Part 2_Ken's Party Store_DCSpec_Rev02-19_05-30-2019.pdf

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761/18031. SAR Ken's Party Store - UST Removal
Solicitation number
RFQ-171-190000000481-3
Issued by
Clinton County, Michigan

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This document is a Pre-Demolition Hazardous Materials Survey report prepared by PM Environmental, Inc. for the State of Michigan, specifically focused on the Ken's Party Store Garage located at 1470 North Clare Avenue in Harrison, Michigan. The survey was conducted on February 28, 2018, to identify, locate, classify, analyze, and estimate quantities of asbestos-containing materials (ACM) and universal wastes that must be removed or managed prior to demolition. The survey covered an approximately 1,000 square foot abandoned garage building with concrete block walls, windows, and a flat roof.

The survey findings revealed several key hazardous materials requiring specialized handling: two types of asbestos-containing materials were identified - interior window glazing (3% chrysotile) and exterior window caulk (5% chrysotile). Additionally, the inspection discovered universal waste including fluorescent bulbs with potential mercury content, ballasts potentially containing polychlorinated biphenyls (PCBs), and high-intensity discharge lighting with mercury vapor. Lead paint testing showed measurable lead concentrations in some paint samples, necessitating specific worker protection protocols under OSHA regulations. The report recommends professional removal of asbestos materials by a licensed abatement contractor, compliance with OSHA lead exposure standards, and proper disposal of universal waste in accordance with local, state, and federal requirements.

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Bidding and Contract Document (2/19) Project Name: Ken’s Party Store File No. 761/18031.SAR

APPENDIX V

LABORATORY ANALYTICAL REPORTS

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-SAGINAW BAY

RE: DEQ/KEN'S PARTY STORE

Bay City, MI 48708

401 Ketchum St., Suite B

Lisa Chadwick

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 05 March 2018 Work Order: 1801138

Price: $3,060.00

Kirby Shane

Laboratory Director

Lab Work Order # 1801138

Page 1 of 39Page 1 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-SAGINAW BAY

401 Ketchum St., Suite B

Lisa Chadwick

DEQ/KEN'S PARTY STORE

Bay City MI, 48708

Site Code: CMI081 03/05/2018

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1801138-01 Water 01/26/2018TMW-1 01/24/2018

1801138-02 Water 01/26/2018TMW-2 01/24/2018

1801138-03 Water 01/26/2018TMW-3 01/24/2018

1801138-04 Water 01/26/2018TMW-4 01/25/2018

1801138-05 Water 01/26/2018TMW-5 01/24/2018

1801138-06 Water 01/26/2018TMW-6 01/24/2018

1801138-07 Water 01/26/2018TMW-7 01/24/2018

1801138-08 Water 01/26/2018TMW-8 01/24/2018

1801138-09 Water 01/26/2018TMW-9 01/24/2018

1801138-10 Water 01/26/2018TMW-10 01/24/2018

1801138-11 Water 01/26/2018TMW-11 01/25/2018

1801138-12 Water 01/26/2018TMW-12 01/25/2018

Notes and Definitions

Y17 Probable petroleum product(s) present.

Y11 Unidentified peaks present in sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

T Reported value is less than the reporting limit (RL). Result is estimated.

KR Reporting limit(s) raised due to low sample volume submitted.

A11 Result is estimated due to high initial verification standard criteria failure.

A09 Result is estimated due to high recovery of batch quality control.

A07 Result(s) and reporting limit(s) are estimated due to poor precision.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

A01 Result(s) and reporting limit(s) are estimated due to low surrogate recovery.

100 Sample is a matrix spike. Result is not available due to matrix interference.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Page 2 of 39Page 2 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 3 of 39Page 3 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11596.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115107 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115102 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 4 of 39Page 4 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-01

RLCAS #

Client ID: TMW-1

QC Batch

Organics-Semivolatiles

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

1.0 ug/L 1 8270Naphthalene91-20-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11545.0 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11538.0 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11579.2 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 5 of 39Page 5 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Volatiles

10 ug/L 10 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

10 ug/L 10 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

50 ug/L 10 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trimethylbenzene526-73-8 01/31/1878 B8A3102

