PWS 12 Feb 2024.pdf

PERFORMANCE WORK STATEMENT

FOR ANALYTICAL LABORATORY SERVICES

12 Feb 2024

1.0 PURPOSE

This scope of work is for analytical services support for the United States (U.S.) Army Corps of Engineers (USACE) Omaha District Geotechnical Engineering and Sciences Branch Chemistry Section (CENWO-ED-GS), in terms of chemical analysis, toxicity testing, microbiological testing including mold identification, air testing, radiochemical testing and asbestos testing. The matrices of interest for analysis are soil, sediment, sludge, groundwater, surface water, biota, air, wipe samples, solid phase microextraction devices (SPMEs), and paint chips. These samples are primarily to be collected from Department of Defense (DoD) Formerly Used Defense Site (FUDS) environmental restoration program. The Contract Laboratory shall provide support to the USACE Project Chemist in terms of providing necessary protocol information required by hazardous waste investigation and remediation programs conducted by, or on behalf of the USACE Omaha District.

2.0 GENERAL DESCRIPTION OF WORK REQUIRED UNDER THIS SCOPE OF

WORK

The Contractor, operating as an independent Contractor and not as an agent of the Government, shall provide all necessary personnel, equipment and materials required to obtain technically valid and legally defensible environmental data that will meet or exceed the analytical method criteria and the most current version of the DoD Quality Systems Manual (QSM) for Environmental Laboratories. The Contract Laboratory shall be able to provide all sample analyses using methods listed in the attached Table 1. For all FUDS projects, the Contract Laboratory shall submit data to the FUDSChem portal, as described in Section 6.1.

If services cannot be provided by the Contract Laboratory, services may be sub-contracted to another laboratory. The sub-contracted laboratory shall meet all of the requirements for the Primary Laboratory as specified in this agreement. For each call order, indicate which analytical services will be contracted out and identify the Sub-contract laboratory(s) that will be performing the analyses and provide all pertinent certifications. Should a subcontracted laboratory only be responsible for a particular analysis (such as asbestos) it will only be required to be certified for that particular analysis upon approval of the CENWO-ED-GS (see Section 4.0).

Calls will be issued under the blanket purchase agreements (BPAs). The USACE Contracting Officer (KO) or Contracting Officer’s Representative (COR) will provide the Contractor with any site-specific information upon issuance of each call. Information provided by the USACE on any site will be dependent on the current status of the site. Each call will define the performance requirements of the Contractor. Calls may require, but will not be limited to, any combination of the requirements stated in Section 3.0 below.

The description of work stated herein provides a general understanding of the Contractor functions to be performed; individual calls will contain the specific performance based requirements. Technical requirements described herein in no way limit the activities that may be required under the terms of this contract.

3.0 QUALITY CONTROL REQUIREMENTS

In addition to the requirements outlined in this Scope of Services, all work performed under this contract shall meet the quality control requirements in most recent version of the DoD QSM for

Environmental Laboratories (available at https://www.denix.osd.mil/ on the Environmental Data Quality Workgroup page) per DoD Instruction 4715.15 (October 2015). Project libraries should at a minimum conform to the latest version of the DoD QSM, unless specifically overridden by the USACE Project Chemist based on project specific data quality objectives (DQOs). The libraries used for analysis and data review shall be provided as part of the data package (Section 6.0).

4.0 LABORATORY CERTIFICATION

Laboratories performing analyses in support of this procurement must have an established and documented laboratory quality system that conforms to ISO/IEC 17025:2017 as implemented by the DoD Quality Systems Manual for Environmental Laboratories (latest version). Laboratories must possess any required state or host nation certification and/or be accredited for each applicable test method under the DoD ELAP or by a nationally recognized laboratory accreditation body (e.g. NELAP), compliant with ISO/IEC 17011:2017. The Contract laboratory must retain current certification under the DoD Environmental Laboratory Accreditation Program (ELAP). The DoD ELAP provides a means for laboratories to demonstrate conformance to the DoD QSM as authorized by DoD Instruction 4715.15. (More information concerning ELAP can also be found at https://www.denix.osd.mil/ under Environmental Data Quality Workgroup). If the Prime Laboratory subcontracts another laboratory which holds a specific accreditation, the Prime Laboratory shall specify the media, analyte, method, and certification for which the sub-contracted laboratory is responsible. All data from the subcontracted laboratory shall be provided to the Prime Laboratory to be delivered to USACE CENWO-ED-GS in accordance with the analytical deliverable package requirements (see Section 6.0).

