Testing_Parameters_W9128F19Q0022.xlsx

XLSX spreadsheet 27 KB Posted Apr 11, 2019

Attached to: Lab Analysis Water Quality Monitoring
Solicitation number: W9128F19Q0022
Issued by: Department of the Army Corps of Engineers Engineering District Omaha

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Testing Parameters W9128F19Q0022 to be used in facilitate submission requirements in solicitation

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Questions_and_answers_for_W9128F19Q0022.docx	DOCX document	Apr 24, 2019
Bid_Sheet_W9128F19Q0022.xlsx	XLSX spreadsheet	Apr 11, 2019
W9128F19Q0022.docx	DOCX document	Apr 10, 2019

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Attachment 1

Physicochemical Water Parameters for Laboratory Analysis

Parameter Units Suggested Method Required Detection Limit Preservation Holding Time Quoter Method Quoter Detection Limit Subcontracted Laboratory

PHYSICAL AND AGGREGATE PROPERTIES
Alkalinity, Total (as CaCO3)	mg/l	SM2320B	6.3	Cool 6oC	14 days
Sediment, Total Suspended	mg/l	ASTMD3977	4	Cool 6oC	7 days
Solids, Total Dissolved	mg/l	SM2540C	10	Cool 6oC	7 days
Solids, Total Suspended	mg/l	SM2540D	4	Cool 6oC	7 days
Turbidity	NTU	SM2130B	0.14	Cool 6oC	2 days
INORGANIC NONMETALLIC
Anions:
Chloride, Dissolved	mg/l	SM4500-CLE	2	Cool 6oC	28 days
Sulfate, Dissolved	mg/l	EPA 300	2.3	Cool 6oC	28 days
Nutrients:
Nitrogen, Ammonia, Total (as N)	mg/l	SM4500G	0.08	H2SO4 /Cool 6oC	28 days
Nitrogen, Kjeldahl, Total (as N)	mg/l	EPA 351.2	0.162	H2SO4/Cool 6oC	28 days
Nitrogen, Nitrite + Nitrate, Total (as N)	mg/l	EPA 353.2	0.066	H2SO4/Cool 6oC	28 days
Phosphorus, Total	mg/l	SM4500PF	0.02	H2SO4/Cool 6oC	28 days
Phosphorus, Total Dissolved	mg/l	SM4500PF	0.02	H2SO4/Cool 6oC	28 days
Orthophosphate Phosphorus, Dissolved	mg/l	SM4500PG	0.02	Cool 6oC	2 days
Other:
Silica, Dissolved (as SiO2)	mg/l	EPA 200.7	0.02	Cool 6oC	28 days
Silica, Total (as SiO2)	mg/l	EPA 200.7	0.02	Cool 6oC	28 days
THMs, Dissolved and Total*	ug/l	EPA 524.2	1	HCl /Cool 6oC	14 days
THM Formation Potential, Dissolved and Total	ug/l	EPA 524.2	4	Cool 6oC	7 days
AGGREGATE ORGANIC CONSTITUENTS
Carbon, Dissolved Organic	mg/l	SM5310B	0.37	H2SO4/Cool 6oC	28 days
Carbon, Total Organic	mg/l	SM5310B	0.37	H2SO4/Cool 6oC	28 days
Carbonaceous Biochemical Oxygen Demand	mg/l	SM5210B	0.999	Cool 6oC	7 days
Chemical Oxygen Demand	mg/l	SM5220D	3.2	H2SO4/Cool 6oC	28 days
Colorized Dissolved Organic Matter	ug/l	Fluorometry	10	Cool 6oC	7 days
Hexane Extractable material	mg/l	EPA 1664B	1.35	H2SO4/Cool 6oC	28 days
METALS
Dissolved and Total Metals Scan
Aluminum	ug/l	EPA 200.7	39	HNO3	6 months
Antimony	ug/l	EPA 200.8	0.028	HNO3	6 months
Arsenic	ug/l	EPA 200.8	0.008	HNO3	6 months
Barium	ug/l	EPA 200.7	1.17	HNO3	6 months
Beryllium	ug/l	EPA 200.7	1	HNO3	6 months
Cadmium	ug/l	EPA 200.8	0.007	HNO3	6 months
Calcium	mg/l	EPA 200.7	0.05	HNO3	6 months
Chromium	ug/l	EPA 200.7	3.54	HNO3	6 months
