SOW ELAP Lab Testing Services.pdf

Scope of Work (SOW) ELAP Laboratory Testing Services Blanket Purchase Agreement (BPA)

1. This BPA is needed to support technical requirements at Pine Bluff Arsenal in relation to the environmental permits. The BPA will be used to obtain laboratory testing services from outside sources.

The BPA shall use costs obtained from a current commercial price list.

2. Vendor shall provide a current commercial price list to the Contracting Officer. Vendor shall provide updated price lists to PBA as applicable.

3. Environmental testing laboratory services may include, but are not limited to:

a. Provide transportation, labor, and equipment for environmental testing of air, soil, wastewater, groundwater, solid and hazardous waste; bio monitoring; and analytical chemistry, as needed. Provide sample pickup and transportation from Pine Bluff Arsenal (PBA) to the off-site laboratory via Federal Express or similar mechanism (courier) agreed to by the contracting officer. Dispose of all samples after testing unless stated otherwise in the order. Contractor shall return empty ice chests to PBA, with billing expenses to be invoiced at the end of each month on a separate Call Number to be issued by PBA (contractor will contact the Environmental Lab for a Call Number - empty return shipments only). For environmental testing, PBA Risk Management and Regulatory Affairs personnel shall collect the samples, apply the security seals to the shipping containers, and provide the Lab Traffic Report (e.g. chain-of-custody and analysis request forms). The contractor shall assist PBA in selection of the most applicable analytical method and/or interpretation of analytical data when needed. If required, method selection will usually be done telephonically before the order is placed. Testing requirements are provided as Enclosure 1. This listing is not meant to be all-inclusive.

The vendor shall provide a valid Laboratory Certification from the Arkansas Department of Environmental Quality (ADEQ) for the testing performed to marcia.a.wayland.civ@army.mil

For restoration testing, quality control/quality assurance and reporting shall meet the requirements of the Department of Defense (DoD) Quality Systems Manual (QSM) for Environmental Laboratories (Version 5.4 dated 2021, including any later versions). Where applicable, the vendor shall provide a valid DoD ELAP Certificate of Accreditation with Scope to marcia.a.wayland.civ@army.mil

The contractor shall provide Method Detection Limit (MDL) and Practical Quantitation Limit (PQL) information for each Method/Target in an Excel spreadsheet provided by the government (see Enclosure 2 – Example MDL PQL Spreadsheet).

The MDL procedures and calculations shall be done in accordance with EPA’s Determination and Procedure for the Determination of the Method Detection Limit, Revision 2 dated December 2016.

The PQL shall be calculated by multiplying the MDL value by a factor of 3.3. The MDL/PQL spreadsheet shall be provided on a yearly basis or whenever a new set of MDLs are generated for a given analysis.

This information should be provided to marcia.a.wayland.civ@army.mil

PBA’s environmental permits specify a Required Practical Quantitation Limit (RPQL) for all analytical targets. For reporting purposes, the PQL should be less than or equal to the RPQL.

All reported target concentrations that fall between the MDL and PQL values should be “'J" flagged.

Reports shall be e-mailed to marcia.a.wayland.civ@army.mil with a copy emailed to shonda.m.gonzalez.civ@army.mil mailto:marcia.a.wayland.civ@army.mil mailto:eddie.g.robinson.civ@mail.mil mailto:eddie.g.robinson.civ@mail.mil mailto:eddie.g.robinson.civ@mail.mil mailto:shonda.m.gonzalez.civ@army.mil

POC for technical issues is Marcia Wayland, 870-540-2898, or Shonda Gonzalez, 870-540-2808.

Calls are to be accepted from authorized persons only. The Contracting Officer will supply the vendor with a list of names of individuals by organizational element authorized to place orders and dollar limitations. Request the following personnel be authorized to place calls:

NAME $ LIMITATION PER CALL PHONE

Shonda Gonzalez $ 10,000.00 870-540-2808 Lorrie Meggs $ 10,000.00 870-540-2817

The following persons should be authorized to make contact with the vendor for detailed information prior to a call being placed:

Shonda Gonzalez Marcia Wayland Lorrie Meggs

4. Sample pickup/shipping details

Close proximity commercial laboratories (less than 100 miles from PBA) shall provide courier services (or access thereto) with the sample pickup price being provided in the laboratories’ price list. This action/price will be identified in each Call as an individual line item by PBA. Contractor is required to notify PBA in writing of any sample pickup/courier price changes.

