PR-15-131-Attachment_2.pdf

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EPA Region 1 Laboratory ISO/IEC 17025 Accreditation
Solicitation number
RFQ-MA-15-00006
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Attachment 2 Laboratory Methods

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Certificate # L2333

Scope of Accreditation For

U.S. EPA, Region 1, New England Regional Laboratory

11 Technology Drive N. Chelmsford, MA 01863

Ernest Waterman 617-918-8632

In recognition of a successful assessment to ISO/IEC 17025:2005, accreditation is granted to U.S. EPA, Region 1, New England Regional Laboratory to perform the following tests:

Accreditation granted through: April 23, 2016

Testing - Environmental

Technology Range, when necessary Methods Used Product Types Remarks

ICP-MS (0.2 to 50 ) ug/L

EIASOP-INGICPMS

EIASOP-INGMETALSPREP

Metals

Drinking water EPA 200.2

EPA 200.8

ICP-AES (8.0 to 110) ug/L (0.8 to 11) mg/kg

EIASOP-INGDVICP

EIASOP-INGMETALSPREP

Metals

Wastewater soil, sediment

Based on EPA 200.7 and 6010B

Preparation Method EIASOP-INGMETALSPREP

Metals Wastewater Based on EPA 200.2

Preparation Method

EIASOP-INGMETALSPREP

Acid Digestion of water for total and dissolved metals

Wastewater Soil, sediments, sludge TCLP extracts

Based on EPA 3005A

Preparation Method EIASOP-INGMETALSPREP

Hot Plate Acid Digestion Wastewater Liquid waste

Based on EPA 3010A

Preparation Method EIASOP-INGMETALSPREP

Acid digestion of Solids Soil, sediments, sludge Based on EPA

3050B

Form 28.6—Revision 5 05/23/06 Page 1 of 5 pmegio Typewritten Text Attachment 2, RFQ-MA-15-00006

Technology Range, when necessary Methods Used Product Types Remarks

ICP-MS

ICP-AES

Calculation based on metals

EIASOP-INGDVICP

Hardness

Drinking water wastewater Based on SM 2340 B

Cold Vapor Atomic

Absorption

EIASOP-NIPPONHG1

Mercury Drinking water ASTM D3223-02

Cold Vapor Atomic

Absorption

EIASOP- NIPPONHG1

Mercury Wastewater

Soil, sediment

Based on EPA 245.1, 7470A

Based on EPA 7471A

Thermal Decomposition

& Atomic Absorption

EIASOP-INGDMA

Mercury

Soil, sediment, tissue Based on EPA 7473

Ion Chromatography EIASOP-INGIC

Anions and cations Drinking water wastewater Based on EPA 300.0

UPLC/MS/MS EIASOP-LCMSClO4W Perchlorate

Drinking water wastewater Based on EPA 331.0

Turbidimeter EIASOP-INGTURB Turbidity

Drinking water wastewater

Based on EPA 180.1 and SM 2310 B

Automated Ion Analyzer -

Lachat

EIASOP-INGCN

Cyanide

Drinking water Wastewater

Soil, sediment

Based on EPA 335.4, EPA 9012B, Lachat

10-204-00-1-x

Automated Ion Analyzer -

Lachat

EIASOP-INGTP

Orthophosphate as P Drinking water

Wastewater Based on Lachat 10-115-01-1-B

Automated Ion Analyzer -

Lachat

EIASOP-INGTP

Total Phosphorous Wastewater

Based on Lachat 10-115-01-1-F

Electrometric EIASOP-INGALKCARB Alkalinity

Drinking water wastewater Based on SM 2320 B

Form 28.6—Revision 5 05/23/06 Page 2 of 5 necessary Methods Used Product Types Remarks