Copper	ug/l	EPA 200.7	5.72	HNO3	6 months
Hardness	mg/l	SM2340B	1	HNO3	6 months
Iron	ug/l	EPA 200.7	13.54	HNO3	6 months
Lead	ug/l	EPA 200.8	0.008	HNO3	6 months
Magnesium	mg/l	EPA 200.7	0.05	HNO3	6 months
Manganese	ug/l	EPA 200.7	2.69	HNO3	6 months
Mercury	ug/l	EPA 245.1	0.002	HNO3	6 months
Nickel	ug/l	EPA 200.7	7.8	HNO3	6 months
Selenium	ug/l	EPA 200.8	0.06	HNO3	6 months
Silver	ug/l	EPA 200.8	0.0054	HNO3	6 months
Sodium	mg/l	EPA 200.7	0.013	HNO3	6 months
Thallium	ug/l	EPA 200.8	0.003	HNO3	6 months
Zinc	ug/l	EPA 200.7	5.92	HNO3	6 months
PESTICIDES
Atrazine	ug/l	ELISA**	0.1	Cool 6oC	7 days
Glyphosate	ug/l	EPA 547	6	Sodium Thiosulfate/ Cool 6oC	14 days
AMPA	ug/l	EPA 547	6	Sodium Thiosulfate/ Cool 6oC	14 days
Imazapyr	ug/l	EEA South Bend Method L304	0.2	Oxalic Acid/Anhydrous Sodium Sulfite/Cool 6oC	14 days
Metolachlor	ug/l	ELISA**	0.1	Cool 6oC	7 days
Total Pesticides Scan
Acetochlor	ug/l	EPA 507	0.08	Cool 6oC	7 days
Alachlor	ug/l	EPA 507	0.09	Cool 6oC	7 days
Ametryn	ug/l	EPA 507	0.15	Cool 6oC	7 days
Atrazine	ug/l	EPA 507	0.1	Cool 6oC	7 days
Benfluralin	ug/l	EPA 507	0.08	Cool 6oC	7 days
Bromacil	ug/l	EPA 507	0.14	Cool 6oC	7 days
Butachlor	ug/l	EPA 507	0.09	Cool 6oC	7 days
Butylate	ug/l	EPA 507	0.09	Cool 6oC	7 days
Chlorpyrifos	ug/l	EPA 507	0.06	Cool 6oC	7 days
Cyanazine	ug/l	EPA 507	0.13	Cool 6oC	7 days
Deisopropylatrazine	ug/l	EPA 507	0.04	Cool 6oC	7 days
Desethylatrazine	ug/l	EPA 507	0.1	Cool 6oC	7 days
Dimethenamid	ug/l	EPA 507	0.09	Cool 6oC	7 days
EPTC	ug/l	EPA 507	0.12	Cool 6oC	7 days
Ethalfluralin	ug/l	EPA 507	0.15	Cool 6oC	7 days
Fonofos	ug/l	EPA 507	0.1	Cool 6oC	7 days
Hexazinone	ug/l	EPA 507	0.13	Cool 6oC	7 days
Isophenphos	ug/l	EPA 507	0.05	Cool 6oC	7 days
Metolachlor	ug/l	EPA 507	0.11	Cool 6oC	7 days
Metribuzin	ug/l	EPA 507	0.09	Cool 6oC	7 days
Oxadiazon	ug/l	EPA 507	0.12	Cool 6oC	7 days
Pendimethalin	ug/l	EPA 507	0.11	Cool 6oC	7 days
Phorate	ug/l	EPA 507	0.07	Cool 6oC	7 days
Prometon	ug/l	EPA 507	0.11	Cool 6oC	7 days
Prometryn	ug/l	EPA 507	0.06	Cool 6oC	7 days
Propachlor	ug/l	EPA 507	0.08	Cool 6oC	7 days
Propazine	ug/l	EPA 507	0.11	Cool 6oC	7 days
Simazine	ug/l	EPA 507	0.13	Cool 6oC	7 days
Terbufos	ug/l	EPA 507	0.09	Cool 6oC	7 days
Triallate	ug/l	EPA 507	0.08	Cool 6oC	7 days
Trifluralin	ug/l	EPA 507	0.08	Cool 6oC	7 days
PETROLEUM COMPOUNDS
Diesel Range Organics	mg/l	DRO	0.04	Cool 6oC	7 days
OA1 or Equivalent
Benzene	ug/l	OA1	0.339	H2SO4/Cool 6oC	14 days
Ethylbenzene	ug/l	OA1	0.309	H2SO4/Cool 6oC	14 days
Methyl tert-Butyl Ether	ug/l	OA1	0.466	H2SO4/Cool 6oC	14 days
Naphthalene	ug/l	OA1	0.631	H2SO4/Cool 6oC	14 days
n-Hexane	ug/l	OA1	0.492	H2SO4/Cool 6oC	14 days
Toluene	ug/l	OA1	0.423	H2SO4/Cool 6oC	14 days
Total Purgeable Hydrocarbons	ug/l	OA1	3.34	H2SO4/Cool 6oC	14 days
Total Xylenes	ug/l	OA1	0.627	H2SO4/Cool 6oC	14 days
* Bromoform, Bromodichloromethane, Chlorodibromomethane, and Chloroform.
** Strategic Diagnostics, Inc. RapidAssay.

