 H2 208.493 1.6 393962.480 5400

Na 23 45 He 9445.237 2.7 1116173.113 625000

{Mg} 24 45 He 9196.779 3.1 549017.653 625000

{Mg} 25 45 He 9160.656 2.0 81419.620 625000

Mg 26 45 He 9094.205 2.6 104551.610 625000

Al 27 45 He 12466.215 3.0 285597.687 225000

P 31 45 He 1710.979 11.5 2845.847 15000

K 39 45 He 3453.999 2.0 241557.507 625000

{Ca} 43 45 He 77644.872 4.8 14526.077 625000

Ca 44 45 He 78853.415 2.9 255808.590 625000

Ti 47 45 He 3245.870 2.5 78980.703 6750

V 51 45 He 40.686 3.0 34380.260 11250

Cr 52 45 He 200.883 2.1 213353.040 11250

(Cr) 53 45 He 201.786 3.3 26042.010 11250

Mn 55 103 He 281.481 2.3 161661.653 22050

Co 59 103 He 76.374 2.9 132603.690 6750

Ni 60 103 He 318.466 2.2 148860.050 11250

(Cu) 63 103 He 3819.123 1.7 4949130.777 11250

Cu 65 103 He 3797.355 1.8 2430390.320 11250

Zn 66 103 He 3092.393 1.8 642318.727 11250

(Zn) 68 103 He 3214.785 2.1 495799.233 11250

As 75 103 He 134.626 1.0 18917.690 2250

(Se) 78 103 He 8.375 7.4 170.333 2250

(Se) 82 103 He 5.046 112.5 75.557 2250

Sr 88 103 He 183.605 2.5 146556.030 11250

(Mo) 95 103 He 118.482 1.8 76553.043 6750

Mo 98 103 He 118.109 1.5 127471.823 6750

Ag 107 103 He 17.880 1.3 37095.300 600

(Ag) 109 103 He 17.926 1.9 35751.927 600

4/1/2023 6:48 AM

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 9.851 2.5 3116.680 6750

(Cd) 114 115 He 13.811 0.1 11081.693 6750

Sn 118 115 He 202.857 1.4 144836.893 5400

Sb 121 115 He 50.230 0.8 43843.953 5400

(Sb) 123 115 He 49.861 0.5 34197.320 5400

Ba 137 159 He 1573.564 3.0 512068.657 11250

(Tl) 203 209 He 0.079 31.8 363.340 9000

Tl 205 209 He 0.079 7.0 788.920 9000

[Pb] 206 209 He 422.337 0.4 630143.863 11250

[Pb] 207 209 He 405.556 0.9 525437.980 11250

Pb 208 209 He 409.662 1.0 2451037.520 11250

Th 232 209 He 0.979 6.0 5771.310 4500

U 238 209 He 0.694 2.7 3983.963 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 208131.147 0.5 202714.773333333 102.67 30 150

Sc (IS) 45 No Gas 1318745.217 1.2 1182756.31 111.5 30 150

Rh (IS) 103 No Gas 2443691.057 0.7 2107039.5 115.98 30 150

Sc (IS) 45 H2 360631.133 0.3 318888.686666667 113.09 30 150

Rh (IS) 103 H2 101926.167 0.9 98679.7966666667 103.29 30 150

115In 115 H2 524724.287 0.6 421564.323333333 124.47 30 150

Sc (IS) 45 He 86703.653 1.7 74004.76 117.16 30 150

Rh (IS) 103 He 2113173.943 1.0 1819840.96666667 116.12 30 150

115In 115 He 168017.353 0.7 143763.77 116.87 30 150

Tb (IS) 159 He 178465.887 1.6 151792.613333333 117.57 30 150

Ho (IS) 165 He 179609.423 0.8 151670.6 118.42 30 150

Bi (IS) 209 He 2179818.177 1.0 1551684.83333333 140.48 30 150

Sample Name 180-151590-c-4-e

File Name 113SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:17:56 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

FailISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 1875.705 1.3 3069615.583 3000