Asbestos:

The Contract Laboratory must be accredited under the National Institute of Standards and Technology (NIST) “National Voluntary Laboratory Accreditation Program (NVLAP)” for bulk asbestos analysis. The laboratory shall be fully equipped and use analysts with demonstrated proficiency conducting polarized light microscopy (PLM) in accordance with 40 Code of Federal Regulations (CFR) 763, Subpart E, Appendix E.

Lead:

Laboratory shall participate in the United States Environmental Protection Agency (EPA) National Lead Laboratory Accreditation Program (NLLAP) accredited by either the American Association for Laboratory Accreditation (A2LA) or the American Industrial Hygiene Association (AIHA) and shall successfully participate in the Environmental Lead Proficiency Analytical Testing (ELPAT) program to perform sample analysis. Laboratories selected to perform blood lead analysis shall be Occupational Health and Safety Administration approved.

All Prime and subcontracted laboratories shall also identify any additional certifications they hold (State specific, etc.).

5.0 ANALYTICAL PROTOCOL

Analytical methods shown in Table 1 are from: Test Methods for Evaluating Solid Waste, USEPA SW-846, Third Edition, or other published methods such as Contract Laboratory Program (CLP), American Society for Testing and Materials (ASTM), 500/600 methods, EPA microbiological methods (http://www.epa.gov/ microbes/moldtech.htm) or other appropriate method manuals. The most recently published version of SW-846 will be used unless otherwise specified on a project specific basis. The laboratory should be aware of and comply with the project specific DQOs and applicable project requirements specified in task orders.

6.0 ANALYTICAL DATA PACKAGE

All data shall be submitted as electronic data deliverables (EDD) and shall have an electronic pdf “hard copy” report. Specific requirements for each are explained below. The electronic submissions, in the form of e-mail documents, files uploaded to FUDSChem, or CD’s are considered to be part of the analytical data package. A maximum of 28 days from sample receipt to delivery of the data package will be allowed, however, quicker turnaround of electronic submissions is favored.

6.1 Electronic Data Deliverables (EDDs)

All EDDs shall be submitted as Staged Electronic Data Deliverables (SEDDs) Stage 2a (5.2) which include all results, units, method, and instrument quality control data. If the laboratory has the capabilities to provide SEDD Stage 2b, 3 or 4, provide a separate table indicating costs associated with the deliverables. The most current version of SEDD shall be used in conjunction with the most current version of the DoD QSM valid values. For all FUDS projects, the SEDDs will be submitted to the FUDSChem portal, run through the compliance checker, and the laboratory must resolve any non-conformances (errors and warnings) with the project library and/or FUDSChem-required Valid Values or Submission Errors. The electronic library will be collectively developed between the USACE and the laboratory. The finalized library will be maintained by USACE, and a copy of the library used for each sample delivery group (SDG) shall be provided upon submittal of the electronic deliverables. Once the electronic deliverables and the “hard copy” pdf report have been uploaded to FUDSChem by the laboratory and project-specific USACE personnel have been notified via the FUDSChem upload portal that the SEDD and report are available, the USACE Project Chemist will review all data to ensure data completeness is appropriate for the validation process (See Section 6.3 for more specific details).