Non-close proximity commercial laboratories (greater than 100 miles from PBA) shall establish a mechanism with Federal Express (FEDEX) whereby PBA can notify FEDEX of samples to be picked up at PBA and FEDEX then transports samples to the laboratory in question. FEDEX/contractor mechanism should allow FEDEX to bill Contractor for shipping costs, which will then be invoiced monthly to PBA.

Contractor shall provide PBA with all pertinent FEDEX information/contacts for this action.

5. To meet requirements for the QA samples, this BPA shall be established with two or more contractors within the discretion of Pine Bluff Arsenal.

6. The selected vendors shall off-load test samples to a 3rd party when requested.

7. Contractor shall comply with all applicable federal, state, and local environmental laws, statutes, regulations, executive orders, permits, Army regulations (with supplements), as well as Major Subordinate Command (MSC) and installation regulation, policy, Host Tenant Agreement, Interagency Service Support Agreement, or Status-of-Forces Agreement. Contractor shall immediately report any conflicts between applicable federal, state, local environmental laws, statutes, executive orders, and provisions of Army Regulation 200-1, and any specifications within this contract to the Contracting Officer Representative (COR).

Glossary of Abbreviations and Acronyms

ADEQ Arkansas Department of Environmental Quality

BPA Blanket Purchase Agreement

DoD Department of Defense

ELAP Environmental Laboratory Accreditation Program

EPA Environmental Protection Agency

MDL Method Detection Limit

PBA Pine Bluff Arsenal

PQL Practical Quantitation Limit

QA Quality Assurance

QSM Quality Systems Manual

RPQL Required Practical Quantitation Limit

SOW Scope of Work

Parameter Test Method

Alkalinity EPA 310.1

Anions EPA 300.0/9056A

Biochemical Oxygen Demand (BOD5) SM 5210 B

BTEX (Soil and Water) EPA 602/EPA 8260C

BTU ASTM D240

Carbon, Total Organic (soil) EPA 9060A

Carbon, Total Organic (water) SM 5310 C

Chemical Oxygen Demand (COD) EPA

Chlorine, Total Residual EPA

Chromium, Hexavalent EPA

Coliform, Fecal or Total SM 9222 D

Conductivity, Specific EPA 120.1

Cyanide, Reactive EPA

Cyanide, Total SM 4500-CN C,E

Dioxin/Furans EPA

Dissolved Gases in Water EPA RSK-175

Explosives EPA

Halides, Total EPA

Halides, Total Organic (TOX) EPA 9020

Hardness EPA 130.1

Herbicides EPA 8151A

Mercury EPA 7470A

Mercury (Low Level) EPA 245.7/EPA 1631A

Metals, Dissolved EPA 200.8/6020A

Metals, Total EPA 200.8/6020A

Metals, Total Recoverable EPA 200.8

Nitrogen, Total Kjeldahl EPA 351.4

Oil and Grease EPA 1664A

Oxygen, Dissolved EPA 360.1

PAH EPA 8270

PCBs (Soil, Water and Oil) EPA 8082A

Perchlorate EPA 314.0/6850

Pesticides EPA 608/8081B pH (aqueous) EPA 150.1 pH (non-aqueous) EPA 9045

Phenolics EPA 420.1

Phosphorus, Total SM 4500-P B,F

Priority Pollutants EPA

Semi-Volatile Organics EPA 8270D

Solids, Total EPA 160.3

Solids, Total Dissolved SM 2540 C

Solids, Total Suspended SM 2540 D

Sulfide, Reactive EPA 9215

Sulfide, Soil and Water EPA

Enclosure 1 - Testing Requirements

Parameter Test Method

Enclosure 1 - Testing Requirements

Sulfite EPA

TCLP Herbicides EPA 8151A

TCLP Metals EPA 6010A

TCLP Pesticides EPA 8081A

TCLP SVOA EPA 8270D

TCLP VOA EPA 8260C

TCLP ZHE (Liquid and Solid) EPA 1311

Total Petroleum Hydrocarbons (TPH) EPA

Total Recoverable Phenolics EPA 420.1

Toxicity Testing (Acute and Chronic) EPA

Turbidity EPA 180.1

Volatile Organics EPA 8260C

Water % EPA 1311

Other

Data Validation packages/deliverables

Courier charge for sample pickup

Empty ice chest return to PBA

Discharge Monitoring Report

Instrumental Scans (GC, IR, LC, etc)

Sample Preps (digestions, fusions, etc)