Be 9 6 No Gas 3.567 1.5 1517.413 3600

(B) 10 103 No Gas 3775.721 1.6 154315.273 3600 LDR HIGH BORON

B 11 103 No Gas 3620.301 2.6 779766.063 3600 LDR HIGH BORON

Si 28 45 H2 828.612 4.1 21900.573 10000

Fe 56 45 H2 624385.425 2.4 887205049.190 625000

Se 78 45 H2 69.316 3.0 4690.463 2250

(Sn) 118 115 H2 2818.526 2.9 6465520.527 5400

Na 23 45 He 127778.115 2.1 14768779.413 625000

{Mg} 24 45 He 92979.493 3.1 5466333.670 625000

{Mg} 25 45 He 93033.561 3.0 814278.350 625000

Mg 26 45 He 92771.271 4.2 1050135.513 625000

Al 27 45 He 178863.856 4.4 4038246.083 225000

P 31 45 He 20987.471 4.5 32851.847 15000 LDR HIGH

K 39 45 He 41826.707 2.4 2575494.553 625000

{Ca} 43 45 He 855695.036 5.0 157759.517 625000 LDR HIGH

Ca 44 45 He 871809.484 3.9 2786540.720 625000 LDR HIGH

Ti 47 45 He 38268.761 4.5 917793.373 6750 LDR HIGH

V 51 45 He 552.864 2.5 460387.983 11250

Cr 52 45 He 3559.842 4.1 3717086.243 11250

(Cr) 53 45 He 3556.230 4.7 451390.070 11250

Mn 55 103 He 5037.525 3.7 2742098.920 22050

Co 59 103 He 1053.163 3.8 1733588.510 6750

Ni 60 103 He 3792.184 4.1 1680378.407 11250

(Cu) 63 103 He 55013.960 5.2 67636426.203 11250 LDR HIGH

Cu 65 103 He 56317.998 4.3 34200675.307 11250 LDR HIGH

Zn 66 103 He 36585.747 3.6 7207980.823 11250 LDR HIGH

(Zn) 68 103 He 38436.695 2.4 5624696.583 11250 LDR HIGH

As 75 103 He 2246.074 3.8 299299.523 2250

(Se) 78 103 He 117.739 2.3 1274.727 2250

(Se) 82 103 He 78.972 12.1 425.567 2250

Sr 88 103 He 2229.283 4.0 1688105.070 11250

(Mo) 95 103 He 1371.614 4.0 840552.687 6750

Mo 98 103 He 1360.611 3.6 1392853.960 6750

Ag 107 103 He 253.480 3.3 498462.223 600

(Ag) 109 103 He 256.281 3.0 484566.177 600

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 129.600 4.0 38712.863 6750

(Cd) 114 115 He 163.595 2.7 149196.587 6750

Sn 118 115 He 2890.540 3.1 2350611.643 5400

Sb 121 115 He 547.317 2.6 544438.713 5400

(Sb) 123 115 He 551.399 2.5 431029.417 5400

Ba 137 159 He 14536.994 2.8 4927763.333 11250 LDR HIGH

(Tl) 203 209 He 0.283 8.6 2051.283 9000

Tl 205 209 He 0.261 2.8 4421.880 9000

[Pb] 206 209 He 1618.378 2.4 6673074.040 11250

[Pb] 207 209 He 1637.565 1.3 5863377.960 11250

Pb 208 209 He 1600.987 2.2 26472183.947 11250

Th 232 209 He 3.360 1.4 52422.857 4500

U 238 209 He 2.878 2.7 45386.853 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 220541.467 1.1 202714.773333333 108.79 30 150

Sc (IS) 45 No Gas 1352951.230 1.3 1182756.31 114.39 30 150

Rh (IS) 103 No Gas 2462646.683 3.3 2107039.5 116.88 30 150

Sc (IS) 45 H2 364051.853 1.7 318888.686666667 114.16 30 150

Rh (IS) 103 H2 90655.563 2.5 98679.7966666667 91.87 30 150

115In 115 H2 638260.400 1.8 421564.323333333 151.4 30 150 ISTD Failed

Sc (IS) 45 He 85495.483 2.3 74004.76 115.53 30 150

Rh (IS) 103 He 2006330.200 2.2 1819840.96666667 110.25 30 150

115In 115 He 191729.843 1.2 143763.77 133.36 30 150

Tb (IS) 159 He 185872.340 0.8 151792.613333333 122.45 30 150

Ho (IS) 165 He 188737.713 1.8 151670.6 124.44 30 150

Bi (IS) 209 He 6024636.840 0.3 1551684.83333333 388.26 30 150 ISTD Failed

4/1/2023 6:56 AM

Sample Name 180-151590-c-4-e @10

File Name 114SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:21:29 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 229.785 1.5 338809.333 3000

Be 9 6 No Gas 0.431 7.4 190.000 3600

(B) 10 103 No Gas 512.137 1.7 22194.153 3600

B 11 103 No Gas 486.208 1.9 111221.773 3600

Si 28 45 H2 87.802 4.1 2530.230 10000

Fe 56 45 H2 69094.797 0.8 95693891.753 625000

Se 78 45 H2 7.926 1.9 527.850 2250

(Sn) 118 115 H2 350.973 0.1 683079.497 5400

Na 23 45 He 14104.710 1.5 1641364.273 625000

{Mg} 24 45 He 10421.973 1.8 614363.710 625000

{Mg} 25 45 He 10392.658 1.2 91203.467 625000

Mg 26 45 He 10288.374 1.6 116793.763 625000

Al 27 45 He 19840.669 1.4 448878.637 225000

P 31 45 He 2316.010 5.3 3757.157 15000

K 39 45 He 4527.389 0.7 304043.400 625000

{Ca} 43 45 He 94173.477 3.2 17400.313 625000

Ca 44 45 He 95116.711 2.1 304705.093 625000

Ti 47 45 He 4168.023 1.4 100159.370 6750

V 51 45 He 59.458 0.6 49616.957 11250

Cr 52 45 He 384.361 0.6 402627.303 11250

(Cr) 53 45 He 395.524 2.0 50354.097 11250

Mn 55 103 He 520.540 1.0 300670.727 22050

Co 59 103 He 108.642 1.8 189753.123 6750

Ni 60 103 He 402.735 1.3 189390.970 11250

(Cu) 63 103 He 5909.274 0.9 7707077.470 11250

Cu 65 103 He 6190.679 0.3 3987653.173 11250

Zn 66 103 He 4156.678 1.5 868660.713 11250

(Zn) 68 103 He 4281.993 1.5 664493.737 11250

As 75 103 He 233.071 0.9 32948.053 2250

(Se) 78 103 He 12.599 9.1 217.000 2250

(Se) 82 103 He 7.328 42.8 87.777 2250

Sr 88 103 He 228.771 1.7 183751.563 11250

(Mo) 95 103 He 136.569 1.0 88792.793 6750

Mo 98 103 He 135.859 1.7 147531.460 6750

Ag 107 103 He 26.293 1.8 54871.770 600

(Ag) 109 103 He 26.457 1.5 53079.493 600

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 13.844 3.2 4400.693 6750

(Cd) 114 115 He 20.645 0.7 16607.437 6750

Sn 118 115 He 351.092 1.3 251448.523 5400

Sb 121 115 He 67.868 2.2 59445.640 5400

(Sb) 123 115 He 68.535 0.6 47173.753 5400

Ba 137 159 He 1567.671 0.2 520978.977 11250

(Tl) 203 209 He 0.012 145.0 252.227 9000

Tl 205 209 He 0.018 24.3 546.680 9000

[Pb] 206 209 He 463.904 1.6 730896.153 11250

[Pb] 207 209 He 442.347 0.7 605210.320 11250

Pb 208 209 He 446.719 0.4 2822404.230 11250

Th 232 209 He 0.947 1.1 5909.150 4500

U 238 209 He 0.778 0.5 4707.547 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 191871.197 0.6 202714.773333333 94.65 30 150

Sc (IS) 45 No Gas 1314193.160 1.1 1182756.31 111.11 30 150

Rh (IS) 103 No Gas 2548566.473 1.9 2107039.5 120.95 30 150

Sc (IS) 45 H2 354695.913 0.7 318888.686666667 111.23 30 150

Rh (IS) 103 H2 99545.697 1.2 98679.7966666667 100.88 30 150

115In 115 H2 540859.677 1.7 421564.323333333 128.3 30 150

Sc (IS) 45 He 85611.657 1.0 74004.76 115.68 30 150

Rh (IS) 103 He 2126625.400 1.5 1819840.96666667 116.86 30 150

115In 115 He 168680.747 1.0 143763.77 117.33 30 150

Tb (IS) 159 He 182195.197 0.4 151792.613333333 120.03 30 150

Ho (IS) 165 He 181574.930 0.4 151670.6 119.72 30 150

Bi (IS) 209 He 2301855.533 0.1 1551684.83333333 148.35 30 150

Sample Name CCV 5280846

File Name 117_CCV.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:32:28 PMAcq Time