6.2 Electronic pdf “hard copy” report

The “hard copy” report format will follow the requirements set forth in Appendix A of the latest version of the DoD QSM v.5.0. Generally, there will be a cover sheet, table of contents, case narrative, analytical results, sample management records, quality assurance (QA)/quality control (QC) information and information for third-party review. The case narrative shall specifically address, but is not limited to: all abnormalities and deviations that may affect data quality of analytical results, any issue in the data package that potentially affects the usability of the data, identification of samples for which manual integration was necessary, numerical results were outside the limits of quantitation, and/or any other factor that could affect sample results (air bubbles or excessive headspace in volatile organic analysis (VOA) sample vials, presence of multiple phases, exceeds holding time, temperature and pH excursions, samples broken upon receipt, etc.) The final report should have a full complement of laboratory qualifiers as well as definitions for those qualifiers. Qualifiers should follow the most current version of the EPA National Functional Guidelines (www.epa.gov/superfund/programs/clp/guidance.htm) and the DoD QSM.

All hard copy reports must include all data to enable the Project Chemist to verify compliance with the latest version of the DoD QSM. An example of report elements required at a minimum for Methods 8260/8270 follows below:

Sample Identification #, Matrix, Prep and Test Method utilized, associated batch information

Case Narrative Chain of Custody, Sample Receipt Forms & Shipping documentation Telephone/email records associated with actions taken on quality issues

QC Verification for gas chromatography-mass spectrometry (GC/MS) (8260/8270) o Tuning

BFB ion abundance criteria and relative abundance, injection date and time (CLP Form V)

Breakdown Check (8270) Responses and tailing factors must be reported for DDT, benzidine, and pentachlorophenol.

o Initial calibrations (ICALs)

Date, time of analysis Show a minimum of 5 points used to determine ICAL Provide Response Factors (RF) and percent relative standard deviations (%RSD) for all analytes Indicate which samples were evaluated as system performance check compounds (SPCCs) and calibration check compounds (CCCs) Indicate method for calculation of calibration curve (linear, least square regression (with r value), non-linear regression (with r2 value & number of points used [6-second order, 7-third order]).

o Secondary Source Verification (ICV) Provide RF and %RSD for all analytes o Continuing Calibration Verification (CCV) Date, time and frequency of CCV analysis Provide RF and %RSD for all analytes Indicate which samples were evaluated as SPCCs and CCCs Present percent drift (%D) o Internal Standard Verification Report Area counts and retention times as well as the upper (200%) and lower (50%) limits and the 12-hour standard for the ICAL (CLP Form VIII).

Sample Results o Analysis results with proper units, reporting limit, method detection limit (MDL)

(limit of detection, limit of quantitation), surrogates, % recovery, and QC limits, percent moisture (soils), etc.

Qualification (flag) Definitions Third Party Document Review Items o Raw data (chromatograms, mass spec results) o Supporting documentation (run logs, sample prep logs, standard prep logs, etc.)

6.3 Submittal Approval Process:

Within 10 business days of receipt of EDDs and the hard copy report, if data is of sufficient quality and completeness, the USACE Project Chemist will submit to the Laboratory a Memorandum of Approval. EDDs shall still be provided via email, share site, or FUDSChem as appropriate as soon as available. The calendar for approval begins when the hard copy report arrives at the USACE CENWO-ED-GS office. If any discrepancies are found during the data review, the Project Chemist will notify the laboratory of the deficiencies to determine corrective measures.

7.0 OTHER REQUIREMENTS

7.1 Sample Handling and Custody Requirements:

The Contract laboratory shall have a procedure documenting proper sample handling and custody of samples. A Cooler Receipt Form shall be completed and e-mailed to the USACE Project Chemist on the day the samples are received or logged in at the laboratory to communicate the condition of the samples upon receipt. Any problems, such as warm samples (>4oC + 2 oC), broken bottles, missing samples, air bubbles in VOA vials, etc. will require immediate notification by laboratory personnel to the USACE Project Chemist prior to sample analysis.

7.2 Input to the Quality Assurance Project Plan (QAPP)

In order to obtain data of sufficient quality to satisfy data quality objectives for scientifically and legally defensible data, the FUDS environmental restoration program requires a QAPP. The QAPP describes organizational pathways of communication, field sampling efforts and laboratory efforts. The Contract laboratory’s input will be required for inclusion in the QAPP. Following the requirements of National Environmental Laboratory Accreditation Conference Chapter 5 and DoD QSM, the Contract laboratory must have a Quality Assurance or Quality System Manual (QA/QSM). For completion of the QAPP, specific areas addressed in the QA/QSM may need to be expanded upon. The Contract laboratory shall provide all additional information required by the USACE Project Chemist.