Third-party review deliverables

Rapid turn-around time cost factors

24 Hours

72 Hours

Method Analyte MDL PQL RPQL Units MDL Study Date Analyst

9056A Nitrate plus Nitrite as N 0.00 0.2 mg/L

314.0 Perchlorate 0.00 0.004 mg/L

6850 Perchlorate 0.00 0.004 mg/L

SM 5310C TOC 0.00 1 mg/L

SM 4500-P E Total Phosphorus 0.00 0.02 mg/L

7470A Mercury 0.00 0.2 ug/L

6020A Arsenic 0.00 5 ug/L

6020A Barium 0.00 5 ug/L

6020A Cadmium 0.00 1 ug/L

6020A Chromium 0.00 5 ug/L

6020A Copper 0.00 5 ug/L

6020A Lead 0.00 3 ug/L

6020A Manganese 0.00 5 ug/L

6020A Mercury 0.00 0.2 ug/L

6020A Selenium 0.00 5 ug/L

6020A Silver 0.00 1 ug/L

6020A Sodium 0.00 100 ug/L

6020A Zinc 0.00 5 ug/L

300.0/9056A Chloride 0.00 1 mg/L

300.0/9056A Fluoride 0.00 0.2 mg/L

300.0/9056A Nitrate 0.00 mg/L

300.0/9056A Nitrite 0.00 mg/L

300.0/9056A Sulfate 0.00 1 mg/L

8081B 4,4'-DDD 0.00 1 ug/L

8081B 4,4'-DDE 0.00 0.1 ug/L

8081B 4,4'-DDT 0.00 0.02 ug/L

8081B Endrin 0.00 0.06 ug/L

8081B Lindane 0.00 0.04 ug/L

8081B Methoxychlor 0.00 1.76 ug/L

8081B Toxaphene 0.00 1 ug/L

8151A 2,4,5-TP 0.00 1 ug/L

8151A 2,4-D 0.00 5 ug/L

Enclosure 2 - Example MDL PQL Spreadsheet

8260C 1,1,1-Trichloroethane 0.00 5 ug/L

8260C 1,1,2,2-Tetrachloroethane 0.00 5 ug/L

8260C 1,1,2-Trichloroethane 0.00 5 ug/L

8260C 1,1-Dichloroethane 0.00 5 ug/L

8260C 1,1-Dichloroethene 0.00 5 ug/L

8260C 1,2,4-Trichlorobenzene 0.00 5 ug/L

8260C 1,2-Dichlorobenzene 0.00 2 ug/L

8260C 1,2-Dichloroethane 0.00 5 ug/L

8260C 1,2-Dichloropropane 0.00 100 ug/L

8260C 1,4-Dichlorobenzene 0.00 2 ug/L

8260C 2-Butanone 0.00 10 ug/L

8260C 2-Chloroethyl vinyl ether 0.00 100 ug/L

8260C 2-Hexanone 0.00 100 ug/L

8260C 4-Methyl-2-pentanone 0.00 100 ug/L

8260C Acetone 0.00 5 ug/L

8260C Benzene 0.00 5 ug/L

8260C Bromodichloromethane 0.00 5 ug/L

8260C Bromoform 0.00 10 ug/L

8260C Bromomethane 0.00 5 ug/L

8260C Carbon disulfide 0.00 1 ug/L

8260C Carbon tetrachloride 0.00 5 ug/L

8260C Chlorobenzene 0.00 10 ug/L

8260C Chloroethane 0.00 5 ug/L

8260C Chloroform 0.00 10 ug/L

8260C Chloromethane 0.00 5 ug/L

8260C cis 1,2-Dichloroethene 0.00 5 ug/L

8260C cis 1,3-Dichloropropene 0.00 5 ug/L

8260C Dibromochloromethane 0.00 5 ug/L

8260C Ethylbenzene 0.00 10 ug/L

8260C m & p-Xylene 0.00 1 ug/L

8260C Methylene chloride 0.00 5 ug/L

8260C o-Xylene 0.00 5 ug/L

8260C Styrene 0.00 1 ug/L

8260C Tetrachloroethene 0.00 1 ug/L

8260C Toluene 0.00 5 ug/L

8260C trans 1,2-Dichloroethene 0.00 5 ug/L

8260C trans 1,3-Dichloropropene 0.00 1 ug/L

8260C Trichloroethene 0.00 1 ug/L

8260C Trichlorofluoromethane 0.00 5 ug/L