Attachment 2

Bacteriological and Biological Parameters for Laboratory Analysis

Parameter Units Suggested Method Required Detection Limit Preservation Holding Time Quoter Method Quoter Detection Limit Subcontracted Laboratory

Bacteriological Parameters:
Fecal Coliform	#/100 ml	SM9222D	1	Cool 6oC	8 hours
E. coli	#/100 ml	SM9222B	1	Cool 6oC	8 hours
Biological Parameters:
Chlorophyll a, Corrected	ug/l	SM10200H2	1	Field Filtered/Cool 6oC	28 days
Microcystins, Total	ug/l	ELISA*	0.1	Cool 6oC	7 days
Phytoplankton	**	**	-----	Lugol’s Solution/Cool 6oC	6 months
Zooplankton	***	***	-----	Lugol’s Solution/Cool 6oC	6 months
Zebra Mussel Veligers	****	****	> 60um	Lugol’s Solution/Cool 6oC	6 months
* Strategic Diagnostics, Inc. EnviroGard Microcystins QuantiTube Test.
** Phytoplankton to be identified to the lowest practical taxa level (i.e., species) and biovolume quantified.
*** Zooplankton to be identified to the lowest practical taxa level (i.e. species) and biomass quantified.
**** Relative abundance of Zebra Mussel veligers > 60 um.

Attachment 3

Sediment Parameters for Laboratory Analysis

Parameter Units Suggested Method Required Detection Limit Preservation Holding Time Quoter Method Quoter Detection Limit Subcontracted Laboratory

Physical and Aggregate Properties
Particle Size	-----	Sieve	0.001 mm	None	ASAP1
Alkalinity, Total	mg/kg	EPA 310.1	10	None	ASAP1
Percent Solids	%	SM2540G	0.01	None	ASAP1
pH	S.U.	EPA 9045	0.1	None	ASAP1
Nutrients
Ammonia, Total as N	mg/kg	SM4500NH3G	0.086	None	ASAP1
Kjeldahl Nitrogen, Total as N	mg/kg	PAI-DK 01	2.81	None	ASAP1
Nitrate/Nitrite, Total as N	mg/kg	EPA 353.2	0.02	None	ASAP1
Phosphorus, Total	mg/kg	EPA 6010B	0.02	None	ASAP1
Aggregate Organic Constituents
Total Organic Carbon	mg/kg	ASTM D5373	0.1 % dry wt	None	ASAP1
Metals Scan (Total)
Aluminum	mg/kg	EPA 6010B	15	None	ASAP1
Antimony	mg/kg	EPA 6010B	10	None	ASAP1
Arsenic	mg/kg	EPA 6010B	10	None	ASAP1
Beryllium	mg/kg	EPA 6010B	0.5	None	ASAP1
Cadmium	mg/kg	EPA 6010B	0.2	None	ASAP1
Calcium	mg/kg	EPA 6010B	15	None	ASAP1
Chromium	mg/kg	EPA 6010B	1	None	ASAP1
Copper	mg/kg	EPA 6010B	1	None	ASAP1
Cyanide	mg/kg	EPA 6010B	1	None	ASAP1
Iron	mg/kg	EPA 6010B	15	None	ASAP1
Lead	mg/kg	EPA 6010B	15	None	ASAP1
Magnesium	mg/kg	EPA 6010B	5	None	ASAP1
Manganese	mg/kg	EPA 6010B	1	None	ASAP1
Mercury	mg/kg	EPA 6010B	0.1	None	ASAP1
Nickel	mg/kg	EPA 6010B	1	None	ASAP1
Selenium	mg/kg	EPA 6010B	10	None	ASAP1
Silver	mg/kg	EPA 6010B	1	None	ASAP1
Thallium	mg/kg	EPA 6010B	10	None	ASAP1
Zinc	mg/kg	EPA 6010B	2	None	ASAP1
Pesticides and PCBs
Atrazine	mg/kg	EPA 507	0.05	None	ASAP1
Organochlorine Pesticide and PCB Scan
DDE	mg/kg	EPA 8081 & 8082	1	None	ASAP1
DDD	mg/kg	EPA 8081 & 8082	1	None	ASAP1
DDT	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Methoxychlor	mg/kg	EPA 8081 & 8082	1.5	None	ASAP1
Aldrin	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Dieldrin	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Endosulfan	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Endrin	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Hepatachlor	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Chlordane	mg/kg	EPA 8081 & 8082	1	None	ASAP1
Lindane	mg/kg	EPA 8081 & 8082	1	None	ASAP1
PCB-Aroclor	mg/kg	EPA 8081 & 8082	10	None	ASAP1
1 Since sediment sample is not preserved “biodegradation” is likely to occur and sample needs to be processed ASAP.