Sample Type CCV

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 200.496 1.7 333739.967 200

Be 9 6 No Gas 206.374 1.1 83534.123 200

(B) 10 103 No Gas 524.253 0.3 22522.423 500

B 11 103 No Gas 506.922 1.4 114900.780 500

Si 28 45 H2 1918.013 0.6 51354.873 2000

Fe 56 45 H2 53448.852 0.4 77557759.140 50000

Se 78 45 H2 207.570 0.3 14330.777 200

(Sn) 118 115 H2 208.251 0.7 399212.520 200

Na 23 45 He 52963.072 1.3 6327118.637 50000

{Mg} 24 45 He 53844.418 0.3 3269751.813 50000

{Mg} 25 45 He 52687.113 0.4 476309.217 50000

Mg 26 45 He 52602.701 0.8 615113.343 50000

Al 27 45 He 50995.663 0.4 1189390.873 50000

P 31 45 He 2555.314 3.1 4260.630 2500

K 39 45 He 53304.719 0.5 3381697.780 50000

{Ca} 43 45 He 52857.591 2.9 10071.253 50000

Ca 44 45 He 53379.397 0.8 176371.443 50000

Ti 47 45 He 207.972 0.9 5154.243 200

V 51 45 He 208.999 0.5 179740.963 200

Cr 52 45 He 205.558 0.1 222262.700 200

(Cr) 53 45 He 207.543 0.6 27272.070 200

Mn 55 103 He 207.460 1.2 120759.023 200

Co 59 103 He 206.082 0.7 362215.090 200

Ni 60 103 He 205.491 0.2 97358.327 200

(Cu) 63 103 He 204.353 1.2 268729.860 200

Cu 65 103 He 206.638 2.3 134187.090 200

Zn 66 103 He 107.882 1.0 23044.963 100

(Zn) 68 103 He 120.816 1.2 19123.803 100 >+\-10%

As 75 103 He 207.523 0.4 29531.727 200

(Se) 78 103 He 199.177 1.8 2244.847 200

(Se) 82 103 He 196.794 12.8 1056.710 200

Sr 88 103 He 204.520 1.5 165368.360 200

(Mo) 95 103 He 213.303 0.2 139575.340 200

Mo 98 103 He 211.265 0.8 230907.193 200

Ag 107 103 He 106.136 1.3 222801.440 100

(Ag) 109 103 He 106.336 0.3 214622.750 100

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 206.963 0.7 65982.293 200

(Cd) 114 115 He 209.617 1.4 166364.453 200

Sn 118 115 He 208.980 0.5 148146.870 200

Sb 121 115 He 203.299 0.8 176038.963 200

(Sb) 123 115 He 205.454 0.7 139800.420 200

Ba 137 159 He 203.334 0.7 67716.390 200

(Tl) 203 209 He 208.862 2.0 327333.980 200

Tl 205 209 He 209.946 0.9 784763.040 200

[Pb] 206 209 He 210.409 1.0 263920.423 200

[Pb] 207 209 He 208.528 1.6 227094.870 200

Pb 208 209 He 206.864 0.8 1040463.657 200

Th 232 209 He 107.514 2.7 501045.083 100

U 238 209 He 104.214 1.7 498763.297 100

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 215395.700 1.2 202714.773333333 106.26 30 150

Sc (IS) 45 No Gas 1351632.220 0.5 1182756.31 114.28 30 150

Rh (IS) 103 No Gas 2527718.920 1.0 2107039.5 119.97 30 150

Sc (IS) 45 H2 371617.650 1.4 318888.686666667 116.54 30 150

Rh (IS) 103 H2 105972.327 1.6 98679.7966666667 107.39 30 150

115In 115 H2 532434.980 3.4 421564.323333333 126.3 30 150

Sc (IS) 45 He 88259.393 0.9 74004.76 119.26 30 150

Rh (IS) 103 He 2140514.913 0.7 1819840.96666667 117.62 30 150

115In 115 He 166835.650 0.2 143763.77 116.05 30 150

Tb (IS) 159 He 182553.170 0.6 151792.613333333 120.26 30 150

Ho (IS) 165 He 183810.757 0.7 151670.6 121.19 30 150

Bi (IS) 209 He 1832229.930 1.9 1551684.83333333 118.08 30 150

Sample Name CCB

File Name 118_CCB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 6:36:07 PMAcq Time

Sample Type CCB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 0.239 121.1 15442.563 5

Be 9 6 No Gas -0.026 N/A 28.667 1

(B) 10 103 No Gas 44.205 9.3 2479.103 80

B 11 103 No Gas 42.534 3.6 12725.433 80

Si 28 45 H2 -4.516 N/A 196.670 500

Fe 56 45 H2 4.323 4.9 21410.137 50

Se 78 45 H2 0.020 307.0 7.587 5

(Sn) 118 115 H2 0.393 1.6 1420.100 5

Na 23 45 He -11.884 N/A 8551.367 500

{Mg} 24 45 He -2.999 N/A 507.790 500

{Mg} 25 45 He -2.167 N/A 78.887 500

Mg 26 45 He -4.236 N/A 83.333 500

Al 27 45 He 7.003 31.5 236.000 30

P 31 45 He -63.685 N/A 43.333 500

K 39 45 He -73.249 N/A 24143.033 500

{Ca} 43 45 He 47.821 92.3 14.443 500

Ca 44 45 He -3.642 N/A 142.223 500

Ti 47 45 He 0.456 3.8 13.333 5

V 51 45 He 0.019 41.4 37.777 1

Cr 52 45 He -0.089 N/A 493.343 2

(Cr) 53 45 He -0.002 N/A 62.223 2

Mn 55 103 He -0.089 N/A 181.113 5

Co 59 103 He -0.009 N/A 134.447 0.5

Ni 60 103 He -0.181 N/A 80.000 1

(Cu) 63 103 He 0.373 24.7 1003.373 2

Cu 65 103 He 0.409 12.8 512.237 2

Zn 66 103 He -0.237 N/A 314.453 15

(Zn) 68 103 He 0.118 18.3 278.893 15

As 75 103 He 0.005 784.8 15.000 1

(Se) 78 103 He -0.259 N/A 80.000 5

(Se) 82 103 He -2.467 N/A 38.890 5

Sr 88 103 He -0.026 N/A 40.000 5

(Mo) 95 103 He 0.094 4.5 108.000 5

Mo 98 103 He 0.111 34.2 194.000 5

Ag 107 103 He 0.113 30.1 288.893 1

(Ag) 109 103 He 0.103 21.4 256.670 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He -0.016 N/A 12.667 1