8260C Vinyl acetate 0.00 5 ug/L

8260C Vinyl chloride 0.00 1 ug/L

8270D 1,2,4-Trichlorobenzene 0.00 10 ug/L

8270D 1,2-Dichlorobenzene 0.00 10 ug/L

8270D 1,3-Dichlorobenzene 0.00 10 ug/L

8270D 1,4-Dichlorobenzene 0.00 10 ug/L

8270D 2,4,5-Trichlorophenol 0.00 10 ug/L

8270D 2,4,6-Trichlorophenol 0.00 10 ug/L

8270D 2,4-Dichlorophenol 0.00 10 ug/L

8270D 2,4-Dimethylphenol 0.00 10 ug/L

8270D 2,4-Dinitrophenol 0.00 50 ug/L

8270D 2,4-Dinitrotoluene 0.00 10 ug/L

8270D 2,6-Dinitrotoluene 0.00 10 ug/L

8270D 2-Chloronaphthalene 0.00 10 ug/L

8270D 2-Chlorophenol 0.00 10 ug/L

8270D 2-Methylnaphthalene 0.00 10 ug/L

8270D 2-Methylphenol 0.00 10 ug/L

8270D 2-Nitroaniline 0.00 50 ug/L

8270D 2-Nitrophenol 0.00 10 ug/L

8270D 3,3'-Dichlorobenzidine 0.00 10 ug/L

8270D 3-Nitroaniline 0.00 50 ug/L

8270D 4,6-Dinitro-2-methylphenol 0.00 50 ug/L

8270D 4-Bromophenyl-phenylether 0.00 10 ug/L

8270D 4-Chloro-3-methylphenol 0.00 10 ug/L

8270D 4-Chloroaniline 0.00 10 ug/L

8270D 4-Chlorophenyl-phenylether 0.00 10 ug/L

8270D 4-Methylphenol 0.00 10 ug/L

8270D 4-Nitroaniline 0.00 10 ug/L

8270D 4-Nitrophenol 0.00 50 ug/L

8270D Acenaphthene 0.00 10 ug/L

8270D Acenaphthylene 0.00 10 ug/L

8270D Anthracene 0.00 10 ug/L

8270D Benzo[a]anthracene 0.00 10 ug/L

8270D Benzo[a]pyrene 0.00 10 ug/L

8270D Benzo[b]fluoranthene 0.00 10 ug/L

8270D Benzo[g,h,i]perylene 0.00 10 ug/L

8270D Benzo[k]fluoranthene 0.00 10 ug/L

8270D Benzoic acid 0.00 50 ug/L

8270D Benzyl alcohol 0.00 10 ug/L

8270D bis(2-Chloroethoxy)methane 0.00 10 ug/L

8270D bis(2-Chloroethyl)ether 0.00 10 ug/L

8270D bis(2-chloroisopropyl)ether 0.00 10 ug/L

8270D bis(2-Ethylhexyl)phthalate 0.00 10 ug/L

8270D Butylbenzylphthalate 0.00 10 ug/L

8270D Chrysene 0.00 10 ug/L

8270D Dibenz[a,h]anthracene 0.00 10 ug/L

8270D Dibenzofuran 0.00 10 ug/L

8270D Diethylphthalate 0.00 10 ug/L

8270D Dimethylphthalate 0.00 10 ug/L

8270D Di-n-butylphthalate 0.00 10 ug/L

8270D Di-n-octylphthalate 0.00 10 ug/L

8270D Fluoranthene 0.00 10 ug/L

8270D Fluorene 0.00 10 ug/L

8270D Hexachlorobenzene 0.00 10 ug/L

8270D Hexachlorobutadiene 0.00 10 ug/L

8270D Hexachlorocyclopentadiene 0.00 10 ug/L

8270D Hexachloroethane 0.00 2 ug/L

8270D Indeno[1,2,3-cd]pyrene 0.00 10 ug/L

8270D Isophorone 0.00 10 ug/L

8270D Naphthalene 0.00 10 ug/L

8270D Nitrobenzene 0.00 10 ug/L

8270D N-Nitroso-di-n-propylamine 0.00 10 ug/L

8270D N-Nitrosodiphenylamine 0.00 10 ug/L

8270D Pentachlorophenol 0.00 10 ug/L

8270D Phenanthrene 0.00 10 ug/L

8270D Phenol 0.00 10 ug/L

8270D Pyrene 0.00 10 ug/L

8270D Pyridine 0.00 10 ug/L