Project/Task Organization: A narrative or organizational chart showing key management and analytical personnel involved with the analysis as well as lines of communication among all project participants, USACE and the lab. Any key subcontractors will also need to be identified.

Analytical Method Requirements: The laboratory shall perform MDL studies on an annual basis, and make these studies available upon request. The MDL and MDL check samples shall be extraction/digestion method specific and instrument specific and shall include any clean-up methods routinely used. Laboratory standard operating procedures (SOPs) must also be available for attachment to the QAPP as an appendix. The SOP must describe the equipment and apparatus utilized and any specific performance requirements associated with it. Further, the SOP shall describe the calibration, calibration verification, method QC elements, their acceptance criteria and procedures taken for corrective actions.

Quality Control Requirements: Provide QA/QC checks done by the laboratory for both field QC samples, but also internal laboratory QC verification. The laboratory shall ensure that results from the laboratory internal quality control checks are reported with the associated batch of analytical data and that the sample results and the QC results can be easily correlated.

Corrective Action: A description of corrective actions taken when results appear unusual, questionable, or the limits of acceptability are exceeded. Provide the limits of acceptability and propose and describe how re-establishment of control is demonstrated.

Instrument /Equipment Testing, Inspection, and Maintenance Requirements: The laboratory will describe the implementation of the Preventative Maintenance systems and their schedule used to ensure the proper functioning of all laboratory and field apparatus.

Identify all equipment by the manufacturer’s name, model number, and accessories. The laboratory should be prepared to provide the types of inspections, documentation, and testing procedures, etc. required for all equipment.

Instrument Calibration and Frequency: For all instruments, the laboratory may have to describe the procedure used for calibrations and the frequency and types of calibration verification checks employed. The laboratory shall indicate how the records of calibrations are maintained and are traceable to the instrument and analyses.

8.0 RESPONSIVENESS

The laboratory shall identify the laboratory manager who has primary responsibility for project coordination and coordination of analyses. Especially when a short analytical turn-around time is required, the laboratory manager or designate should respond to USACE telephone or e-mail requests for information on short notice. Unresolved inquiries could result in re-performance of analyses in order to obtain data of known quality.

Table 1

Table 1 - Price List - Analytical Lab Services

Description

Methods Method of

Surveillance

Organics

Volatile Organics (VOC) current TCL list

5 ml purge 8260 100%

Inspection

25 ml purge 8260 100% Inspection unpreserved 7 day holding 8260

100% Inspection

VOC - Drinking Water 524.3

100% Inspection

VOC, PCE + TCE + 11-DCE + 12DCE +

VC

5 ml purge 8260 100%

Inspection

25 ml purge 8260 100%

Inspection unpreserved 7 day holding 8260 100%

Inspection

VOC, BTEX

5 ml purge 8260 100%

Inspection

25 ml purge 8260 100%

Inspection total in air NIOSH 1500

100%

Inspection

VOC, BTEX + MTBE

5 ml purge 8260

100% Inspection

25 ml purge 8260

100%

Inspection

1,4-Dioxane

25 ml purge 8260 SIM 100%

Inspection

UM-94

100%

Inspection

8270 SIM

Semi-Volatile Organics (BNA) TCL list

100% Inspection

100%

Inspection

Polynuclear Aromatic Hydrocarbons

(PAH)

100%

Inspection low level 8270 SIM 100%

Inspection

100%

Inspection Hydrocarbon Dissolved Gasses (Methand, Ethane, Ethene) RSK 175

Dissolved gas - CO2

RSK 175

Modified

100% Inspection

Toxic Organic Compunds includes individually certified clean 6-L Summa TO-14

100% Inspection

Toxic Organic Compunds includes individually certified clean 6-L Summa TO-15

100% Inspection

Toxic Organic Compunds (sorbent tubes) TO-17 100%

Inspection

Polyflourinated Compounds (PFAS) LC/MS/MS 1633 100%

Inspection

Polyflourinated Compounds (PFAS) LC/MS/MS

Direct Inject Screening(8421 or similar)