(Cd) 114 115 He 0.014 112.1 56.667 1

Sn 118 115 He 0.400 34.8 536.680 5

Sb 121 115 He 0.285 4.3 301.117 2

(Sb) 123 115 He 0.254 26.6 211.113 2

Ba 137 159 He 0.173 26.6 69.333 10

(Tl) 203 209 He -0.017 N/A 152.223 1

Tl 205 209 He 0.004 182.5 381.120 1

[Pb] 206 209 He 0.144 31.9 293.337 1

[Pb] 207 209 He 0.120 44.1 211.113 1

Pb 208 209 He 0.128 15.2 1045.577 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 217935.587 0.8 202714.773333333 107.51 30 150

Sc (IS) 45 No Gas 1368088.627 1.1 1182756.31 115.67 30 150

Rh (IS) 103 No Gas 2554135.430 0.8 2107039.5 121.22 30 150

Sc (IS) 45 H2 375812.097 0.8 318888.686666667 117.85 30 150

Rh (IS) 103 H2 109177.820 1.2 98679.7966666667 110.64 30 150

115In 115 H2 531856.153 3.1 421564.323333333 126.16 30 150

Sc (IS) 45 He 88551.157 1.1 74004.76 119.66 30 150

Rh (IS) 103 He 2173838.453 0.6 1819840.96666667 119.45 30 150

115In 115 He 167668.750 0.5 143763.77 116.63 30 150

Tb (IS) 159 He 177715.937 0.5 151792.613333333 117.08 30 150

Ho (IS) 165 He 178126.193 1.2 151670.6 117.44 30 150

Bi (IS) 209 He 1812215.967 0.6 1551684.83333333 116.79 30 150

4/1/2023 6:57 AM

Sample Name ICSA 5280837

File Name 127ICSA.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:09:04 PMAcq Time

Sample Type ICSA

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas -0.357 N/A 13971.123 5

Be 9 6 No Gas -0.051 N/A 18.000 1

(B) 10 103 No Gas 14.595 11.1 1198.943 80

B 11 103 No Gas 14.328 5.5 6292.453 80

Si 28 45 H2 -0.913 N/A 286.670 500

Fe 56 45 H2 106127.468 0.5 152063433.957 50

Se 78 45 H2 0.023 236.4 7.587 5

(Sn) 118 115 H2 0.164 58.9 966.733 5

Na 23 45 He 106102.881 1.7 12531716.447 500

{Mg} 24 45 He 105080.150 2.2 6312906.553 500

{Mg} 25 45 He 104056.515 2.0 930660.307 500

Mg 26 45 He 104844.274 1.5 1212984.880 500

Al 27 45 He 102028.897 1.3 2354533.917 30

K 39 45 He 107168.821 1.1 6698664.733 500

{Ca} 43 45 He 101861.376 1.8 19201.427 500

Ca 44 45 He 104254.220 1.8 340700.907 500

Ti 47 45 He 2077.456 1.6 50927.913 5

V 51 45 He 0.041 39.6 55.553 1

Cr 52 45 He 0.533 8.5 1150.050 2

(Cr) 53 45 He 0.509 46.7 127.780 2

Mn 55 103 He 0.399 8.7 453.343 5

Co 59 103 He 0.298 10.3 661.130 0.5

Ni 60 103 He 0.030 172.9 175.557 1

(Cu) 63 103 He 0.126 27.8 651.133 2

Cu 65 103 He 0.249 36.5 393.340 2

Zn 66 103 He 0.614 19.4 480.010 15

(Zn) 68 103 He 0.641 5.0 350.007 15

As 75 103 He 0.051 77.3 21.000 1

(Se) 78 103 He -0.889 N/A 70.667 5

(Se) 82 103 He -1.342 N/A 43.330 5

Sr 88 103 He 0.713 6.8 625.573 5

(Mo) 95 103 He 2122.466 1.2 1363932.503 5

Mo 98 103 He 2117.684 1.9 2273119.583 5

Ag 107 103 He 0.044 30.1 138.890 1

(Ag) 109 103 He 0.043 4.0 128.890 1

Cd 111 103 He 0.193 24.3 77.667 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

(Cd) 114 115 He 0.164 3.0 177.000 1

Sn 118 115 He 0.187 36.9 385.563 5

Sb 121 115 He 0.413 3.6 413.343 2

(Sb) 123 115 He 0.420 12.5 325.560 2

Ba 137 159 He 2.947 2.7 992.040 10

(Tl) 203 209 He -0.026 N/A 140.000 1

Tl 205 209 He -0.008 N/A 335.563 1

[Pb] 206 209 He 0.237 4.4 408.900 1

[Pb] 207 209 He 0.259 20.7 362.230 1

Pb 208 209 He 0.237 8.4 1593.383 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 210217.493 0.8 202714.773333333 103.7 30 150

Sc (IS) 45 No Gas 1351703.000 0.5 1182756.31 114.28 30 150

Rh (IS) 103 No Gas 2492656.007 1.6 2107039.5 118.3 30 150

Sc (IS) 45 H2 366984.033 1.0 318888.686666667 115.08 30 150

Rh (IS) 103 H2 104569.680 1.1 98679.7966666667 105.97 30 150

115In 115 H2 524251.000 2.4 421564.323333333 124.36 30 150

Sc (IS) 45 He 87332.820 0.5 74004.76 118.01 30 150

Rh (IS) 103 He 2102789.500 0.5 1819840.96666667 115.55 30 150

115In 115 He 168116.987 1.4 143763.77 116.94 30 150

Tb (IS) 159 He 182056.030 1.0 151792.613333333 119.94 30 150

Ho (IS) 165 He 183368.497 2.3 151670.6 120.9 30 150

Bi (IS) 209 He 1817803.887 0.8 1551684.83333333 117.15 30 150

Sample Name ICSAB 5297791

File Name 130ICSB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:20:02 PMAcq Time

Sample Type ICSB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 19.406 1.7 42982.900 20