Attachment 4

Elutriate Testing Parameters for Laboratory Analysis

Parameter Units Suggested Method Required Detection Limit Preservation Holding Time Quoter Method Quoter Detection Limit Subcontracted Laboratory

Sample Preparation
Elutriate Sample Preparation	-----	1:4 Sediment to Receiving Water	-----	None	ASAP1
Physical And Aggregate Properties
Alkalinity, Total	mg/l	SM2320B	6.3	None	ASAP1
Colorized Dissolved Organic Matter	ug/l	Fluorometry	10	None	ASAP1
pH	SU	EPA 150.1	0.1	None	ASAP1
Solids, Total Dissolved	mg/l	SM2540C	10	None	ASAP1
Solids, Total Suspended	mg/l	SN2450D	4	None	ASAP1
Turbidity	NTU	SM2130B	0.14	None	ASAP1
Nutrients
Ammonia, Total as N	mg/l	SM4500G	0.08	None	ASAP1
Kjeldahl Nitrogen, Total as N	mg/l	EPA 351.2	0.162	None	ASAP1
Nitrate/Nitrite, Total as N	mg/l	EPA 353.2	0.066	None	ASAP1
Phosphorus, Dissolved	mg/l	SM4500PF	0.02	None	ASAP1
Phosphorus, Orthophosphate	mg/l	SM4500PG	0.02	None	ASAP1
Phosphorus, Total	mg/l	SM4500PF	0.02	None	ASAP1
Aggregate Organic Constituents
Chemical Oxygen Demand	mg/l	SM5220D	3.2	None	ASAP1
Carbon, Total Organic	mg/l	SM5310B	0.37	None	ASAP1
Carbonaceous Biochemical Oxygen Demand	mg/l	SM5210B	0.999	None	ASAP1
THM Formation Potential, Dissolved	ug/l	EPA 524.2	4	None	ASAP1
Metals Scan (Dissolve/Total/Total Recoverable)
Aluminum	ug/l	EPA 200.7 & 200.8	39	None	ASAP1
Antimony	ug/l	EPA 200.7 & 200.8	0.028	None	ASAP1
Arsenic	ug/l	EPA 200.7 & 200.8	0.008	None	ASAP1
Barium	ug/l	EPA 200.7 & 200.8	1.17	None	ASAP1
Beryllium	ug/l	EPA 200.7 & 200.8	1	None	ASAP1
Cadmium	ug/l	EPA 200.7 & 200.8	0.007	None	ASAP1
Calcium	ug/l	EPA 200.7 & 200.8	1,000	None	ASAP1
Chromium	ug/l	EPA 200.7 & 200.8	3.54	None	ASAP1
Copper	ug/l	EPA 200.7 & 200.8	5.72	None	ASAP1
Cyanide	ug/l	EPA 200.7 & 200.8	10	None	ASAP1
Iron	ug/l	EPA 200.7 & 200.8	13.54	None	ASAP1
Lead	ug/l	EPA 200.7 & 200.8	0.008	None	ASAP1
Magnesium	ug/l	EPA 200.7 & 200.8	50	None	ASAP1
Manganese	ug/l	EPA 200.7 & 200.8	2.69	None	ASAP1
Mercury	ug/l	EPA 200.7 & 200.8	0.002	None	ASAP1
Nickel	ug/l	EPA 200.7 & 200.8	7.8	None	ASAP1
Selenium	ug/l	EPA 200.7 & 200.8	0.06	None	ASAP1
Silver	ug/l	EPA 200.7 & 200.8	0.005	None	ASAP1
Thallium	ug/l	EPA 200.7 & 200.8	0.003	None	ASAP1
Zinc	ug/l	EPA 200.7 & 200.8	5.92	None	ASAP1
Pesticides and PCBs
Atrazine	ug/l	NEP	0.1	None	ASAP1
Organochlorine Pesticide and PCB Scan
DDE	ug/l	EPA 8081 & 8082	0.005	None	ASAP1
DDD	ug/l	EPA 8081 & 8082	0.005	None	ASAP1
DDT	ug/l	EPA 8081 & 8082	0.005	None	ASAP1
Methoxychlor	ug/l	EPA 8081 & 8082	0.005	None	ASAP1
Aldrin	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
Dieldrin	ug/l	EPA 8081 & 8082	0.001	None	ASAP1
Endosulfan	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
Endrin	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
Heptachlor	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
Chlordane	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
Lindane	ug/l	EPA 8081 & 8082	0.01	None	ASAP1
PCB-Aroclor	ug/l	EPA 8081 & 8082	0.001	None	ASAP1
1 Since sediment sample is not preserved “biodegradation” is likely to occur and sample needs to be processed ASAP.

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