100% Inspection

Polyflourinated Compounds (PFAS) LC/MS/MS 537 Modified 100%

Inspection

Polyflourinated Compounds (PFAS) LC/MS/MS DoD QSM Table

B-15 100%

Inspection

Organochlorine Pesticides 8081 100%

Inspection

Chlorinated Herbicides 8151 100%

Inspection

Organophosphorus Pesticides GC/HPLC 8141 100%

Inspection

Polychlorinated biphenyls (PCBs) 8082 100%

Inspection

Dioxin/Furan

100%

Inspection

100%

Inspection low resolution 1613 100%

Inspection

Explosives preparation puck mill grinding 8330B

Inspection

Explosives

100% Inspection

Hydrazine, MMH, UDMH 8315 Modified 100%

Inspection

White phosphorus 7580 100%

Inspection

PETN/NG 8330B

100%

Inspection

Nitroguanidine 8330B Modified 100%

Inspection

Picramic Acid and Picric Acid 8330B Modified 100%

Inspection

Nitroaromatics, Nitroamines, Nitrate Esters, PETN, NG 8330 B

Perchlorate

LC/EMI/MS 331.0

100%

Inspection

IC/EMI/MS 332.0

100%

Inspection

HPLC/ESI/MS/MS 6850

100%

Inspection

IC/ESI/MS/MS 6860

100%

Inspection ion chromatography 314.0 100%

Inspection

Glycols: ethylene & propolyene glycol 8015 100%

Inspection Petroleum/ Underground Storage Tanks

Hydrocarbon Identification Method for Soil and Water (fingerprint) 8015

100% Inspection

TPH-GRO 8015

100%

Inspection

OA-1

100%

Inspection

TPH-DRO 8015

100%

Inspection

OA-2

100%

Inspection

TPH-RRO 8015

100%

Inspection Method for the Determination of Volatile Petroleum Hydrocarbons (VPH) Fractions MAVPH

Method for the Determination of Extractable Petroleum Hydrocarbons (EPH) Fractions MAEPH

Oil and Grease (Gravimetric) 413.1

Inspection

Oil and Grease (IR) 413.2 100%

Inspection

Oil and Grease 1664A

Metals Packages

MMRP Small Arms Range Constituents 100%

Inspection

Cu, Zn, Pb, SB 6010

Cu, Zn, Pb, SB 6020

RCRA Metals (8 total):

100%

Inspection

As, Ba, Cd, Cr, Pb, Se, Ag 6010

As, Ba, Cd, Cr, Pb, Se, Ag 6020

Hg by CV AA 7470/7471

Priority Pollutant Metals (13 total):

100%

Inspection

Ag, As, Be, Cd, Cr, Cu, Pb, Ni, Se, Sb, Tl, Zn 200.7/6010

Ag, As, Be, Cd, Cr, Cu, Pb, Ni, Se, Sb, Tl, Zn 200.8/6020

Hg by CV AA 245.2/7470

CLP TAL (24 total):

Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Mo, Ni, K, Ag, Na, V, Zn, Sb, As, Cd, Pb, Se, Tl, Al, Ba, Be, Ca, Cr, Co, Cu, Fe, Mg, Mn, Mo, Ni, K, Ag, Na, V, Zn, Sb, As, Cd, Pb, Se, Tl, Hg by CV AA 7470/7471

Other Metals Analytical and Preparation Methods

Mercury, Cold Vapor AA 7470/7471

100% Inspection

Chromium, Hexavalent water 7196 A

100% Inspection soil 7196 A (3060A)

Inspection

Lead (Pb) - paint chips, wipes, air 200.8/6020

100% Inspection

Individual Metals (ICP)

100% Inspection

Individual Metals (ICP/MS)

100% Inspection

Leaching Proceedures

TCLP

100% Inspection

SPLP

100% Inspection

General Chemistry

Alkalinity (Carbonate)