Be 9 6 No Gas 19.628 1.9 7497.880 20

(B) 10 103 No Gas 57.212 4.6 2895.847 50

B 11 103 No Gas 55.493 2.4 14922.990 50

Si 28 45 H2 465.502 1.4 12692.127 500

Fe 56 45 H2 102678.023 2.6 148857580.750 100000

Se 78 45 H2 49.202 2.8 3398.580 50

Na 23 45 He 104048.100 1.3 12330595.067 100000

{Mg} 24 45 He 101679.779 0.7 6129704.480 100000

{Mg} 25 45 He 101840.210 1.1 913933.503 100000

Mg 26 45 He 100626.403 1.3 1168085.753 100000

Al 27 45 He 98155.259 0.4 2272837.750 100000

P 31 45 He 97723.391 1.1 156346.673 100000

K 39 45 He 104790.742 1.2 6572624.463 100000

{Ca} 43 45 He 100557.291 1.6 19020.070 100000

Ca 44 45 He 101300.440 0.9 332170.620 100000

Ti 47 45 He 2009.170 1.4 49418.503 2000

V 51 45 He 19.938 1.3 17044.400 20

Cr 52 45 He 20.920 2.0 22980.273 20

(Cr) 53 45 He 21.360 5.4 2841.403 20

Mn 55 103 He 20.442 0.5 11849.287 22

Co 59 103 He 20.479 0.4 35359.467 20

Ni 60 103 He 19.854 1.9 9351.937 20

(Cu) 63 103 He 20.751 1.3 27145.350 20

Cu 65 103 He 20.873 2.4 13476.290 20

Zn 66 103 He 22.130 5.6 4906.407 22

(Zn) 68 103 He 24.211 4.0 3951.673 25

As 75 103 He 20.673 4.4 2890.960 20

(Se) 78 103 He 45.330 9.9 561.343 50

(Se) 82 103 He 46.674 6.2 283.340 50

Sr 88 103 He 20.499 0.9 16274.893 20

(Mo) 95 103 He 2078.713 0.9 1330791.000 2000

Mo 98 103 He 2095.597 0.3 2241173.583 2000

Ag 107 103 He 20.371 1.1 41894.177 20

(Ag) 109 103 He 21.012 0.6 41540.007 20

Cd 111 103 He 20.801 2.5 6505.173 20

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

(Cd) 114 115 He 21.823 0.6 17433.430 20

Sn 118 115 He 100.661 1.0 71786.013 100

Sb 121 115 He 20.633 1.7 17989.373 22

(Sb) 123 115 He 21.247 1.6 14550.957 22

Ba 137 159 He 27.749 0.8 9243.093 26

(Tl) 203 209 He 20.277 0.8 31478.373 20

Tl 205 209 He 20.071 0.8 74257.037 20

[Pb] 206 209 He 20.128 1.5 24981.337 20

[Pb] 207 209 He 20.194 0.2 21746.790 20

Pb 208 209 He 20.101 0.5 99991.593 20

Th 232 209 He 20.921 1.6 96330.203 20

U 238 209 He 20.060 0.6 94635.907 20

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 202367.217 0.3 202714.773333333 99.83 30 150

Sc (IS) 45 No Gas 1338438.573 0.2 1182756.31 113.16 30 150

Rh (IS) 103 No Gas 2441606.630 0.6 2107039.5 115.88 30 150

Sc (IS) 45 H2 371315.420 0.3 318888.686666667 116.44 30 150

Rh (IS) 103 H2 102944.587 2.0 98679.7966666667 104.32 30 150

115In 115 H2 530245.953 2.5 421564.323333333 125.78 30 150

Sc (IS) 45 He 87628.003 1.0 74004.76 118.41 30 150

Rh (IS) 103 He 2094935.473 0.9 1819840.96666667 115.12 30 150

115In 115 He 167539.513 1.3 143763.77 116.54 30 150

Tb (IS) 159 He 182367.177 1.7 151792.613333333 120.14 30 150

Ho (IS) 165 He 179688.363 1.6 151670.6 118.47 30 150

Bi (IS) 209 He 1805281.943 0.6 1551684.83333333 116.34 30 150

Sample Name CCVL 5280780

File Name 131SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:23:40 PMAcq Time

Sample Type CRI

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 4.612 3.5 20991.240 5

Be 9 6 No Gas 0.989 3.0 414.677 1

(B) 10 103 No Gas 86.490 3.9 4127.257 80

B 11 103 No Gas 82.372 0.7 20891.213 80

Si 28 45 H2 485.334 2.6 13175.867 500

Fe 56 45 H2 55.928 0.8 95653.063 50

Se 78 45 H2 5.157 2.0 360.513 5

(Sn) 118 115 H2 5.392 6.2 10964.497 5

Na 23 45 He 536.942 1.4 73462.740 500

{Mg} 24 45 He 519.861 0.5 32024.307 500

{Mg} 25 45 He 526.554 2.5 4823.017 500

Mg 26 45 He 515.064 0.2 6111.283 500

Al 27 45 He 33.203 2.0 840.027 30

P 31 45 He 461.927 6.3 883.363 500

K 39 45 He 466.342 2.4 57601.680 500

{Ca} 43 45 He 641.584 14.7 126.667 500

Ca 44 45 He 550.348 0.6 1956.810 500

Ti 47 45 He 5.787 2.9 144.333 5

V 51 45 He 1.058 3.7 924.477 1

Cr 52 45 He 1.997 1.9 2721.377 2

(Cr) 53 45 He 2.026 4.7 325.560 2

Mn 55 103 He 4.986 6.0 3133.683 5

Co 59 103 He 0.469 2.7 975.590 0.5

Ni 60 103 He 0.786 11.5 537.790 1

(Cu) 63 103 He 1.851 2.7 2934.757 2

Cu 65 103 He 1.981 5.3 1526.753 2

Zn 66 103 He 5.282 4.2 1473.413 5

(Zn) 68 103 He 5.772 7.0 1160.053 5

As 75 103 He 0.991 12.8 155.333 1

(Se) 78 103 He 4.646 8.5 132.333 5

(Se) 82 103 He 2.197 229.9 62.223 5 >+\-30%

Sr 88 103 He 5.064 3.2 4162.853 5

(Mo) 95 103 He 5.931 3.7 3933.887 5

Mo 98 103 He 5.743 1.1 6359.433 5

Ag 107 103 He 1.069 2.7 2296.870 1

(Ag) 109 103 He 1.132 3.7 2334.650 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 0.987 1.9 333.000 1

(Cd) 114 115 He 1.102 3.4 907.030 1

Sn 118 115 He 5.171 3.0 3853.880 5

Sb 121 115 He 2.059 2.7 1809.017 2

(Sb) 123 115 He 2.053 4.1 1413.413 2

Ba 137 159 He 10.034 1.7 3253.053 10

(Tl) 203 209 He 0.989 5.5 1672.337 1

Tl 205 209 He 0.998 4.7 3956.170 1

[Pb] 206 209 He 1.072 4.7 1410.083 1

[Pb] 207 209 He 1.108 1.2 1245.623 1

Pb 208 209 He 1.074 1.9 5612.720 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 203494.863 1.0 202714.773333333 100.38 30 150