50 ug/L 10 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

10 ug/L 10 82601,2,4-Trimethylbenzene95-63-6 01/31/18380 B8A3102

10 ug/L 10 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

10 ug/L 10 82601,3,5-Trimethylbenzene108-67-8 01/31/18120 B8A3102

10 ug/L 10 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

10 ug/L 10 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

50 ug/L 10 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

50 ug/L 10 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

50 Xug/L 10 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

200 ug/L 10 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

50 ug/L 10 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

50 ug/L 10 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

10 ug/L 10 8260Benzene71-43-2 01/31/18ND B8A3102

10 ug/L 10 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

10 ug/L 10 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

10 ug/L 10 8260Bromoform75-25-2 01/31/18ND B8A3102

50 ug/L 10 8260Bromomethane74-83-9 01/31/18ND B8A3102

10 ug/L 10 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

10 ug/L 10 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

10 ug/L 10 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

50 ug/L 10 8260Chloroethane75-00-3 01/31/18ND B8A3102

10 ug/L 10 8260Chloroform67-66-3 01/31/18ND B8A3102

50 ug/L 10 8260Chloromethane74-87-3 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

50 ug/L 10 8260Cyclohexane110-82-7 01/31/18ND B8A3102

10 ug/L 10 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

10 ug/L 10 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 6 of 39Page 6 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Volatiles

50 ug/L 10 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

50 ug/L 10 8260Diethyl ether60-29-7 01/31/18ND B8A3102

50 ug/L 10 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

10 ug/L 10 8260Ethylbenzene100-41-4 01/31/1835 B8A3102

50 ug/L 10 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

50 ug/L 10 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

10 ug/L 10 8260Hexane110-54-3 01/31/1828 B8A3102

10 ug/L 10 8260Isopropylbenzene98-82-8 01/31/1816 B8A3102

20 ug/L 10 8260m & p - Xylene1330-20-7 01/31/1838 B8A3102

50 ug/L 10 8260Methylene chloride75-09-2 01/31/18ND B8A3102

10 ug/L 10 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

50 Xug/L 10 8260Naphthalene91-20-3 01/31/18ND B8A3102

10 ug/L 10 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

10 ug/L 10 8260n-Propylbenzene103-65-1 01/31/1872 B8A3102

10 ug/L 10 8260o-Xylene95-47-6 01/31/1817 B8A3102

10 ug/L 10 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

10 ug/L 10 8260Styrene100-42-5 01/31/18ND B8A3102

10 ug/L 10 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

500 ug/L 10 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

50 ug/L 10 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

10 ug/L 10 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

50 ug/L 10 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

10 ug/L 10 8260Toluene108-88-3 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

10 ug/L 10 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11597.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115106 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115102 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 7 of 39Page 7 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-02

RLCAS #

Client ID: TMW-2

QC Batch

Organics-Semivolatiles See note Y17

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/185.7 B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

1.0 ug/L 1 8270Naphthalene91-20-3 02/09/187.4 B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11551.8 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11540.6 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11567.1 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 8 of 39Page 8 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Volatiles

10 ug/L 10 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

10 ug/L 10 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

10 ug/L 10 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

10 ug/L 10 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

50 ug/L 10 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

10 ug/L 10 82601,2,3-Trimethylbenzene526-73-8 01/31/18530 B8A3102

50 ug/L 10 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

10 ug/L 10 82601,2,4-Trimethylbenzene95-63-6 01/31/181600 B8A3102

10 ug/L 10 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

10 ug/L 10 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

10 ug/L 10 82601,3,5-Trimethylbenzene108-67-8 01/31/18480 B8A3102

10 ug/L 10 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

10 ug/L 10 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

50 ug/L 10 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

50 ug/L 10 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

50 Xug/L 10 82602-Methylnaphthalene91-57-6 01/31/1862 B8A3102

200 ug/L 10 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

50 ug/L 10 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

50 ug/L 10 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

10 ug/L 10 8260Benzene71-43-2 01/31/18ND B8A3102

10 ug/L 10 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

10 ug/L 10 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

10 ug/L 10 8260Bromoform75-25-2 01/31/18ND B8A3102

50 ug/L 10 8260Bromomethane74-83-9 01/31/18ND B8A3102

10 ug/L 10 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

10 ug/L 10 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

10 ug/L 10 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

50 ug/L 10 8260Chloroethane75-00-3 01/31/18ND B8A3102

10 ug/L 10 8260Chloroform67-66-3 01/31/18ND B8A3102

50 ug/L 10 8260Chloromethane74-87-3 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