Gravimetric

EIASOP-INGTSS-TDS-

VRES

Total dissolved solids total suspended solids

Drinking water waste water

Based on EPA 160.1 and 160.2

Electrometric 1-14 pH units EIASOP-INGPH pH

Drinking water, wastewater

Based on EPA 9040B and SM 4500-

H+

GC/MS EIASOP-VOAGCMS

Volatile organic compounds

Drinking water Wastewater

Soil, sediment, sludge

EPA524.2

Based on EPA

8260B, EPA 624

Preparation method EIASOP-VOAGCMS

Aqueous Phase Purge & Trap

Soil, sediment

Based on EPA 5030B

Preparation Method EIASOP-VOAGCMS

Solid phase Purge & Trap Soil, Sediment Based on EPA 5035

GC/MS

EIASOP-BNAGCMS

EIASOP-BNAW

EIASOP-BNAS

Acid, Base/Neutral Organic Compounds

Wastewater Soil, sediment, sludge, oil

Based on EPA

8270C, EPA 625

Preparation Method

EIASOP-GCPESWALL

EIASOP-BNAW

Separatory Funnel Extraction Wastewater Based on EPA

3510C

Preparation Method

EIASOP-PESTSOIL

EIASOP-BNAS

Pressurized Fluid Extraction

Soil, sediment, sludge

Based on EPA 3545A

GC-ECD EIASOP-GCPESWALL

PCBs in Aqueous Samples

Based on EPA

8082A, EPA 608

GC-ECD EIASOP-PESTSOIL

PCBs in Solid samples

Soil, sediment, sludge, oil Based on EPA 8082

GC-ECD

EIASOP-GCPESWALL

Chlorinated Organic

Compounds in aqueous samples

Wastewater Based on EPA

8081A, EPA 608

Form 28.6—Revision 5 05/23/06 Page 3 of 5 necessary Methods Used Product Types Remarks

GC-ECD

EIASOP-PESTSOIL

Chlorinated Organic

Compounds in solid samples

Soil, sediment, sludge

Based on EPA 8081A

Clean up Method EIASOP-PESFLOR

Florisil Clean-up

Wastewater soil, sediments.

Oil, sludge

Based on EPA 3620B

Clean up Method EIASOP-PESGPC

Gel Permeation Clean-up

Wastewater Soil, sediment oil, sludge

Based on EPA 3640A

Clean-up Method

EIASOP-PESTSOIL

Sulfuric acid/Permanganate

Clean-up

Soil, sediment, sludge, oil

Based on EPA 3665A

Setaflash Closed Tester EIASOP-Flash

Ignitability/Flashpoint Liquid waste

Based on ASTM D3278

EPA 1020A

Thermal Decomposition

& Atomic Absorption

ECASOP-MilestoneSOP Mercury Tissue

Based on EPA 7473

Membrane Filtration

ECASOP-FecalColiformMF Fecal Coliforms by Membrane filtration

Ambient surface water, Drinking water Waste water

Based on SM 9222 D

Membrane Filtration

ECASOP-TotalColiformMF Total Coliforms by Membrane filtration

Ambient surface water, Drinking water wastewater

Based on SM 9222 B

Pour Plate ECASOP-HPCMethod Heterotrophic Plate Count Drinking water Based on SM 9215 B

Multi tube fermentation

ECASOP-MTF

Total Coliform E. coli by multi tube fermentation

Ambient surface water, Drinking water wastewater

Based on SM 9221 F

+ SM 9222B

Enzyme substrate

ECASOP-TC/ECColilert Total Coliform/e.coli by defined substrate

Ambient surface water, Drinking water wastewater

Based on SM 9223 B

Form 28.6—Revision 5 05/23/06 Page 4 of 5 necessary Methods Used Product Types Remarks

Enzyme substrate

ECASOP-ENTERO

Enterococci by Defined

Substrate

Ambient surface water, Fathead minnow Chronic

Toxicity Testing

ECASOP-FHCHRTOX

Chronic Toxicity Test Method for Pimephales promelas, Ambient surface water, Wastewater

Based on EPA 1000.0

EPA/821/R-02/013

Daphnid Chronic

Toxicity Testing

ECASOP- Cd Chronic tox test Chronic Toxicity Test Method for Ceriodaphnia dubia, Ambient surface water, Wastewater

Based on EPA 1002.0

EPA/821/R-02/013

Notes:

1) This laboratory does not offer commercial testing service.

Approved by: Date: January 2, 2015 R. Douglas Leonard Chief Technical Officer

Issued: 4/23/13 Revised: 12/19/13 Revised: 1/2/15

Form 28.6—Revision 5 05/23/06 Page 5 of 5

For
U.S. EPA, Region 1, New England Regional Laboratory
Remarks
Product Types
Methods Used

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