Sc (IS) 45 No Gas 1318730.867 0.8 1182756.31 111.5 30 150

Rh (IS) 103 No Gas 2470980.117 1.0 2107039.5 117.27 30 150

Sc (IS) 45 H2 370102.130 0.5 318888.686666667 116.06 30 150

Rh (IS) 103 H2 104695.403 1.3 98679.7966666667 106.1 30 150

115In 115 H2 531277.360 1.5 421564.323333333 126.03 30 150

Sc (IS) 45 He 87640.180 0.7 74004.76 118.43 30 150

Rh (IS) 103 He 2145490.817 0.6 1819840.96666667 117.89 30 150

115In 115 He 164435.897 0.3 143763.77 114.38 30 150

Tb (IS) 159 He 177012.120 0.6 151792.613333333 116.61 30 150

Ho (IS) 165 He 176083.163 0.8 151670.6 116.1 30 150

Bi (IS) 209 He 1769976.560 1.2 1551684.83333333 114.07 30 150

4/1/2023 6:58 AM

Sample Name CCV 5280846

File Name 133_CCV.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:31:01 PMAcq Time

Sample Type CCV

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 198.806 0.7 324125.013 200

Be 9 6 No Gas 205.015 0.5 81243.340 200

(B) 10 103 No Gas 494.935 1.4 21408.590 500

B 11 103 No Gas 477.712 0.8 109037.533 500

Si 28 45 H2 1910.711 2.9 52841.270 2000

Fe 56 45 H2 52515.468 0.3 78709759.097 50000

Se 78 45 H2 205.903 0.4 14682.137 200

(Sn) 118 115 H2 203.577 0.6 397565.293 200

Na 23 45 He 52928.383 1.7 6425985.577 50000

{Mg} 24 45 He 53495.494 0.9 3301832.717 50000

{Mg} 25 45 He 52627.327 1.2 483517.760 50000

Mg 26 45 He 52315.654 1.8 621718.743 50000

Al 27 45 He 50878.280 0.7 1206059.000 50000

P 31 45 He 2472.668 2.4 4193.947 2500

K 39 45 He 53770.896 1.2 3466691.320 50000

{Ca} 43 45 He 54398.548 1.5 10534.917 50000

Ca 44 45 He 53603.853 0.7 180020.237 50000

Ti 47 45 He 210.820 1.8 5309.963 200

V 51 45 He 205.125 1.0 179292.340 200

Cr 52 45 He 205.245 1.0 225557.710 200

(Cr) 53 45 He 208.210 2.7 27803.077 200

Mn 55 103 He 204.646 0.9 121106.473 200

Co 59 103 He 203.284 0.8 363247.287 200

Ni 60 103 He 202.046 0.5 97317.047 200

(Cu) 63 103 He 200.143 0.4 267581.830 200

Cu 65 103 He 201.018 0.8 132727.263 200

Zn 66 103 He 105.485 1.3 22917.013 100

(Zn) 68 103 He 119.199 1.2 19182.733 100 >+\-10%

As 75 103 He 203.953 0.3 29506.347 200

(Se) 78 103 He 203.675 3.0 2331.860 200

(Se) 82 103 He 212.491 5.2 1155.610 200

Sr 88 103 He 204.538 1.0 168133.667 200

(Mo) 95 103 He 209.295 0.8 139230.407 200

Mo 98 103 He 208.829 0.9 232037.300 200

Ag 107 103 He 103.890 0.7 221716.600 100

(Ag) 109 103 He 104.901 1.1 215244.670 100

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He 205.358 0.2 66559.737 200

(Cd) 114 115 He 205.688 1.0 166296.713 200

Sn 118 115 He 204.062 0.6 147373.103 200

Sb 121 115 He 202.167 0.7 178337.443 200

(Sb) 123 115 He 202.479 1.5 140347.013 200

Ba 137 159 He 201.427 1.4 67670.897 200

(Tl) 203 209 He 209.903 0.8 329166.230 200

Tl 205 209 He 208.573 0.3 780015.160 200

[Pb] 206 209 He 206.846 1.7 259542.873 200

[Pb] 207 209 He 207.363 1.4 225945.593 200

Pb 208 209 He 207.076 0.5 1042015.543 200

Th 232 209 He 104.177 2.3 485802.617 100

U 238 209 He 104.478 2.0 500255.050 100

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 210863.967 0.2 202714.773333333 104.02 30 150

Sc (IS) 45 No Gas 1372078.990 2.2 1182756.31 116.01 30 150

Rh (IS) 103 No Gas 2541005.797 1.1 2107039.5 120.6 30 150

Sc (IS) 45 H2 383819.757 0.9 318888.686666667 120.36 30 150

Rh (IS) 103 H2 109551.790 1.1 98679.7966666667 111.02 30 150

115In 115 H2 542270.083 2.2 421564.323333333 128.63 30 150

Sc (IS) 45 He 89707.163 1.3 74004.76 121.22 30 150

Rh (IS) 103 He 2176052.137 0.6 1819840.96666667 119.57 30 150

115In 115 He 169965.497 1.5 143763.77 118.23 30 150

Tb (IS) 159 He 184153.560 0.7 151792.613333333 121.32 30 150

Ho (IS) 165 He 183327.870 0.5 151670.6 120.87 30 150

Bi (IS) 209 He 1832926.733 1.1 1551684.83333333 118.12 30 150

Sample Name CCB

File Name 134_CCB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:34:39 PMAcq Time

Sample Type CCB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas -0.165 N/A 13977.147 5