310.1 or 310.2

Asbestos (PLM Test Method) 600/R-93/116

100% Inspection

Biochemical Oxygen Demand 405.1

100% Inspection

Chemical Oxygen Demand

410.1 or 410.4

100% Inspection

Chloride 325.2

100% Inspection

Chlorine – Residual 330.5

100% Inspection

Common Anions 300.1

100% Inspection

(Cl-, Br-, NO3-, NO2-, PO43-, SO4-)

SM 4110 B/C

Inspection

Conductivity 120.1

100% Inspection

Corrosivity to Steel 1110 A

100% Inspection

Cyanide - Amenable 335.1

100% Inspection

Cyanide - Reactive water (manual) 9010 / 9014

100% Inspection water (automated) 9010 / 9012

100% Inspection

Cyanide soil (manual) 9013 / 9014

100% Inspection soil (automated) 9013 / 9012

100% Inspection

Flashpoint 1010 A

ASTM D93

Inspection

Fluoride 340.2

100% Inspection

Hardness – Total

130.2 or 130.1

100% Inspection

Hardness - Ca and Mg

SM2340B

100% Inspection

Ignitability of solids

100% Inspection

Major Cations Na, (Na, K, Ca, and Mg (aq)

Na, K, Ca, Mg, Fe, Mn, and Al (soil)

100%

Moisture (%)

Mold Identification (www.epa.gov/nerlcwww/moldtech.htm)

Mold Technologies

Nitrogen – Ammonia 353.2

100% Inspection

Nitrogen – Nitrite 354.1

353.2

Inspection

Nitrogen - Nitrate and Nitrite 353.2

100% Inspection

Nitrogen - Total Kjeldahl 351.2

SM 4500

Inspection

Paint Filter / Liquid Release Test

100% Inspection pH water

100% Inspection soil

100% Inspection probe 150.1

100% Inspection

Phenolic Compounds

420.1 or 420.2

100% Inspection

Phosphate – Ortho 365.2

365.1

SM 4500 PE

Inspection

Phosphate – Total or Total Phosphorus 365.4

SM 4500 PF

Inspection

Salinity

SM2520B

100% Inspection

Solids – Dissolved 160.1

100% Inspection

Suspended

160.2 or SM

2540D 100%

Inspection

Total 160.3

100% Inspection

Settleable 160.5

100% Inspection

Soilids Volatile 160.4

100% Inspection

Specify Gravity

ASTM D854

SM 2710F

Inspection

Sulfate 375.2

SM 4500 SO4F

Inspection

Sulfide 376.2

9034 B

SM 4500S2E

Inspection

Sulfite 377.1

100% Inspection

Phosphorus – Total

SM 4500 PF

100% Inspection

Surfactant Test (MBAS) 425.1

SM 5540

Inspection

Temperature 170.1

100% Inspection

TOC

100% Inspection

TOC (soil) Lloyd Kahn

100% Inspection

TOX

100% Inspection

Turbidity 180.1

100% Inspection

Bromide 320.1

100% Inspection

Fats, Oils and Grease

100% Inspection

Volatile Fatty Acids 9056M

100% Inspection

AOX (Absorbable Organic Halides) 1653, 9020 or

100%

Inspection

Surfactant Test (MBAS) 425.1

100% Inspection

Acidity 305.2

100% Inspection

Radiochemistry

Gross Alpha 900.0

100% Inspection

Gross Beta 900.0

100% Inspection

Gamma Spectroscopy 901.1

100% Inspection

Radium-226 903.1

100% Inspection

Radium-228 904.0

100%

Chemical Warfare Methods

Mustard Breakdown Products (thioglycol, 1,4-dithiane, 1,4-oxathiane)

Lewisite Breakdown Products (CVAA and CVAO)

Compatibility Analyses

Solubility Observation

100% Inspection

Reactivity (air/water) Observation

100% Inspection

Density Observation

100% Inspection pH

100% Inspection

Flashpoint

Seta-flash (SW- 1010) or Pensky-

Martin

100% Inspection

Flammability Flame test

100% Inspection

Oxidizer Test strip

100% Inspection

Sulfide (Characteristic of Reactivity)