10 ug/L 10 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

50 ug/L 10 8260Cyclohexane110-82-7 01/31/18210 B8A3102

10 ug/L 10 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

10 ug/L 10 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 9 of 39Page 9 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Volatiles

50 ug/L 10 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

50 ug/L 10 8260Diethyl ether60-29-7 01/31/18ND B8A3102

50 ug/L 10 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

10 ug/L 10 8260Ethylbenzene100-41-4 01/31/181700 B8A3102

50 ug/L 10 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

50 ug/L 10 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

10 ug/L 10 8260Hexane110-54-3 01/31/18200 B8A3102

10 ug/L 10 8260Isopropylbenzene98-82-8 01/31/1889 B8A3102

200 ug/L 100 8260m & p - Xylene1330-20-7 02/01/187900 B8A3102

50 ug/L 10 8260Methylene chloride75-09-2 01/31/18ND B8A3102

10 ug/L 10 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

50 Xug/L 10 8260Naphthalene91-20-3 01/31/18380 B8A3102

10 ug/L 10 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

10 ug/L 10 8260n-Propylbenzene103-65-1 01/31/18230 B8A3102

10 ug/L 10 8260o-Xylene95-47-6 01/31/181800 B8A3102

10 Tug/L 10 8260sec-Butylbenzene135-98-8 01/31/189.9 B8A3102

10 ug/L 10 8260Styrene100-42-5 01/31/18ND B8A3102

10 ug/L 10 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

500 ug/L 10 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

50 ug/L 10 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

10 ug/L 10 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

50 ug/L 10 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

10 ug/L 10 8260Toluene108-88-3 01/31/18310 B8A3102

10 ug/L 10 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

10 ug/L 10 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

10 ug/L 10 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

10 ug/L 10 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11594.1 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115103 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-11599.0 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 10 of 39Page 10 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-03

RLCAS #

Client ID: TMW-3

QC Batch

Organics-Semivolatiles See note Y17

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/09/1853 B8A2608

1.0 ug/L 1 8270Acenaphthene83-32-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Anthracene120-12-7 02/09/18ND B8A2608

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/09/18ND B8A2608

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/09/18ND B8A2608

1.0 ug/L 1 8270Chrysene218-01-9 02/09/18ND B8A2608

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluoranthene206-44-0 02/09/18ND B8A2608

1.0 ug/L 1 8270Fluorene86-73-7 02/09/18ND B8A2608

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/09/18ND B8A2608

10 ug/L 10 8270Naphthalene91-20-3 02/16/18270 B8A2608

1.0 ug/L 1 8270Phenanthrene85-01-8 02/09/18ND B8A2608

1.0 ug/L 1 8270Pyrene129-00-0 02/09/18ND B8A2608

24.1-11563.3 %Surrogate: 2-Fluorobiphenyl 827002/09/18 B8A2608

17.8-11548.3 %Surrogate: Nitrobenzene-d5 827002/09/18 B8A2608

41.8-11573.1 %Surrogate: p-Terphenyl-d14 827002/09/18 B8A2608

Page 11 of 39Page 11 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 12 of 39Page 12 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11598.2 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115106 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115101 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 13 of 39Page 13 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-04

RLCAS #

Client ID: TMW-4

QC Batch

Organics-Semivolatiles

5.3 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.1 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.1 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11534.2 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11535.3 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11574.7 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 14 of 39Page 14 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 15 of 39Page 15 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11597.7 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115108 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115103 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 16 of 39Page 16 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-05

RLCAS #

Client ID: TMW-5

QC Batch

Organics-Semivolatiles

5.5 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.1 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.1 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.1 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.2 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.1 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.2 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.1 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.1 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.1 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11558.5 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11559.9 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11573.8 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 17 of 39Page 17 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 02/02/18ND B8B0202