Be 9 6 No Gas -0.050 N/A 18.000 1

(B) 10 103 No Gas 27.742 5.1 1734.557 80

B 11 103 No Gas 26.594 4.8 8916.000 80

Si 28 45 H2 -5.005 N/A 183.337 500

Fe 56 45 H2 0.610 47.8 15904.260 50

Se 78 45 H2 -0.056 N/A 2.253 5

(Sn) 118 115 H2 0.307 9.4 1236.753 5

Na 23 45 He 0.426 421.9 10071.213 500

{Mg} 24 45 He -8.460 N/A 175.557 500

{Mg} 25 45 He -8.056 N/A 25.557 500

Mg 26 45 He -8.982 N/A 27.777 500

Al 27 45 He 0.108 234.6 74.667 30

P 31 45 He -63.115 N/A 44.443 500

K 39 45 He -72.415 N/A 24306.700 500

{Ca} 43 45 He 7.081 429.6 6.663 500

Ca 44 45 He -14.194 N/A 107.777 500

Ti 47 45 He 0.080 50.6 4.000 5

V 51 45 He -0.004 N/A 17.777 1

Cr 52 45 He -0.105 N/A 477.790 2

(Cr) 53 45 He -0.071 N/A 53.337 2

Mn 55 103 He -0.145 N/A 145.560 5

Co 59 103 He -0.026 N/A 102.223 0.5

Ni 60 103 He -0.270 N/A 36.667 1

(Cu) 63 103 He -0.133 N/A 322.230 2

Cu 65 103 He -0.125 N/A 157.780 2

Zn 66 103 He -0.446 N/A 264.450 15

(Zn) 68 103 He -0.377 N/A 196.673 15

As 75 103 He -0.062 N/A 5.333 1

(Se) 78 103 He 0.227 429.3 83.667 5

(Se) 82 103 He -3.865 N/A 31.110 5

Sr 88 103 He -0.055 N/A 15.553 5

(Mo) 95 103 He 0.123 2.9 124.667 5

Mo 98 103 He 0.124 13.0 204.667 5

Ag 107 103 He 0.091 14.8 238.890 1

(Ag) 109 103 He 0.106 18.8 257.783 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 103 He -0.028 N/A 8.667 1

(Cd) 114 115 He -0.028 N/A 24.000 1

Sn 118 115 He 0.270 27.6 446.677 5

Sb 121 115 He 0.347 2.7 357.787 2

(Sb) 123 115 He 0.278 17.0 228.893 2

Ba 137 159 He -0.006 N/A 11.333 10

(Tl) 203 209 He 0.008 151.9 186.667 1

Tl 205 209 He 0.031 52.3 467.790 1

[Pb] 206 209 He -0.011 N/A 98.890 1

[Pb] 207 209 He 0.013 142.9 93.333 1

Pb 208 209 He 0.013 94.2 461.117 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 205918.747 1.0 202714.773333333 101.58 30 150

Sc (IS) 45 No Gas 1332085.500 1.4 1182756.31 112.63 30 150

Rh (IS) 103 No Gas 2481998.087 2.2 2107039.5 117.8 30 150

Sc (IS) 45 H2 374535.747 2.0 318888.686666667 117.45 30 150

Rh (IS) 103 H2 108238.790 2.5 98679.7966666667 109.69 30 150

115In 115 H2 524494.823 4.2 421564.323333333 124.42 30 150

Sc (IS) 45 He 88964.763 0.7 74004.76 120.21 30 150

Rh (IS) 103 He 2132995.537 1.2 1819840.96666667 117.21 30 150

115In 115 He 168872.203 1.3 143763.77 117.47 30 150

Tb (IS) 159 He 175965.760 1.2 151792.613333333 115.93 30 150

Ho (IS) 165 He 176217.877 1.1 151670.6 116.18 30 150

Bi (IS) 209 He 1772725.033 2.0 1551684.83333333 114.25 30 150

Sample Name HIGH A 5272196

File Name 135SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:38:18 PMAcq Time

Sample Type QC1

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Fe 56 45 H2 602994.981 0.3 933353847.357 625000

(Sn) 118 115 H2 5502.525 1.0 9843832.560 5400

Na 23 45 He 630568.371 3.8 78370776.883 625000

{Mg} 24 45 He 586019.173 2.3 37076971.860 625000

{Mg} 25 45 He 593578.398 4.0 5589489.917 625000

Mg 26 45 He 580662.980 2.2 7074635.830 625000

Al 27 45 He 219581.478 2.5 5336674.167 225000

P 31 45 He 14108.877 2.3 23825.770 15000

K 39 45 He 642060.685 2.3 42116333.883 625000

{Ca} 43 45 He 608185.304 3.3 120697.863 625000

Ca 44 45 He 619264.757 2.8 2130455.057 625000

Ti 47 45 He 6614.119 2.7 170748.030 6750

(Mo) 95 103 He 7344.689 2.4 4565895.833 6750

Mo 98 103 He 7078.691 3.3 7349876.500 6750

Sn 118 115 He 5761.538 1.7 3796748.737 5400

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 190461.587 1.1 202714.773333333 93.96 30 150

Sc (IS) 45 No Gas 1354595.863 0.3 1182756.31 114.53 30 150

Rh (IS) 103 No Gas 2291367.150 0.3 2107039.5 108.75 30 150

Sc (IS) 45 H2 396460.270 0.7 318888.686666667 124.33 30 150

Rh (IS) 103 H2 107928.723 0.9 98679.7966666667 109.37 30 150

115In 115 H2 497653.643 1.2 421564.323333333 118.05 30 150

Sc (IS) 45 He 91998.897 2.0 74004.76 124.31 30 150

Rh (IS) 103 He 2034754.850 1.7 1819840.96666667 111.81 30 150

115In 115 He 155369.413 1.8 143763.77 108.07 30 150

Tb (IS) 159 He 179123.790 1.3 151792.613333333 118.01 30 150

Ho (IS) 165 He 177293.547 1.4 151670.6 116.89 30 150

Bi (IS) 209 He 1643868.370 1.3 1551684.83333333 105.94 30 150

4/1/2023 6:59 AM

Sample Name HIGH B 5272197

File Name 136SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:41:52 PMAcq Time

Sample Type QC2

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Be 9 6 No Gas 3769.514 2.3 1495356.540 3600