40 CFR 261.23

100% Inspection

Cyanide (Characteristic of Reactivity)

40 CFR 261.23

100% Inspection

Gross Halogen Beilstein

100% Inspection

PCB

Chlor-n-Oil

100% Inspection

Waste Blending Test Observation

100% Inspection

Cleanup Methods

Cleanup

100% Inspection

Florisil Cleanup

100% Inspection

Acid-Base Partition Cleanup

100% Inspection

Sulfur Cleanup

100% Inspection

Sulfuric Acid/Permanganate Cleanup

100% Inspection

Alumina Cleanup

100% Inspection

Alumina Column Cleanup and Separation of Petroleum Wastes 3611

Silica Gel Cleanup

100% Inspection

Gel-Permeation Cleanup

100%

Layered Silica Cleanup (neutral, basic, neutral, acidic, acidic) 1613

ENVI-carb included with

PFAS

100%

Inspection

Miscellaneous Items

Methanol kit for 5035 (1 Vial)

100% Inspection

NaHSO4 kit for low-level volatiles (3 Vial)

100%

Inspection

California Wet Extraction

CAL-WET CCR

Title 22 100%

Inspection

Asbestos

TEM

100% Inspection

Asbestos

PLM

100% Inspection

Acid Base Accounting SOBEK Method

100% Inspection

Microbiological

Heterotrophic Plate Count

SM9215D

100% Inspection

Algal Growth Potential

DM8111

100% Inspection

Algal species Composition:

Phytoplankton lab SOP 100%

Inspection

Algal Species Composition: Periphyton lab SOP

100% Inspection

Chlorophyll A

SM10200H

100% Inspection

E. Coli

SM9223B

100% Inspection

Fecal Coliform

SM9221

100% Inspection

Total Coliform

SM9223B

100% Inspection

Microcystin lab SOP

100% Inspection

In Vitro Bioaccessibility IVBA Assay for PB in soil 1340

Microarrays (Microbial Insights)

Dehalococodies, PCR

Functional Gene Analysis

Elutriate generation State Specific

100% Inspection

Elutriate generation USACE Manual

100% Inspection

Soil Process Parameters

Particle Size without hydrometer

ASTM D422

Particle Size with hydrometer

ASTM D422

100% Inspection

Grain Size

ASTM C136-

84A 100%

Inspection

Bulk Density

ASTM D2937

100% Inspection

Particle Density

ASTM D4253

100% Inspection

Permeability

ASTM D2432 /

D5084 100%

Inspection

Soil Permeability

MOSA 28-4.2

100% Inspection

Air Permeability

ASTM C204

100% Inspection pH

ASTM G51 /

D4972 100%

Eh

Humic Content

ASTM D2974

100% Inspection

Porosity

MOSA 18-2

100%

Transmissivity

Field Capacity

Cation Exchange Capacity

Halogen Content

Soil Nutrients (P, N, K)

Plasticity

Ash Fusion Temp.

Compaction

ASTM D698

100%

Density

Tension

Ash Content

ASTM D2974

100%

Bearing Capacity

Shrink-swell

Soil Oxidant Demand lab SOP

Benthic Oxygen Condition lab SOP

100% Inspection

Organic Content (sediment) lab SOP

100% Inspection

Environmental Microbiological Diagnostic Tools (EMBTs)

Microarray - petroleum

Microarray - chlorinated

Dehalococodies, PCR

Functional Gene Analysis

Stable Isotope Probing (SIP)

CSIA-Compound Specific Isotopic Analysis

Data Deliverables

Base Package -

EDD - SEDD 2A (current version) 100%

Level IV report - electronic pdf

CD with both EDD and Level IV report 100%

Inspection complaince checker - validation of all edds

Additional Items -

SEDD 2B (current version) 100%

Inspection

SEDD 3 (current version) 100%

Inspection

SEDD 4 (current version) 100%

Inspection

ERPIMS (current version) 100%

Inspection

FUDSCHEM (current version) 100%

Inspection

ERIS (current version) 100%

OTHER