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 02/02/18ND B8B0202

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 02/02/1817 B8B0202

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 02/02/18110 B8B0202

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 02/02/18ND B8B0202

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 02/02/18ND B8B0202

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 02/02/1857 B8B0202

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 02/02/18ND B8B0202

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 02/02/18ND B8B0202

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 02/02/18200 B8B0202

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 02/02/18ND B8B0202

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 02/02/1813 B8B0202

20 ug/L 1 82602-Propanone (acetone)67-64-1 02/02/18ND B8B0202

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 02/02/18ND B8B0202

5.0 ug/L 1 8260Acrylonitrile107-13-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Benzene71-43-2 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromochloromethane74-97-5 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromodichloromethane75-27-4 02/02/18ND B8B0202

1.0 ug/L 1 8260Bromoform75-25-2 02/02/18ND B8B0202

5.0 ug/L 1 8260Bromomethane74-83-9 02/02/18ND B8B0202

1.0 ug/L 1 8260Carbon disulfide75-15-0 02/02/18ND B8B0202

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 02/02/18ND B8B0202

1.0 ug/L 1 8260Chlorobenzene108-90-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Chloroethane75-00-3 02/02/18ND B8B0202

1.0 ug/L 1 8260Chloroform67-66-3 02/02/18ND B8B0202

5.0 ug/L 1 8260Chloromethane74-87-3 02/02/18ND B8B0202

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 02/02/18ND B8B0202

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 02/02/18ND B8B0202

5.0 ug/L 1 8260Cyclohexane110-82-7 02/02/18ND B8B0202

1.0 ug/L 1 8260Dibromochloromethane124-48-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Dibromomethane74-95-3 02/02/18ND B8B0202

Page 18 of 39Page 18 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Volatiles See note Y11

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 02/02/18ND B8B0202

5.0 ug/L 1 8260Diethyl ether60-29-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 02/02/18ND B8B0202

1.0 ug/L 1 8260Ethylbenzene100-41-4 02/02/182.3 B8B0202

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 02/02/18ND B8B0202

5.0 ug/L 1 8260Hexachloroethane67-72-1 02/02/18ND B8B0202

1.0 ug/L 1 8260Hexane110-54-3 02/02/1864 B8B0202

1.0 ug/L 1 8260Isopropylbenzene98-82-8 02/02/185.7 B8B0202

2.0 ug/L 1 8260m & p - Xylene1330-20-7 02/02/18ND B8B0202

5.0 ug/L 1 8260Methylene chloride75-09-2 02/02/18ND B8B0202

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 02/02/18ND B8B0202

5.0 Xug/L 1 8260Naphthalene91-20-3 02/02/18ND B8B0202

1.0 ug/L 1 8260n-Butylbenzene104-51-8 02/02/18ND B8B0202

1.0 ug/L 1 8260n-Propylbenzene103-65-1 02/02/1831 B8B0202

1.0 ug/L 1 8260o-Xylene95-47-6 02/02/18ND B8B0202

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 02/02/1813 B8B0202

1.0 ug/L 1 8260Styrene100-42-5 02/02/18ND B8B0202

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 02/02/18ND B8B0202

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 02/02/18ND B8B0202

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 02/02/18ND B8B0202

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 02/02/18ND B8B0202

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 02/02/18ND B8B0202

1.0 ug/L 1 8260Toluene108-88-3 02/02/18ND B8B0202

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 02/02/18ND B8B0202

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 02/02/18ND B8B0202

1.0 ug/L 1 8260Trichloroethylene79-01-6 02/02/18ND B8B0202

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 02/02/18ND B8B0202

1.0 ug/L 1 8260Vinyl chloride75-01-4 02/02/18ND B8B0202

85-115102 %Surrogate: Bromofluorobenzene 826002/02/18 B8B0202

82.7-115104 %Surrogate: Dibromofluoromethane 826002/02/18 B8B0202

85-115102 %Surrogate: Toluene-d8 826002/02/18 B8B0202

Page 19 of 39Page 19 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-06

RLCAS #

Client ID: TMW-6

QC Batch

Organics-Semivolatiles See note Y17

5.0 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/188.0 B8A3108

1.0 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.0 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.0 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.0 ug/L 1 8270Naphthalene91-20-3 02/23/182.1 B8A3108

1.0 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11564.3 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11566.0 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11569.5 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 20 of 39Page 20 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 21 of 39Page 21 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/31/18ND B8A3102