(B) 10 103 No Gas 3544.092 2.6 151191.163 3600

B 11 103 No Gas 3380.361 1.6 760232.537 3600

Si 28 45 H2 9222.951 1.5 261907.913 10000

Se 78 45 H2 2366.051 2.1 174018.287 2250

V 51 45 He 11096.672 0.7 9809414.887 11250

Cr 52 45 He 10729.954 1.8 11896203.140 11250

(Cr) 53 45 He 11253.955 1.0 1516828.340 11250

Mn 55 103 He 19846.191 1.3 12011039.247 22050

Co 59 103 He 6736.926 1.6 12329132.287 6750

Ni 60 103 He 11102.058 1.6 5469894.503 11250

(Cu) 63 103 He 11225.407 2.2 15348610.503 11250

Cu 65 103 He 11335.892 2.8 7654799.973 11250

Zn 66 103 He 12223.200 1.6 2677787.740 11250

(Zn) 68 103 He 12956.518 1.2 2107806.027 11250 QC2 Main CR1 Failed

As 75 103 He 2242.211 2.0 332215.813 2250

(Se) 78 103 He 2234.773 1.6 25365.240 2250

(Se) 82 103 He 2328.626 2.2 12446.557 2250

Sr 88 103 He 10484.354 1.0 8828122.703 11250

Cd 111 103 He 6976.485 1.6 2316243.667 6750

(Cd) 114 115 He 6925.958 2.4 5728741.500 6750

Sb 121 115 He 5646.156 1.9 5095230.217 5400

(Sb) 123 115 He 5690.789 1.9 4035812.477 5400

Ba 137 159 He 10996.438 1.4 3715207.083 11250

(Tl) 203 209 He 8643.872 1.6 13816194.173 9000

Tl 205 209 He 8664.380 1.6 33030055.353 9000

[Pb] 206 209 He 11433.295 1.6 14626127.197 11250

[Pb] 207 209 He 10784.245 1.6 11980071.747 11250

Pb 208 209 He 11069.479 1.8 56785446.633 11250

Th 232 209 He 4548.666 1.0 21621685.810 4500

U 238 209 He 4398.673 1.3 21481034.703 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 211218.470 1.2 202714.773333333 104.19 30 150

Sc (IS) 45 No Gas 1388431.073 1.9 1182756.31 117.39 30 150

Rh (IS) 103 No Gas 2570148.660 3.0 2107039.5 121.98 30 150

Sc (IS) 45 H2 396065.133 0.8 318888.686666667 124.2 30 150

Rh (IS) 103 H2 114417.873 1.9 98679.7966666667 115.95 30 150

115In 115 H2 561983.317 1.4 421564.323333333 133.31 30 150

Sc (IS) 45 He 90732.193 0.6 74004.76 122.6 30 150

Rh (IS) 103 He 2229712.760 0.4 1819840.96666667 122.52 30 150

115In 115 He 173943.213 1.2 143763.77 120.99 30 150

Tb (IS) 159 He 185233.910 0.5 151792.613333333 122.03 30 150

Ho (IS) 165 He 183323.493 0.6 151670.6 120.87 30 150

Bi (IS) 209 He 1869366.243 0.6 1551684.83333333 120.47 30 150

Sample Name HIGH C 5272198

File Name 140SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30331A.b

3/31/2023 7:56:17 PMAcq Time

Sample Type QC3

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 951.590 1.2 1658721.460 1000

Ag 107 103 He 650.950 1.9 1342598.173 600

(Ag) 109 103 He 660.945 1.3 1310770.087 600

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 233769.140 0.7 202714.773333333 115.32 30 150

Sc (IS) 45 No Gas 1335023.887 2.0 1182756.31 112.87 30 150

Rh (IS) 103 No Gas 2506895.430 1.8 2107039.5 118.98 30 150

Sc (IS) 45 H2 369555.713 1.8 318888.686666667 115.89 30 150

Rh (IS) 103 H2 106636.437 2.1 98679.7966666667 108.06 30 150

115In 115 H2 527728.770 1.4 421564.323333333 125.18 30 150

Sc (IS) 45 He 87132.773 0.5 74004.76 117.74 30 150

Rh (IS) 103 He 2103724.640 1.0 1819840.96666667 115.6 30 150

115In 115 He 165187.537 0.1 143763.77 114.9 30 150

Tb (IS) 159 He 175214.380 1.4 151792.613333333 115.43 30 150

Ho (IS) 165 He 174396.623 1.0 151670.6 114.98 30 150

Bi (IS) 209 He 1808806.803 1.5 1551684.83333333 116.57 30 150

4/26/2023 12:39 PM

Sample Name METHOD:6020A,6020B,200.8

File Name 009_CCB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30424A.b

4/24/2023 10:27:51 AMAcq Time

Sample Type CCB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName ---

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

PDF processed with CutePDF evaluation edition www.CutePDF.comPDF processed with CutePDF evaluation edition www.CutePDF.com

4/26/2023 12:40 PM

Sample Name STD1 5260745

File Name 010CALB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30424A.b

4/24/2023 10:31:31 AMAcq Time

Sample Type CalBlk

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 010CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 6 No Gas 0.000 N/A 19588.657 1000

Be 9 45 No Gas 0.000 N/A 50.000 1000

(B) 10 45 No Gas 0.000 N/A 1458.970 1000

B 11 45 No Gas 0.000 N/A 7091.703 1000

Si 28 45 H2 0.000 N/A 406.673 1000

Fe 56 115 H2 0.000 N/A 7695.393 1000

Se 78 45 H2 0.000 N/A 4.920 1000

(Sn) 118 115 H2 0.000 N/A 633.373 1000

Na 23 45 He 0.000 N/A 15622.643 1000

{Mg} 24 45 He 0.000 N/A 314.450 1000

{Mg} 25 45 He 0.000 N/A 30.000 1000

Mg 26 45 He 0.000 N/A 61.110 1000

Al 27 45 He 0.000 N/A 142.667 1000

P 31 45 He 0.000 N/A 302.227 1000

K 39 45 He 0.000 N/A 29648.573 1000

{Ca} 43 45 He 0.000 N/A 6.670 1000

Ca 44 45 He 0.000 N/A 185.557 1000

Ti 47 45 He 0.000 N/A 3.000 1000

V 51 45 He 0.000 N/A 30.000 1000

Cr 52 45 He 0.000 N/A 574.457 1000

(Cr) 53 45 He 0.000 N/A 91.113 1000

Mn 55 45 He 0.000 N/A 123.333 1000

Co 59 103 He 0.000 N/A 100.000 1000

Ni 60 45 He 0.000 N/A 66.670 1000

(Cu) 63 45 He 0.000 N/A 416.677 1000

Cu 65 45 He 0.000 N/A 184.447 1000

Zn 66 103 He 0.000 N/A 277.780 1000

(Zn) 68 103 He 0.000 N/A 202.227 1000

As 75 103 He 0.000 N/A 16.667 1000

(Se) 78 103 He 0.000 N/A 73.333 1000

(Se) 82 103 He 0.000 N/A 34.443 1000

Sr 88 115 He 0.000 N/A 25.553 1000

(Mo) 95 103 He 0.000 N/A 40.000 1000

Mo 98 45 He 0.000 N/A 65.333 1000

Ag 107 103 He 0.000 N/A 52.220 1000

(Ag) 109 103 He 0.000 N/A 57.777 1000

Name Mass ISTD…