85-11595.5 %Surrogate: Bromofluorobenzene 826001/31/18 B8A3102

82.7-115107 %Surrogate: Dibromofluoromethane 826001/31/18 B8A3102

85-115100 %Surrogate: Toluene-d8 826001/31/18 B8A3102

Page 22 of 39Page 22 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-07

RLCAS #

Client ID: TMW-7

QC Batch

Organics-Semivolatiles

5.2 ug/L 1 82702-Methylnaphthalene91-57-6 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthene83-32-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Acenaphthylene208-96-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Anthracene120-12-7 02/23/18ND B8A3108

1.0 ug/L 1 8270Benz[a]anthracene56-55-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[a]pyrene50-32-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[b]fluoranthene205-99-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[g,h,i]perylene191-24-2 02/23/18ND B8A3108

1.0 ug/L 1 8270Benzo[k]fluoranthene207-08-9 02/23/18ND B8A3108

1.0 ug/L 1 8270Chrysene218-01-9 02/23/18ND B8A3108

2.1 ug/L 1 8270Dibenz[a,h]anthracene53-70-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluoranthene206-44-0 02/23/18ND B8A3108

1.0 ug/L 1 8270Fluorene86-73-7 02/23/18ND B8A3108

2.1 ug/L 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 02/23/18ND B8A3108

1.0 ug/L 1 8270Naphthalene91-20-3 02/23/18ND B8A3108

1.0 ug/L 1 8270Phenanthrene85-01-8 02/23/18ND B8A3108

1.0 ug/L 1 8270Pyrene129-00-0 02/23/18ND B8A3108

24.1-11548.8 %Surrogate: 2-Fluorobiphenyl 827002/23/18 B8A3108

17.8-11549.7 %Surrogate: Nitrobenzene-d5 827002/23/18 B8A3108

41.8-11572.2 %Surrogate: p-Terphenyl-d14 827002/23/18 B8A3108

Page 23 of 39Page 23 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-08

RLCAS #

Client ID: TMW-8

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/31/18ND B8A3102

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/31/18ND B8A3102

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/31/18ND B8A3102

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/31/18ND B8A3102

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/31/18ND B8A3102

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/31/18ND B8A3102

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/31/18ND B8A3102

5.0 ug/L 1 82602,2,4-Trimethylpentane540-84-1 01/31/18ND B8A3102

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/31/18ND B8A3102

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/31/18ND B8A3102

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/31/18ND B8A3102

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/31/18ND B8A3102

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Benzene71-43-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/31/18ND B8A3102

1.0 ug/L 1 8260Bromoform75-25-2 01/31/18ND B8A3102

5.0 ug/L 1 8260Bromomethane74-83-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/31/18ND B8A3102

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/31/18ND B8A3102

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloroethane75-00-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Chloroform67-66-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Chloromethane74-87-3 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/31/18ND B8A3102

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/31/18ND B8A3102

5.0 ug/L 1 8260Cyclohexane110-82-7 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Dibromomethane74-95-3 01/31/18ND B8A3102

Page 24 of 39Page 24 of 40

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1801138-08

RLCAS #

Client ID: TMW-8

QC Batch

Organics-Volatiles

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/31/18ND B8A3102

5.0 ug/L 1 8260Diethyl ether60-29-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/31/18ND B8A3102

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/31/18ND B8A3102

1.0 ug/L 1 8260Hexane110-54-3 01/31/18ND B8A3102

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/31/18ND B8A3102

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/31/18ND B8A3102

5.0 ug/L 1 8260Methylene chloride75-09-2 01/31/18ND B8A3102

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/31/18ND B8A3102

5.0 Xug/L 1 8260Naphthalene91-20-3 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/31/18ND B8A3102

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/31/18ND B8A3102

1.0 ug/L 1 8260o-Xylene95-47-6 01/31/18ND B8A3102

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Styrene100-42-5 01/31/18ND B8A3102

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/31/18ND B8A3102

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/31/18ND B8A3102

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/31/18ND B8A3102

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/31/18ND B8A3102

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/31/18ND B8A3102

1.0 ug/L 1 8260Toluene108-88-3 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/31/18ND B8A3102

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/31/18ND B8A3102

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/31/18ND…

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